Test Results Units MQL By Analytical DF Date / Time …...Lab No : Delta Water Non-Ozonated Sampled:...

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REPORT OF ANALYSISReport Number :

Project Information :

TN 38104

17-257-0252

21146

Delta Water PBC dba/Delta Water

1400 Union Ave

Mr. Jereme Cavallo

Memphis

Analytical Testing

Report Date :

Received :

09/21/2017

9/14/2017

Sample ID :

Lab No :

Sampled:Delta Water Non-Ozonated

92613 Matrix:

9/14/2017 11:15

Aqueous

Test Results Units MQL By AnalyticalMethod

Date / TimeAnalyzed

DF

<1 MPN/100mL 1Total Coliform 1 09/14/17 14:10 9223B-2004SBA

491 µS/cm 0.010Conductivity 1 09/15/17 09:05 2510B-2011SBA

<1 MPN/100mL 1E-coli 1 09/14/17 14:10 9223B-2004SBA

2.89 mg/L 0.100Nitrate (NO3-N) 1 09/14/17 13:45 EPA-300.0BKN

7.8 s.u.pH 1 09/14/17 15:35 4500H+B-2011TSP

314 mg/L 7.00Total Dissolved Solids 1 09/15/17 09:05 2510B-2011SBA

55.3 mg/L 0.100Total Calcium 1 09/20/17 23:39 EPA-200.7CCR

<0.005 mg/L 0.005Total Copper 1 09/20/17 23:39 EPA-200.7CCR

202 mg/L 0.100Hardness as CaCO3(SM-2340B) 1 09/20/17 23:39 EPA-200.7

<0.100 mg/L 0.100Total Iron 1 09/20/17 23:39 EPA-200.7CCR

<0.006 mg/L 0.006Total Lead 1 09/20/17 23:39 EPA-200.7CCR

15.6 mg/L 0.100Total Magnesium 1 09/20/17 23:39 EPA-200.7CCR

Qualifiers/

DefinitionsMethod Quantitation LimitMQLDilution FactorDF

Page 2 of 5

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Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. !"#$#%#� &'()*(��+,-./.#0#� ��&('(1*� � 2!�34+!5� &'6(171� � 89:#/� ��&81(')('17(�11�6� !;<#0/#/� &77�(6*(�=.//.//.>>.�� ?#".@,;0.#� ��&AB('� � 3?� &'1*�� C<"#D,%#� ��&BE11�� 2.;F.0.#� &((1(6�G90H-I<J� &B((')� 89009//99��&83(A(A)� 45!�� &83(((1A�� G90H-I<J�KL8��&'1��

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12/20/2016 Delta Water PBC dba/Delta Water Mr. Jereme Cavallo 1400 Union Ave Memphis, TN, 38104 Ref: Analytical Testing

Lab Report Number: 16-333-0328 Client Project Description: Analysis Required for Source Approval

Dear Mr. Jereme Cavallo: Waypoint Analytical, Inc. received sample(s) on 11/28/2016 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '~' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,

Andy Parrish Project Manager

Page 1 of 39

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Page 5 of 39

#=CL#

December 20, 2016

LIMS USE: FR - PROJECT MANAGER

LIMS OBJECT ID: 35279584

35279584Project:Pace Project No.:

RE:

Project ManagerWaypoint2790 Whitten RoadMemphis, TN 38133

16-333-0328: EXP 3133

Dear Project Manager:Enclosed are the analytical results for sample(s) received by the laboratory on November 29, 2016.The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Sakina [email protected] Manager

Enclosures

cc: Accounts Payable, Waypoint

Mr. Nathan A. Pera, Waypoint

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, LLC.

Pace Analytical Services, LLC

8 East Tower Circle

Ormond Beach, FL 32174

(386)672-5668

Page 1 of 32

Page 6 of 39

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

Pennsylvania Certification IDs

1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601L-A-B DOD-ELAP Accreditation #: L2417Alabama Certification #: 41590Arizona Certification #: AZ0734Arkansas CertificationCalifornia Certification #: 04222CAColorado CertificationConnecticut Certification #: PH-0694Delaware CertificationFlorida/TNI Certification #: E87683Georgia Certification #: C040Guam CertificationHawaii CertificationIdaho CertificationIllinois CertificationIndiana CertificationIowa Certification #: 391Kansas/TNI Certification #: E-10358Kentucky Certification #: 90133Louisiana DHH/TNI Certification #: LA140008Louisiana DEQ/TNI Certification #: 4086Maine Certification #: PA00091Maryland Certification #: 308Massachusetts Certification #: M-PA1457Michigan/PADEP CertificationMissouri Certification #: 235

Montana Certification #: Cert 0082Nebraska Certification #: NE-05-29-14Nevada Certification #: PA014572015-1New Hampshire/TNI Certification #: 2976New Jersey/TNI Certification #: PA 051New Mexico Certification #: PA01457New York/TNI Certification #: 10888North Carolina Certification #: 42706North Dakota Certification #: R-190Oregon/TNI Certification #: PA200002Pennsylvania/TNI Certification #: 65-00282Puerto Rico Certification #: PA01457Rhode Island Certification #: 65-00282South Dakota CertificationTennessee Certification #: TN2867Texas/TNI Certification #: T104704188-14-8Utah/TNI Certification #: PA014572015-5USDA Soil Permit #: P330-14-00213Vermont Dept. of Health: ID# VT-0282Virgin Island/PADEP CertificationVirginia/VELAP Certification #: 460198Washington Certification #: C868West Virginia DEP Certification #: 143West Virginia DHHR Certification #: 9964CWisconsin CertificationWyoming Certification #: 8TMS-L

Ormond Beach Certification IDs

8 East Tower Circle, Ormond Beach, FL 32174Alabama Certification #: 41320Connecticut Certification #: PH-0216Delaware Certification: FL NELAC ReciprocityFlorida Certification #: E83079Georgia Certification #: 955Guam Certification: FL NELAC ReciprocityHawaii Certification: FL NELAC ReciprocityIllinois Certification #: 200068Indiana Certification: FL NELAC ReciprocityKansas Certification #: E-10383Louisiana Certification #: FL NELAC ReciprocityLouisiana Environmental Certificate #: 05007Maryland Certification: #346Michigan Certification #: 9911Mississippi Certification: FL NELAC ReciprocityMissouri Certification #: 236Montana Certification #: Cert 0074

Nebraska Certification: NE-OS-28-14Nevada Certification: FL NELAC ReciprocityNew York Certification #: 11608North Carolina Environmental Certificate #: 667North Carolina Certification #: 12710Oklahoma Certification #: D9947Pennsylvania Certification #: 68-00547Puerto Rico Certification #: FL01264South Carolina Certification: #96042001Tennessee Certification #: TN02974Texas Certification: FL NELAC ReciprocityUS Virgin Islands Certification: FL NELAC ReciprocityVirginia Environmental Certification #: 460165Wyoming Certification: FL NELAC ReciprocityWest Virginia Certification #: 9962CWisconsin Certification #: 399079670Wyoming (EPA Region 8): FL NELAC Reciprocity





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#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

Lab ID Sample ID Matrix Date Collected Date Received

35279584001 16-333-0328 Water 11/28/16 10:40 11/29/16 10:20





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#=SA#

SAMPLE ANALYTE COUNT

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

Lab ID Sample ID Method

Analytes

Reported LaboratoryAnalysts

35279584001 16-333-0328 EPA 504.1 2 PASI-OSMH

EPA 508.1 21 PASI-OJTJ

EPA 552.2 7 PASI-OSMH

EPA 524.2 49 PASI-OJLR

SM7500RnB-07 1 PASI-PANJV

EPA 900.0 1 PASI-PANEG

EPA 903.1 1 PASI-PAACM

EPA 904.0 1 PASI-PAJLW

ASTM D5811-95 1 PASI-PALAL

EPA 906.0 1 PASI-PAWRR

ASTM D5174-97 1 PASI-PARMK

EPA 420.4 1 PASI-OTK1





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#=HO#

SUMMARY OF DETECTION

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

Parameters AnalyzedResult

Lab Sample ID

Report Limit QualifiersUnitsMethod

Client Sample ID

35279584001 16-333-0328

Radon 282.5 ±73.6 (71.9)

C:NA T:NA

pCi/L 12/02/16 21:55 1pSM7500RnB-07

Gross Alpha 1.64U ±0.905

(1.64) C:NAT:NA

pCi/L 12/06/16 21:16EPA 900.0

Radium-226 0.584U ±0.350

(0.584)C:NA T:92%

pCi/L 12/15/16 10:27EPA 903.1

Radium-228 1.04U ±0.545(1.04)

C:68%T:84%

pCi/L 12/16/16 11:35EPA 904.0

Strontium-90 0.465U ±0.238

(0.465)C:97% T:NA

pCi/L 12/08/16 20:17 N2ASTM D5811-95

Tritium -49.9 ± 138(251) C:NA

T:NA

pCi/L 12/09/16 17:32EPA 906.0

Total Uranium 0.193U ±0.005

(0.193)C:NA T:NA

ug/L 12/19/16 16:04ASTM D5174-97

Phenolics, Total Recoverable 0.018 mg/L 12/15/16 14:490.010EPA 420.4





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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

Sample: 16-333-0328 Lab ID: 35279584001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL

Comments: • Split off 500 ml amber un-preserved bottle for Tritium analysis.• Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the samplepreservation requirement of pH <2 for radiochemistry analysis.

Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504.1 GCS EDB and DBCP

1,2-Dibromo-3-chloropropane 0.0047U ug/L 12/06/16 04:38 96-12-812/05/16 17:040.019 0.0047 1

1,2-Dibromoethane (EDB) 0.0071U ug/L 12/06/16 04:38 106-93-412/05/16 17:040.0095 0.0071 1

Analytical Method: EPA 508.1 Preparation Method: EPA 508.1508.1 GCS Pesticides

Alachlor 0.034U ug/L 12/05/16 17:08 15972-60-811/30/16 10:150.19 0.034 1

Atrazine 0.061U ug/L 12/05/16 17:08 1912-24-911/30/16 10:150.096 0.061 1

gamma-BHC (Lindane) 0.0029U ug/L 12/05/16 17:08 58-89-911/30/16 10:150.019 0.0029 1

Chlordane (Technical) 0.045U ug/L 12/05/16 17:08 57-74-911/30/16 10:150.19 0.045 1

Endrin 0.0067U ug/L 12/05/16 17:08 72-20-811/30/16 10:150.0096 0.0067 1

Heptachlor 0.012U ug/L 12/05/16 17:08 76-44-811/30/16 10:150.038 0.012 1

Heptachlor epoxide 0.0029U ug/L 12/05/16 17:08 1024-57-311/30/16 10:150.019 0.0029 1

Hexachlorobenzene 0.018U ug/L 12/05/16 17:08 118-74-1 L311/30/16 10:150.096 0.018 1

Hexachlorocyclopentadiene 0.031U ug/L 12/01/16 17:28 77-47-4 L311/30/16 10:150.096 0.031 1

Methoxychlor 0.049U ug/L 12/05/16 17:08 72-43-511/30/16 10:150.096 0.049 1

PCB-1016 (Aroclor 1016) 0.077U ug/L 12/05/16 17:08 12674-11-211/30/16 10:150.096 0.077 1

PCB-1221 (Aroclor 1221) 0.028U ug/L 12/05/16 17:08 11104-28-211/30/16 10:150.096 0.028 1

PCB-1232 (Aroclor 1232) 0.028U ug/L 12/05/16 17:08 11141-16-511/30/16 10:150.096 0.028 1

PCB-1242 (Aroclor 1242) 0.049U ug/L 12/05/16 17:08 53469-21-911/30/16 10:150.096 0.049 1

PCB-1248 (Aroclor 1248) 0.060U ug/L 12/05/16 17:08 12672-29-611/30/16 10:150.096 0.060 1

PCB-1254 (Aroclor 1254) 0.022U ug/L 12/05/16 17:08 11097-69-111/30/16 10:150.096 0.022 1

PCB-1260 (Aroclor 1260) 0.063U ug/L 12/05/16 17:08 11096-82-511/30/16 10:150.096 0.063 1

PCB, Total 0.077U ug/L 12/05/16 17:08 1336-36-311/30/16 10:150.096 0.077 1

Simazine 0.066U ug/L 12/05/16 17:08 122-34-911/30/16 10:150.067 0.066 1

Toxaphene 0.58U ug/L 12/05/16 17:08 8001-35-211/30/16 10:150.96 0.58 1SurrogatesDecachlorobiphenyl (S) 56 % 12/05/16 17:08 2051-24-3 S511/30/16 10:1570-130 1

Analytical Method: EPA 552.2 Preparation Method: EPA 552.2552.2 Haloacetic Acids

Dibromoacetic Acid 0.00037U mg/L 12/02/16 14:49 631-64-111/30/16 11:250.0010 0.00037 1

Dichloroacetic Acid 0.00037U mg/L 12/02/16 14:49 79-43-611/30/16 11:250.0010 0.00037 1

Haloacetic Acids (Total) 0.00037U mg/L 12/02/16 14:4911/30/16 11:250.0010 0.00037 1

Monobromoacetic Acid 0.00037U mg/L 12/02/16 14:49 79-08-311/30/16 11:250.0010 0.00037 1

Monochloroacetic Acid 0.00037U mg/L 12/02/16 14:49 79-11-811/30/16 11:250.0010 0.00037 1

Trichloroacetic Acid 0.00037U mg/L 12/02/16 14:49 76-03-911/30/16 11:250.0010 0.00037 1Surrogates2,3-Dibromopropanoic Acid (S) 102 % 12/02/16 14:49 600-05-511/30/16 11:2570-130 1

Analytical Method: EPA 524.2524.2 MSV

Benzene 0.25U ug/L 12/09/16 17:00 71-43-20.50 0.25 1

Bromobenzene 0.25U ug/L 12/09/16 17:00 108-86-10.50 0.25 1

Bromodichloromethane 0.25U ug/L 12/09/16 17:00 75-27-41.0 0.25 1

Bromoform 0.25U ug/L 12/09/16 17:00 75-25-21.0 0.25 1

Bromomethane 0.25U ug/L 12/09/16 17:00 74-83-90.50 0.25 1



without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM


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ANALYTICAL RESULTS

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133





Carbon tetrachloride 0.25U ug/L 12/09/16 17:00 56-23-50.50 0.25 1

Chlorobenzene 0.25U ug/L 12/09/16 17:00 108-90-70.50 0.25 1

Chloroethane 0.28U ug/L 12/09/16 17:00 75-00-3 L30.50 0.28 1

Chloroform 0.25U ug/L 12/09/16 17:00 67-66-31.0 0.25 1

Chloromethane 0.46U ug/L 12/09/16 17:00 74-87-30.50 0.46 1

2-Chlorotoluene 0.25U ug/L 12/09/16 17:00 95-49-80.50 0.25 1

4-Chlorotoluene 0.25U ug/L 12/09/16 17:00 106-43-40.50 0.25 1

Dibromochloromethane 0.25U ug/L 12/09/16 17:00 124-48-11.0 0.25 1

Dibromomethane 0.25U ug/L 12/09/16 17:00 74-95-30.50 0.25 1

1,2-Dichlorobenzene 0.25U ug/L 12/09/16 17:00 95-50-10.50 0.25 1



Dichlorodifluoromethane 0.49U ug/L 12/09/16 17:00 75-71-8 L30.50 0.49 1

1,1-Dichloroethane 0.25U ug/L 12/09/16 17:00 75-34-30.50 0.25 1

1,2-Dichloroethane 0.25U ug/L 12/09/16 17:00 107-06-20.50 0.25 1

1,1-Dichloroethene 0.25U ug/L 12/09/16 17:00 75-35-40.50 0.25 1

cis-1,2-Dichloroethene 0.25U ug/L 12/09/16 17:00 156-59-20.50 0.25 1

trans-1,2-Dichloroethene 0.25U ug/L 12/09/16 17:00 156-60-50.50 0.25 1

1,2-Dichloropropane 0.25U ug/L 12/09/16 17:00 78-87-50.50 0.25 1



1,1-Dichloropropene 0.25U ug/L 12/09/16 17:00 563-58-60.50 0.25 1

1,3-Dichloropropene 0.25U ug/L 12/09/16 17:00 10061-02-6 N20.50 0.25 1

Ethylbenzene 0.25U ug/L 12/09/16 17:00 100-41-40.50 0.25 1

Methylene Chloride 0.44U ug/L 12/09/16 17:00 75-09-20.50 0.44 1

Methyl-tert-butyl ether 0.25U ug/L 12/09/16 17:00 1634-04-4 L30.50 0.25 1

Styrene 0.25U ug/L 12/09/16 17:00 100-42-50.50 0.25 1

1,1,1,2-Tetrachloroethane 0.25U ug/L 12/09/16 17:00 630-20-60.50 0.25 1

Tetrachloroethene 0.25U ug/L 12/09/16 17:00 127-18-40.50 0.25 1

Toluene 0.25U ug/L 12/09/16 17:00 108-88-30.50 0.25 1

Total Trihalomethanes (Calc.) 0.25U ug/L 12/09/16 17:001.0 0.25 1

1,2,4-Trichlorobenzene 0.41U ug/L 12/09/16 17:00 120-82-10.50 0.41 1

1,1,1-Trichloroethane 0.25U ug/L 12/09/16 17:00 71-55-60.50 0.25 1

1,1,2-Trichloroethane 0.25U ug/L 12/09/16 17:00 79-00-50.50 0.25 1

Trichloroethene 0.25U ug/L 12/09/16 17:00 79-01-60.50 0.25 1

Trichlorofluoromethane 0.25U ug/L 12/09/16 17:00 75-69-4 L30.50 0.25 1

1,2,3-Trichloropropane 0.43U ug/L 12/09/16 17:00 96-18-40.50 0.43 1

Vinyl chloride 0.39U ug/L 12/09/16 17:00 75-01-40.50 0.39 1

Xylene (Total) 0.25U ug/L 12/09/16 17:00 1330-20-70.50 0.25 1

m&p-Xylene 0.25U ug/L 12/09/16 17:00 179601-23-10.50 0.25 1

o-Xylene 0.25U ug/L 12/09/16 17:00 95-47-60.50 0.25 1Surrogates4-Bromofluorobenzene (S) 86 % 12/09/16 17:00 460-00-470-130 1

Toluene-d8 (S) 96 % 12/09/16 17:00 2037-26-570-130 1





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ANALYTICAL RESULTS

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133





Surrogates1,2-Dichloroethane-d4 (S) 111 % 12/09/16 17:00 17060-07-070-130 1

Analytical Method: EPA 420.4420.4 Phenolics, Total

Phenolics, Total Recoverable 0.018 mg/L 12/15/16 14:490.010 0.0050 1





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#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

337540

EPA 524.2

EPA 524.2

524.2 MSV

Associated Lab Samples: 35279584001

Parameter Units

Blank

Result

Reporting

Limit Qualifiers

METHOD BLANK: 1808332


Matrix: Water

AnalyzedMDL

1,1,1,2-Tetrachloroethane ug/L 0.25U 0.50 12/09/16 15:320.25

1,1,1-Trichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25

1,1,2-Trichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25

1,1-Dichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25

1,1-Dichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25

1,1-Dichloropropene ug/L 0.25U 0.50 12/09/16 15:320.25

1,2,3-Trichloropropane ug/L 0.43U 0.50 12/09/16 15:320.43

1,2,4-Trichlorobenzene ug/L 0.41U 0.50 12/09/16 15:320.41

1,2-Dichlorobenzene ug/L 0.25U 0.50 12/09/16 15:320.25

1,2-Dichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25

1,2-Dichloropropane ug/L 0.25U 0.50 12/09/16 15:320.25



1,3-Dichloropropene ug/L 0.25U 0.50 N212/09/16 15:320.25



2-Chlorotoluene ug/L 0.25U 0.50 12/09/16 15:320.25

4-Chlorotoluene ug/L 0.25U 0.50 12/09/16 15:320.25

Benzene ug/L 0.25U 0.50 12/09/16 15:320.25

Bromobenzene ug/L 0.25U 0.50 12/09/16 15:320.25

Bromodichloromethane ug/L 0.25U 1.0 12/09/16 15:320.25

Bromoform ug/L 0.25U 1.0 12/09/16 15:320.25

Bromomethane ug/L 0.25U 0.50 12/09/16 15:320.25

Carbon tetrachloride ug/L 0.25U 0.50 12/09/16 15:320.25

Chlorobenzene ug/L 0.25U 0.50 12/09/16 15:320.25

Chloroethane ug/L 0.28U 0.50 12/09/16 15:320.28

Chloroform ug/L 0.25U 1.0 12/09/16 15:320.25

Chloromethane ug/L 0.46U 0.50 12/09/16 15:320.46

cis-1,2-Dichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25

Dibromochloromethane ug/L 0.25U 1.0 12/09/16 15:320.25

Dibromomethane ug/L 0.25U 0.50 12/09/16 15:320.25

Dichlorodifluoromethane ug/L 0.49U 0.50 12/09/16 15:320.49

Ethylbenzene ug/L 0.25U 0.50 12/09/16 15:320.25

m&p-Xylene ug/L 0.25U 0.50 12/09/16 15:320.25

Methyl-tert-butyl ether ug/L 0.25U 0.50 12/09/16 15:320.25

Methylene Chloride ug/L 0.44U 0.50 12/09/16 15:320.44

o-Xylene ug/L 0.25U 0.50 12/09/16 15:320.25

Styrene ug/L 0.25U 0.50 12/09/16 15:320.25

Tetrachloroethene ug/L 0.25U 0.50 12/09/16 15:320.25

Toluene ug/L 0.25U 0.50 12/09/16 15:320.25

Total Trihalomethanes (Calc.) ug/L 0.25U 1.0 12/09/16 15:320.25





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#=QC#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

AnalyzedMDL

trans-1,2-Dichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25

Trichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25

Trichlorofluoromethane ug/L 0.25U 0.50 12/09/16 15:320.25

Vinyl chloride ug/L 0.39U 0.50 12/09/16 15:320.39

Xylene (Total) ug/L 0.25U 0.50 12/09/16 15:320.25

1,2-Dichloroethane-d4 (S) % 108 70-130 12/09/16 15:32

4-Bromofluorobenzene (S) % 92 70-130 12/09/16 15:32

Toluene-d8 (S) % 101 70-130 12/09/16 15:32

Parameter Units

LCS

Result

% Rec

Limits Qualifiers% RecConc.

1808333LABORATORY CONTROL SAMPLE & LCSD:

LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1808334

1,1,1,2-Tetrachloroethane ug/L 4.55 89 70-1301015.1 13 40

1,1,1-Trichloroethane ug/L 5.05 101 70-1301035.1 2 40

1,1,2-Trichloroethane ug/L 5.15 102 70-1301125.6 8 40

1,1-Dichloroethane ug/L 4.95 99 70-1301045.2 5 40

1,1-Dichloroethene ug/L 5.85 115 70-1301175.9 2 40

1,1-Dichloropropene ug/L 5.55 109 70-1301115.5 1 40

1,2,3-Trichloropropane ug/L 3.75 75 70-130944.7 23 40

1,2,4-Trichlorobenzene ug/L 5.75 115 70-1301105.5 4 40

1,2-Dichlorobenzene ug/L 4.25 84 70-130874.3 3 40

1,2-Dichloroethane ug/L 5.95 118 70-1301145.7 3 40

1,2-Dichloropropane ug/L 3.95 78 70-130914.5 14 40



1,3-Dichloropropene ug/L 8.1 N210 81 70-130818.1 0 40



2-Chlorotoluene ug/L 4.25 83 70-130804.0 5 40

4-Chlorotoluene ug/L 4.15 81 70-130884.4 9 40

Benzene ug/L 5.35 105 70-1301115.6 6 40

Bromobenzene ug/L 4.35 86 70-130834.2 3 40

Bromodichloromethane ug/L 4.65 92 70-130924.6 1 40

Bromoform ug/L 4.05 79 70-130834.2 5 40

Bromomethane ug/L 4.75 93 70-130864.3 8 40

Carbon tetrachloride ug/L 5.65 112 70-1301195.9 6 40

Chlorobenzene ug/L 4.75 95 70-1301055.2 10 40

Chloroethane ug/L 7.4 L05 149 70-1301517.6 2 40

Chloroform ug/L 5.45 108 70-1301055.3 3 40

Chloromethane ug/L 5.15 103 70-130763.8 30 40

cis-1,2-Dichloroethene ug/L 5.55 111 70-1301095.4 2 40

Dibromochloromethane ug/L 4.55 91 70-130824.1 10 40

Dibromomethane ug/L 5.05 100 70-1301085.4 8 40

Dichlorodifluoromethane ug/L 6.6 L05 132 70-1301256.2 5 40





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#=QC#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1808334

Ethylbenzene ug/L 4.85 96 70-1301015.0 4 40

m&p-Xylene ug/L 9.610 96 70-130969.6 0 40

Methyl-tert-butyl ether ug/L 7.8 L05 157 70-1301698.4 7 40

Methylene Chloride ug/L 5.35 106 70-130934.7 13 40

o-Xylene ug/L 4.65 93 70-130954.8 2 40

Styrene ug/L 4.35 85 70-130814.0 5 40

Tetrachloroethene ug/L 4.45 88 70-130964.8 8 40

Toluene ug/L 5.05 100 70-1301035.1 3 40

Total Trihalomethanes (Calc.) ug/L 18.520 92 70-1309118.2 2 40

trans-1,2-Dichloroethene ug/L 5.55 110 70-1301135.6 3 40

Trichloroethene ug/L 5.25 104 70-1301185.9 12 40

Trichlorofluoromethane ug/L 7.0 L05 139 70-1301487.4 6 40

Vinyl chloride ug/L 5.75 113 70-1301175.9 3 40

Xylene (Total) ug/L 14.215 95 70-1309614.4 1 40

1,2-Dichloroethane-d4 (S) % 109 70-130103

4-Bromofluorobenzene (S) % 102 70-130102

Toluene-d8 (S) % 100 70-13099





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#=QC#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


336353

EPA 504.1

EPA 504.1

504 EDB DBCP


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

AnalyzedMDL

1,2-Dibromo-3-chloropropane ug/L 0.0049U 0.020 12/06/16 03:520.0049

1,2-Dibromoethane (EDB) ug/L 0.0075U 0.010 12/06/16 03:520.0075

Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1801781

1,2-Dibromo-3-chloropropane ug/L 0.20.25 80 70-1301130.28 34 40

1,2-Dibromoethane (EDB) ug/L 0.21.25 84 70-1301130.28 30 40

Parameter Units

MS

Result

% Rec

Limits Qual% RecConc.

1801877MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpike

Result

35279833001

1801878

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

1,2-Dibromo-3-chloropropane

ug/L .44 121 65-135114 6 40.440.0047U 0.53 0.50

1,2-Dibromoethane (EDB) ug/L .44 135 65-135120 12 40.440.0072U 0.59 0.52





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#=QC#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


335264

EPA 508.1

EPA 508.1

508 GCS Pesticide


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

AnalyzedMDL

Alachlor ug/L 0.035U 0.20 12/01/16 06:280.035

Atrazine ug/L 0.063U 0.10 12/01/16 06:280.063

Chlordane (Technical) ug/L 0.047U 0.20 12/01/16 06:280.047

Endrin ug/L 0.0070U 0.010 12/01/16 06:280.0070

gamma-BHC (Lindane) ug/L 0.0030U 0.020 12/01/16 06:280.0030

Heptachlor ug/L 0.012U 0.040 12/01/16 06:280.012

Heptachlor epoxide ug/L 0.0030U 0.020 12/01/16 06:280.0030

Hexachlorobenzene ug/L 0.019U 0.10 12/01/16 06:280.019

Hexachlorocyclopentadiene ug/L 0.032U 0.10 12/01/16 06:280.032

Methoxychlor ug/L 0.051U 0.10 12/01/16 06:280.051

PCB-1016 (Aroclor 1016) ug/L 0.080U 0.10 12/01/16 06:280.080

PCB-1221 (Aroclor 1221) ug/L 0.029U 0.10 12/01/16 06:280.029

PCB-1232 (Aroclor 1232) ug/L 0.029U 0.10 12/01/16 06:280.029

PCB-1242 (Aroclor 1242) ug/L 0.051U 0.10 12/01/16 06:280.051

PCB-1248 (Aroclor 1248) ug/L 0.062U 0.10 12/01/16 06:280.062

PCB-1254 (Aroclor 1254) ug/L 0.023U 0.10 12/01/16 06:280.023

PCB-1260 (Aroclor 1260) ug/L 0.066U 0.10 12/01/16 06:280.066

Simazine ug/L 0.069U 0.070 12/01/16 06:280.069

Toxaphene ug/L 0.61U 1.0 12/01/16 06:280.61

Decachlorobiphenyl (S) % 93 70-130 12/01/16 06:28

Parameter Units

LCS

Result

% Rec


1795134LABORATORY CONTROL SAMPLE:

LCSSpike

Alachlor ug/L 1.11 112 70-130

Atrazine ug/L 1.51.2 117 70-130

Chlordane (Technical) ug/L 0.047U

Endrin ug/L 0.060.05 119 70-130

gamma-BHC (Lindane) ug/L 0.11.1 113 70-130

Heptachlor ug/L 0.26.2 128 70-130

Heptachlor epoxide ug/L 0.12.1 125 70-130

Hexachlorobenzene ug/L 0.75 L0.5 149 70-130

Hexachlorocyclopentadiene ug/L 0.78 L0.5 156 70-130

Methoxychlor ug/L 0.60.5 121 70-130

PCB-1016 (Aroclor 1016) ug/L 0.080U










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Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


Parameter Units

LCS

Result

% Rec



LCSSpike


Simazine ug/L 1.0.88 114 70-130

Toxaphene ug/L 0.61U

Decachlorobiphenyl (S) % 114 70-130

Parameter Units

MS

Result

% Rec



MSSpike

Result

7555964002

1795367

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Alachlor ug/L 2.2 108 65-135109 1 402.2ND 2.4 2.4

Atrazine ug/L 2.8 92 65-13575 20 402.8ND 2.5 2.1

Chlordane (Technical) ug/L 40ND 0.10U 0.10U

Endrin ug/L .11 116 65-135130 12 40.11ND 0.13 0.14

gamma-BHC (Lindane) ug/L .22 104 65-135103 1 40.22ND 0.23 0.23

Heptachlor ug/L .44 114 65-135115 0 40.44ND 0.51 0.51

Heptachlor epoxide ug/L .22 121 65-135122 1 40.22ND 0.27 0.27

Hexachlorobenzene ug/L 1.1 135 65-135131 4 401.1ND 1.5 1.5

Hexachlorocyclopentadiene ug/L 1.1 124 65-135132 7 401.1ND 1.4 1.5

Methoxychlor ug/L 1.1 126 65-135121 4 401.1ND 1.4 1.3

PCB-1016 (Aroclor 1016) ug/L 40ND 0.18U 0.18U







Simazine ug/L 1.9 94 65-13590 4 401.9ND 1.8 1.8

Toxaphene ug/L 40ND 1.4U 1.4U

Decachlorobiphenyl (S) % 101 70-130102 40





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#=QC#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


335276

EPA 552.2

EPA 552.2

5522 Haloacetic Acids


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

AnalyzedMDL

Dibromoacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037

Dichloroacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037

Haloacetic Acids (Total) mg/L 0.00037U 0.0010 12/02/16 09:520.00037

Monobromoacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037

Monochloroacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037

Trichloroacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037

2,3-Dibromopropanoic Acid (S) % 95 70-130 12/02/16 09:52

Parameter Units

LCS

Result

% Rec



LCSSpike

Dibromoacetic Acid mg/L 0.011.01 107 70-130

Dichloroacetic Acid mg/L 0.010.01 100 70-130

Haloacetic Acids (Total) mg/L 0.050.05 99

Monobromoacetic Acid mg/L 0.0095.01 95 70-130

Monochloroacetic Acid mg/L 0.0092.01 92 70-130

Trichloroacetic Acid mg/L 0.010.01 103 70-130

2,3-Dibromopropanoic Acid (S) % 109 70-130

Parameter Units

MS

Result

% Rec



MSSpike

Result

35279528001

1795377

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Dibromoacetic Acid mg/L .01 74 70-13074 0 30.015.1 ug/L 0.012 0.013

Dichloroacetic Acid mg/L M1.01 58 70-13056 2 30.012.5 ug/L 0.0083 0.0081

Haloacetic Acids (Total) mg/L .05 73 78 6.058.7 ug/L 0.045 0.048

Monobromoacetic Acid mg/L .01 93 70-13093 0 30.010.37Uug/L

0.0093 0.0093

Monochloroacetic Acid mg/L M1,R1.01 59 70-13088 39 30.010.37Uug/L

0.0059 0.0088

Trichloroacetic Acid mg/L .01 79 70-13080 0 30.011.2 ug/L 0.0091 0.00912,3-Dibromopropanoic Acid(S)

% 75 70-13078





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#=QC#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


Parameter Units

MS

Result

% Rec



MSSpike

Result

35279706001

1795379

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Dibromoacetic Acid mg/L .01 84 70-13082 2 30.010.37Uug/L

0.0084 0.0082

Dichloroacetic Acid mg/L M1.01 61 70-13060 2 30.013.1 ug/L 0.0092 0.0090

Haloacetic Acids (Total) mg/L .05 77 79 2.0510 ug/L 0.048 0.050

Monobromoacetic Acid mg/L .01 94 70-13096 3 30.010.37Uug/L

0.0094 0.0096

Monochloroacetic Acid mg/L M1.01 68 70-13085 22 30.010.37Uug/L

0.0068 0.0085

Trichloroacetic Acid mg/L .01 78 70-13073 4 30.016.9 ug/L 0.015 0.0142,3-Dibromopropanoic Acid(S)

% 95 70-13094





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#=QC#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


337822

EPA 420.4

EPA 420.4

420.4 Phenolics


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

AnalyzedMDL

Phenolics, Total Recoverable mg/L 0.0050U 0.010 12/15/16 14:440.0050

Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1816951

Phenolics, Total Recoverable mg/L 0.41.4 102 90-1101000.40 3 20





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#=ARR#

ANALYTICAL RESULTS - RADIOCHEMISTRY

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


Parameters Act ± Unc (MDC) Carr Trac Units Analyzed CAS No. Qual

• Split off 500 ml amber un-preserved bottle for Tritium analysis.• Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the samplepreservation requirement of pH <2 for radiochemistry analysis.

Comments:

Method

PWS: Site ID: Sample Type:

Radon 282.5 ± 73.6 (71.9)C:NA T:NA

pCi/L 12/02/16 21:55 10043-92-2 1pSM7500RnB-07

Gross Alpha 1.64U ± 0.905 (1.64)C:NA T:NA

pCi/L 12/06/16 21:16 12587-46-1EPA 900.0

Radium-226 0.584U ± 0.350 (0.584)C:NA T:92%

pCi/L 12/15/16 10:27 13982-63-3EPA 903.1

Radium-228 1.04U ± 0.545 (1.04)C:68% T:84%

pCi/L 12/16/16 11:35 15262-20-1EPA 904.0

Strontium-90 0.465U ± 0.238 (0.465)C:97% T:NA

pCi/L 12/08/16 20:17 10098-97-2 N2ASTM D5811-95

Tritium -49.9 ± 138 (251)C:NA T:NA

pCi/L 12/09/16 17:32 10028-17-8EPA 906.0

Total Uranium 0.193U ± 0.005 (0.193)C:NA T:NA

ug/L 12/19/16 16:04 7440-61-1ASTM D5174-97





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#=QCR#

QUALITY CONTROL - RADIOCHEMISTRY

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


242497

EPA 904.0

EPA 904.0

904.0 Radium 228


Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers



Matrix: Water

Analyzed

Radium-228 pCi/L 12/16/16 11:350.0511 ± 0.373 (0.857) C:66% T:81%





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#=QCR#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


242090

SM7500RnB-07

SM7500RnB-07

7500Rn B Radon





Matrix: Water

Analyzed

Radon pCi/L 12/02/16 21:2223.8 ± 19.9 (32.0) C:NA T:NA





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#=QCR#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


242496

EPA 903.1

EPA 903.1

903.1 Radium-226





Matrix: Water

Analyzed

Radium-226 pCi/L 12/15/16 10:090.000 ± 0.313 (0.701) C:NA T:95%





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#=QCR#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


242576

ASTM D5811-95

ASTM D5811-95

ASTM D5811 Sr 89/90 Eichrom





Matrix: Water

Analyzed

Strontium-90 pCi/L N212/08/16 13:290.407 ± 0.612 (1.30) C:96% T:NA





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#=QCR#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


242582

EPA 906.0

EPA 906.0

906.0 Tritium





Matrix: Water

Analyzed

Tritium pCi/L 12/09/16 16:3082.6 ± 148 (252) C:NA T:NA





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#=QCR#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


242328

EPA 900.0

EPA 900.0

900.0 Gross Alpha/Beta





Matrix: Water

Analyzed

Gross Alpha pCi/L 12/07/16 09:29-0.104 ± 0.561 (1.63) C:NA T:NA





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#=QCR#


Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133


QC Batch:

QC Batch Method:

Analysis Method:


242704

ASTM D5174-97

ASTM D5174-97

D5174.97 Total Uranium KPA





Matrix: Water

Analyzed

Total Uranium ug/L 12/19/16 15:55-0.011 ± -0.001 (0.193) C:NA T:NA





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#=QL#

QUALIFIERS

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.

ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.

Act - Activity

Unc - Uncertainty: SDWA = 1.96 sigma count uncertainty, all other matrices = Expanded Uncertainty (95% confidence interval).Gamma Spec = Expanded Uncertainty (95.4% Confidence Interval)

(MDC) - Minimum Detectable Concentration

Trac - Tracer Recovery (%)

Carr - Carrier Recovery (%)

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - Ormond BeachPASI-O

Pace Analytical Services - GreensburgPASI-PA

ANALYTE QUALIFIERS

Sample 35279584001 from this analytical project was analyzed outside of the recommended Radon-222 hold time of fourdays. Results reported are decay corrected to the sample collection date and time supplied by the client.

1p

Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0

Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples.

L3

Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1

The lab does not hold NELAC/TNI accreditation for this parameter.N2

RPD value was outside control limits.R1

Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5





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#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

35279584

16-333-0328: EXP 3133

Lab ID Sample ID QC Batch Method QC Batch Analytical Method

Analytical

Batch

35279584001 336353 33645616-333-0328 EPA 504.1 EPA 504.1

35279584001 335264 33546916-333-0328 EPA 508.1 EPA 508.1

35279584001 335276 33574616-333-0328 EPA 552.2 EPA 552.2

35279584001 33754016-333-0328 EPA 524.2

35279584001 24209016-333-0328 SM7500RnB-07

35279584001 24232816-333-0328 EPA 900.0

35279584001 24249616-333-0328 EPA 903.1

35279584001 24249716-333-0328 EPA 904.0

35279584001 24257616-333-0328 ASTM D5811-95

35279584001 24258216-333-0328 EPA 906.0

35279584001 24270416-333-0328 ASTM D5174-97

35279584001 33782216-333-0328 EPA 420.4





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Test Results Units MQL By Analytical DF Date / Time …...Lab No : Delta Water Non-Ozonated Sampled:...

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