Teknokroma Capillary Columns

7TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s

Fig. 1. Verification of Hydrothermal Treatment

1 - 2-Octanone 5 - 2,6-Dimethylphenol2 - C-10 6 - 2,6-Dimethylaniline3 - 1-Octanol 7 - C-124 - C-11 8 - C-13

2

1

4

5

63

7 8

Fig. 2. Deactivation Stage (Intermediate Test)

1 - 2-Octanone2 - C-103 - 1-Octanol4 - C-115 - 2,6-Dimethylphenol6 - 2,6-Dimethylaniline7 - C-128 - C-13

Teknokroma Capillary ColumnsTeknokroma has been at the forefront of chromatographic developments in Spain.From its beginnings at 1979, and in order to find the right solutions to the widearray of analytical problems that appear daily in a laboratory, Teknokroma hasalways been involved in the Spanish and European market, not only with columnsfrom the leading world manufactures, but also of those of our own manufacture.

A few years ago, Teknokroma introduced the basic line of high resolution capillarycolumns (Teknokroma columns) which were very well received in the market.Due to the on going research effort carried out by our Research Department incollaboration with the Consejo Superior de Investigaciones Científicas (CSIC) andthe Instituto Químico de Sarriá (IQS) and the support obtained from various publicadministrations (CDTI, CIDEM, MINER and FCTAC) we have been able tocontinuously update and expand our product line with other stationary phases.

All of our columns are manufactured according to a strict established protocol,and within the ISO 9001:2000 quality rules.

Stage 1:Stage 1:Stage 1:Stage 1:Stage 1: Hydrothermal treatmentStage 2:Stage 2:Stage 2:Stage 2:Stage 2: Deactivation processStage 3:Stage 3:Stage 3:Stage 3:Stage 3: Wetting, bonding and crosslinkingStage 4:Stage 4:Stage 4:Stage 4:Stage 4: Quality control

Stage 1: Hydrothermal Treatment

Teknokroma starts its manufacturing process with the selection of the best possiblefused silica tubing. This tube presents an extremely reduced tolerance of internaldiameters and has a polyimide outer coating capable of withstanding the highesttemperatures without loss of its flexible mechanical characteristics. Each one of thebatches of silica used in the process is conveniently characterized as an essentialstep to set the Hydrothermal Treatment conditions (Fig. 1) that will give rise to asurface containing a high and constant density of silanol groups, which will laterbe properly deactivated.

This treatment is indispensable, as the different capillary tubing manufacturedbatches present a very low and irregularly distributed silanol group density due tothe high temperature manufacturing process (~2000ºC).

Stage 2: Deactivation process

The deactivation process, which is different for each type of stationary phase, iscarefully controlled (fig. 2), ensuring that the tubing surface has acquired thenecessary chemical inertness and surface tension in order to be able to proceedwith the second stage of stationary phase deposition. This step also facilitates theintroduction of specific functional groups on the tubing wall which are very usefulfor the later binding of the stationary phase or to give the columns a given endpoint characteristics.

Stage 3: Wetting, bonding and crosslinking

Stationary phase selection for optimum wetting of the column is a critical point inregards to column quality. Teknokroma uses extremely pure polymers for itsphases, in order to guarantee that our columns will respond to the requirementsthat our customers expect in terms of efficiency, reproducibility, stability andminimal bleeding.

The polymers used are carefully fractionated to eliminate the low molecular weightcomponents and trace catalyst. This results in a higher thermal stability and lowerbleeding. Then, these polymers are tested by means of spectroscopic (FTIR, UV,NMR), chromatographic (GPC) techniques and by differential thermal analysis.Fig. 3 shows the molecular exclusion chromatography of the polymer TRB-5 withits corresponding thermogravimetric curve in Fig. 4.

The crosslinking and bonding of the stationary phase is achieved by avoiding theuse of peroxides which are the cause of many of the problems related to residualactivity due to phase degradation and thermal instability exhibited in numerousimported columns.

TKG 1095

Fig. 3. GPC Chromatogram of TRB-5 polymer

TKG 1097

TKG 1096

TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s

8 TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s

Fig. 4 DTA curve of TRB-5 polymer

Fig. 5 Quality Control Test

Column: TBR-5TBR-5TBR-5TBR-5TBR-5, 60m x 0.25 mm ID x 0.25 µm.Carrier gas: He, 25 psi.Oven: 110°C (Isothermal).Injection: 1µl, split. (1:100:250ºC)Concentration: Approx. 5ng of each compound on columnDetector: FID, 250°C

Peak Name1 - 2-Octanone2 - C-103 - 1-Octanol4 - C-115 - 2,6-Dimethylphenol6 - 2,6-Dimethylaniline7 - C-128 - C-13

Fig. 6. GROB test

Column: TRB-5TRB-5TRB-5TRB-5TRB-5, 30m x 0.25 mm ID x 0.25 µm.Carrier gas: He, 12 psi.Injection: 1µl, split, (1:100), 260ºCDetector: FID, 280°C

Peak Name1 - 2,3-Butanediol2 - C-103 - 1-Octanol4 - 2,6-Dimethylphenol5 - C-116 - Nonanal7 - 2-Ethylhexanoic acid8 - 2,6-Dimethylaniline9 - E-1010 - Dicyclohexylamine11 - E-1112 - E-12

TKG 1099 TKG 1100

The fact that a given stationary phase is crosslinked and/or chemically bonded tothe capillary tube inner wall allows, if necessary, the recovery or regeneration ofan accidentally contaminated column by washing it with the adequate series ofsolvents.

Stage 4. Quality Control

S E L E C T P R O V E N Q U A L I T Y

When you buy a Teknokroma capillary column you receive a product designed andmanufactured in our laboratory with the aim to help you solve your analyticalproblems and which meets all of our quality criteria.At the same time you obtain from our Technical Department at Teknokroma theassurance that we will be at your side to help you with all the problems andconcerns experience in the lab.Remember that each column is individually tested and the accompanying test datais the proof that the column meets our quality specifications and thus we expect itto meet your demands. Each one of the columns obtained by this process isrigorously controlled by means of a strict Quality Control Test (fig. 5 and 6), whichensures that you will receive a guaranteed quality product.

Stationary Phase

The selection of the ideal column for a given analysis may look like a complexproblem since we need to be right on the selection of the polarity of the stationaryphase as well as column length, internal diameter and film thickness.The polarity of the stationary phase is chosen depending on the kind of compoundsyou wish to separate. Non polar phases, such as TRB-1 and TRB-5, separate com-pounds by their boiling points. Intermediate polarity phases such as TRB-WAX, TRB-1701, combine retention by boiling point with the more selective interactionthrough hydrogen bridges or dipolar moments, etc., and thus provide a higherselectivity. The principal mechanisms of polar phases such as TR-CN100(Cyanosilicone with 100% of cyano propyl groups) lie in the dipole-dipoleinteractions between the functional groups of the stationary phase and those fromthe substances to be separated. These type of phases retain polar compounds morethan non polar ones.

In general, non polar phases are more thermally stable than the polar phases. Inother words, the higher the column polarity, the lower its thermal stability. Most ofthe Teknokroma columns are cross-linked, which results in high thermal stability.The cross-linking in a stationary phase produces slight changes in thephysicochemical characteristics of the phase as well as in its polarity relative to theuncross-linked phase. Thus TEKNOKROMA also offers in its catalog columns withnon bonded phases that show the selectivity of the original phase (for instanceTR-SE30, TR-SE54, TR-20M, etc.).

Length

The efficiency of a chromatographic column (number of theoretical plates permeter) is a function of its length. The standard length used for most of theseparations is 25-30 meters. With this length one can obtain a high efficiency withrelative short times of analysis. Columns of 15m are used for rapid controlanalyses, reaction monitoring, etc. as well as for the chromatography of highmolecular weight substances while columns of 50-60 m, 100 m or 150 m areused for very complex samples. Teknokroma exclusively manufactures a 150 mcolumn for detail analyses of petroleum and essential oil hydrocarbons. As ageneral rule, we can say that in a constant temperature chromatographic analysis,the number of theoretical plates and analysis time are directly proportional to thecolumn length while resolution is directly proportional to the square root of thetheoretical plates. Thus, we need to take into account that when we double columnlength, its resolution only increases by 40% whereas analysis time doubles.

Teknokroma Capillary Columns

TKG 1098

9

TKG 1101


Internal Diameter

The column internal diameter is inversely proportional to its separation power. Thesmaller the diameter, the larger the efficiency and thus a higher resolution but atthe same time the loading capacity decreases.For samples containing a large number of substances where you may need a givenresolution, it is recommended to use small internal diameter columns (0.20-0.25mm) and for samples with a high range of concentrations higher internal diametercolumns are recommended (0.32-0.53 mm) since these larger diameters allow forthe injection of a higher sample amount.

Columns of 0.53 mm ID (semicapillary) have a loading capacity similar to that ofpacked columns, which they replace in many analyzes, with better resolution,higher chemical inertness and lower analysis time.The 0.32-0-53 mm ID columns can be used with either the injector for capillarycolumns or with the packed column injector, due to the high flow-rates at whichthey can operate.

In the increasingly used GC-MS systems it is recommended to work with small IDcolumns (0.10mm, 0.15mm, 0.18mm, 0.20 mm and 0.22 mm) so as not toexceed the capacity of the vacuum system. Recently, capillary columns of 0.1 mmID have appeared on the market. These generate high plate numbers or, in otherwords, to reduce analysis time without losing resolution. The high efficiency ofthese columns (7000-10000 plates/meter) allows the resolution of complexsamples using shorter column lengths, thus with very short analysis times, with theresulting cost reduction for the laboratory. Evidently, their loading capacity is alimiting factor and in order to obtain the best performance from these columns weneed to take into account instrumental factors (injector-detector).

Film Thickness

The film thickness of the stationary phase deposited inside the capillary columnexerts an influence on the number of effective theoretical plates that can beobtained with the column for a given separation, on its loading capacity, on thebleed level and on the elution temperature of a compound.A film thickness of 0.25-0.32 mm is the standard thickness allowing for acompromise between loading capacity and resolution; and for the injection ofsamples with a wide volatility range.

Thick films increase retention of the most volatile components whereas thin filmsprovide faster elution at lower temperatures.As a general rule, thin films (0.1 mm) must be used for compounds with a highmolecular weight such as triglycerides, antioxidants, etc., which have elutiontemperatures over 300°C. Thick films must be used for low boiling substancesbecause thick films increase the interaction between the substances and thestationary phase. Specifically, 3-5 µm films are used to separate solvents, gases,and very volatile substances at room temperature or lower.

When the thickness of the stationary phase increases, thermal stability decreases,and thus the bleed level is higher which will limit the maximum operatingtemperature of the column.

The β factor defines the relation between the column internal diameter and thestationary phase thickness, thereby helping you to select the most appropriatecolumn for your analysis.

In addition, the β factor allows for the easy exchange of columns since, for a givenanalysis with the same stationary phase, similar β factors will result in the sameor very similar retention times and capacity factors. Of course, this implies takinginto account the column loading capacity (phase thickness and internal diameter).

Factor ββββββββββ Column suitable for the separation of:Column suitable for the separation of:Column suitable for the separation of:Column suitable for the separation of:Column suitable for the separation of:

>400 High molecular weight compounds100 - 400 All purpose use<100 Volatile compounds of low molecular weight

Bleed Level

The bleed level of stationary phase from a capillary column is the parameter whichwill determine the level of sensitivity in a given assay. It is directly related to theamount of stationary phase in the column and thus with the film thickness. It alsoincreases exponentially with temperature (fig.7).

A low bleed level will allow you to work without problems with the whole range ofmodern high sensitivity detectors and at the same time will result in lesscontamination. This will also allow the quantification of high boiling point or highmolecular weight compounds which are analyzed by means of high temperaturegradients.


Fig. 7. Bleed level (GROB test)

Column: TRB-5TRB-5TRB-5TRB-5TRB-5,15m x 0.25mm ID x 0.25µm.Carrier gas: He, 6 psi.Injection: 1µl, split. (1:100), 280ºCDetector: FID, 350°C

Bleed level (FID) <4pA (325°C)

325ºC

1 0

Stationary Phase Cross Reference (Table 1)

Maximum Efficiency

All manufacturing stages for capillary columns have been optimized in order to beable to offer our customers columns of very high efficiency.

Maximum Reproducibility

When you select a Teknokroma column for your analyses you can be assured thateach of the steps in the production process has been thoroughly controlled toensure that there are no deviations from the established quality parameters. All ofthe steps incorporate the maximum possible automation procedures.This translates into a high reproducibility level with regards to the chromatographicperformance of our columns.


TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s

AMORKONKET AMORKONKET AMORKONKET AMORKONKET AMORKONKET

,RUFLUSBRT,SM1-BRT,th1-BRT,1-BRT,051LORTEP-BRT,LORTEP-BRT

03-ES,7882-BRT,ANOP2.05.BRT

NOITISOPMOCESAHP NOITISOPMOCESAHP NOITISOPMOCESAHP NOITISOPMOCESAHP NOITISOPMOCESAHP

enaxolisyloplyhtemid%001

TNELIGA TNELIGA TNELIGA TNELIGA TNELIGA

1-ARTLU,101PH,1-PH7882-BD,th1-BD,1-BD

OCLEPUS OCLEPUS OCLEPUS OCLEPUS OCLEPUS

1-YTIUQE,1-BPSRUFLUS1-BPS

KETSER KETSER KETSER KETSER KETSER

7882-xtR,1-xtR

NAIRAV NAIRAV NAIRAV NAIRAV NAIRAV

BC5LIS-PCSMBC5LIS-PC

EGS EGS EGS EGS EGS

1-PB

HCETLLA HCETLLA HCETLLA HCETLLA HCETLLA

1-TA

XERDAUQ XERDAUQ XERDAUQ XERDAUQ XERDAUQ

1-700

ERUTUCNEMONPSU ERUTUCNEMONPSU ERUTUCNEMONPSU ERUTUCNEMONPSU ERUTUCNEMONPSU

83G,2G,1G

,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT,ENIMA5-BRT,LORETS-BRT45-ES,72G-BRT,526.5-BRT

lynehpid%5-lyhtemid%59enaxolisylop

5-BD,2-ARTLU,5-PH5-SAP,th5-BD,526.5-BD

5-YTIUQE.5-BPS,5-CAS.5-ETP

MTQ5-ETP

,5-ITX,5-xtRSM5-xtR

BC8LIS-PC 5-PB 5-TA 2-700 63G,72G

5X.ateM 5X.ateM 5X.ateM 5X.ateM 5X.ateM lynehpid%5-lyhtemid%59enelynehplisylop

SM5-BD.AT5-PH 5-NDM SMliS5-xtR BC8LIS-PCSM/deelBwoL

5-XPB sm5-TA SM5-700

34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT %49-lynehplyporponayc%6enaxolisyloplyhtemid

426-PH,1031-PH426-BD,1031-BD

1031-BPS34G-IVO

,1031-xtR426-xtR

426-XPB 426-TA 34G

41-BRT 41-BRT 41-BRT 41-BRT 41-BRT lyhtemid%68-lynehpid%41enaxolisylop

BC31LIS-PC


LOCOV.02-BPS 02-TA 7-700 23G.82G


53-BD.53-PH 53-BPS 53-xtR ,53-XPB806-XPB

53-TA 11-700 24G

1071-BRT 1071-BRT 1071-BRT 1071-BRT 1071-BRT %68-lynehplyporponayc%41enaxolisyloplyhtemid

1071-SAP.1071-PH1071-BD

1071-BPS 1071-xtR BC91LIS-PC 01-PB 1071-TA 1071-700

522-BRT 522-BRT 522-BRT 522-BRT 522-BRT %05-lynehplyporponayc%05enaxolisyloplyhtemid

522-BD.522-PH 522-xtR BC34LIS-PC 522-PB 522-TA 522-700 91G.7G

GAP-BRT GAP-BRT GAP-BRT GAP-BRT GAP-BRT %05-enelyhteylop%05locylqenelyporpylop

GAP

PAFF-BRT PAFF-BRT PAFF-BRT PAFF-BRT PAFF-BRT roflocylgenelyhteylopdetaertsdnuopmoccidica

PAFF-BD.PAFF-PH 0001-PS.LOKUN BD-XAWLIBATS BC85XAW-PC 12-PB ,0001-TAPAFF

PAFF-700 53G.52G


,71-BD,+05-PH806-BD

.05-BPS0522-BPS

05-xtR BC42LIS-PC 05-TA 71-700 3G

th05-BRT th05-BRT th05-BRT th05-BRT th05-BRT lyhtemid%05-lynehpid%05enaxolisylop

th71BD 56-xtR BC-BAT TH56-700 71G

05F-BRT 05F-BRT 05F-BRT 05F-BRT 05F-BRT lyporporoulfirt%05enaxolisyloplyhtem%05

002-BD.012-BD 002-xtR 012-TA 012-700 6G

XAW-BRT XAW-BRT XAW-BRT XAW-BRT XAW-BRT locylgenelyhteylop%001 ,XAW-BDXAWONNI.M02-PHrteXAW-BD

01XAWOCLEPUSM02xawobraC

XAWLIBATS BC25XAW-PC 02-PB XAW-TA WC-700 ,61G,51G,41G93G.02G

BD-XAW-BRT BD-XAW-BRT BD-XAW-BRT BD-XAW-BRT BD-XAW-BRT roflocylgenelyhteylopdetaertsdnuopmoccisab

xaWcisaB-PH,MAC enimA-xawobraC BC15XAW-PC

xaW.ateM xaW.ateM xaW.ateM xaW.ateM xaW.ateM locylgenelyhteylop%001 XAW-BD,XAW-PH BC75XAW-PC

agemO-XAW-BRT agemO-XAW-BRT agemO-XAW-BRT agemO-XAW-BRT agemO-XAW-BRT locylgenelyhteylop%001 XAWAGEMO XAWEMAF

001NC-RT 001NC-RT 001NC-RT 001NC-RT 001NC-RT lyporponaycsib%001enaxolisylop

0432-PS 0432-tR 88LIS-PC

LOSERC-RT LOSERC-RT LOSERC-RT LOSERC-RT LOSERC-RT esahpdednobnonyrateirporp LOSERC-PC


71-PH 3G

COV.ateM COV.ateM COV.ateM COV.ateM COV.ateM esahpdednobyrateirporp COV-PH,2.205-BD LOCOV 2.205-xtR

806-BRT 806-BRT 806-BRT 806-BRT 806-BRT esahpdednobyrateirporp 806-PH 806-BPS 806-PB

PECT-RT PECT-RT PECT-RT PECT-RT PECT-RT enaporp)yxohteonayc(sirt-3,2,1 PECT PECT-tR PECT-PC

InterInterInterInterInternal diameter (mm)nal diameter (mm)nal diameter (mm)nal diameter (mm)nal diameter (mm) Theoretical Plates (N/m)Theoretical Plates (N/m)Theoretical Plates (N/m)Theoretical Plates (N/m)Theoretical Plates (N/m)0,10 7.000 - 9.0000,20 4.700 - 5.5000,25 3.300 - 4.6000,32 2.700 - 3.7000,53 1.400 - 2.200

Wide Stationary Phase Selection

Teknokroma incorporates in its catalogue a selection of capillary columns preparedwith the stationary phases most commonly used in the field of gas chromatography(Table 1).

11

TRB-1

Column: TRB-1TRB-1TRB-1TRB-1TRB-1, P/N TR-111226Dimensions: 25m x 0.15mm x 1.2µmInjection: 1µL Test SP-4-7300, split 1:100, 280ºCCarrier gas: H2, constant pressure 22 psi (151.6 KPa).Oven program: 145ºC (isothermal)Detector: FID, 300ºC

Peak Name

1 Methylene chloride2 2-Octanone3 C-104 1-Octanol5 2,6-Dimethylphenol6 C-117 2,6-Dimethylaniline8 C-12

TKG 1102

TRB-1

100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase

• 100% Dimethylpolysiloxane.• Non-polar phase• Column for general use• High thermal stability• Ideal column for the analysis of petrochemical products and industrial solvents

Structure of Poly(dimethyl)siloxane

Si OOCH3

CH3

m

TRB-1


TRB-1 Equ iva lent PhaseTRB-1 Equ iva lent PhaseTRB-1 Equ iva lent PhaseTRB-1 Equ iva lent PhaseTRB-1 Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-1,HP101,ULTRA-1, DB-1Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: SPB-1, EQUITY-1Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-1, Rtx -2887VVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL 5 CBS G ES G ES G ES G ES G E: BP-1.A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1Macherey-Nagel:Macherey-Nagel:Macherey-Nagel:Macherey-Nagel:Macherey-Nagel: OPTIMA-1

TRB-1

InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,100,100,100,100,10 10 0,10 -60 to 325/350 TR-110141TR-110141TR-110141TR-110141TR-11014110 0,40 -60 to 320/340 TR-110441TR-110441TR-110441TR-110441TR-110441

20 0,10 -60 to 325/350 TR-110181TR-110181TR-110181TR-110181TR-110181

20 0,40 -60 to 320/340 TR-110481TR-110481TR-110481TR-110481TR-110481

0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-113B89TR-113B89TR-113B89TR-113B89TR-113B89

15 0,15 -60 to 325/350 TR-111319TR-111319TR-111319TR-111319TR-111319

15 0,35 -60 to 325/350 TR-110319TR-110319TR-110319TR-110319TR-11031915 0,50 -60 to 325/350 TR-110519TR-110519TR-110519TR-110519TR-110519


25 0,35 -60 to 325/350 TR-110329TR-110329TR-110329TR-110329TR-110329


30 0,35 -60 to 325/350 TR-110339TR-110339TR-110339TR-110339TR-110339


50 0,33 -60 to 325/350 TR-113359TR-113359TR-113359TR-113359TR-113359


60 0,15 -60 to 325/350 TR-111369TR-111369TR-111369TR-111369TR-111369

60 0,50 -60 to 325/350 TR-110569TR-110569TR-110569TR-110569TR-110569

0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-110112TR-110112TR-110112TR-110112TR-110112

15 0,25 -60 to 325/350 TR-110212TR-110212TR-110212TR-110212TR-110212


25 0,10 -60 to 325/350 TR-110122TR-110122TR-110122TR-110122TR-110122



30 0,25 -60 to 325/350 TR-110232TR-110232TR-110232TR-110232TR-110232


50 0,10 -60 to 325/350 TR-110152TR-110152TR-110152TR-110152TR-110152


50 1,00 -60 to 320/340 TR-111052TR-111052TR-111052TR-111052TR-111052


60 0,50 -60 to 325/350 TR-110562TR-110562TR-110562TR-110562TR-110562

60 1,00 -60 to 325/350 TR-111062TR-111062TR-111062TR-111062TR-111062

100 1,00 -60 to 325/350 TR-111092TR-111092TR-111092TR-111092TR-111092105 1,00 -60 to 325/350 TR-1110K2TR-1110K2TR-1110K2TR-1110K2TR-1110K2

0,320,320,320,320,32 15 0,10 -60 to 325/350 TR-110113TR-110113TR-110113TR-110113TR-110113


15 1,00 -60 to 325/350 TR-111013TR-111013TR-111013TR-111013TR-111013


25 0,25 -60 to 325/350 TR-110223TR-110223TR-110223TR-110223TR-110223

25 0,50 -60 to 325/350 TR-110523TR-110523TR-110523TR-110523TR-110523

1 2


Si OOCH3

CH3

m

TRB-1ht


0,250,250,250,250,25 15 0,10 -60 a 395 TR-610112

30 0,10 -60 a 395 TR-610132

0,320,320,320,320,32 15 0,10 -60 a 390 TR-610113

30 0,10 -60 a 390 TR-610133

TRB-1ht

Column: Retention Gap (intermediate polarity) 5m x 0.53mm(TR-200055) + TRB-1htTRB-1htTRB-1htTRB-1htTRB-1ht ( TR-610113)Dimensions: 15m x 0.32mm x 0.10µmInjection: 0.3µL Poliwax 655 (0.1% in CS2), on column (sec. cool 30 s), 280ºCCarrier gas: H2, constant flow 2mL/minOven temperature: 50ºC(2 min) @ 15ºC/min to 380ºC(5 min)Detector: FID, 390ºC

380ºC380ºC380ºC380ºC380ºC<10 pA<10 pA<10 pA<10 pA<10 pA

TKG 1103

TRB-1htTRB-1ht

100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.

• 100% Dimethylpolysiloxane• Non-polar phase• Produced specially for high temperature analyses (Max.temp. 400ºC).• Fused silica tubing with polyimide coating for high temperatures.• Uses: analysis of compounds with high boiling point, triglycerides, waxes, etc.

TRB-1


TRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: DB-1htR e s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Stx-1HTA l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1 ht


25 1,00 -60 to 325/350 TR-111023TR-111023TR-111023TR-111023TR-111023


30 0,25 -60 to 325/350 TR-110233TR-110233TR-110233TR-110233TR-110233


30 3,00 -60 to 280/300 TR-113033TR-113033TR-113033TR-113033TR-113033


50 0,50 -60 to 325/350 TR-110553TR-110553TR-110553TR-110553TR-110553


60 0,10 -60 to 325/350 TR-110163TR-110163TR-110163TR-110163TR-110163


60 1,00 -60 to 325/350 TR-111063TR-111063TR-111063TR-111063TR-111063



15 0,50 -60 to 320/340 TR-110515TR-110515TR-110515TR-110515TR-110515


15 5,00 -60 to 270/290 TR-115015TR-115015TR-115015TR-115015TR-115015


25 0,50 -60 to 320/340 TR-110525TR-110525TR-110525TR-110525TR-110525


25 5,00 -60 to 270/290 TR-115025TR-115025TR-115025TR-115025TR-115025


30 0,88 -60 to 310/330 TR-110835TR-110835TR-110835TR-110835TR-110835


30 3,00 -60 to 270/290 TR-113035TR-113035TR-113035TR-113035TR-113035



50 1,50 -60 to 310/330 TR-111555TR-111555TR-111555TR-111555TR-111555


60 0,10 -60 to 320/340 TR-110165TR-110165TR-110165TR-110165TR-110165


60 3,00 -60 to 270/290 TR-113065TR-113065TR-113065TR-113065TR-113065


100 3,00 -60 to 270/290 TR-113095TR-113095TR-113095TR-113095TR-113095

105 3,00 -60 to 270/290 TR-1130K5TR-1130K5TR-1130K5TR-1130K5TR-1130K5

13

Structure of Poly(dimethyl)siloxane Si OOCH3

CH3

m

TRB-1ms

Column: TRB-1msTRB-1msTRB-1msTRB-1msTRB-1ms, P/N TR-510262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1µL Test MX5 (10 to 20 ng/comp. on column), split 1:100, 280ºCCarrier gas: H2, constant pressure 25 psi (172 KPa).Oven temperature: 100ºC @ 6ºC/min to 325ºC(5 min)Detector: FID, 340ºC

Peak Name

1 Methylene chloride2 1,2-Hexanediol3 Nitroso-di-n-propylamine4 Benzoic acid5 C-146 2,4-Dinitrophenol7 4-Nitrophenol8 4-Nitroaniline9 Pentachlorophenol10 Carbazole11 C-2012 C-2113 C-2214 Benzo(b)fluoranthene15 Benzo(k)fluoranthene

TKG 1104

TRB-1msTRB-1ms


• 100% Dimethylpolysiloxane.

• These columns, with a selectivity identical to the TRB-1, fulfil column bleedspecifications that make them compatible with analysis of trace componentswith GC/MS. Therefore, the standard column of 30 m x 0.25 mm x 0.25 µmhas a guaranteed maximum bleed of 4 pA at 325 °C.

• Great chemical inertness towards active constituents and excellent thermalstability.

• Improved signal/noise ratio, which enables greater sensitivity to be obtainedwith the MS, ECD, NPD, SCD, etc. detectors and provides greater precision inquantitative analysis at trace levels.

• Less column bleed means less detectors contamination and greater speed inconditioning columns.


TRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-1MS, DB-1MSRe s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-1msVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL 5 CB MSA l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1 MS

TRB-1ms


0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-5133B9TR-5133B9TR-5133B9TR-5133B9TR-5133B915 0,33 -60 to 325/350 TR-513319TR-513319TR-513319TR-513319TR-513319

25 0,33 -60 to 325/350 TR-513329TR-513329TR-513329TR-513329TR-513329


60 0,33 -60 to 325/350 TR-513369TR-513369TR-513369TR-513369TR-513369



30 0,25 -60 to 325/350 TR-510232TR-510232TR-510232TR-510232TR-510232


60 0,25 -60 to 325/350 TR-510262TR-510262TR-510262TR-510262TR-510262

60 1,00 -60 to 325/350 TR-511062TR-511062TR-511062TR-511062TR-511062

1 4


Si OOCH3

CH3

m

TRB-Petrol



• Column for analyzing complex mixtures of hydrocarbons according to theASTM regulations (American Society for Testing and Materials).

• Sufficient resolution power to undertake PNA, PONA and PIANO analysis.

TRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: DB-PetroSupe l c oSupe l c oSupe l c oSupe l c oSupe l c o: Petrocol DH

TRB-PetrolInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 100 0,50 -60 to 300/320 TR-110592TR-110592TR-110592TR-110592TR-110592

TRB- SULFUR

Column: TRB-SULFURTRB-SULFURTRB-SULFURTRB-SULFURTRB-SULFUR, 30 m x 0.32 mm x 4.0 µmMercaptans

Peak Names

1- SH22- Methyl mercaptan3- Ethyl mercaptan4- 2-propylmercaptan5- Terbutyl mercaptan6- Methyl ethyl sulfide7- 1-propylmercaptan8- 2-butyl mercaptan9- T.H.T.


Si OOCH3

CH3

m

TKG 1105

TRB-Sulfur



• Column specially designed for the analysis of sulphurous compounds(in natural gas, petrol derivates, wines, beer, etc.)

• Guaranteed thermal stability, with low column bleed.

TRB-Petrol

TRB-Sulfur


TRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent Phase

Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: SPB-1 SULFUR

TRB-SulfurInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,320,320,320,320,32 30 4,00 -60 to 270/290 TR-114033TR-114033TR-114033TR-114033TR-114033

15

TRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent Phase

Supelco: Supelco: Supelco: Supelco: Supelco: Petrocol DH 150.

TRB-Petro.150InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 150 1,00 -60 to 300/320 TR-1110G2TR-1110G2TR-1110G2TR-1110G2TR-1110G2

Si OOCH3

CH3

m


TRB-PETROL

Column: TRB-PETROLTRB-PETROLTRB-PETROLTRB-PETROLTRB-PETROL, 100m x 0.25mm x 0.50µm TR 110592Temperature: 60ºC (isothermal)Injector: 260ºCCarrier gas: H2, 34 psiInjection: Test for hydrocarbons, split (1:100)Detector: FID, 260º

tr (min.) Compound

6.39 n-Hexane7.70 Benzene8.03 Cyclohexane9.37 n-Heptane12.47 Toluene16.02 n-Octane22.93 m-Xylene23.08 p-Xylene30.83 n-Nonane

TKG 1106

TRB-Petrol

TRB-Petro. 150TRB-Petro.150



• Maximum resolution for hydrocarbon analysis

• Detailed hydrocarbon analysis.

• Volatiles in essential oil and beverages


1 6 TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s

TRB-Petro.150

TRB-PETRO.15O

Column: TRB-PETRO.150TRB-PETRO.150TRB-PETRO.150TRB-PETRO.150TRB-PETRO.150, P/N TR-I110G2Dimensions: 150m x 0.25mm x 1.0µmInjection: 0.1µ1 unleaded gasoline,split 100:1 @ 280°CCarrier gas: He, 75psi (517 kPa) @ 35°COven program: 35°C(hold 135 min.) to 200°C @ 2°C/min. (hold 20 min)Detector: FID @ 280°C

1. n-Butane2. Isopentane3. n-Pentane4. 2,2-Dimethylbutane5. Cyclopentane6. 2,3-Dimethylbutane7. 2-Methylpentane8. 3-Methylpentane9. n-Hexane10. 2,4-Dimethylpentane

11. Benzene12. 2-Methylhexane13. 2,3-Dimethylpentane14.3-Methylhexane15. 2,2,4- Trimethylpentane16. n-Heptane17.2,5-Dimethylhexane18. 2,4-Dimethylhexane19.2,3,4-Trimethylpentane20. Toluene

21. 2,3,3- Trimethylpentane22. 2,3-Dimethylhexane23. 2-Methylheptane24. 3-Methylheptane25.2-Methyl-1-heptene26. n-Octane27. Ethylbencene28. m-Xylene29. p-Xylene30. o-Xylene

17

TKG 1107

31. 1-Nonene32. n-Nonane33. Isopropylbenzene34. 3,3,5- Trimethylheptane35. 2,4,5- Trimethylheptane36. n-propylbenzene37.1-Methyl-3-ethylbenzene38. 1-Methyl-4-ethylbenzene39.1,3,5-Trimethylbenzene40. 3,3,4- Trimethylheptane

41. 1-Methyl-2-ethylbenzene42. 1,2,4- Trimethylbenzene43. Isobuthylbenzene44. sec-Buthylbenzene45. n-Decane .46. 1,2,3- Trimethylbenzene47.lndane48. 1,3-Diethylbenzene49. n-Butylbenzene50.1,4-Dimethyl-2-ethylbenzene

51. 1,3- Dimethyl-4-ethylbenzene52. 1,2-Dimethyl-4-ethylbenzene53. 1,2,4,5- Tetramethylbenzene54.1,2,3,5-Tetramethylbenzene55. Naphthalene56.2-Methylnaphthalene57.1-Methylnaphthalene58. Dimethylnaphthalenes

TRB-Petro.150


1 8

TRB-50.2PONA



• Column designed for the complete analysis of PONA hydrocarbons (P-Paraffins, O-Olefins, N-Naphthenes and A-Aromatics) in petrol-derived productsaccording to the ASTM regulations, method D5134.

Structure of Poly(dimethyl)siloxane Si OOCH3

CH3

m

TRB-50.2PONAInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,200,200,200,200,20 50 0,50 -60 to 320/340 TR-110559TR-110559TR-110559TR-110559TR-110559

Si OOCH3

CH3

m

TRB-2887InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,530,530,530,530,53 10 2,65 -60 to 340/360 TR-192645TR-192645TR-192645TR-192645TR-192645


TRB-2887

Column: TRB-2887TRB-2887TRB-2887TRB-2887TRB-2887, P/N TR-192645Dimensions: 10m x 0.53mm x 2.65µmInjection: 1µL standard RS-31222, split 1:10, 300ºCCarrier gas: H2, constant pressure 5 psi (34.4 KPa)Oven temperature: 40ºC @ 15ºC/min to 350ºC(5 min)Detector: FID, 360ºC. Baseline not compensed

Peak Name

1 n-hexane (C-6)2 n-heptane (C-7)3 n-octane (C-8)4 n-nonane (C-9)5 n-decane (C-10)6 n-undecane (C-11)7 n-dodecane (C-12)8 n-tetradecane (C-14)9 n-hexadecane (C-16)10 n-octadecane (C-18)11 n-eicosane (C-20)12 n-tetracosane (C-24)13 n-octacosane (C-28)14 n-dotriacontane( C-32)15 n-hexatriacotane (C-36)16 n-tetracontane (C-40)17 n-tetratetracontane (C-44)TKG 1108

TRB-2887


• 100% Dimethylpolysiloxane

• Designed specifically for simulated distillation according to the ASTM methodD2887.

TRB-50.2PONA

TRB-2887


TRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-PONASupe l c oSupe l c oSupe l c oSupe l c oSupe l c o: Petrocol DH 50.2Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-1 PONAVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL PONA CBS G ES G ES G ES G ES G E: BP-1 PONA


Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: DB-2887Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: PETROCOL-2887Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-2887

19

TRB-5

(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.

• It is the most versatile and universal stationary phase in the gaschromatography analysis field.

• The low percentage of phenyl in the polymer structure gives it a characteristicaffinity towards the compounds with aromatic rings. This phase, the mostpopular one, due to its great thermal stability and chemical inertness is thestationary phase of choice for any type of analysis.

• It allows the analysis of acidic and basic compounds.

• It is ideal for the analysis in the environmental field. Analysis of dioxines,PCB´s, PCT´s, polyaromatic compounds, phenols, herbicides, organochlorinatedand organophosphorus pesticides, aromatic hydrocarbons, solvents, drugs,oils, etc...

Structure of Poly(dimethyldiphenyl)siloxane

m n

Si OO SiCH3

CH3O

TRB-5

Column: TRB-5TRB-5TRB-5TRB-5TRB-5, P/N TR-120232Dimensions: 30m x 0.25mm x 0.25µmInjection: 1µL chlorinated pesticides mixture, splitless @230ºC (25-270 ppb on column)Carrier gas: H2, constant pressure 12 psi (87.7 KPa) 150ºCOven temperature: 150ºC to 225ºC@ 2ºC/min (10 min.)Detector: ECD, 310ºC

Peak Name

1. 2,4,5,6-tetrachloro-m-xylene2. γ-BHC3. δ-BHC4. heptachlor5. aldrin6. β-BHC7. δ-BHC

8. heptachlor epoxide9. endosulfan I10. γ-chlordane11.α-chlordane12. 4,4´- DDE13. dieldrin14. endrin15. 4,4´- DDD

16. endosulfan II17. 4,4´- DDT18. endrin aldehyde19. endosulfan sulfate20. methoxychlor21. endrin ketone22. decachlorobiphenyl

TKG 1109

TRB-5


2 0 TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s


0,100,100,100,100,10 10 0,10 -60 to 325/350 TR-120141TR-120141TR-120141TR-120141TR-120141


20 0,40 -60 to 320/350 TR-120481TR-120481TR-120481TR-120481TR-120481

0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-1233B9TR-1233B9TR-1233B9TR-1233B9TR-1233B915 0,15 -60 to 325/350 TR-121319TR-121319TR-121319TR-121319TR-121319

15 0,35 -60 to 325/350 TR-120319TR-120319TR-120319TR-120319TR-120319


25 0,33 -60 to 325/350 TR-123329TR-123329TR-123329TR-123329TR-123329


30 0,15 -60 to 325/350 TR-121339TR-121339TR-121339TR-121339TR-121339


50 0,15 -60 to 325/350 TR-121359TR-121359TR-121359TR-121359TR-121359


50 0,50 -60 to 325/350 TR-120559TR-120559TR-120559TR-120559TR-120559


60 0,50 -60 to 325/350 TR-120569TR-120569TR-120569TR-120569TR-120569

0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-120112TR-120112TR-120112TR-120112TR-120112

15 0,25 -60 to 325/350 TR-120212TR-120212TR-120212TR-120212TR-120212


25 0,10 -60 to 325/350 TR-120122TR-120122TR-120122TR-120122TR-120122


25 1,00 -60 to 320/350 TR-121022TR-121022TR-121022TR-121022TR-121022


30 0,50 -60 to 325/350 TR-120532TR-120532TR-120532TR-120532TR-120532


50 0,25 -60 to 325/350 TR-120252TR-120252TR-120252TR-120252TR-120252


60 0,10 -60 to 325/350 TR-120162TR-120162TR-120162TR-120162TR-120162


60 1,00 -60 to 325/350 TR-121062TR-121062TR-121062TR-121062TR-121062

0,320,320,320,320,32 15 0,10 -60 to 325/350 TR-120113TR-120113TR-120113TR-120113TR-120113

15 0,25 -60 to 325/350 TR-120213TR-120213TR-120213TR-120213TR-120213


15 3,00 -60 to 280/350 TR-123013TR-123013TR-123013TR-123013TR-123013

25 0.10 -60 to 325/350 TR-120123TR-120123TR-120123TR-120123TR-120123

TRB-5TRB-5InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,320,320,320,320,32 25 0,25 -60 to 325/350 TR-120223TR-120223TR-120223TR-120223TR-120223


25 3,00 -60 to 280/350 TR-123023TR-123023TR-123023TR-123023TR-123023


30 0,50 -60 to 325/350 TR-120533TR-120533TR-120533TR-120533TR-120533


50 0,10 -60 to 325/350 TR-120153TR-120153TR-120153TR-120153TR-120153


50 1,00 -60 to 325/350 TR-121053TR-121053TR-121053TR-121053TR-121053


60 0,25 -60 to 325/350 TR-120263TR-120263TR-120263TR-120263TR-120263


60 3,00 -60 to 280/350 TR-123063TR-123063TR-123063TR-123063TR-123063



15 3,00 -60 to 270/290 TR-123015TR-123015TR-123015TR-123015TR-123015


25 0,50 -60 to 320/340 TR-120525TR-120525TR-120525TR-120525TR-120525


25 5,00 -60 to 270/290 TR-125025TR-125025TR-125025TR-125025TR-125025


30 0,88 -60 to 310/330 TR-120835TR-120835TR-120835TR-120835TR-120835


30 3,00 -60 to 270/290 TR-123035TR-123035TR-123035TR-123035TR-123035


50 0,50 -60 to 320/340 TR-120555TR-120555TR-120555TR-120555TR-120555



60 0,50 -60 to 320/340 TR-120565TR-120565TR-120565TR-120565TR-120565


60 5,00 -60 to 270/290 TR-125065TR-125065TR-125065TR-125065TR-125065


RestekRestekRestekRestekRestek: Rtx-5, Rtx XTIAgilent/JWAgilent/JWAgilent/JWAgilent/JWAgilent/JW: HP-5, Ultra-2, DB-5, DB-5.625Supelco:Supelco:Supelco:Supelco:Supelco: SPB-5, PTE-5, SAC-5, Equity-5

Chromapack/VChromapack/VChromapack/VChromapack/VChromapack/Varianar ianar ianar ianar ian: CP-SIL8CBAlltechAl ltechAl ltechAl ltechAl ltech: AT-5Macherey-NagelMacherey-NagelMacherey-NagelMacherey-NagelMacherey-Nagel: OPTIMA-5QuadrexQuadrexQuadrexQuadrexQuadrex: 007-2SGESGESGESGESGE: BP-5

21

IRGANOX 1010

Column: TRB-5ht, TRB-5ht, TRB-5ht, TRB-5ht, TRB-5ht, 15m X 0,25 mm X 0,10 µm, P/N TR-620112Injection: 1µ1 (Irganox 1010, 12mg/ml chloroform), split (1:60), 370ºCCarrier gas: H2, 6psi (41,3 kPa)Oven temp.: 150°C to 380ºC (10 min.) @ 30°C/min.Detector: FID to 390°C


m n

Si OO SiCH3

CH3O


m n

Si OO SiCH3

CH3O

TKG 1110

Sterols

Column: TRB-Sterol, TRB-Sterol, TRB-Sterol, TRB-Sterol, TRB-Sterol, 30m X 0,22 mm X 0,22 µm, P/N TR-182238Oven Temp.: 265ºCInjector: 280ºCCarrier gas: H2, 18 psi (124 kPa)Injection: 0,5 µl sterols standard, (25 mg/ml.) split(1:100)Detector: FID 300°C

TKG 1111

TRB-5ht/Inox-5htTRB-5ht/Inox-5ht


• Produced specially for analysis at high temperature up to 400ºC.

• Fused silica tube covered with polyimide, resistant to high temperatures, orstainless steel tube (specially deactivated).

• Excellent symmetry for compounds with high boiling points.

• Preferably used for the analysis of waxes, triglycerides, sterol esters,polyoxyethylenated alcohols, etc.

TRB-5ht/Inox-5htInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 15 0,10 -60 to 395 TR-620112TR-620112TR-620112TR-620112TR-620112

30 0,10 -60 to 395 TR-620132TR-620132TR-620132TR-620132TR-620132

0,320,320,320,320,32 15 0,10 -60 to 390 TR-620113TR-620113TR-620113TR-620113TR-62011330 0,10 -60 to 390 TR-620133TR-620133TR-620133TR-620133TR-620133

TRB-SterolTRB-Sterol


• Column specifically designed for the analysis of complex mixtures of sterols,from either animal or plant origin.

• Deactivation method of the capillary tube wall, developed by Teknokroma,that guarantees a high chemical inertness a low bleeding level and allows theanalysis of sterols without derivatization.

• The column is specifically tested for sterols.

TRB-5-SterolInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,220,220,220,220,22 30 0,22 -60 to 325-350 TR-182238TR-182238TR-182238TR-182238TR-182238


TRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent Phase

Agi lentAgi lentAgi lentAgi lentAgi lent: DB-5ht

TRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent Phase

SupelcoSupelcoSupelcoSupelcoSupelco: SAC-5

2 2

TRB-5ms

TRB-5ms


• The TRB-5ms Column uses the same stationary phase as TRB-5, but thepolymer synthesis process, the capillary deactivation technique and thebonding and crosslinking procedures have been optimized to obtain theminimum possible bleeding level and an exceptional chemical inertness.

• The bleeding specifications for a column of 30m x 0,25 mm x 0,25 µm(P/N 520232) inidcate that it is lower than 4 pA at 325ºC.

• Column recommended to work with any selective detector.

• Ideal column to connect with a mass detector. Its ultra-low bleeding joined toits high chemical inertness allows for a better signal/noise ratio (highersensitivity level), and therefore better detection and quantification of samplecomponents at low concentrations.

TRB -5ms Equ iva lent PhaseTRB-5ms Equ iva lent PhaseTRB-5ms Equ iva lent PhaseTRB-5ms Equ iva lent PhaseTRB-5ms Equ iva lent Phase

RestekRestekRestekRestekRestek: Rtx 5msAgli lent/JWAgli lent/JWAgli lent/JWAgli lent/JWAgli lent/JW: : : : : HP-5MSSupelcoSupelcoSupelcoSupelcoSupelco: PTE-5, Equity-5Macherey-NagelMacherey-NagelMacherey-NagelMacherey-NagelMacherey-Nagel: OPTIMA-5VVVVVarianar ianar ianar ianar ian: CP-Sil8-MS


m n

Si OO SiCH3

CH3O


TRB-5MSInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,200,200,200,200,20 12 0,33 -60 to 325-350 TR-5233B9TR-5233B9TR-5233B9TR-5233B9TR-5233B9

15 0,33 -60 to 325-350 TR-523319TR-523319TR-523319TR-523319TR-523319

25 0,33 -60 to 325-350 TR-523329TR-523329TR-523329TR-523329TR-523329

30 0,33 -60 to 325-350 TR-523339TR-523339TR-523339TR-523339TR-523339

50 0,33 -60 to 325-350 TR-523359TR-523359TR-523359TR-523359TR-523359

60 0,33 -60 to 325-350 TR-523369TR-523369TR-523369TR-523369TR-523369

0,250,250,250,250,25 15 0,10 -60 to 325-350 TR-520112TR-520112TR-520112TR-520112TR-520112

15 0,25 -60 to 325-350 TR-520212TR-520212TR-520212TR-520212TR-520212

15 1,00 -60 to 325-350 TR-521012TR-521012TR-521012TR-521012TR-521012

30 0,10 -60 to 325-350 TR-520132TR-520132TR-520132TR-520132TR-520132

30 0,25 -60 to 325-350 TR-520232TR-520232TR-520232TR-520232TR-520232

30 1,00 -60 to 325-350 TR-521032TR-521032TR-521032TR-521032TR-521032

60 0,10 -60 to 325-350 TR-520162TR-520162TR-520162TR-520162TR-520162

60 0,25 -60 to 325-350 TR-520262TR-520262TR-520262TR-520262TR-520262

60 1,00 -60 to 325-350 TR-521062TR-521062TR-521062TR-521062TR-521062

0,320,320,320,320,32 15 0,10 -60 to 325-350 TR-520113TR-520113TR-520113TR-520113TR-520113

15 0,25 -60 to 325-350 TR-520213TR-520213TR-520213TR-520213TR-520213

15 0,50 -60 to 325-350 TR-520513TR-520513TR-520513TR-520513TR-520513

15 1,00 -60 to 325-350 TR-521013TR-521013TR-521013TR-521013TR-521013

30 0,10 -60 to 325-350 TR-520133TR-520133TR-520133TR-520133TR-520133

30 0,25 -60 to 325-350 TR-520233TR-520233TR-520233TR-520233TR-520233

30 0,50 -60 to 325-350 TR-520533TR-520533TR-520533TR-520533TR-520533

30 1,00 -60 to 325-350 TR-521033TR-521033TR-521033TR-521033TR-521033

60 0,10 -60 to 325-350 TR-520163TR-520163TR-520163TR-520163TR-520163

60 0,25 -60 to 325-350 TR-520263TR-520263TR-520263TR-520263TR-520263

60 0,50 -60 to 325-350 TR-520563TR-520563TR-520563TR-520563TR-520563

60 1,00 -60 to 325-350 TR-521063TR-521063TR-521063TR-521063TR-521063

0,530,530,530,530,53 15 0,50 -60 to 320-340 TR-520515TR-520515TR-520515TR-520515TR-520515

15 1,00 -60 to 320-340 TR-521015TR-521015TR-521015TR-521015TR-521015

15 1,50 -60 to 310-330 TR-521515TR-521515TR-521515TR-521515TR-521515

30 0,50 -60 to 320-340 TR-520535TR-520535TR-520535TR-520535TR-520535

30 1,00 -60 to 320-340 TR-521035TR-521035TR-521035TR-521035TR-521035

30 1,50 -60 to 310-330 TR-521535TR-521535TR-521535TR-521535TR-521535

23

Peak Name

1. Methylene chloride2. 1,2-Hexanediol3. Nitroso-di-n-propylamine4. Benzoic acid5. C-146. 2,4-Dinitrophenol7. 4-Nitrophenol8. 4-Nitroaniline9. Pentachlorophenol10. Carbazole11. C-2012. C-2113. C-2214. Benzo(b)fluoranthene15. Benzol(k)fluoranthene16. Benzo(ghi)perylene

Test MX5

Column: TRB-5ms, TRB-5ms, TRB-5ms, TRB-5ms, TRB-5ms, P/N TR-520232Dimensions: 30 m x 0,25 mm x 0,25 µmInjection: 1µ1, split (1:100), 5 to 10 ng/comp. on column, 280ºCCarrier gas: H2, 12 psi (87,7 kPa)Oven temp.: 100°C to 325ºC (5 min.) @ 6°C/min.Detector: FID to 300°CSample: Test MX5

Injection of 1ng/peak on columnExceptional symmetry

Excellent resolution

Bleedinglevel <2pA

TKG 1112

TRB-5msThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetry in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thatappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPA official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.


2 4

Amines Test

Column: TRB-5AmineTRB-5AmineTRB-5AmineTRB-5AmineTRB-5Amine, P/N TR-210532Dimensions: 30 m x 0.25 mm x 0.50 µmInjection: 1 µL (split 1:50), 280ºCCarrier gas: H2, 12 psi (87.7 kPa).Oven temperature: 100ºC to 280ºC (5 min.) @ 20ºC/min.Detector: FID, 300ºCSample: Test SP-48278 (500ng/µl)

Peak Name

1 Methyl tert-butyl ether2 Benzylamine3 n-Octylamine4 n-Nonylamine5 2,4-Dimethylaniline6 2,6-Dimethylaniline7 n-Decylamine8 C-159 C-1610 C-1711 Tri-n-hexylamine12 C-1813 C-20

TKG 1113

TRB-5AmineTRB-5Amine

9595959595% % % % % Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.

• Column specially designed for the analysis of amines.

• Basic deactivation of the column surface with reagents synthetized in ourlaboratories, that jointly with the crosslinking method have permitted theminimization of the absorption level and tailing of basic compounds, like thealkylamines, alcoholamines, basic pharmaceuticals, aromatic amines, etc.

• Selectivity and thermal stability equivalent to the TRB-5 columns.


m n

Si OO SiCH3

CH3O

TRB-5AmineInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 15 0,50 -60 to 300/315 TR-210512TR-210512TR-210512TR-210512TR-21051215 1,00 -60 to 300/315 TR-211012TR-211012TR-211012TR-211012TR-21101230 0,50 -60 to 300/315 TR-210532TR-210532TR-210532TR-210532TR-21053230 1,00 -60 to 300/315 TR-211032TR-211032TR-211032TR-211032TR-21103260 0,50 -60 to 300/315 TR-210562TR-210562TR-210562TR-210562TR-21056260 1,00 -60 to 300/315 TR-211062TR-211062TR-211062TR-211062TR-211062

0,320,320,320,320,32 15 0,50 -60 to 300/315 TR-210513TR-210513TR-210513TR-210513TR-21051315 1,00 -60 to 300/315 TR-211013TR-211013TR-211013TR-211013TR-21101315 1,50 -60 to 290/305 TR-211513TR-211513TR-211513TR-211513TR-21151330 0,50 -60 to 300/315 TR-210533TR-210533TR-210533TR-210533TR-21053330 1,00 -60 to 300/315 TR-211033TR-211033TR-211033TR-211033TR-21103330 1,50 -60 to 290/305 TR-211533TR-211533TR-211533TR-211533TR-21153360 0,50 -60 to 300/315 TR-210563TR-210563TR-210563TR-210563TR-21056360 1,00 -60 to 300/315 TR-211063TR-211063TR-211063TR-211063TR-21106360 1,50 -60 to 290/305 TR-211563TR-211563TR-211563TR-211563TR-211563


TRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent Phase

RestekRestekRestekRestekRestek: Rtx-5AmineSupelcoSupelcoSupelcoSupelcoSupelco: PTA-5


25

TRB-5. 625

TRB-5.625InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-2633B9TR-2633B9TR-2633B9TR-2633B9TR-2633B925 0,33 -60 to 325/350 TR-263329TR-263329TR-263329TR-263329TR-26332950 0,33 -60 to 325/350 TR-263359TR-263359TR-263359TR-263359TR-263359

0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-260112TR-260112TR-260112TR-260112TR-26011215 0,25 -60 to 325/350 TR-260212TR-260212TR-260212TR-260212TR-26021215 0,50 -60 to 325/350 TR-260512TR-260512TR-260512TR-260512TR-26051215 1,00 -60 to 325/350 TR-261012TR-261012TR-261012TR-261012TR-26101230 0,10 -60 to 325/350 TR-260132TR-260132TR-260132TR-260132TR-26013230 0,25 -60 to 325/350 TR-260232TR-260232TR-260232TR-260232TR-26023230 0,50 -60 to 325/350 TR-260532TR-260532TR-260532TR-260532TR-26053230 1,00 -60 to 325/350 TR-261032TR-261032TR-261032TR-261032TR-26103260 0,10 -60 to 325/350 TR-260162TR-260162TR-260162TR-260162TR-26016260 0,25 -60 to 325/350 TR-260262TR-260262TR-260262TR-260262TR-260262

0,320,320,320,320,32 15 0,10 -60 to 325/350 TR-260113TR-260113TR-260113TR-260113TR-26011315 0,25 -60 to 325/350 TR-260213TR-260213TR-260213TR-260213TR-26021315 0,50 -60 to 325/350 TR-260513TR-260513TR-260513TR-260513TR-26051315 1,00 -60 to 325/350 TR-261013TR-261013TR-261013TR-261013TR-26101330 0,10 -60 to 325/350 TR-260133TR-260133TR-260133TR-260133TR-26013330 0,25 -60 to 325/350 TR-260233TR-260233TR-260233TR-260233TR-26023330 0,50 -60 to 325/350 TR-260533TR-260533TR-260533TR-260533TR-26053330 1,00 -60 to 325/350 TR-261033TR-261033TR-261033TR-261033TR-26103360 0,10 -60 to 325/350 TR-260163TR-260163TR-260163TR-260163TR-260163

0,530,530,530,530,53 15 1,50 -60 to 320/340 TR-261515TR-261515TR-261515TR-261515TR-26151530 0,50 -60 to 320/340 TR-260535TR-260535TR-260535TR-260535TR-26053530 1,00 -60 to 310/330 TR-261035TR-261035TR-261035TR-261035TR-26103560 0,25 -60 to 325/350 TR-260263TR-260263TR-260263TR-260263TR-260263

TRB-5. 625


• Specially manufactured column to fulfil the level of inertness required by theEPA methods for the analysis of semivolatile compounds, designed formethods 625, 1625, 8270 and CLP protocols.

• Inertness and minimum absorption for acidic, basic and neutral compounds.


m n

Si OO SiCH3

CH3O

TRB-G27

TRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent Phase

RestekRestekRestekRestekRestek: Rtx-XTI-5SupelcoSupelcoSupelcoSupelcoSupelco: PTE-5Agilent:Agi lent:Agi lent:Agi lent:Agi lent: DB.5.625

TRB-G27InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,530,530,530,530,53 30 5,00 -60 to 270/290 TR-175035TR-175035TR-175035TR-175035TR-175035

TRB-G27


• Column which fulfils the specifications of the American Pharmacopea (USP),for the test of organic volatile impurities (OVI) in pharmaceutical products.Methods <USP 467>.


m n

Si OO SiCH3

CH3O

TRB -G27 Equ iva lent PhaseTRB-G27 Equ iva lent PhaseTRB-G27 Equ iva lent PhaseTRB-G27 Equ iva lent PhaseTRB-G27 Equ iva lent Phase

RestekRestekRestekRestekRestek: Rtx-G27SupelcoSupelcoSupelcoSupelcoSupelco: G27


2 6

Peak Name

1 Methanol2 Ethanol3 Acetonitrile4 Acetone5 Isopropanol6 Ethyl ether7 Methylene chloride8 n-Propanol9 Methyl ethyl ketone (MEK)10 n-Hexane11 Ethyl acetate12 Chloroform13 Tetrahydrofuran (THF)14 Cyclohexane15 1,2-Dicholoroethane16 Benzene17 Carbon tetrachloride18 n-Butanol19 n-Heptane20 Trichloroethylene21 1,4-Dioxane22 Pyridine23 Toluene24 Dimethylformamide (DMF)25 p-Xylene26 m-Xylene27 o-Xylene

Residual solvents in Pharmaceutical Products

Column: TRB-G27TRB-G27TRB-G27TRB-G27TRB-G27, 30 m x 0,53 mm x 5,0 µm, P/N TR-175035Injectioon: 220ºC, (split 1:80), 5 m phenylmethyl deactivated retention gapCarrier Gas: He, 4,5 psi (31kPa), 35 cm/s. to 35ºCOven Temp: 35ºC (10 min.) to 100ºC @ 5º C/min. to 240ºC (5 min.) @ 25ºC/min.Detector: FID@ 250ºCSample: 0,02 µl solvent mixture

TKG 1114

TRB-G27

Meta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent Phase

RestekRestekRestekRestekRestek: Rtx-5Sil MSAgilent/JWAgilent/JWAgilent/JWAgilent/JWAgilent/JW::::: DB.5 MS, HP-5TASupelco:Supelco:Supelco:Supelco:Supelco: MDN-5Chromopack/VChromopack/VChromopack/VChromopack/VChromopack/Varian: arian: arian: arian: arian: CP-SIL8CB MSAlltech: AT-5msQuadrex: Quadrex: Quadrex: Quadrex: Quadrex: 007-5MSSGE:SGE:SGE:SGE:SGE: BPX-5

Meta.X5Meta.X5

Silphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedphase.phase.phase.phase.phase.

• Choice column for the analysis of semivolatile compounds with GC ,EM.

• Polymer synthesis designed and developed by scientists at Teknokroma.

• Selectivity similar to TRB-5.

• New generation of column incorporates arylene groups in the polymerstructure, and this improves the thermal stability, reduces the bleeding leveland provides optimal resolution for aromatic compounds.

• Manufacturing procedures of this Teknokroma column guarantees maximalinertness and minimal bleeding level.

• Quality control test (MX5) that guarantees total inertness and optimal signal/noise ratio (S/N) for the more active compounds that normally sufferadsorption problems, like 2,4-dinitropherol, 4 nitroaniline andpentachlorophenol.

Structure of Polysiloxane containing p-silphenylene

SiSiCH3

CH3CH3

CH3OO Si

R1O

R2x y


27

Compare Column Bleed Levels

Increase of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofthe stationarthe stationarthe stationarthe stationarthe stationary phase when the temperature increases.y phase when the temperature increases.y phase when the temperature increases.y phase when the temperature increases.y phase when the temperature increases.

Column: Meta.X5Meta.X5Meta.X5Meta.X5Meta.X5, 30 m X 0,25 mm X 0,25 µm, P/N TR-820232Injection: 100ºC,Carrier Gas: H2, 12 psi (82,7 kPa)Oven Temp: 100ºC to 325ªC (5 min.) @ 20º C/min.Detector: FID@ 340ºC

Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)

Peak Name

1 Meta.X52 Manufacturer A3 Manufacturer B4 Manufacturer C

pA

TKG 1115

Meta.X5InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-8233B9TR-8233B9TR-8233B9TR-8233B9TR-8233B925 0,33 -60 to 325/350 TR-823329TR-823329TR-823329TR-823329TR-82332950 0,33 -60 to 325/350 TR-823359TR-823359TR-823359TR-823359TR-823359

0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-820112TR-820112TR-820112TR-820112TR-82011215 0,25 -60 to 325/350 TR-820212TR-820212TR-820212TR-820212TR-82021215 0,50 -60 to 325/350 TR-820512TR-820512TR-820512TR-820512TR-82051215 1,00 -60 to 325/350 TR-821012TR-821012TR-821012TR-821012TR-82101230 0,10 -60 to 325/350 TR-820132TR-820132TR-820132TR-820132TR-82013230 0,25 -60 to 325/350 TR-820232TR-820232TR-820232TR-820232TR-82023230 0,50 -60 to 325/350 TR-820532TR-820532TR-820532TR-820532TR-82053230 1,00 -60 to 325/350 TR-821032TR-821032TR-821032TR-821032TR-82103260 0,10 -60 to 325/350 TR-820162TR-820162TR-820162TR-820162TR-82016260 0,25 -60 to 325/350 TR-820262TR-820262TR-820262TR-820262TR-820262


Meta.X5


0,320,320,320,320,32 15 0,50 -60 to 325/350 TR-820513TR-820513TR-820513TR-820513TR-82051315 1,00 -60 to 325/350 TR-821013TR-821013TR-821013TR-821013TR-82101330 0,10 -60 to 325/350 TR-820133TR-820133TR-820133TR-820133TR-82013330 0,25 -60 to 325/350 TR-820233TR-820233TR-820233TR-820233TR-82023330 0,50 -60 to 325/350 TR-820533TR-820533TR-820533TR-820533TR-82053330 1,00 -60 to 325/350 TR-821033TR-821033TR-821033TR-821033TR-82103360 0,10 -60 to 325/350 TR-820163TR-820163TR-820163TR-820163TR-82016360 0,25 -60 to 325/350 TR-820263TR-820263TR-820263TR-820263TR-820263



2 8

Signal/Noise ratio

The reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature wheninterinterinterinterinterferences in the identif ication process are minimized.ferences in the identif ication process are minimized.ferences in the identif ication process are minimized.ferences in the identif ication process are minimized.ferences in the identif ication process are minimized.

Column: Meta.X5 Meta.X5 Meta.X5 Meta.X5 Meta.X5, P/N TR-820232Dimensions: 30m x 0.25mm x 0,25 µmInjection:1,0 µL (splitless, 1 min.) 300ºCCarrier gas: He, 12 ml/min. constant flow.Oven temperature: 60ºC (1 min.) to 320º (15 min.) @30ºC/min.Detector: MSD(SIM), transfer line 300ºCSample: DCB/n-Hexane

Signal/Noise ratioSignal/Noise ratioSignal/Noise ratioSignal/Noise ratioSignal/Noise ratio

S/N = 831ng of Decachlorobiphenyl (DCB)

time TKG 1116

Meta.X5

Separation of aromatic polycyclic hydrocarbons (EPA Method 610)

Column: Meta.X5 Meta.X5 Meta.X5 Meta.X5 Meta.X5, P/N TR-820232Dimensions: 30m x 0.25mm x 0,50 µmInjection:0,3 µL (splitless, 1´) 300ºCCarrier gas: H2, 16 PSI (110,2 kPa). Cte.Oven temperature: 40ºC (1 min.) to 200º @ 20ºC/min to 310ºC (5 min.)@4ºC/minDetector: FID, 340ºCSample: Test PAH (aprox. 12ng/comp. in column)

Peak Name

1 Naphathalene2 Acenaphthylene3 Acenaphthene4 Fluorene5 Phenanthrene6 Anthracene7 Fluoranthene8 Pyrene9 Chrysene10 Benz (a) anthracene11 Benz (b) fluoranthene12 Benz (k) fluoranthene13 Benz (a) pyrene14 Indeno (1,2,3-cd) pyrene15 Dibenzo (ah) anthracene16 Benzo (ghi) perylene

All cr it ical pair peaksAll cr it ical pair peaksAll cr it ical pair peaksAll cr it ical pair peaksAll cr it ical pair peakswell separatedwell separatedwell separatedwell separatedwell separated


TKG 1117

29

TRB-1301

9494949494% % % % % Dimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.

• (6%)Cyanopropyl-phenyl-(94%)dimethylpolysiloxane.

• Ideal column for analyzing mixtures of acidic and basic compounds with awide range of polarity.

• This column of intermediate polarity is very useful for analyzing pesticides andherbicides.



0,320,320,320,320,32 15 0,25 -20 to 280/300 TR-600213TR-600213TR-600213TR-600213TR-60021315 1 00 -20 to 260/280 TR-601013TR-601013TR-601013TR-601013TR-60101330 0,25 -20 to 280/300 TR-600233TR-600233TR-600233TR-600233TR-60023330 1,00 -20 to 260/280 TR-601033TR-601033TR-601033TR-601033TR-60103360 0,25 -20 to 280/300 TR-600263TR-600263TR-600263TR-600263TR-60026360 1,00 -20 to 260/280 TR-601063TR-601063TR-601063TR-601063TR-601063

0,530,530,530,530,53 15 1,00 -20 to 260/280 TR-601015TR-601015TR-601015TR-601015TR-60101530 1,00 -20 to 260/280 TR-601035TR-601035TR-601035TR-601035TR-60103560 1,00 -20 to 260/280 TR-601065TR-601065TR-601065TR-601065TR-601065

TRB-1301

Column: TRB-1301TRB-1301TRB-1301TRB-1301TRB-1301, P/N TR-601032Dimensions: 30m x 0.25mm x 1.0µmInjection: 0.5µL standard SP-4-7301 (500 ng/mL), split 1:50, 260ºCCarrier gas: H2, constant pressure 12 psi (82.7 KPa).Oven temperature: 165ºCDetector: FID, 280ºC

Peak Name

1 Methylene chloride2 C-103 2-Octanone4 C-115 1-Octanol6 C-127 2,6-Dimethylphenol8 2,6-Dimethylaniline9 C-1310 C-14

TRB-1301 Equ iva lent PhaseTRB -1301 Equ iva lent PhaseTRB -1301 Equ iva lent PhaseTRB -1301 Equ iva lent PhaseTRB -1301 Equ iva lent Phase

Agi lentAgi lentAgi lentAgi lentAgi lent: HP-1301, HP-624, DB-1301, DB-624SupelcoSupelcoSupelcoSupelcoSupelco: SPB-1301, OVI-G43RestekRestekRestekRestekRestek: Rtx-1301, Rtx-624SGESGESGESGESGE: BPX-624AlltechAl ltechAl ltechAl ltechAl ltech: AT-624

TRB-1301

Structure of Poly(dimethylcyanopropylphenyl)siloxane

Si OO SiCH3

CH3

CH2)3CN

O(

m n

TKG 1118


3 0


Si OO SiCH3

CH3

CH2)3CN

O(

m n

TRB-624

Column: TRB-624TRB-624TRB-624TRB-624TRB-624, P/N TR-601462Dimensions: 60m x 0.25mm x 1.4µmInjection: 1µL solvents mixture, split 1:100 (20-600 ng/comp.), 260ºCCarrier gas: H2, constant pressure 25 psi (172.3 KPa).Oven temperature: 50ºC(5min) @ 6ºC/min to 220ºCDetector: FID, 280ºC

Peak Name

1- Diethylether2- Acetone3- Methyl acetate4- Vinyl acetate5- MEK6- Ethyl acetate7- Tetrahydrofuran8- Cyclohexane9- Benzene10- Isopropyl acetate11- 2-Pentanone

12- 3-Pentanone13- Propyl acetate14- Pyridine15- Toluene16- Isobutyl acetate17- Butyl acetate18- Ethyl benzene19- m-Xylene/p-Xylene20- o-Xylene21- Diisobutylketone22- Nitrobenzene

TRB-624TRB-624


• (6%) Cyanopropyl-phenyl - (94%) dimethylpolysiloxane.

• Column developed specially for environmental analysis of volatile compounds(“Volatile Priority Pollutants”).

• Column perfectly compatible with EPA methods 501.3, 502.2, 524.2, 601,602, 8010, 8015, 8020, 8221, 8240 and 8260.

• Excellent inertness against active compounds.


TKG 1119

TRB -624 Equ iva lent PhaseTRB-624 Equ iva lent PhaseTRB-624 Equ iva lent PhaseTRB-624 Equ iva lent PhaseTRB-624 Equ iva lent Phase

Agilent: HP-1301, HP-624, DB-1301, DB-624Supelco: SPB-1301, OVI-G43Restek: Rtx-1301, Rtx-624SGE: BPX-624Alltech: AT-624


0,200,200,200,200,20 25 1,12 -20 to 240/260 TR-601129TR-601129TR-601129TR-601129TR-6011290,250,250,250,250,25 30 1,40 -20 to 240/260 TR-601432TR-601432TR-601432TR-601432TR-601432

60 1,40 -20 to 240/260 TR-601462TR-601462TR-601462TR-601462TR-6014620,320,320,320,320,32 30 1,80 -20 to 240/260 TR-601833TR-601833TR-601833TR-601833TR-601833

60 1,80 -20 to 240/260 TR-601863TR-601863TR-601863TR-601863TR-6018630,530,530,530,530,53 30 3,00 -20 to 240/260 TR-603035TR-603035TR-603035TR-603035TR-603035



31

TRB-624

Column: TRB-624TRB-624TRB-624TRB-624TRB-624, P/N TR-601462Dimensions: 60m x 0.25mm x 1.4µmInjection: 0.2µL, split 1:5, 260ºCCarrier gas: He,constant pressure 25 psi (172.3 KPa).Oven temperature: 40ºC(8min) @7ºC/min to 160ºC(5min)Detector: FID, 280ºC

Peak Name

1- Heptane (isomers mixture)2- Acetone3- Tetrahydrofuran4- Ethyl acetate5- Isopropyl acetate6- Methanol7- MEK8- Isopropanol9- Ethanol10- n-Propyl acetate11- MIBK12- n-Propanol13- Toluene14- Butyl acetate15- Methoxypropanol16- Methoxypropyl acetate

TRB-624

TKG 1120

TRB-G43


• (6%) Cyanopropyl-phenyl - (94%) dimethylpolysiloxane (USP G43).

• Fulfils the specifications of the American (USP) and European (EP)pharmacopoeia for the analysis of residual solvents (OVI) in pharmaceuticalproducts, USP method <467> and EP method 2.4.24.

• Column with chemical inertness and low bleed guaranteed.

• Specially tested for complete separation of the five solvents regulated byUSP Method 467.

• For this analysis, pharmacopoeia recommends the use of a guard column of5m (P/N TR-200055) to trap the non-volatile impurities in the sample.

TRB-G43


Si OO SiCH3

CH3

CH2)3CN

O(

m n

Peak Name

1- Methanol2- 1,2-Dichloroethene3- Acetonitrile4- Methylene chloride5- n-Hexane6- Cis-1,2-dichloroethene7- Nitromethane8- Chloroform9- Cyclohexane10- 1,1,1-Trichloroethane11- Carbon tetrachloride12- Benzene13- 1,2-Dimethoxyethane14- 1,2-Dichloroethane

15- Trichloroethylene16- Methylcyclohexane17- 1,4-Dioxane18- Pyridine19- Toluene20- 2-Hexanone21- Chlorobenzene22- Dimethylformamide23- Ethylbenzene24- m-Xylene25- p-Xylene26- o-Xylene27- N,N-dimethylacetamide28- 1,2,3,4-Tetrahydronaphthalene

TRB-G43

Column: TRB-G43TRB-G43TRB-G43TRB-G43TRB-G43, P/N TR-163035Dimensions: 30m x 0.53mm x 3.0µmInjection:, split 1:2, 250ºC, 5m x 0.53mm intermediate polarity column (TR-200055)Sample: 0.5 mL headspace 80ºC (2t static head space sampler) 28 Class 1 Mix and Class 2 Mix A, Mix B residual solvents at the regulatory limit concentration.Carrier gas: He, constant pressure 4.8 psi (33.1 KPa), 35 cm/s (40ºC)Oven temperature: 40ºC(20min) @ 10ºC/min to 240ºC(10min)Detector: FID, 250ºC

TKG 1121


3 2

TRB-G43

Column: TRB-G43TRB-G43TRB-G43TRB-G43TRB-G43, P/N TR-163035Dimensions: 30m x 0.53mm x 3.0µmInjection: 1mL headspace (2t static head space sampler), split 1:2 (liner1 mm ID), 5m x 0.53mm intermediate polarity precolumn (TR-200055),100 µL standard vial 20 mL + 5 mL H2O + 1g sodium sulfate, 140ºCCarrier gas: He, constant pressure 7 psi (48.2 KPa).Oven temperature: 40ºC(20min) @ 35ºC/min to 240ºC(20min)Detector: FID, 260ºC

Peak Name

1- Methylene chloride 600 ppm2- Chloroform 60 ppm3- Benzene 2 ppm4- Trichloroethylene 80 ppm5- 1,4-Dioxane 380 ppm

TRB-G43


TKG 1122

TRB-G43InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,530,530,530,530,53 30 3,00 -20 to 240/260 TR-163035TR-163035TR-163035TR-163035TR-163035

TRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent Phase

Agi lentAgi lentAgi lentAgi lentAgi lent: HP-1301, HP-624, DB-1301, DB-624Supelco:Supelco:Supelco:Supelco:Supelco: SPB-1301, OVI-G43Restek:Restek:Restek:Restek:Restek: Rtx-1301, Rtx-624SGE: SGE: SGE: SGE: SGE: BPX-624Alltech:Al ltech:Al ltech:Al ltech:Al ltech: AT-624USP Nomenclature: G43

33

TRB-14

Column: TRB-14TRB-14TRB-14TRB-14TRB-14, P/N TR-801263Dimensions: 60m x 0.32mm x 1.2µmInjection: 0.1µL Amines mixture (0.02-0.2% in Acetonitrile),split 1:25, 200ºCCarrier gas: He, constant pressure 14 psi (96.5 Kpa)Oven temperature: 40ºC(2min) @ 10ºC/min to 250ºCDetector: FID, 280ºC

Peak Name

1 Methylamine2 Acetonitrile3 Diethylamine4 Triethylamine

1

2

4

3

TRB-14TRB-14

(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inkedphase.phase.phase.phase.phase.

• (14%) Diphenyl- (86%) dimethylpolysiloxane.

• Column of intermediate polarity without cyanopropyl groups in its structure.

• Chemical inertness and low bleed guaranteed.

• Confirmation column alongside TRB-1 and TRB-5.


0,250,250,250,250,25 15 0,20 -20 to 300/330 TR-802112TR-802112TR-802112TR-802112TR-802112



30 1,20 -20 to 300/330 TR-801232TR-801232TR-801232TR-801232TR-801232


60 1,20 -20 to 300/330 TR-801262TR-801262TR-801262TR-801262TR-801262


15 1,20 -20 to 300/330 TR-801213TR-801213TR-801213TR-801213TR-801213


30 1,20 -20 to 300/330 TR-801233TR-801233TR-801233TR-801233TR-801233


60 1,20 -20 to 300/330 TR-801263TR-801263TR-801263TR-801263TR-801263


30 1,00 -20 to 300/330 TR-801035TR-801035TR-801035TR-801035TR-801035

30 2,00 -20 to 300/330 TR-802035TR-802035TR-802035TR-802035TR-802035

60 1,00 -20 to 300/330 TR-801065TR-801065TR-801065TR-801065TR-801065

60 2,00 -20 to 300/330 TR-802065TR-802065TR-802065TR-802065TR-802065


m n

Si OO SiCH3

CH3O

TKG 1123



VVVVVarian:arian:arian:arian:arian: CP-SIL 13 CB

3 4

TRB-20



30 0,25 -20 to 300/320 TR-200232TR-200232TR-200232TR-200232TR-200232


60 1,00 -20 to 280/300 TR-201062TR-201062TR-201062TR-201062TR-201062


30 0,25 -20 to 300/320 TR-200233TR-200233TR-200233TR-200233TR-200233


60 1,00 -20 to 280/300 TR-201063TR-201063TR-201063TR-201063TR-201063



60 0,50 -20 to 260/280 TR-200565TR-200565TR-200565TR-200565TR-200565

60 1,00 -20 to 260/280 TR-201065TR-201065TR-201065TR-201065TR-201065

TRB-20

(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inkedphase.phase.phase.phase.phase.

• (20%) Diphenyl-(80%) dimethylpolysiloxane.

• Column of intermediate polarity without cyanopropyl groups in its structure

• Excellent confirmation column.

TRB-20


Peak Name

1- Methanol2- Acetaldehyde3- Ethanol4- Isopropanol5- Acetone6- n-Propanol

Retention time


m n

Si OO SiCH3

CH3O

TRB-20

Column: TRB-20TRB-20TRB-20TRB-20TRB-20, P/N TR-203035Dimensions: 30m x 0.53mm x 3.0µmInjection: Alcohols in blood, 0.5 µL Head Space, split 5:1, 200ºCCarrier gas: He, constant pressure 10 psi (69Kpa)Oven temperature: 40ºC (isothermal)Detector: FID, 200ºC

TKG 1124


Supelco:Supelco:Supelco:Supelco:Supelco: SPB-20, VOCOLAlltechAl ltechAl ltechAl ltechAl ltech: AT-20Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-502

35

TRB-35TRB-35

(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inkedphase.phase.phase.phase.phase.


• Column of intermediate polarity without cyanopropyl groups in its structure.

• Excellent confirmation column.


Agilent: Agi lent: Agi lent: Agi lent: Agi lent: HP-35, DB-35Supelco:Supelco:Supelco:Supelco:Supelco: SPB-35RestekRestekRestekRestekRestek: Rtx-35SGE:SGE:SGE:SGE:SGE: BPX-35AlltechAl ltechAl ltechAl ltechAl ltech: AT-35Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-11


0,250,250,250,250,25 15 0,15 -20 to 300/320 TR-351312TR-351312TR-351312TR-351312TR-351312



60 0,25 -20 to 300/320 TR-350262TR-350262TR-350262TR-350262TR-350262


15 0,50 -20 to 290/310 TR-350513TR-350513TR-350513TR-350513TR-350513


30 0,50 -20 to 290/310 TR-350533TR-350533TR-350533TR-350533TR-350533


60 0,50 -20 to 290/310 TR-350563TR-350563TR-350563TR-350563TR-350563


30 0,50 -20 to 260/280 TR-350535TR-350535TR-350535TR-350535TR-350535


60 1,00 -20 to 260/280 TR-351065TR-351065TR-351065TR-351065TR-351065

1

2

3

4 5

67

8

9

10 11

TRB-35

Column: TRB-35TRB-35TRB-35TRB-35TRB-35, P/N TR-350535Dimensions: 30m x 0.53mm x 0.5µmInjection: 1 µL Grob Test, split 1:25, 260ºCCarrier gas: H2, constant pressure 3 psi (20.7 Kpa)Oven temperature: 40ºC @ 6ºC/min to 280ºC(5min)Detector: FID, 260ºC

Peak Name

1 Methylene chloride2 2,3-Butanediol3 C-104 C-115 1-Octanol6 Nonanal7 2,6-Dimethylphenol8 2,6-Dimethylaniline9 C-10 FAME10 C-11 FAME11 C-12 FAME


m n

Si OO SiCH3

CH3O

TKG 1125


3 6

TRB-1701TRB-1701

(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.

• (14%) Cyanopropyl-phenyl- (86%)dimethylpolysiloxane.

• Intermediate polarity column of wide use.

• Historically used in the analysis of pesticides.


0,200,200,200,200,20 15 0,20 -20 to 280/280 TR-132119TR-132119TR-132119TR-132119TR-132119


0,250,250,250,250,25 15 0,25 -20 to 280/280 TR-130212TR-130212TR-130212TR-130212TR-130212


30 0,10 -20 to 280/280 TR-130132TR-130132TR-130132TR-130132TR-130132


30 1,00 -20 to 260/280 TR-131032TR-131032TR-131032TR-131032TR-131032


60 0,50 -20 to 270/280 TR-130562TR-130562TR-130562TR-130562TR-130562

60 1,00 -20 to 260/280 TR-131062TR-131062TR-131062TR-131062TR-131062


TRB-1701

Column: TRB-1701TRB-1701TRB-1701TRB-1701TRB-1701, P/N TR-131565Dimensions: 60m x 0.53mm x 1.5µmInjection: 1 µL standard SP-4-7301, split 1:50, 260ºCCarrier gas: H2, constant pressure 6.2 psi (42.7 Kpa)Oven temperature: 130ºCDetector: FID, 280ºC

Peak Name

1 Methylene chloride2 C-103 2-Octanone4 C-115 1-Octanol6 C-127 2,6-Dimethylphenol9 C-138 2,6-Dimethylaniline10 C-14

TRB-225

(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.

• (50%) Cyanopropylphenyl - (50%) dimethyl polysiloxane.

• Medium/high polarity column.

• Excellent for separating cis-trans isomers of FAMES and sugar derivatives.


Si OO SiCH3

CH3

CH2)3CN

O(

m n

TRB-225

TKG 1126


Agilent: Agilent: Agilent: Agilent: Agilent: HP-225, DB-225RestekRestekRestekRestekRestek: Rtx-225VVVVVarian:arian:arian:arian:arian: CP-SIL 43 CBSGE:SGE:SGE:SGE:SGE: BP-225AlltechAl ltechAl ltechAl ltechAl ltech: AT-225Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-225


Si OO SiCH3

CH3

CH2)3CN

O(

m n

TRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent Phase

Agilent: Agilent: Agilent: Agilent: Agilent: HP-1701, PAS-1701, DB-1701Supelco:Supelco:Supelco:Supelco:Supelco: SPB-1701RestekRestekRestekRestekRestek: Rtx-1701VVVVVarianar ianar ianar ianar ian: CP-SIL 19 CBSGE:SGE:SGE:SGE:SGE: BP-10AlltechAl ltechAl ltechAl ltechAl ltech: AT-1701Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-1701

37

TRB-225

Column: TRB-225TRB-225TRB-225TRB-225TRB-225, P/N TR-251332Dimensions: 30m x 0.25mm x 0.15µmInjection: 1 µL standard SP-4-7301, split 1:50, 260ºCCarrier gas: H2, constant pressure 12 psi (82.7 Kpa)Oven temperature: 110ºCDetector: FID, 280ºC

Peak Name

1 Methylene chloride2 C-103 C-114 C-125 2-Octanone6 C-137 1-Octanol8 C-149 2,6-Dimethylphenol10 2,6-Dimethylaniline

TRB-225 TRB-50TRB-50

(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inkedphase.phase.phase.phase.phase.

• (50%) Diphenyl-(50%) dimethyl polysiloxane.

• Medium polarity column.

• Excellent column for confirmation of TRB-5 analyses.


0,250,250,250,250,25 15 0,15 0 to 300/320 TR-501312TR-501312TR-501312TR-501312TR-50131215 0,25 0 to 300/320 TR-500212TR-500212TR-500212TR-500212TR-500212

15 0,50 0 to 290/310 TR-500512TR-500512TR-500512TR-500512TR-500512

30 0,15 0 to 300/320 TR-501332TR-501332TR-501332TR-501332TR-501332

30 0,25 0 to 300/320 TR-500232TR-500232TR-500232TR-500232TR-500232

30 0,50 0 to 290/310 TR-500532TR-500532TR-500532TR-500532TR-500532

60 0,15 0 to 300/320 TR-501362TR-501362TR-501362TR-501362TR-501362

60 0,25 0 to 300/320 TR-500262TR-500262TR-500262TR-500262TR-500262

60 0,50 0 to 290/310 TR-500562TR-500562TR-500562TR-500562TR-500562

0,320,320,320,320,32 15 0,15 0 to 300/320 TR-501313TR-501313TR-501313TR-501313TR-501313

15 0,25 0 to 300/320 TR-500213TR-500213TR-500213TR-500213TR-500213

15 0,50 0 to 290/310 TR-500513TR-500513TR-500513TR-500513TR-500513

30 0,15 0 to 300/320 TR-501333TR-501333TR-501333TR-501333TR-501333

30 0,25 0 to 300/320 TR-500233TR-500233TR-500233TR-500233TR-500233

30 0,50 0 to 290/310 TR-500533TR-500533TR-500533TR-500533TR-500533

60 0,15 0 to 300/320 TR-501363TR-501363TR-501363TR-501363TR-501363

60 0,25 0 to 300/320 TR-500263TR-500263TR-500263TR-500263TR-500263

60 0,50 0 to 290/310 TR-500563TR-500563TR-500563TR-500563TR-500563

0,530,530,530,530,53 15 0,50 0 to 270/290 TR-500515TR-500515TR-500515TR-500515TR-500515

15 1,00 0 to 260/280 TR-501015TR-501015TR-501015TR-501015TR-501015

30 0,50 0 to 270/290 TR-500535TR-500535TR-500535TR-500535TR-500535

30 1,00 0 to 260/280 TR-501035TR-501035TR-501035TR-501035TR-501035

60 0,50 0 to 270/290 TR-500565TR-500565TR-500565TR-500565TR-500565

60 1,00 0 to 260/280 TR-501065TR-501065TR-501065TR-501065TR-501065


m n

Si OO SiCH3

CH3O

TKG 1127



Agilent: Agi lent: Agi lent: Agi lent: Agi lent: HP-50, +DB-17, DB-608SupelcoSupelcoSupelcoSupelcoSupelco: SPB-50, SPB-2250RestekRestekRestekRestekRestek: Rtx-50VVVVVarian:arian:arian:arian:arian: CP-SIL 24 CBAlltechAl ltechAl ltechAl ltechAl ltech: AT-50Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-17


0,200,200,200,200,20 15 0,20 40 to 220/240 TR-252119TR-252119TR-252119TR-252119TR-252119

30 0,20 40 to 220/240 TR-252139TR-252139TR-252139TR-252139TR-252139

0,250,250,250,250,25 15 0,15 40 to 220/240 TR-251312TR-251312TR-251312TR-251312TR-251312

15 0,25 40 to 220/240 TR-250212TR-250212TR-250212TR-250212TR-250212

30 0,15 40 to 220/240 TR-251332TR-251332TR-251332TR-251332TR-25133230 0,25 40 to 220/240 TR-250232TR-250232TR-250232TR-250232TR-250232

0,320,320,320,320,32 15 0,15 40 to 220/240 TR-251313TR-251313TR-251313TR-251313TR-251313


30 0,25 40 to 220/240 TR-250233TR-250233TR-250233TR-250233TR-250233

0,530,530,530,530,53 15 1,00 40 to 200/220 TR-251015TR-251015TR-251015TR-251015TR-251015

30 1,00 40 to 200/220 TR-251035TR-251035TR-251035TR-251035TR-251035

3 8


m n

Si OO SiCH3

CH3O

TRB-50ht

Column: TRB-50htTRB-50htTRB-50htTRB-50htTRB-50ht, P/N TR-531312Dimensions: 15m x 0.25mm x 0.15mmInjection: 0.2mL Triglycerides Palm Oil in Isooctane(50 mg/mL), split 1:12Carrier gas: H2, constant pressure, 9psi (56 KPa)Oven temperature: 340ºC(1min)@0.5ºC/min to 355ºC(5min)Injector: 380ºC (high temperature septum)Detector: FID, 380ºC

Peak Name

1 D322 D343 D364 MPP5 MOM6 PPP7 MOP8 MLP9 PPS10 POP11 MOO12 PLP13 MLO14 PSS15 POS16 POO17 PLS18 PLO19 PLL20 SOS21 SOO22 OOO23 SLO24 OLO25 OLL26 SOA27 AOO

12

3

4

5

610

7

8

9

11

1314

15

16

17

18

19 2021

22

2324

25 26 27

12

Structure of Poly(methyltrifluoroproyl)siloxane

n

(CH2)2CF3

O Si OCH3

TKG 1128


TRB-50htTRB-50ht

(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase


• Medium polarity column with high thermal stability.

• Best column for triglycerides analysis.

TRB-F50(50%) T(50%) T(50%) T(50%) T(50%) Trif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedphase.phase.phase.phase.phase.

• (50%) Trifluoropropyl-(50%) Methylpolysiloxane.

• High polarity column.

• Column designed for the EPA 609 and 8140 methods.

TRB -50ht Equ iva lent PhaseTRB-50ht Equ iva lent PhaseTRB-50ht Equ iva lent PhaseTRB-50ht Equ iva lent PhaseTRB-50ht Equ iva lent Phase

Agilent: Agi lent: Agi lent: Agi lent: Agilent: DB17htRestekRestekRestekRestekRestek: Rtx-65VVVVVarian:arian:arian:arian:arian: TAB-CBQuadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-65HT

TRB-50htInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 15 0,10 50 to 370 TR-530112TR-530112TR-530112TR-530112TR-530112

15 0,15 50 to 370 TR-531312TR-531312TR-531312TR-531312TR-531312

30 0,10 50 to 370 TR-530132TR-530132TR-530132TR-530132TR-530132

30 0,15 50 to 370 TR-531332TR-531332TR-531332TR-531332TR-531332

TRB-F50InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)


15 0,50 45 to 240/260 TR-570512TR-570512TR-570512TR-570512TR-570512


30 0,50 45 to 240/260 TR-570532TR-570532TR-570532TR-570532TR-570532


15 0,50 45 to 240/260 TR-570513TR-570513TR-570513TR-570513TR-570513


30 0,50 45 to 240/260 TR-570533TR-570533TR-570533TR-570533TR-570533

0,530,530,530,530,53 15 1,00 45 to 220/240 TR-571015TR-571015TR-571015TR-571015TR-571015

30 1,00 45 to 220/240 TR-571035TR-571035TR-571035TR-571035TR-571035

39

TRB-F50

Column: TRB-F50TRB-F50TRB-F50TRB-F50TRB-F50, P/N TR-570533Dimensions: 30m x 0.32mm x 0.5µmInjection: 1µL standard SP-4-7301 (500 ng/mL comp), split 1:50, 260ºCCarrier gas: H2, constant pressure, 7psi (48.2 KPa)Oven temperature: 100ºCDetector: FID, 280ºC Peak Name

1 Methylene chloride2 C-103 C-114 C-125 1-Octanol6 C-137 2-Octanone8 2,6-Dimethylphenol9 C-1410 2,6-Dimethylaniline

12

3

4

56

8

7

9

10

TRB-PAG

Column: TRB-PTRB-PTRB-PTRB-PTRB-PAGAGAGAGAG, P/N TR-550232Dimensions: 30m x 0.25mm x 0.25µmInjectionn: 1 µL Test Grob, split 1:25, 260ºCCarrier gas: H2, constant pressure 11 psi(75.8 Kpa)Oven temperature: 40ºC @ 6ºC/min to230ºC(5min)Detector: FID, 260ºC

1

2

3

4

5 6

7

9

1011

8

12

Peak Name

1 C-102 C-113 Nonanal4 2,3-Butanediol5 1-Octanol6 C-10 FAME7 Dicyclohexylamine8 2,6-Dimethylaniline9 C-11 FAME10 2,6-Dimethylphenol11 C-12 FAME12 2-Ethyl hexanoic acid

TKG 1129

TKG 1130

TRB-F50

50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylene e e e e glycol, glycol, glycol, glycol, glycol, bonded and bonded and bonded and bonded and bonded and crosslinkedcrosslinkedcrosslinkedcrosslinkedcrosslinked phase. phase. phase. phase. phase.

• (50%) Polyethylene-(50%) polypropylene glycol.

• Phase polarity slightly lower than TRB-WAX due to the inclusion of groups ofpropylene oxide.

• Polarity similar to UCON phase.

TRB-PAG

TRB-PAGInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 15 0,25 30 to 220/230 TR-550212TR-550212TR-550212TR-550212TR-550212


0,320,320,320,320,32 15 0,25 30 to 220/230 TR-550213TR-550213TR-550213TR-550213TR-550213


0,530,530,530,530,53 15 0,50 30 to 220/230 TR-550515TR-550515TR-550515TR-550515TR-550515


Structure of Poly(ethylenepropylene)glycol

CH2 CH2 OOm

CH2 CH2 OCH2 n


TRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent Phase

Agilent: Agi lent: Agi lent: Agi lent: Agilent: DB-210, DB-200RestekRestekRestekRestekRestek: Rtx-200Alltech:Al ltech:Al ltech:Al ltech:Al ltech: AT-210Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-210

TRB -PTRB -PTRB -PTRB -PTRB -PAG Equ iva lent PhaseAG Equ iva lent PhaseAG Equ iva lent PhaseAG Equ iva lent PhaseAG Equ iva lent Phase

Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: PAG

4 0

TKG 1131

TRB-WAXTRB-WAX

(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.

• 100% Polyethylene glycol (PEG).


• Wide range of working temperatures and high thermal stability (270º C)

• Ideal for separating alcohols, aldehydes, ketones and aromatic isomers (BTX)

Structure of Polyethylene glycol

CH2 CH2 OOm

TRB-WAXInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,100,100,100,100,10 10 0,10 40 to 260/270 TR-140141TR-140141TR-140141TR-140141TR-140141

10 0,20 40 to 260/270 TR-142141TR-142141TR-142141TR-142141TR-142141

20 0,10 40 to 260/270 TR-140181TR-140181TR-140181TR-140181TR-140181

20 0,20 40 to 260/270 TR-142181TR-142181TR-142181TR-142181TR-142181

0,200,200,200,200,20 15 0,20 40 to 260/270 TR-142119TR-142119TR-142119TR-142119TR-142119

15 0,40 40 to 260/270 TR-140419TR-140419TR-140419TR-140419TR-140419

30 0,20 40 to 260/270 TR-142139TR-142139TR-142139TR-142139TR-142139

30 0,40 40 to 260/270 TR-140439TR-140439TR-140439TR-140439TR-140439

60 0,20 40 to 260/270 TR-142169TR-142169TR-142169TR-142169TR-142169

60 0,40 40 to 260/270 TR-140469TR-140469TR-140469TR-140469TR-140469

0,250,250,250,250,25 15 0,10 40 to 260/270 TR-140112TR-140112TR-140112TR-140112TR-140112

15 0,25 40 to 260/270 TR-140212TR-140212TR-140212TR-140212TR-140212

15 0,50 40 to 260/270 TR-140512TR-140512TR-140512TR-140512TR-140512

30 0,10 40 to 260/270 TR-140132TR-140132TR-140132TR-140132TR-140132

30 0,25 40 to 260/270 TR-140232TR-140232TR-140232TR-140232TR-140232

30 0,50 40 to 260/270 TR-140532TR-140532TR-140532TR-140532TR-140532

30 1,00 40 to 260/270 TR-141032TR-141032TR-141032TR-141032TR-141032

60 0,10 40 to 260/270 TR-140162TR-140162TR-140162TR-140162TR-140162

60 0,25 40 to 260/270 TR-140262TR-140262TR-140262TR-140262TR-140262

60 0,50 40 to 260/270 TR-140562TR-140562TR-140562TR-140562TR-140562


0,320,320,320,320,32 15 0,10 40 to 260/270 TR-140113TR-140113TR-140113TR-140113TR-140113

15 0,25 40 to 260/270 TR-140213TR-140213TR-140213TR-140213TR-140213

15 0,50 40 to 260/270 TR-140513TR-140513TR-140513TR-140513TR-140513

30 0,10 40 to 260/270 TR-140133TR-140133TR-140133TR-140133TR-140133

30 0,25 40 to 260/270 TR-140233TR-140233TR-140233TR-140233TR-140233

30 0,50 40 to 260/270 TR-140533TR-140533TR-140533TR-140533TR-140533

50 1,20 40 to 230/240 TR-141253TR-141253TR-141253TR-141253TR-141253

60 0,10 40 to 260/270 TR-140163TR-140163TR-140163TR-140163TR-140163

60 0,25 40 to 260/270 TR-140263TR-140263TR-140263TR-140263TR-140263

60 0,50 40 to 260/270 TR-140563TR-140563TR-140563TR-140563TR-140563

60 1,00 40 to 230/240 TR-141063TR-141063TR-141063TR-141063TR-141063

60 1,20 40 to 230/240 TR-141263TR-141263TR-141263TR-141263TR-141263

100 1,00 40 to 230/240 TR-141093TR-141093TR-141093TR-141093TR-141093

0,530,530,530,530,53 10 1,00 40 to 240/250 TR-141045TR-141045TR-141045TR-141045TR-141045

15 1,00 40 to 240/250 TR-141015TR-141015TR-141015TR-141015TR-141015

30 1,00 40 to 240/250 TR-141035TR-141035TR-141035TR-141035TR-141035

30 1,33 40 to 240/250 TR-141735TR-141735TR-141735TR-141735TR-141735

30 2,00 40 to 240/250 TR-142035TR-142035TR-142035TR-142035TR-142035

60 1,00 40 to 240/250 TR-141065TR-141065TR-141065TR-141065TR-141065

60 2,00 40 to 240/250 TR-142065TR-142065TR-142065TR-142065TR-142065

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s

TRB-WAX

Column: TRB-WTRB-WTRB-WTRB-WTRB-WAXAXAXAXAX, P/N TR-140262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1 µL Test SP-4-7302 (500 ng/mL comp.),split 1:25, 260ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 155ºC (Isothermal)Detector: FID, 280ºC

Peak Name

1 Methylene chloride2 2-Octanone3 C-154 1-Octanol5 C-166 C-177 C-188 2,6-Dimethylaniline9 2,6-Dimethylphenol10 C-20

TRB -WTRB -WTRB -WTRB -WTRB -WAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-20M, INNOWAX, DB-WAX, DBWAXetrS upe l c oSupe l c oSupe l c oSupe l c oSupe l c o: SUPELCOWAX-10, Carbowax 20MRe s t e kRe s t e kRe s t e kRe s t e kRe s t e k: STABILWAXVVVVVa r i aa r i aa r i aa r i aa r i an: CP-WAX 52CBS G ES G ES G ES G ES G E: BP-20A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-WAX

41

TRB-FFAP

Column: TRB-FFTRB-FFTRB-FFTRB-FFTRB-FFAPAPAPAPAP, P/N TR-150262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1 µL Test SP-4-7302 (500 ng/mL comp.),split 1:100, 260ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 155ºCDetector: FID, 280ºC Peak Name

1 Methylene chloride2 2-Octanone3 C-154 1-Octanol5 C-166 C-177 C-188 2,6-Dimethylaniline9 2,6-Dimethylphenol10 C-20

TKG 1132

TRB-FFAPInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)


60 0,30 40 to 240/250 TR-152169TR-152169TR-152169TR-152169TR-152169


60 0,25 40 to 240/250 TR-150262TR-150262TR-150262TR-150262TR-150262


30 0,25 40 to 240/250 TR-150233TR-150233TR-150233TR-150233TR-150233


60 0,50 40 to 240/250 TR-150563TR-150563TR-150563TR-150563TR-150563

0,530,530,530,530,53 15 0,50 40 to 240/250 TR-150515TR-150515TR-150515TR-150515TR-150515

15 1,00 40 to 230/240 TR-151015TR-151015TR-151015TR-151015TR-151015


60 0,50 40 to 240/250 TR-150565TR-150565TR-150565TR-150565TR-150565

60 1,00 40 to 230/240 TR-151065TR-151065TR-151065TR-151065TR-151065

TRB-FFAP

TRB-FFAP

Polyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.

• 100% Polyethylene glycol (PEG) esterified with nitroterephthalic acid.

• Ideal for analysis of free acids (without derivatization), phenols and glycols.

• High thermal stability (250ºC)



CH2 CH2 OOm

TRB -FFTRB -FFTRB -FFTRB -FFTRB -FFAP Equ iva lent PhaseAP Equ iva lent PhaseAP Equ iva lent PhaseAP Equ iva lent PhaseAP Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-FFAP, DB-FFAPSupe l c oSupe l c oSupe l c oSupe l c oSupe l c o: NUKOL, SP-1000Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: STABILWAX-DAVVVVVa r i aa r i aa r i aa r i aa r i an: CP-WAX 58 CBS G ES G ES G ES G ES G E: BP-21A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1000, FFAPQuad r e xQuad r e xQuad r e xQuad r e xQuad r e x: 007-FFAP

4 2

TRB-WAX.DB

Column: TRB-WTRB-WTRB-WTRB-WTRB-WAX.AX.AX.AX.AX.DBDBDBDBDB, P/N TR-932162Dimensions: 60m x 0.25mm x 0.20µmInjection: 1 µL Test SP-4-8278 (500 ng/mL comp.), split1:50, 260ºCCarrier gas: H2, constantpressure 24 psi (168 Kpa)Oven temperature: 120ºC (isothermal)Detector: FID, 280ºC

Peak Name1 Tert-butylmethylether2 N-octylamine3 N-nonylamine4 C-155 N-decylamine6 C-167 Benzylamine8 C-179 Tri-n-hexylamine10 C-1811 2,6-Dimethylaniline12 2,4-Dimethylaniline13 C-20

TKG 1133

TRB-WAXOmega

TRB-WAX. DB

(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.

• 100% basic deactivated Polyethylene glycol (PEG).

• Excellent for analysing basic nonderivatized compounds

• Ideal for separating amines and nitrosamines.


CH2 CH2 OOm

TRB -WTRB -WTRB -WTRB -WTRB -WAX .AX .AX .AX .AX .D BD BD BD BD B Equ iva lent Phase Equ iva lent Phase Equ iva lent Phase Equ iva lent Phase Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: CAM, HP-BasicWaxVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-WAX 51SupelcoSupelcoSupelcoSupelcoSupelco: Carbowax-AmineRestekRestekRestekRestekRestek: Stabilwax-DB

TRB-WAX.DBInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 15 0,20 60 to 210/220 TR-932112TR-932112TR-932112TR-932112TR-932112

15 0,25 60 to 210/220 TR-930212TR-930212TR-930212TR-930212TR-930212


30 0,50 60 to 210/220 TR-930532TR-930532TR-930532TR-930532TR-930532

60 0,20 60 to 210/220 TR-932162TR-932162TR-932162TR-932162TR-932162

0,320,320,320,320,32 15 0,25 60 to 210/220 TR-930213TR-930213TR-930213TR-930213TR-930213


30 1,00 60 to 210/220 TR-931033TR-931033TR-931033TR-931033TR-931033

60 1,00 60 to 210/220 TR-931063TR-931063TR-931063TR-931063TR-931063

0,530,530,530,530,53 15 1,00 60 to 210/220 TR-931015TR-931015TR-931015TR-931015TR-931015


30 1,50 60 to 210/220 TR-931535TR-931535TR-931535TR-931535TR-931535

60 1,00 60 to 210/220 TR-931065TR-931065TR-931065TR-931065TR-931065

(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.


• High polarity column

• Specially designed for analysis of Omega 3 and Omega 6 fatty acids methylesters.


CH2 CH2 OOm

TRB-WAXOmegaInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 30 0,25 40 to 260/270 TR-840232TR-840232TR-840232TR-840232TR-840232

0,320,320,320,320,32 30 0,25 40 to 260/270 TR-840233TR-840233TR-840233TR-840233TR-840233

0,530,530,530,530,53 30 0,50 40 to 260/270 TR-840535TR-840535TR-840535TR-840535TR-840535

TRB-WAX.DB

TRB -WTRB -WTRB -WTRB -WTRB -WAXOmega Equ iva len t PhaseAXOmega Equ iva len t PhaseAXOmega Equ iva len t PhaseAXOmega Equ iva len t PhaseAXOmega Equ iva len t Phase

SupelcoSupelcoSupelcoSupelcoSupelco: OmegawaxRestekRestekRestekRestekRestek: Famewax


43

TRB-WAXOmega

Column: TR-WTR-WTR-WTR-WTR-WAXOmegaAXOmegaAXOmegaAXOmegaAXOmega, P/N TR-840233Dimensions: 30m x 0.32mm x 0.25µmInjection: 1µL test SP-4-8476, split 1:90, 250ºCCarrier gas: H2, 9.5 psi (65.4 KPa)Oven temperature: 200ºC (Isothermal)Detector: FID, 260ºC

Peak Name

1- C14:02- C16:03- C18:04- C18:1n95- C18:1n76- C18:2n67- C18:4n38- C20:09- C20:5n3 (EPA)10- C22:011- C21:5n312- C23:013- C22:5n314- C24:015- C22:6n3 (DHA)16- C24:1n9

12

3

4

6

57

8

9 EP

A

1011

12

13 14 16

15 D

HA

TKG 1134

Meta.WAX

TRB-WAXOmega

(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.



• Minimum operating temperature 20º C.

• Designed for analyzing volatiles in alcoholic beverages.

• Excellent symmetry for aldehyde and glycol peaks.



CH2 CH2 OOm

Meta.WAXInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)


15 0,50 20 to 240/250 TR-810512TR-810512TR-810512TR-810512TR-810512


30 0,50 20 to 240/250 TR-810532TR-810532TR-810532TR-810532TR-810532



15 1,00 20 to 230/240 TR-811013TR-811013TR-811013TR-811013TR-811013


30 1,00 20 to 230/240 TR-811033TR-811033TR-811033TR-811033TR-811033



0,530,530,530,530,53 15 1,20 20 to 230/240 TR-811215TR-811215TR-811215TR-811215TR-811215

30 1,20 20 to 230/240 TR-811235TR-811235TR-811235TR-811235TR-811235

Me ta .WMeta .WMeta .WMeta .WMeta .WAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent Phase

Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-WAX, DB-WAXVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-WAX 57 CBRestekRestekRestekRestekRestek: Rtx-WAX

4 4

TKG 1135

TR-CN100(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase

• 100% Cyanopropyl polysiloxane.

• Column of maximum polarity.

• Designed for separating fatty acids methyl esters (FAMEs)

• High selectivity towards cis-trans isomers of FAMEs.

TR-CN100InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)


60 0,20 0 to 240/250 TR-882162TR-882162TR-882162TR-882162TR-882162

0,320,320,320,320,32 15 0,20 0 to 240/250 TR-882113TR-882113TR-882113TR-882113TR-882113

30 0,20 0 to 240/250 TR-882133TR-882133TR-882133TR-882133TR-882133

60 0,20 0 to 240/250 TR-882163TR-882163TR-882163TR-882163TR-882163

0,530,530,530,530,53 15 0,20 0 to 225/250 TR-882115TR-882115TR-882115TR-882115TR-882115

30 0,20 0 to 225/250 TR-882135TR-882135TR-882135TR-882135TR-882135

60 0,20 0 to 225/250 TR-882165TR-882165TR-882165TR-882165TR-882165

TR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent Phase

SupelcoSupelcoSupelcoSupelcoSupelco: SP-2340, SP-2380RestekRestekRestekRestekRestek: Rt-2340, Rt-2330VVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL 88

Meta.WAX


Meta.WAX

Column: Meta.WMeta.WMeta.WMeta.WMeta.WAXAXAXAXAX, P/N TR-810532Dimensions: 30m x 0.25mm x 0.5µmInjection: 1µL Standard Alcohols, split 1:25, 260ºCCarrier gas: He, 12 psi (82.7 KPa)Oven temperature: 35ºC(10min) @ 8ºC/min to 220ºC (15min)Detector: FID, 260ºC

Peak Name

1- Acetaldehyde2- Methyl acetate3- Acetal4- Ethyl acetate5- Methanol6- Ethanol7- Ethyl butyrate8- 2-Butanol9- n-Propanol10- Isobutanol11- 1-Butanol12- 4-Methyl-2-pentanol (I. St.)13- Ethyl hexanoate14- 2-Methyl-1-butanol15- 3-Methyl-1-butanol16- Hexanol17- Ethyl lactate18- Ethyl octanoate19- Benzaldehyde20- Ethyl nonanoate21- Ethyl decanoate22- 4-Ethylphenol

Structure of Poly(biscyanopropyl)siloxane

n(CH2)3CN

(CH2)3CN

Si OO

n

45

TR-CN100

Column: TR-CN100TR-CN100TR-CN100TR-CN100TR-CN100, P/N TR-882162Dimensions: 60m x 0.25mm x 0.20µmInyection: 1µL SP-47885 FAMES (10 mg/mL), split 1:100, 260ºCCarrier gas: He, 20.15 cm/s to 185ºCOven temperature: 90ºC(7min) @ 5ºC/min to 240ºC(15min)Detector: FID, 260ºC

Peak Name

1- Butyric acid methyl ester (C4:0)2- Caproic acid methyl ester (C6:0)3- Caprylic acid methyl ester (C8:0)4- Capric acid methyl ester (C10:0)5- Undecanoic acid methyl ester (C11:0)6- Lauric acid methyl ester (C12:0)7- Tridecanoic acid methyl ester (C13:0)8- Myristic acid methyl ester (C14:0)9- Myristoleic acid methyl ester (C14:1)10- Pentadecanoic acid methyl ester (C15:0)11- Cis-10-pentadecenoic acid methyl ester (C15:1)12- Palmitic acid methyl ester (C16:0)13- Palmitoleic acid methyl ester (C16:1)14- Heptadecanoic acid methyl ester (C17:0)15- Cis-10-heptadecenoic acid methyl ester (C17:1)16- Stearic acid methyl ester (C18:0)17- Oleic acid methyl ester (C18:1n9c)18- Elaidic acid methyl ester (C18:1n9t)

19- Linoleic acid methyl ester (C18:2n6c)20- Linolelaidic acid methyl ester (C18:2n6t)21- γ-Linolenic acid methyl ester (C18:3n6)22- Linolenic acid methyl ester (C18:3n3)23-Arachidic acid methyl ester (C20:0)24- Cis-11-eicosenoic acid methyl ester (C20:1)25- Cis-11,14-eicosadienoic acid methyl ester (C20:2)26- Cis-8,11,14-eicosatrienoic acid methyl ester (C20:3n6)27- Cis-11,14,17-eicosatrienoic acid methyl ester (C20:3n3)28- Arachidonic acid methyl ester (C20:4n6)29- Cis-5,8,11,14,17-eicosapentaenoic acid methyl ester (C20:5n3)30- Heneicosanoic acid methyl ester (C21:0)31- Behenic acid methyl ester (C22:0)32- Erucic acid methyl ester (C22:1n9)33- Cis-13,16-docosadienoic acid methyl ester (C22:2)34- Cis-4,7,10,13,16,19-docosahexaenoic acid methyl ester(C22:6n3)35- Tricosanoic acid methyl ester (C23:0)36- Lignoceric acid methyl ester (C24:0)37- Nervonic acid methyl ester (C24:1)

1

23

4

5

6

8

8

910

11

12

1314

15

16

18

2019

10

17

21

24

22

25

30

31

26

32 28+3

5

33

36

29

37

34

TKG 1136

TR-CN100


4 6

TR-CRESOL

Column: TR-CRESOLTR-CRESOLTR-CRESOLTR-CRESOLTR-CRESOL, P/N TR-712162Dimensions: 60m x 0.25mm x 0.20µmInjection: 1 µL standard Cresols (5000 ng/mL comp.), split 1:25, 150ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 130ºCDetector: FID, 150ºC Peak Name

1 Methylene chloride2 Phenol3 o-Cresol4 2,6-Xylenol5 p-Cresol6 m-Cresol7 o-Ethylphenol8 2,4-Xylenol9 2,5-Xylenol10 2,3-Xylenol11 p-Ethylphenol12 m-Ethylphenol13 3,5-Xylenol14 3,4-Xylenol

1

23

4 5

6

7

8

9

101112

13

14

1

2

3

TR-17

Column: TR-17TR-17TR-17TR-17TR-17 P/N TR-502045Dimensions: 10m X 0,53 mm X 2.0 µmInjector: 260ºCCarrier gas: He, 6.5 psiInjection: 1ml standard, split (1:4)Oven Temperature: 180ºCDetector: FID, 280ºC

Peak Name

1- o-toluensulphonamide2- p-toluensulphonamide3 caffeine

TKG 1137 TKG 1138

TR-CRESOL TR-17TR-CRESOL

PropietarPropietarPropietarPropietarPropietary nonbonded phase.y nonbonded phase.y nonbonded phase.y nonbonded phase.y nonbonded phase.

• Stationary phase of perfectly defined purity.

• Column specially designed for analysis of phenolic compounds (phenols,cresylic acids).

• Derivatization of phenolic compounds is not required to obtain suitableresolution.

• Resolves m-cresol/p-cresol and 2.4-xylenol/2.5-xylenol pairs, which are notseparated with other columns used for this analysis such as TRB-5 andTRB-WAX .

TR-CRESOLInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 30 0,20 130 TR-712132TR-712132TR-712132TR-712132TR-712132

60 0,20 130 TR-712162TR-712162TR-712162TR-712162TR-712162

m n

Si OO SiCH3

CH3O


TR-17

PolymethylphenylsiloxanePolymethylphenylsiloxanePolymethylphenylsiloxanePolymethylphenylsiloxanePolymethylphenylsiloxane

• Polymethylphenylsiloxane.

• Recommended by pharmacopoeia for determining the impurities of sodiumsaccharin (o-p-toluenesulphonamides).

TR-17InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,530,530,530,530,53 10 2,0 0 to 220/240 TR-502045TR-502045TR-502045TR-502045TR-502045

TR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent Phase

VVVVVa r i a na r i a na r i a na r i a na r i a n: CP-CRESOL

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n s

TR-17 Equ iva lent PhaseTR -17 Equ iva lent PhaseTR -17 Equ iva lent PhaseTR -17 Equ iva lent PhaseTR -17 Equ iva lent Phase

Agilent:Agi lent:Agi lent:Agi lent:Agi lent: HP-17

47

1

2

3

4

56

78

9

Meta.VOC

Column: Meta .VOCMeta .VOCMeta .VOCMeta .VOCMeta .VOC, P/N TR-941863Dimensions: 60m x 0.32mm x 1.8µmInjection: 1 µL Test SP-4-8423(500 ng/mL comp.), split 1:100, 280ºCCarrier gas: H2, constant pressure15psi (103.4 Kpa)Oven temperature: 150ºCDetector: FID, 280ºC Peak Name

1 Methylene chloride2 C-103 2-Octanone4 C-115 1-Octanol6 2,6-Dimethylphenol7 2,6-Dimethylaniline8 C-139 C-14

TKG 1139

Meta.VOCMeta.VOC

ProprietarProprietarProprietarProprietarProprietary bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.

• Developed for analysis of volatile organic compounds (VOC)

• Intermediate polarity column.

Meta.VOCInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,200,200,200,200,20 10 1,20 -20 to 240/250 TR-941249TR-941249TR-941249TR-941249TR-941249

0,250,250,250,250,25 30 1,50 -20 to 240/250 TR-941532TR-941532TR-941532TR-941532TR-941532

60 1,50 -20 to 240/250 TR-941562TR-941562TR-941562TR-941562TR-941562

0,320,320,320,320,32 60 1,80 -20 to 240/250 TR-941863TR-941863TR-941863TR-941863TR-941863

60 3,00 -20 to 240/230 TR-943063TR-943063TR-943063TR-943063TR-943063

0,530,530,530,530,53 30 3,00 -20 to 240/230 TR-943035TR-943035TR-943035TR-943035TR-943035

60 3,00 -20 to 240/230 TR-943065TR-943065TR-943065TR-943065TR-943065


TRB-608

ProprietarProprietarProprietarProprietarProprietary bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.

• Specifically designed for analysing chlorinated pesticides and PCBs

• Designed for the EPA 508, 608 and 8080 methods.


0,250,250,250,250,25 30 0,25 -20 to 300/310 TR-360232TR-360232TR-360232TR-360232TR-360232

0,530,530,530,530,53 15 0,50 -20 to 290/300 TR-360515TR-360515TR-360515TR-360515TR-360515

30 0,50 -20 to 290/300 TR-360535TR-360535TR-360535TR-360535TR-360535

TRB-608

TRB 608

Column: TRB-608TRB-608TRB-608TRB-608TRB-608, P/N TR-360232Dimensions: 30m x 0.25mm x 0.25mmInjection: 1 µL Grob Test, split 1:100, 280ºCCarrier gas: H2, constant pressure11 psi (75.8 Kpa)Oven temperature: 40ºC @ 6ºC/minto 300ºC(5min)Detector: FID, 340ºC

Meta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent Phase

Agilent:Agi lent:Agi lent:Agi lent:Agi lent: DB-502.2, HP-VOCSupelco:Supelco:Supelco:Supelco:Supelco: VOCOLRestek:Restek:Restek:Restek:Restek: Rtx-502.2


Agilent:Agi lent:Agi lent:Agi lent:Agi lent: HP-608Supelco:Supelco:Supelco:Supelco:Supelco: SPB-608SGE:SGE:SGE:SGE:SGE: BP-608

1

2 34

5

6

7

8

910 11

Peak Name

1 Methylene chloride2 2,3-Butanediol3 C-104 C-115 1-Octanol6 Nonanal7 2,6-Dimethylphenol8 2,6-Dimethylaniline9 C-10 FAME10 C-11 FAME11 C-12 FAME

TKG 1140

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s - - - - - S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r yyyyyTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n s

4 8

Peak Name

1 Isooctane2 C-113 C-124 Benzene5 C-136 Toluene7 Ethylbenzene8 p-Xylene9 Cumene

TR-TCEP

Column: TR-TCEPTR-TCEPTR-TCEPTR-TCEPTR-TCEP, P/N TR-960462Dimensions: 60m x 0.25mm x 0.40µmInjection: 1 µL standard (20 ng/mL comp.), split 1:50, 170ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 110ºCDetector: FID, 170ºC

Meta.WAX 400

Column: Meta.WMeta.WMeta.WMeta.WMeta.WAX 400AX 400AX 400AX 400AX 400, P/N TR-402153Dimensions: 50m x 0.32mm x 0.20µmInjection: 1µL standard (split 1:50), 175ºCCarrier gas: He, 11 psi (75.8 Kpa)Oven Temperature: 30ºC(5 min.) @ 4ºC/min to 60ºC(10 min.)Detector Temperature: FID, 175ºC

Peak Name

1 Acetaldehyde2 Ethyl Acetate3 Methanol4 Ethanol5 2-Butanol6 n-Propanol7 Allyl alcohol8 2-Methyl-1-propanol (isobutanol)9 1-Butanol10 2-Methyl-1-butanol (amyl alcohol)11 3-Methyl-1-butanol (isoamyl alcohol)

TR-TCEP

1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase


• Column for analysis of alcohols in gasoline.

• Separation of the aliphatic hydrocarbons up to C12 in aromatics.

Meta.WAX 400

100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.

• Column designed for analysis of volatiles in alcoholic beverages and solvents.

• Maximum resolution of amylic alcohols.

• High number of plates even at very low temperature (<20ºC)

TR-TCEP

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s - - - - - S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r yyyyy

Meta.WAX 400

Structure of Polyethyleneglycol CH2 CH2 OOm

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n s

TKG 1141TKG 1142

TR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent Phase

Supelco:Supelco:Supelco:Supelco:Supelco: TCEPRestekRestekRestekRestekRestek: Rt-TCEPVVVVVarian: ar ian: ar ian: ar ian: ar ian: CP-TCEP

Me ta .WMeta .WMeta .WMeta .WMeta .WAX 400 Equ iva lent PhaseAX 400 Equ iva lent PhaseAX 400 Equ iva lent PhaseAX 400 Equ iva lent PhaseAX 400 Equ iva lent Phase

VVVVVarian: arian: arian: arian: arian: CP Carbowax 400

TR-TCEPInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 30 0,40 0 to 135 TR-960432TR-960432TR-960432TR-960432TR-960432

60 0,40 0 to 135 TR-960462TR-960462TR-960462TR-960462TR-960462

Meta.WAX 400InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,320,320,320,320,32 50 0,20 0 to 60/80 TR-402153TR-402153TR-402153TR-402153TR-402153

49

Fig. 9. Lemon oil in a 100 µµµµµm column

Column TRB-5, 10m x 0,1 mm ID X 0,33 µm

Fig. 8. Lemon oil in a conventional column

Column TRB-1, 50m x 0,25 mm ID X 0,33 µm

10 minutes

Teknokroma Microbore Columns (0,1mm ID)• MINIMUM BLEED LEVEL (approximately 10 times less than that of a

conventional column of 0.25 mm ID).

• HIGH ANALYTICAL SPEED (the analysis are approximately 3 times faster than aconventional column of 0.25 mm ID).

These columns of 100 µm internal diameter also enable them to be connected to aconventional chromatograph fitted with a SPLIT/SPLITLESS injector, and due to itsgreat efficiency (~7,000-10,000 plates/m) and its reduced diameter, theanalysis can be undertaken with greater speed compared to standard capillarycolumns, without loss of peak resolving power. Having such a high level ofefficiency enables the analysis of complex mixtures, with a large number ofcomponents. The standard length is 10 metres (Fig. 8 and Fig. 9).

Limiting factors

1. WORKING PRESSURE (GAS FLOW)

With microbore columns the working pressures are higher so that more precautionsshould be taken regarding gas leaks from the injector cavity or with ferrules.

At optimed pressure the carrier gas flow is low (H2~0.2cc/min, He ~0.1cc/min),which is good for working with mass detectors, since it does not exceed itsemptying capacity. Not optimizing these parameters may cause losses in peakresolution.

2. SAMPLE CAPACITY

In these columns with a small diameter the sample that can be injected is muchsmaller than with a column with a conventional diameter. Its sample capacity isaround ten times less than that of a column of 0.25 mm ID.

3. INJECTOR

The columns of 0.1 mm ID are compatible with the injection techniques in Split-splitless. It is not recommended to work with direct or on-column injection.The glass liners, with internal diameters of 2-4 mm, are not the most suitablesince, due to their large dead volume, and the fact that one is working with smallgas carrying flows, it is difficult for there to be a correct sweep in the injectionzone. This transforms into an enlarging of peaks, with the subsequent loss ofresolution (especially for liners of 4 mm). It is highly recommended to work withliners of 0.75-1 mm diameter.

Working with this type of small volume liner, along with the microbore columns,means that one must be extremely careful with the purity of the samples that areinjected. The samples must be clean and the non-volatile residues must beminimised in order to avoid contaminations that cause absorption of analytes,decompositions, the appearance of ghost peaks, etc.

4. DETECTOR

The gas flows of the detector must be optimised for working with the microborecolumns. It is possible that in some detectors the auxiliary gas flow(make up) willhave to be increased in order to minimise its dead volume and enable the correctsweep of the compounds that leave the column at very low flow levels.Since the peaks elute very fast and are very narrow (the peak widths are generallyless than 1 s) it is necessary to work at very high speeds on the electrometer andwith fast integration so that the quantification of the peaks is correct.The small volume of these columns means that the stationary phase quantitydeposited in them is very small compared to a conventional column. This, alongwith the low flow levels with which it works, causes the bleed level (proportionalto the quantity of the phase and flow) to be minimal, even at high temperatures,thus favouring the signal/noise ratio and contributing to the detectors not gettingcontaminated.

TKG 1143

TKG 1144

40 minutes

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r e C o l u m n sC o l u m n sC o l u m n sC o l u m n sC o l u m n s

Teknokroma Microbore columns of 100 µmPhasePhasePhasePhasePhase Length (m)Length (m)Length (m)Length (m)Length (m) (df µm)(df µm)(df µm)(df µm)(df µm) P/NP/NP/NP/NP/NTRB-1TRB-1TRB-1TRB-1TRB-1 10 0.1 TR-110141TR-110141TR-110141TR-110141TR-110141

10 0.4 TR-110441TR-110441TR-110441TR-110441TR-11044120 0.1 TR-110181TR-110181TR-110181TR-110181TR-11018120 0.4 TR-110481TR-110481TR-110481TR-110481TR-110481

TRB-5TRB-5TRB-5TRB-5TRB-5 10 0.1 TR-120141TR-120141TR-120141TR-120141TR-12014110 0.4 TR-120441TR-120441TR-120441TR-120441TR-12044120 0.1 TR-120181TR-120181TR-120181TR-120181TR-12018120 0.4 TR-120481TR-120481TR-120481TR-120481TR-120481

TRB-WTRB-WTRB-WTRB-WTRB-WAXAXAXAXAX 10 0.1 TR-140141TR-140141TR-140141TR-140141TR-14014110 0.2 TR-142141TR-142141TR-142141TR-142141TR-14214120 0.1 TR-140181TR-140181TR-140181TR-140181TR-14018120 0.2 TR-142181TR-142181TR-142181TR-142181TR-142181

5 0

TKG 1145

Teknokroma Microbore Columns

TRB-WAX

Column: TRB-WTRB-WTRB-WTRB-WTRB-WAXAXAXAXAX, P/N TR-140141Dimensions: 10m x 0.10mm x 0.10µmInjection: 1µL standard FAMES, (200ng/comp), split 1:50, 280ºCCarrier gas: H2, constant pressure 50 psi (344.5 Kpa)Oven temperature: 40ºC(1min) @ 25ºC/min to 195ºC @ 3ºC/min to 205ºC @ 8ºC/min to 230ºC(1min)Detector: FID, 280ºC

20 Linolelaidic acid methyl ester (C18:2n6t)21 γ-Linolenic acid methyl ester (C18:3n6)22 Linolenic acid methyl ester (C18:3n3)23 Arachidic acid methyl ester (C20:0)24 Cis-11-eicosenoic acid methyl ester (C20:1)25 Cis-11,14-eicosadienoic acid methyl ester (C20:2)26 Cis-8,11,14-eicosatrienoic acid methyl ester (C20:3n6)27 Heneicosanoic acid methyl ester (C21:0)28 Cis-11,14,17-eicosatrienoic acid methyl ester (C20:3n3)29 Arachidonic acid methyl ester (C20:4n6)30 Cis-5,8,11,14,17-eicosapentaenoic acid methyl ester (C20:5n3)31 Behenic acid methyl ester (C22:0)32 Erucic acid methyl ester (C22:1n9)33 Cis-13,16-docosadienoic acid methyl ester (C22:2)34 Tricosanoic acid methyl ester (C23:0)35 Lignoceric acid methyl ester (C24:0)36 Cis-4,7,10,13,16,19-docosahexaenoic acid methyl ester (C22:6n3)37 Nervonic acid methyl ester (C24:1)

Peak Name

1 Butyric acid methyl ester (C4:0)2 Caproic acid methyl ester (C6:0)3 Caprylic acid methyl ester (C8:0)4 Capric acid methyl ester (C10:0)5 Undecanoic acid methyl ester (C11:0)6 Lauric acid methyl ester (C12:0)7 Tridecanoic acid methyl ester (C13:0)8 Myristic acid methyl ester (C14:0)9 Myristoleic acid methyl ester (C14:1)10 Pentadecanoic acid methyl ester (C15:0)11 Cis-10-pentadecenoic acid methyl ester (C15:1)12 Palmitic acid methyl ester (C16:0)13 Palmitoleic acid methyl ester (C16:1)14 Heptadecanoic acid methyl ester (C17:0)15 Cis-10-heptadecenoic acid methyl ester (C17:1)16 Stearic acid methyl ester (C18:0)17 Oleic acid methyl ester (C18:1n9c)18 Elaidic acid methyl ester (C18:1n9t)19 Linoleic acid methyl ester (C18:2n6c)

1

2

34

5

6

7

8

12

910

11 1314

15

16

17, 18

1920

2122

23

24

25

26

27

2829

30

31

32

33

34

35

36-37Excellent Resolution

in 12 minutes

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r e C o l u m n sC o l u m n sC o l u m n sC o l u m n sC o l u m n s

51

TKG 1147

Custom Capillary ColumnsTeknokroma also provides you with the possibility of working with nonbonded andbonded custom capillary columns, which are still described today in officialmethods, or which appear in the scientific bibliography. We can supply you withthese columns in the size and phase thickness that you require for a similar priceas our standard Teknokroma columns. As an example:

TR-101 - 100% polydimethylsiloxane phase(“silicone fluid”).

TR-SE-30 - 100% polydimethylsiloxane phase.

TR-SE-52 - 5% phenyl -95% dimethylpolysiloxane phase.

TR-SE-54 - 5% phenyl-1% vinyl-94% dimethylpolysiloxane phase.

TR-20M - polyethylene glycol 100% (Carbowax 20M) phase.

We can also supply you with columns for inverse gas chromatography, used for thecharacterisation of polymers. Teknokroma can coat your polymer in our fused silicacolumn.

F O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TC O N TC O N TC O N TC O N TC O N T A C T O U RA C T O U RA C T O U RA C T O U RA C T O U R T E C H N I C A L D E PT E C H N I C A L D E PT E C H N I C A L D E PT E C H N I C A L D E PT E C H N I C A L D E P A RA RA RA RA R T M E N TT M E N TT M E N TT M E N TT M E N T

TRB-240

Column: TRB-240 TRB-240 TRB-240 TRB-240 TRB-240 (OV-240-OH), P/N TR-240262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1 µL Grob Test, split 1:25, 260ºCCarrier gas: H2, constant pressure 11 psi (75.8 Kpa)Oven temperature: 40ºC @ 6ºC/min to 260ºC(5min)Detector: FID, 260ºC

Peak Name

1 Methylene chloride2 C-103 C-114 2,3-Butanediol5 Nonanal6 1-Octanol7 C-10 FAME8 2,6-Dimethylaniline9 C-11 FAME10 2,6-Dimethylphenol11 C-12 FAME

TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - C u s t o my C o l u m n s - C u s t o my C o l u m n s - C u s t o my C o l u m n s - C u s t o my C o l u m n s - C u s t o m

5 2

NON POLAR

Methyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarsolvents.solvents.solvents.solvents.solvents.

InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,250,250,250,250,25 3x1 TR-100012TR-100012TR-100012TR-100012TR-100012

1X5 TR-100052TR-100052TR-100052TR-100052TR-100052

1X10 TR-100042TR-100042TR-100042TR-100042TR-100042

1X20 TR-100082TR-100082TR-100082TR-100082TR-100082

0,320,320,320,320,32 3x1 TR-100013TR-100013TR-100013TR-100013TR-100013

1X5 TR-100053TR-100053TR-100053TR-100053TR-100053

1X10 TR-100043TR-100043TR-100043TR-100043TR-100043

1X20 TR-100083TR-100083TR-100083TR-100083TR-100083

0,530,530,530,530,53 3x1 TR-100015TR-100015TR-100015TR-100015TR-100015

1X5 TR-100055TR-100055TR-100055TR-100055TR-100055

1X10 TR-100045TR-100045TR-100045TR-100045TR-100045

1X20 TR-100085TR-100085TR-100085TR-100085TR-100085

UNIVERSAL PRESS FIT CONNECTORS

DeactivatedDeactivatedDeactivatedDeactivatedDeactivated DescriptionDescriptionDescriptionDescriptionDescriptionUniversalUniversalUniversalUniversalUniversal

TR-33001TR-33001TR-33001TR-33001TR-33001 Universal Press Fit 12pk

TR-33002TR-33002TR-33002TR-33002TR-33002 Universal Press Fit Angled Y/unit

Guard Columns (Retention Gap)

NON POLAR

MEDIUM POLAR (INTERMEDIATE)

POLAR

AQUASAFE

BASE-DEACTIVATED

MEDIUM POLAR (INTERMEDIATE)

Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,hexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solvents


0,250,250,250,250,25 3x1 TR-200012TR-200012TR-200012TR-200012TR-200012

1X5 TR-200052TR-200052TR-200052TR-200052TR-200052

1X10 TR-200042TR-200042TR-200042TR-200042TR-200042

1X20 TR-200082TR-200082TR-200082TR-200082TR-200082

0,320,320,320,320,32 3x1 TR-200013TR-200013TR-200013TR-200013TR-200013

1X5 TR-200053TR-200053TR-200053TR-200053TR-200053

1X10 TR-200043TR-200043TR-200043TR-200043TR-200043

1X20 TR-200083TR-200083TR-200083TR-200083TR-200083

0,530,530,530,530,53 3x1 TR-200015TR-200015TR-200015TR-200015TR-200015

1X5 TR-200055TR-200055TR-200055TR-200055TR-200055

1X10 TR-200045TR-200045TR-200045TR-200045TR-200045

1X20 TR-200085TR-200085TR-200085TR-200085TR-200085

G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )

53

Guard Columns (Retention Gap)

Teknokroma Metal Capillary ColumnsStainless steel Teknokroma columns (TR-INOX)

• Chemical inertness comparable to that of fused silica• Bonded and crosslinked• Ideal for chromatographs in industrial control processes• Practically unbreakable• Enables the use of high analysis temperatures

Teknokroma can supply you with Teknokroma stainless steel columns with a 0.53mm internal diameter and with an external diameter similar to that of fused silicasemi-capillary columns, enabling you to use the same standard ferrules of0.8 mm ID.

These columns are available with our most popular stationary phases.To order a metallic column simply add the prefix INOX at the end of thecorresponding reference to the column in the catalog.

For example: TRB-2887 of 10m x 0.53 mm x 2.65µm P/N TR-192645P/N TR-192645P/N TR-192645P/N TR-192645P/N TR-192645With stainless steel tube, 10m x 0.53 mm x 2.65µm P/N TR-192645INOXP/N TR-192645INOXP/N TR-192645INOXP/N TR-192645INOXP/N TR-192645INOX

5-inch column cage

For columns that have to be placed in the oven of the 6850 chromatograph, thecolumn must be rolled up in a 5 inch cage.To order a column in a 5 inch cage you just need to add a 5 to the end of thecatalog number of the corresponding column.

For example: TRB-5, 30m x 0.25 mm x 0.25µm P/N TR-120232P/N TR-120232P/N TR-120232P/N TR-120232P/N TR-120232With 5 inch cage, TRB-5, 30m x 0.25 mm x 0.25µm P/N TR-1202325P/N TR-1202325P/N TR-1202325P/N TR-1202325P/N TR-1202325

POLAR

Polyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widerange of similar polar solvents.range of similar polar solvents.range of similar polar solvents.range of similar polar solvents.range of similar polar solvents.


0,250,250,250,250,25 3x1 TR-300012TR-300012TR-300012TR-300012TR-300012

1X5 TR-300052TR-300052TR-300052TR-300052TR-300052

1X10 TR-300042TR-300042TR-300042TR-300042TR-300042

1X20 TR-300082TR-300082TR-300082TR-300082TR-300082

0,320,320,320,320,32 3x1 TR-300013TR-300013TR-300013TR-300013TR-300013

1X5 TR-300053TR-300053TR-300053TR-300053TR-300053

1X10 TR-300043TR-300043TR-300043TR-300043TR-300043

1X20 TR-300083TR-300083TR-300083TR-300083TR-300083

0,530,530,530,530,53 3x1 TR-300015TR-300015TR-300015TR-300015TR-300015

1X5 TR-300055TR-300055TR-300055TR-300055TR-300055

1X10 TR-300045TR-300045TR-300045TR-300045TR-300045

1X20 TR-300085TR-300085TR-300085TR-300085TR-300085

AQUASAFE

ProprietarProprietarProprietarProprietarProprietary deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.


0,250,250,250,250,25 3x1 TR-310012TR-310012TR-310012TR-310012TR-310012

1X5 TR-310052TR-310052TR-310052TR-310052TR-310052

1X10 TR-310042TR-310042TR-310042TR-310042TR-310042

1X20 TR-310082TR-310082TR-310082TR-310082TR-310082

AQUASAFE (Cont.)InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)

0,320,320,320,320,32 3x1 TR-310013TR-310013TR-310013TR-310013TR-310013

1X5 TR-310053TR-310053TR-310053TR-310053TR-310053

1X10 TR-310043TR-310043TR-310043TR-310043TR-310043

1X20 TR-310083TR-310083TR-310083TR-310083TR-310083

0,530,530,530,530,53 3x1 TR-310015TR-310015TR-310015TR-310015TR-310015

1X5 TR-310055TR-310055TR-310055TR-310055TR-310055

1X10 TR-310045TR-310045TR-310045TR-310045TR-310045

1X20 TR-310085TR-310085TR-310085TR-310085TR-310085

BASE-DEACTIVATED

ProprietarProprietarProprietarProprietarProprietary deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basiccompoundscompoundscompoundscompoundscompounds


0,250,250,250,250,25 3x1 TR-320012TR-320012TR-320012TR-320012TR-320012

1X5 TR-320052TR-320052TR-320052TR-320052TR-320052

1X10 TR-320042TR-320042TR-320042TR-320042TR-320042

1X20 TR-320082TR-320082TR-320082TR-320082TR-320082

0,320,320,320,320,32 3x1 TR-320013TR-320013TR-320013TR-320013TR-320013

1X5 TR-320053TR-320053TR-320053TR-320053TR-320053

1X10 TR-320043TR-320043TR-320043TR-320043TR-320043

1X20 TR-320083TR-320083TR-320083TR-320083TR-320083

0,530,530,530,530,53 3x1 TR-320015TR-320015TR-320015TR-320015TR-320015

1X5 TR-320055TR-320055TR-320055TR-320055TR-320055

1X10 TR-320045TR-320045TR-320045TR-320045TR-320045

1X20 TR-320085TR-320085TR-320085TR-320085TR-320085

Columns for the Agilent GC 6850

G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )

5 4

USP Capillary Column EquivalentsEDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG

DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKETTNELAVIUQEYRALLIPAC

1G1G1G1G1G lioenaxolisyloplyhtemiD sm1-BRT,1-BRT

2G2G2G2G2G mugenaxolisyloplyhtemiD sm1-BRT,1-BRT

3G3G3G3G3G enaxolisyloplyhtem%05-lynehp%05 05-BRT

5G5G5G5G5G enaxolislyporponayc-3 001NC-RT

8G8G8G8G8G enaxolislyhtemlynehp%01-lyporponayc-3-%09 001NC-RT

9G9G9G9G9G enaxolisyloplynivlyhteM sm1-BRT,1-BRT

41G 41G 41G 41G 41G )0501-159=WM(locylgenelyhteyloP XAW-BRT

51G 51G 51G 51G 51G )0703-0003=WM(locylgenelyhteyloP XAW-BRT

61G 61G 61G 61G 61G )00051=WM(locylgenelyhteyloP XAW-BRT

91G 91G 91G 91G 91G enaxolislyhtemlyporponayc%52-lynehp%52 522-BRT

02G 02G 02G 02G 02G )024-083=WM(locylgenelyhteyloP 004XAW.ateM

52G 52G 52G 52G 52G APTlocylgenelyhteyloP PAFF-BRT

72G 72G 72G 72G 72G enaxolisyloplyhtem%59-lynehp%5 5X.ateM,sm5-BRT,5-BRT

82G 82G 82G 82G 82G enaxolisyloplyhtemid-%57-lynehp%52 02-BRT

23G 23G 23G 23G 23G enaxolisyloplyhtemid-%08-lyhtemlynehp%02 02-BRT

53G 53G 53G 53G 53G dicacilahthperetortiNhtiwlocylgenelyhteyloP PAFF-BRT

63G 63G 63G 63G 63G enaxolisyloplyhtemlynehp%5-lyniv%1 5X.ateM,sm5-BRT,5-BRT

93G 93G 93G 93G 93G )0051=WM(locylgenelyhteyloP XAW-BRT

24G 24G 24G 24G 24G enaxolisyloplyhtemid%56-lynehpid%53 53-BRT

34G 34G 34G 34G 34G enaxolisyloplyhtemid%49-lynehplyporponayc%6 34G-RT,1031-BRT,426-BRT

64G 64G 64G 64G 64G enaxolisyloplyhtemid%68-lynehplyporponayc%41 1071-BRT


55

EPA Drinking Water Test MethodsEPA METHODEPA METHODEPA METHODEPA METHOD APPLICATIONAPPLICATIONAPPLICATIONAPPLICATION RECOMMENDEDRECOMMENDEDRECOMMENDEDRECOMMENDED TEKNOKROMA CAPILLARY COLUMNTEKNOKROMA CAPILLARY COLUMNTEKNOKROMA CAPILLARY COLUMNTEKNOKROMA CAPILLARY COLUMN PART NUMBERPART NUMBERPART NUMBERPART NUMBER

501.3501.3501.3501.3 Trihalomethanes by GC/MS and SIM TRB-624 30m x 0.53mm x 3.0 mm TR-603035

TRB-624 75m x 0.53mm x 3.0 mm TR-603075

TRB-624 105m x 0.53mm x 3.0 mm TR-6030K5

TRB-624 30m x 0.25mm x 1.0 mm TR-601032

502.2502.2502.2502.2 Vo l a t i l e ha l oge na te d O rg an i c s i n Wat e r b y Pu r ge & Tr a pGC/PID/ELCD

TRB-624 30m x 0.53mm x 3.0 mm TR-603035

503.1503.1503.1503.1 Volatile Aromatics & Unsaturated Organics by Purge & Trap GC TRB-624 30m x 0.53mm x 3.0 mm TR-603035

TRB-624 30m x 0.25mm x 1.4 mm TR-601432

504.1504.1504.1504.1 1,2-Dibromoethane (EDB), 1,2-Dibromo-3-chloropropane TRB-1 30m x 0.32mm x 0.25 mm TR-110233

(DBCP), and 1,2,3-Trichloropropane (123TCP) by GC/MS TRB-624 30m x 0.53mm x 3.0 mm TR-603035

TRB-624 30m x 0.25mm x 1.4 mm TR-601432

505505505505 Organohalide Pesticides & Aroclors by GC/ECD TRB-1 30m x 0.32mm x 1.0 mm TR-111033

TRB-50 30m x 0.32mm x 0.5 mm TR-500533

TRB-50 30m x 0.25mm x 0.25 mm TR-500232

507507507507 Nitrogen & Phosphorous containing Pesticides in Water TRB-5 30m x 0.25mm x 0.25 mm TR-120232

by GC/NPD TRB-5ms 30m x 0.25mm x 0.25 mm TR-520232

TRB-1701 30m x 0.25mm x 0.25 mm TR-130233

508508508508 Chlorinated Pesticides in Water by GC/MS TRB-5 30m x 0.25mm x 0.25 mm TR-120232

TRB-5ms 30m x 0.25mm x 0.25 mm TR-520232

TRB-1701 30m x 0.25mm x 0.25 mm TR-130233

513513513513 2,3,7,8-Tetrachlorodibenzo-p-dioxin by GC/MS TRB-5ms 60m x 0.25mm x 0.10 mm TR-520162

515.2515.2515.2515.2 Determination of chlorinated acids in water using TRB-1 30m x 0.32mm x 0.25 mm TR-110233

liquid-solid extraction and GC/ECD TRB-5 30m x 0.32mm x 0.25 mm TR-120233

TRB-1701 30m x 0.32mm x 0.25 mm TR-130233

TRB-5ms 30m x 0.32mm x 0.25 mm TR-520233

524.2524.2524.2524.2 Measurement of purgeable organic compounds in water TRB-624 30m x 0.25mm x 1.4 mm TR-601432

by Purge & Trap capillary column GC/MS TRB-624 30m x 0.53mm x 3.0 mm TR-603035

TRB-624 75m x 0.53mm x 3.0 mm TR-603075

TRB-624 60m x 0.32mm x 1.8 mm TR-601863

525525525525 Capillary column GC/MS Organic compounds in drinking waterby liquid-solid extraction

TRB-5 30m x 0.32mm x 0.25 mm TR-120233

TRB-5ms 30m x 0.25mm x 0.25 mm TR-520232


5 6

EPA Solid Waste Test MethodsDOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP

0108 0108 0108 0108 0108 scinagroelitalovdetanegolaH 426-BRT 0.3xmm35.0xm57 mm 570306-RT

426-BRT 4.1xmm52.0xm03 mm 234106-RT

5108 5108 5108 5108 5108 scinagroelitalovdetanegolaH-noN 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 4.1xmm52.0xm03 mm 234106-RT

1208/0208 1208/0208 1208/0208 1208/0208 1208/0208 cinagroelitalovcitamorA 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 4.1xmm52.0xm03 mm 234106-RT

1308/0308 1308/0308 1308/0308 1308/0308 1308/0308 elirtinoteca,elirtinolyrca,nielorcA 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 4.1xmm52.0xm03 mm 234106-RT

1408/0408 1408/0408 1408/0408 1408/0408 1408/0408 slonehP 5-BRT 5.1xmm35.0xm03 mm 535121-RT

sm5-BRT 52.0xmm52.0xm03 mm 232025-RT

1608/0608 1608/0608 1608/0608 1608/0608 1608/0608 sretseetalahthP 1-BRT 5.1xmm35.0xm51 mm 515111-RT

sm1-BRT 4.0xmm52.0xm03 mm 234015-RT

0808 0808 0808 0808 0808 sBCPdnasedicitsepenirolhconagrO 5-BRT 5.1xmm35.0xm03 mm 535121-RT


2808/1808 2808/1808 2808/1808 2808/1808 2808/1808 rolhcorAsasBCPdnasedicitsepenirolhconagrO 5-BRT 5.1xmm35.0xm03 mm 535121-RT

1071-BRT 0.1xmm35.0xm03 mm 530131-RT

1908/0908 1908/0908 1908/0908 1908/0908 1908/0908 senotekscilcycdnascitamoraortiN 5-BRT 5.1xmm35.0xm03 mm 535121-RT


0018 0018 0018 0018 0018 snobracordyhcitamoraraelcunyloP 5-BRT 52.0xmm23.0xm03 mm 332021-RT

sm5-BRT 52.0xmm23.0xm03 mm 332025-RT

1218/0218 1218/0218 1218/0218 1218/0218 1218/0218 snobracordyhdetanirolhC 1-BRT 0.1xmm23.0xm03 mm 330111-RT


0418 0418 0418 0418 0418 sedicitsepsurohpsohponagrO 1-BRT 5.1xmm23.0xm03 mm 535111-RT

1071-BRT 0.1xmm35.0xm03 mm 530131-RT

1-BRT 52.0xmm52.0xm03 mm 232011-RT

1418 1418 1418 1418 1418 sedicitsepsurohpsohponagrO 5-BRT 5.1xmm35.0xm51 mm 515121-RT

sm5-BRT 52,0xmm52.0xm51 mm 212025-RT

1518/0518 1518/0518 1518/0518 1518/0518 1518/0518 sedicibrehdetanirolhC 5-BRT 0.1xmm35.0xm52 mm 520121-RT

1071-BRT 0.1xmm35.0xm03 mm 530131-RT

sm5-BRT 52,0xmm52.0xm51 mm 232025-RT


57

DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP

0428 0428 0428 0428 0428 scinagroelitalovrofSM/CG 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 0.3xmm35.0xm57 mm 570306-RT

426-BRT 0.3xmm35.0xm501 mm 5K0306-RT

426-BRT 0.1xmm52.0xm03 mm 230106-RT

0528 0528 0528 0528 0528 scinagroelitalov-imesrofSM/CG sm5-BRT 05,0xmm52.0xm03 mm 235025-RT

0628 0628 0628 0628 0628 seuqinhcetyrallipacscinagroelitalovrofdohtemSM/CG 426-BRT 0,3xmm35.0xm03 mm 530306-RT

426-BRT 0,3xmm35.0xm57 mm 570306-RT

426-BRT 0,3xmm35.0xm501 mm 5K0306-RT

426-BRT 0,1xmm52.0xm03 mm 230106-RT

0728 0728 0728 0728 0728 seuqinhcetyrallipacscinagroelitalov-imesrofdohtemSM/CG 5-BRT 0,1xmm52.0xm03 mm 230121-RT

sm5-BRT 0,1xmm52.0xm03 mm 230125-RT

0828 0828 0828 0828 0828 dnasnixoid-p-oznebiddetanirolhcylopfosisylanAsnarufoznebiddetanirolhcylop

5-BRT 52,0xmm52.0xm03 mm 232021-RT

sm5-BRT 52,0xmm52.0xm06 mm 261025-RT


106 106 106 106 106 snobracolahelbaegruP 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 0.3xmm35.0xm57 mm 570306-RT

426-BRT 0.3xmm35.0xm501 mm 5K0306-RT

426-BRT 0.1xmm52.0xm03 mm 230106-RT

206 206 206 206 206 scitamoraelbaegruP 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 0.3xmm35.0xm501 mm 5K0306-RT

426-BRT 0.1xmm52.0xm03 mm 230106-RT

306 306 306 306 306 elirtinolyrcadnanielorcA 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 0.1xmm52.0xm03 mm 230106-RT

506/406 506/406 506/406 506/406 506/406 senidiznebdnaslonehP sm5-BRT 4.1xmm35.0xm03 mm 534125-RT

sm5-BRT 52.0xmm52.0xm03 mm 232025-RT

606 606 606 606 606 sretseetalahthP 5-BRT 5.1xmm35.0xm51 mm 515121-RT

sm5-BRT 52.0xmm52.0xm03 mm 232025-RT

EPA Solid Waste Test Methods

EPA Waste Water Test Methods


5 8


606 606 606 606 606 sretseetalahthP 5-BRT 5.1xmm35.0xm51 mm 515121-RT

sm5-BRT 52.0xmm52.0xm03 mm 232025-RT

706 706 706 706 706 senimasortiN 5-BRT 5.1xmm35.0xm03 mm 535121-RT

sm5-BRT 05.0xmm52.0xm03 mm 235025-RT

806 806 806 806 806 sBCPdnasedicitsepenirolhconagrO 5-BRT 0.1xmm35.0xm05 mm 550121-RT

sm5-BRT 21.0xmm52.0xm05 mm 257025-RT

906 906 906 906 906 enorohposidnascitamoraortiN 5-BRT 5.1xmm35.0xm03 mm 535121-RT


016 016 016 016 016 snobracordyHcitamorAcilcycyloP 5-BRT 52.0xmm23.0xm03 mm 332021-RT

sm5-BRT 01.0xmm23.0xm03 mm 331025-RT

116 116 116 116 116 srehteolaH 5-BRT 5.1xmm35.0xm51 mm 515121-RT

sm5-BRT 05.0xmm52.0xm03 mm 235025-RT

216 216 216 216 216 snobracordyhdetanirolhC 5-BRT 0.1xmm23.0xm03 mm 330121-RT


316 316 316 316 316 nixoid-p-oznebidorolhcartet-8,7,3,2 sm5-BRT 01.0xmm52.0xm06 mm 261025-RT

516 516 516 516 516 sedicibrehdetanirolhC 1071-BRT 0.1xmm35.0xm03 mm 530131-RT

1071-BRT 52.0xmm52.0xm03 mm 232031-RT

916 916 916 916 916 sedicibrehenizairT 05-BRT 0.1xmm35.0xm03 mm 530105-RT

05-BRT 05.0xmm52.0xm03 mm 235005-RT

426 426 426 426 426 selbaegruP 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 0.3xmm35.0xm57 mm 570306-RT

426-BRT 0.3xmm35.0xm501 mm 5K0306-RT

426-BRT 4.1xmm52.0xm03 mm 234106-RT

526 526 526 526 526 sdicadnaslartuen/esaB sm5-BRT 52.0xmm23.0xm03 mm 332025-RT

sm1-BRT 52.0xmm52.0xm03 mm 232015-RT

086 086 086 086 086 tnemides/liosdnaretawnisBCPdnasedicitseP 5-BRT 52.0xmm23.0xm03 mm 332021-RT

sm5-BRT 52.0xmm23.0xm03 mm 332025-RT

4261 4261 4261 4261 4261 SM/CGnoitulidepotosiybsdnuopmoccinagroelitaloV 426-BRT 0.3xmm35.0xm03 mm 530306-RT

426-BRT 4.1xmm52.0xm03 mm 234106-RT

5261 5261 5261 5261 5261 noitulidepotosiybsdnuopmoccinagroelitalovimeS 5-BRT 52.0xmm52.0xm03 mm 232021-RT

sm5-BRT 52.0xmm52.0xm03 mm 232025-RT

3561 3561 3561 3561 3561 noitalycaSMutis-niybretawetsawnislonehpdetanirolhCSM/deelbwolCGdna

5-BRT 52.0xmm23.0xm03 mm 332021-RT

sm5-BRT 52.0xmm23.0xm03 mm 332025-RT

EPA Waste Water Test Methods


59

Packed Columns

NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED TROPPUSDILOS TROPPUSDILOS TROPPUSDILOS TROPPUSDILOS TROPPUSDILOS EDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU

htraesuoeciliS tropocliS brosomorhC PHW A1S

dehsaw-esabdna-dicahtobdnaA1Ssadetaert,htraesuoeciliS tropocliS WBW BA1S

,dehsaw-dica,Cº009evobarednibyalcahtiwdenrubrodeniclac,kcirberifdehsurCdezinalisebyam

brosomorhC SCDMDWAP C1S

htraesuoecilisdetaertnU brosomorhC WANW SN1S

nag/2m05nahtsselfoaeraecafruslanimonhtiwremylopocenezneblynivid-enerytS4.0-3.0foretemaiderop.eva µµµµµ m

brosomorhC 101 2S

g/2m006ot005foaeraecafruslanimonhtiwremylopocenezneblynivid-enerytS5700.0foretemaiderop.evadna µµµµµ m

peseyaH kcaparoPQ Q 3S

lanimonagnivahspuorgN-dna0-citamorahtiwremylopocenezneblynivid-enerytS6700.0foretemaiderop.evadnag/2m006ot004foaeraecafrus µµµµµ m

peseyaH kcaparoPR R 4S

hsem06-04,remylopenelyhteroulfartetthgiewralucelomhgiH brosomorhC T 5S

dnag/2m053-052foaeraecafruslanimonhtiwremylopocenezneblynivid-enerytS1900.0foretemaiderop.eva µµµµµ m

brosomorhC kcaparoP,201 peseyaH, 6S

g/2m21foaeraecafruslanimonagnivahnobracdezitihparG kcalBobraC 7S

enezneblynividenerytsdnaenidiryp-lyniv-4foremylopoC peseyaH kcaparoP,S S 8S

edixoenelynehp-p-lynehpid-6,2nodesabremylopsuoroP xaneT AT 9S

enezneblynividdnaetirtinolyrcaforemylopocdeknil-ssorcylhgiH peseyaH C 01S

llamshtiwdeifidom,g/2m001foaeraecafruslanimonagnivahnobracdezitihparGdnuopmoclocylgenelyhteylopdnamutalortepfostnuoma

kcalBobraC 0051tR%3021/08B 11S

G g/2m001foaeraecafruslanimonagnivahnobracdezitihpar kcalBobraC B 21S

- Solid Supports for USP Methods

TTTTT e k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n s

6 0

These columns have been used for the last 50 years in all kinds of analyses forgas chromatography.

"Packed colum use today is understandable due to the wide range of solid supportpackings available and to their high on-column sample capacity. These aspectsmake packed columns quite versatile for a wide range of applications".

"Today Packed columns are still demostrating their utility in the solution of manyanalytical problems where it is not necessary to use the high resolution of capillarycolumns".

"Teknokroma has packed columns since its beginnings and have always provided awide range and latest advantages in this area of gas chromatography. Within thesenew advances we showcase the latest advance in micro-packed columns (0,75mmand 1,00mm ID) and new bonded phase packings".

WE CAN SUPPLWE CAN SUPPLWE CAN SUPPLWE CAN SUPPLWE CAN SUPPLY YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!

TTTTTubingubingubingubingubing ExterExterExterExterExternal Diameter (OD)nal Diameter (OD)nal Diameter (OD)nal Diameter (OD)nal Diameter (OD) InterInterInterInterInternal Diameter (ID)nal Diameter (ID)nal Diameter (ID)nal Diameter (ID)nal Diameter (ID)

Glass 1/4’’ 2mm, 3mm and 4 mm

Stainless Steel 1/4 ’’ and 1/8’’ 4mm, 3mm and 2 mm

Silcosteel 1/4’’ and 1/8’’ 5.2mm and 2 mm

1/16’’ 0.75mm and 1 mm

Nickel, Teflon and Copper 1/8’’ 2 mm

ChromatographChromatographChromatographChromatographChromatograph ConfigurationConfigurationConfigurationConfigurationConfiguration TTTTTubingubingubingubingubing DimmensionsDimmensionsDimmensionsDimmensionsDimmensions PhasePhasePhasePhasePhase SupporSupporSupporSupporSupportttttModelModelModelModelModel (%)(%)(%)(%)(%) (mesh)(mesh)(mesh)(mesh)(mesh)

Agllient 5890 ON-Column Glass 1.8m x 1/4’’ OD 3% Chromosorb W-HP

X 2mm ID SE-30 80/100 mesh

Columns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anextra cost (please inquire).extra cost (please inquire).extra cost (please inquire).extra cost (please inquire).extra cost (please inquire).

To order a packed column it is necessary to supply the following parameters:


Packed Columns


NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT EDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU

TAhcetllA MT 0001- 052/05 53G

nozeipA L 003/05 -

nozeipA M 003/05 -

43enotneB 081/0 -

)FECB(edimamrof)lyhteonayC-2(-sib-N,N 521/02 -

)TBMB(enidiulot-p-ib-’a,a-)enedilyznebyxohteM-p(-sib-N,N 051 -

)AEEB(etapidA)lyhteyxohte-2(-siB 051 -

)AEMB(etapidA)lyhteyxohtem-2(-siB 051 -

xawobraC 004 001/02 02G

xawobraC 045 571/04 93G

xawobraC 006 521/02 -

xawobraC 0001 051/04 41G

xawobraC 0541 571/05 -

xawobraC 0533 002/06 51G

xawobraC 0006 002/06 -

xawobraC M02 522/06 61G

xawobraC 22222 APT-M0 052/06 52G

)lyhteM(ktsc053,002-CD 052/02 -

)lyhteM(ktsc005,002-CD 052/02 -

)lyhehP-%52(,055-CD 522/02 82G

lisxeD CG003 004/05 33G

etaelaMlytub-n-iD 05/02 -

etalahthplyced-n-iD 571/01 -

etacabes)lyxehlyhte-2(iD 521/0 11G

etapidAlocylgenelyhteiD 012/02 -

etaniccuSlocylgenelyhteiD 002/02 4G

lorecylgiD 001/02 -

etanofluslyhtemiD-4,2 05/0 -

etalahthPlynoniD 051/02 -

etalahthPlycedosiiD 051/02 42G

etapidAlocylgenelyhtE 012/001 -

etaniccuSlocylgenelyhtE 012/001 -

134-CFdaroulF 002/04 -

PAFF 052/05 53G

52-41lionobracolaH 051 -

lapegI 036-OC 002/03 -

lapegI )lonyxonoN(088-OC 002/001 13G

lapegI 099-OC 002/001 -

F-leK 01.oNliO 001 -

etaniccuSlocylglytnepoeN 032/05 12G

VO MT )muglyhteM(1- 053/001 2G

61

Packed Columns

PACKED COLUMNS

Column: 5% Carbowax 20M CarboBlack B/AW, 80/120 meshDimensions: 2m x 1/8" OD X 2mm ID, (Silcosteel)Injection: 1 µl standard, 175ºCCarrier Gas: He, 15mL/minOven temperature: 60ºC(6min) @ 10ºC/min to150ºC(7min)Detector: FID, 175ºC

Peak Name

1- Acetaldehyde2- Methanol3- Acetone4- Ethyl formate5- Ethanol6- Ethyl acetate7- n-Propanol8- Secbutanol9- Isobutanol10- Acetic acid11- Amyl alcohol12- Isoamyl alcohol13- n-Amyl alcohol14- Propionic acid

NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT EDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU

VO MT )lynehp%05(71- 053/02 3G

VO MT )lynehp%05(lyniV-71- +003 -

VO MT )lynehp%57(52- 003 71G

VO MT )diulflyhteM(101- 053/02 1G

VO MT )lyporporoulfirT%05(012- +572/02 6G

VO MT )lyhtemlyporponayc%52,lynehp%52(522- +052/02 91G

VO MT )lyllaonayciD(572- +052 -

VO MT 1071- 052/0 -

β,β β,β β,β β,β β,β elirtinoiporpidyxO- 57/0 -

etaniccuSenimalonahteidlynehP 032/0 21G

etapidalocylgenelyhteyloP 522/0 32G

enimienelyhteyloP 571/0 -

421-SO)sgnir5(rehtelynehpyloP 002/0 -

831-SO)sgnir6(rehtelynehpyloP 522/0 -

locylgenelyporpyloP 051/0 -

enimienelyporpyloP 002/0 -

)lyporporoulfirT%05(1-FQ 052/02 -

)muglyhteM(03-ES 003/57 -

)edargCG(03-ES 003/57 2G

)lynehP%5(25-ES 003/05 72G

)lyniV%1,lynehP%5(45-ES 003/05 63G

elirtinocabeS 051 -

raliS )enociliSlynehPlyporponayC%05(PC5 052/05 7G

raliS )enociliSlynehPlyporponayC%09(PC9 052/05 8G

raliS )enociliSlyporponayC%001(C01 052/05 5G

lotibroS 051/001 31G

0021-PS 002/52 -

)enocilislyhteM(0012-PS 053/0 1G

)enaxolislynehplyporponaycyloP(0032-PS 572/02 7G

enaxolis)lynehplyporponayc-%02-lyporponaycsib-%08(yloP(0332-PS 572/52 8G

)enaxolislyporponaycsibyloP(0432-PS 572/52 5G

enelauqS 051/02 -

XOREPUS )WM000.000.4(4 003 -

XOREPUS )WM000.02(M02 052/06 -

)EPECT(lotirhtyreatnePdetalyhteonaycarteT 051/03 -

)DEEHT(enimaiDenelyhtelyhteyxordyharteT 521 -

)PECT(enaporp)yxohteonayc-2(-sirT-3,2,1 081/02 -

notirT 001-X 002/0

notirT )lonahteyxohteyloPyxonehplytcO(503-X 052/02 -

)289W-CU(89-WCU +003/08 9G

)locylGenelyklayloP(X-0081-BLNOCU 002 81G

dimasreV 009 572 -

For other stationarFor other stationarFor other stationarFor other stationarFor other stationary phases please inquirey phases please inquirey phases please inquirey phases please inquirey phases please inquire

TKG 1146


6 2

17 mm17 mm17 mm17 mm17 mm12.7 mm12.7 mm12.7 mm12.7 mm12.7 mm11.5 mm11.5 mm11.5 mm11.5 mm11.5 mm11 mm11 mm11 mm11 mm11 mm10 mm10 mm10 mm10 mm10 mm9.5 mm9.5 mm9.5 mm9.5 mm9.5 mm9 mm9 mm9 mm9 mm9 mm5 mm5 mm5 mm5 mm5 mm

Measure Guideyour old septum here

GC Septa

CenterGuideTM Septa for Improved Performance

• Center point guides the needle for easy penetration.• Reduce needle bending• Precision molding assures accurate fit• Available in selected sizes of our premium septa• Improves injection life in some applications

The CenterGuideTM design is currently available in many sizes of our septa SeptaSeptaSeptaSeptaSeptaBTOBTOBTOBTOBTOTMTMTMTMTM, Maratahon, Maratahon, Maratahon, Maratahon, MaratahonTMTMTMTMTM and Advanced Green and Advanced Green and Advanced Green and Advanced Green and Advanced GreenTMTMTMTMTM.....

Septum Size ChartInstrInstrInstrInstrInstrumentumentumentumentument Septum sizeSeptum sizeSeptum sizeSeptum sizeSeptum size

(mm)(mm)(mm)(mm)(mm)

Agilent (HP)Agilent (HP)Agilent (HP)Agilent (HP)Agilent (HP)

5880A, 5890, 6890, 6850 11

5700, 5880 9.5/10

On-Column Injection 5

CE InstrCE InstrCE InstrCE InstrCE Instruments (TMQ)uments (TMQ)uments (TMQ)uments (TMQ)uments (TMQ)

TRACE GC 17

Finnigan (TQM)Finnigan (TQM)Finnigan (TQM)Finnigan (TQM)Finnigan (TQM)

GC 9001 9.5

GCQ 9.5

GCQ w/TRACE 17

QCQ 9.5

TRACE 2000 9.5

Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)

8000 Series 17

InstrInstrInstrInstrInstrumentumentumentumentument Septum sizeSeptum sizeSeptum sizeSeptum sizeSeptum size(mm)(mm)(mm)(mm)(mm)

PerkinElmerPerkinElmerPerkinElmerPerkinElmerPerkinElmer

Sigma Series 11

900, 990 11

8000 Series 11

Auto SYS 11

Auto SYS XL 11

Pye/UnicamPye/UnicamPye/UnicamPye/UnicamPye/UnicamAll models 7

ShimadzuShimadzuShimadzuShimadzuShimadzuAll models Plug

VVVVVarianarianarianarianarianInjector Type:

Varian Packed Column 9.5/10

Split/splitless

Varian 1078/1079 10/11

Varian 1177 9

Varian 1075/1077 11

Septa BTO TM ( Bleed and Temperature Optimized )

• Extended Temperature Range , Low Bleed• Maximum Temperature 400 ºC in most instruments• Virtually eliminates injection-port sticking• Pre-conditioned; packaged in glass to prevent contamination• Each batch GC-FID tested• Ideal for use with low bleed “Mass Spec” capillary columns

This septa has a excellent performance. You can use this septa at 400 ºC with most modern GCs, for some models 375 ºC isthe maximum; for 17 mm injectors the maximum is 300 ºC. When you need a septa that you need to use with hightemperature and low bleed this is the septa you should use.The BTO Septa has been optimized to reduce injection port adhesion. Is a ideal septa for trace analysis, high injection porttemperature.The BTO Septa are pre-conditioned and packages in glass to prevent contamination.

ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K298787TR-K298787TR-K298787TR-K298787TR-K298787 5 mm Septa BTO for HP OCI port “Center Guide” 50TR-K298705TR-K298705TR-K298705TR-K298705TR-K298705 9,5 mm 3/8” Septa BTO 50TR-K298745TR-K298745TR-K298745TR-K298745TR-K298745 10 mm Septa BTO 50TR-K298717TR-K298717TR-K298717TR-K298717TR-K298717 11mm 7/16” Septa BTO “Center Guide” 50TR-K298775TR-K298775TR-K298775TR-K298775TR-K298775 11,5 mm Septa BTO for Varian 50TR-K298725TR-K298725TR-K298725TR-K298725TR-K298725 12,7 mm 1/2" Septa BTO 50TR-K298815TR-K298815TR-K298815TR-K298815TR-K298815 17 mm Septa BTO 50

Cylindrical for Shimadzu InstrumentsTR-K298735TR-K298735TR-K298735TR-K298735TR-K298735 Plug Type Septa BTO for Shimadzu 50

CenterGuide Septa Advanced GreenTM

G C S e p t aG C S e p t aG C S e p t aG C S e p t aG C S e p t a

63

17 mm17 mm17 mm17 mm17 mm12.7 mm12.7 mm12.7 mm12.7 mm12.7 mm11.5 mm11.5 mm11.5 mm11.5 mm11.5 mm11 mm11 mm11 mm11 mm11 mm10 mm10 mm10 mm10 mm10 mm9.5 mm9.5 mm9.5 mm9.5 mm9.5 mm9 mm9 mm9 mm9 mm9 mm5 mm5 mm5 mm5 mm5 mm

Measure Guideyour old septum here

GC SeptaMarathon Septa TM (The premium Septa for Autosamplers)

• Outstanding Lifetime• Premium Septum for autosamplers• Ideal for Overnight Runs• Up to 400 injections per Septum• Maximum Temperature 350 ºC• Soft, 45 Durometer, Easy On Autosampler Needles

The septa Marathon, has developed and advanced GC septum for autosampler use, with significantly longer life. The Marathonseptum typically achieves 400 injections without failure, when used with a rounded-tip (HP-style) needles and autosampler orneedle guide. Now you can make extended autosampler runs without fear of sample loss, caused by blow-back of leakingcarrier gas. The Marathon septum is also ideal for standard manual-injection GC and GC/MS.It is packaged in glass vials.

ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K239587TR-K239587TR-K239587TR-K239587TR-K239587 5 mm Marathon for HP OCI port “Center Guide” 25TR-K239188TR-K239188TR-K239188TR-K239188TR-K239188 9,5 mm 3/8” Marathon 25TR-K239287TR-K239287TR-K239287TR-K239287TR-K239287 11mm 7/16” Marathon “Center Guide” 25TR-K239788TR-K239788TR-K239788TR-K239788TR-K239788 11,5 mm Marathon for Varian 25TR-K239388TR-K239388TR-K239388TR-K239388TR-K239388 12,7 mm 1/2" Marathon 25TR-K239688TR-K239688TR-K239688TR-K239688TR-K239688 17 mm Marathon 25

Cylindrical for Shimadzu InstrumentsTR-K239488TR-K239488TR-K239488TR-K239488TR-K239488 Plug Type Marathon for Shimadzu 25

Septa Advanced Green 3TM

• True Long-Life, High Temperature Green Septum• More injections per Septum• Reduced Injection Port Sticking• Maximum Temperature 350 ºC

The Septum Advanced Green 3 was specifically created to combine significantly longer injection life, low bleed and lowinjection port adhesion. The result is a green septum good for general purpose use.The septum are packaged in glass vials for high purity.

ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K246525TR-K246525TR-K246525TR-K246525TR-K246525 5 mm Advanced Green 3TM for HP OCI port “Center Guide” 50TR-K246124TR-K246124TR-K246124TR-K246124TR-K246124 9,5 mm 3/8” Advanced Green 3TM 50TR-K246225TR-K246225TR-K246225TR-K246225TR-K246225 11mm 7/16” Advanced Green 3TM “Center Guide” 50TR-K246724TR-K246724TR-K246724TR-K246724TR-K246724 11,5 mm Advanced Green 3TM for Varian 50TR-K246324TR-K246324TR-K246324TR-K246324TR-K246324 12,7 mm 1/2" Advanced Green 3TM 50TR-K246624TR-K246624TR-K246624TR-K246624TR-K246624 17 mm Advanced Green 3TM 50

Cylindrical for Shimadzu InstrumentsTR-K246424TR-K246424TR-K246424TR-K246424TR-K246424 Plug Type Advanced Green 3TM for Shimadzu 50


6 4

Septa 77TM

This is our high-quality septum, suitable for most applications. It has been the standard septum in GC and GC/MS labs foryears. Septa 77 features low bleed with excellent resealing capability and good temperature endurance. Septa 77 is carefullyprocessed, then packaged in glass bottles for purity. Maximum temperature is 300 ºC, except in 17 mm injection ports,270ºC.

ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K237785TR-K237785TR-K237785TR-K237785TR-K237785 5 mm Septa 77 for HP 5880/90 OCI Port 50TR-K237765TR-K237765TR-K237765TR-K237765TR-K237765 6 mm Septa 77 for Hitachi (4,5 mm thick) 50TR-K237755TR-K237755TR-K237755TR-K237755TR-K237755 1/4" Septa 77 50TR-K237705TR-K237705TR-K237705TR-K237705TR-K237705 9,5 mm 3/8” Septa 77 50TR-K237745TR-K237745TR-K237745TR-K237745TR-K237745 10mm Septa 77 50TR-K237715TR-K237715TR-K237715TR-K237715TR-K237715 7/16” Septa 77 50TR-K237725TR-K237725TR-K237725TR-K237725TR-K237725 12,7 mm 1/2" Septa 77 50

Cylindrical for Shimadzu InstrumentsTR-K237735TR-K237735TR-K237735TR-K237735TR-K237735 Plug Type Septa 77 for Shimadzu 50

MicrosepTM Septa F-174 Medium-Performance Septum

This is a good -performance silicone septum faced on side with a layer of TFE teflon. Thickness is approximately 3 mm. Thecolor is White/yellow . Sold in packages of 50.

ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K230905TR-K230905TR-K230905TR-K230905TR-K230905 9,5 mm 3/8” Microsep Septa F-174 100TR-K230115TR-K230115TR-K230115TR-K230115TR-K230115 11 mm 7/16” Microsep Septa F-174 100TR-K230125TR-K230125TR-K230125TR-K230125TR-K230125 12,5 mm 1/2” Microsep Septa F-174 100

Tekno Blue Septa (Economy Blue Septa)

The septa Tekno Blue are designed for non-demanding, routine applications. They are easy to penetrate, with a durometerrating of 40-45. These septa can be used up to 200-250 ºC and are suitable for 90 % of all GC analysis. Made from silicone.The package is for 100 pieces.

ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K00500TR-K00500TR-K00500TR-K00500TR-K00500 6,4 mm 1/4" Tekno Blue Septa 100TR-K00510TR-K00510TR-K00510TR-K00510TR-K00510 9,5 mm 3/8” Tekno Blue Septa 100TR-K00520TR-K00520TR-K00520TR-K00520TR-K00520 11 mm 7/16” Tekno Blue Septa 100TR-K00530TR-K00530TR-K00530TR-K00530TR-K00530 12,5 mm 1/2" Tekno Blue Septa 100

Tekno Red Septa (General Purpose Septa)

• The Tekno Red Septa is a very low bleed septa .• Is easy to penetrate• Have a long injection lifetime at 300 ºC• Maximum temperature 350• Durometer hardness is 45-55

ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K00300TR-K00300TR-K00300TR-K00300TR-K00300 9,5 mm 3/8” Tekno Red 50TR-K00320TR-K00320TR-K00320TR-K00320TR-K00320 11 mm 7/16” Tekno Red 50TR-K00330TR-K00330TR-K00330TR-K00330TR-K00330 12,5 mm 1/2" Tekno Red 50

GC Septa


65

GC Ferrules

Graphite Ferrules

• The best material for high temperature use.• Upper temperature limit 450ºC• High-purity Graphite minimizes bleed effects and detector interferences in GC• Preferred by capillary GC use• Smoother surface cleanser edges• Perfect sealing material for glass, and fused silica• Reusable if not overtightened• Not recommended for GC/MS connections

FerFerFerFerFerrrrrrules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Short Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211165TR-K211165TR-K211165TR-K211165TR-K211165 1/16" to 0.5 mm 0.25 - 0.32 mm id 10TR-K211168TR-K211168TR-K211168TR-K211168TR-K211168 1/16" to 0.8 mm 0.53 mm id 10TR-K211160TR-K211160TR-K211160TR-K211160TR-K211160 1/16" to 1.0 mm 0.53 - 0.65 mm id 10

G C F e rG C F e rG C F e rG C F e rG C F e r rrrrr u l e su l e su l e su l e su l e s

Capillary Column Ferrules

GraphiteThe best material for high temperature use. This is also the softest ferrule material, so it seals gas tight without the risk ofbreaking the column. It does not stick to glass at higher temperatures and may be reused or moved along the column severaltimes if not overtightened; seals with finger-tight pressures. Its one-piece design fits both SwangelokTM and ParkerTM fittings,and does not need a back ferrule. Upper temperature limit is 450ºC.

VespelTM/Graphite60% polymide - 40% graphite. This is especially recommended for GC/MS interface applications. Our one-piece design requiresno back ferrule, and can be reused if not over-tightened. Upper temperature limit is 400ºC.

VespelTM

100% high-temperature polymide. VespelTM is fairly hard and tends to stick to glass columns, usually not reusable. One-piecedesign requires no back ferrule. Upper temperature limit is 350ºC.

TeflonTM

These ferrules are made from 100% TeflonTM in a one-piece design that requires no bback ferrule. Almost completely inert, fairlysoft. Upper temperature limit is 250ªC.

Ferrules for Agilent (HP) HP 5890 and 6890Ferrules ending with HP are reducing ferrules designed to fit all inlets and detectors on the HP 5890 and 6890, except theMSD. The MSD should be used with standard 1/16" ferrules, preferably made from Vespel/Graphite.

Ferrules for Thermo Quest/Fisons/CE Instruments.See in pages 66 and 67.

Ferrules for Perkin Elmer Sigma SeriesUse 1/8" ferrules

Ferrules/Capillary Columns0.25 mm id columns use 0.4 mm id ferrules0.32 mm id columns use 0.5 mm id ferrules0.53 mm id columns use 0.8 mm id ferrules

Agilent / Hewlett-Packard - Graphite

Graphite Ferrules

6 6

Graphite Standard FerGraphite Standard FerGraphite Standard FerGraphite Standard FerGraphite Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211104TR-K211104TR-K211104TR-K211104TR-K211104 1/16" to 0.4 mm 0.25 mm id 10TR-K211105TR-K211105TR-K211105TR-K211105TR-K211105 1/16" to 0.5 mm 0.32 mm id 10TR-K211108TR-K211108TR-K211108TR-K211108TR-K211108 1/16" to 0.8 mm 0.53 mm id 10TR-K211110TR-K211110TR-K211110TR-K211110TR-K211110 1/16" to 1.0 mm 0.65 mm id 10

Graphite 2-Hole Standard FerGraphite 2-Hole Standard FerGraphite 2-Hole Standard FerGraphite 2-Hole Standard FerGraphite 2-Hole Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211124TR-K211124TR-K211124TR-K211124TR-K211124 1/16" 2-hole 0.4mm/0.4mm 0.25 mm id 10TR-K211125TR-K211125TR-K211125TR-K211125TR-K211125 1/16" 2-hole 0.5mm/0.5mm 0.32 mm id 10

Reducing Graphite FerReducing Graphite FerReducing Graphite FerReducing Graphite FerReducing Graphite Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211204TR-K211204TR-K211204TR-K211204TR-K211204 1/8" to 0.4 mm 0.25 mm id 10TR-K211205TR-K211205TR-K211205TR-K211205TR-K211205 1/8" to 0.5 mm 0.32 mm id 10TR-K211208TR-K211208TR-K211208TR-K211208TR-K211208 1/8" to 0.8 mm 0.53 mm id 10TR-K211210TR-K211210TR-K211210TR-K211210TR-K211210 1/8" to 1/16" 1/16" od 10TR-K211405TR-K211405TR-K211405TR-K211405TR-K211405 1/4" to 0.5 mm 0.32 mm id 10TR-K211408TR-K211408TR-K211408TR-K211408TR-K211408 1/4" to 0.8 mm 0.53 mm id 10TR-K211420TR-K211420TR-K211420TR-K211420TR-K211420 1/4" to 1/8" 1/8" od 10TR-K211410TR-K211410TR-K211410TR-K211410TR-K211410 1/4" to 1/16" 1/16" od 10

Graphite 2-Hole Reducing FerGraphite 2-Hole Reducing FerGraphite 2-Hole Reducing FerGraphite 2-Hole Reducing FerGraphite 2-Hole Reducing Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211222TR-K211222TR-K211222TR-K211222TR-K211222 1/8" 2 hole 0.5mm/ 0.5mm 0.32 mm id 10

Special ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite Ferrrrrrules for Shimadzuules for Shimadzuules for Shimadzuules for Shimadzuules for ShimadzuReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K211500TR-K211500TR-K211500TR-K211500TR-K211500 5 mm for Shimadzu 5 mm od columns 10

Special ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite Ferrrrrrules for Carlo Erbaules for Carlo Erbaules for Carlo Erbaules for Carlo Erbaules for Carlo ErbaReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211904TR-K211904TR-K211904TR-K211904TR-K211904 0.4 mm ID for M8 nut 0.25 mm id 10TR-K211905TR-K211905TR-K211905TR-K211905TR-K211905 0.5 mm ID for M8 nut 0.32 mm id 10TR-K211908TR-K211908TR-K211908TR-K211908TR-K211908 0.8 mm ID for M8 nut 0.53 mm id 10

Special ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite Ferrrrrrules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferrrrrru leuleuleuleuleReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211982TR-K211982TR-K211982TR-K211982TR-K211982 Cup Ferrule 0.25 mm ID for M4 nut 0.20 mm id 2TR-K211983TR-K211983TR-K211983TR-K211983TR-K211983 Cup Ferrule 0.35 mm ID for M4 nut 0.25 mm id 2TR-K211984TR-K211984TR-K211984TR-K211984TR-K211984 Cup Ferrule 0.45 mm ID for M4 nut 0.32 mm id 2TR-K211988TR-K211988TR-K211988TR-K211988TR-K211988 Cup Ferrule 0.8 mm ID for M4 nut 0.53 mm id 2TR-K211948TR-K211948TR-K211948TR-K211948TR-K211948 Graphite Liner Seal 8 mm 1

Graphite Straight FerGraphite Straight FerGraphite Straight FerGraphite Straight FerGraphite Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211100TR-K211100TR-K211100TR-K211100TR-K211100 1/16" 1/16" 10TR-K211200TR-K211200TR-K211200TR-K211200TR-K211200 1/8" 1/8" 10TR-K211400TR-K211400TR-K211400TR-K211400TR-K211400 1/4" 1/4" 10TR-K211600TR-K211600TR-K211600TR-K211600TR-K211600 3/8" 3/8" 10TR-K211800TR-K211800TR-K211800TR-K211800TR-K211800 1/2" 1/2" 5

O-Ring made of VO-Ring made of VO-Ring made of VO-Ring made of VO-Ring made of VitonitonitonitonitonTMTMTMTMTM for Agilent for Agilent for Agilent for Agilent for AgilentReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K211973TR-K211973TR-K211973TR-K211973TR-K211973 O-Ring made of Viton for HP 12

GC Ferrules


1/16"- Graphite Ferrules

Carlo Erba - Graphite for M8 nut

Fisons /Carlo Erba "Cup" Graphite Ferrulefor M4 nut.

8 mm Graphite Liner Seal for Fisons/CE

O-ring made of Viton for Agilent HP

67G C F e rG C F e rG C F e rG C F e rG C F e r rrrrr u l e su l e su l e su l e su l e s

VerspelTM / Graphite Ferrules

• Precision drilled (id)• One-piece design no black ferrule• Stable to 400ºC• Recommended for GC/MS interface applications• Can be re-used• 40% graphite, 60% high temp DuPont polymide

FerFerFerFerFerrrrrrules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Short Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213163TR-K213163TR-K213163TR-K213163TR-K213163 1/16" to 0.3 mm 0.10 mm id 10TR-K213164TR-K213164TR-K213164TR-K213164TR-K213164 1/16" to 0.4 mm 0.25 mm id 10TR-K213165TR-K213165TR-K213165TR-K213165TR-K213165 1/16" to 0.5 mm 0.32 mm id 10TR-K213168TR-K213168TR-K213168TR-K213168TR-K213168 1/16" to 0.8 mm 0.53 mm id 10

VVVVVespelespelespelespelespelTMTMTMTMTM/Graphite Standard Fer/Graphite Standard Fer/Graphite Standard Fer/Graphite Standard Fer/Graphite Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213103TR-K213103TR-K213103TR-K213103TR-K213103 1/16" to 0.3 mm - 10TR-K213104TR-K213104TR-K213104TR-K213104TR-K213104 1/16" to 0.4 mm 0.25 mm id 10TR-K213105TR-K213105TR-K213105TR-K213105TR-K213105 1/16" to 0.5 mm 0.32 mm id 10TR-K213108TR-K213108TR-K213108TR-K213108TR-K213108 1/16" to 0.8 mm 0.53 mm id 10TR-K213110TR-K213110TR-K213110TR-K213110TR-K213110 1/16" to 1.0 mm 0.65 mm id 10

VVVVVespelespelespelespelespelTMTMTMTMTM/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213124TR-K213124TR-K213124TR-K213124TR-K213124 1/16" 2-hole 0.4mm/0.4mm 0.25 mm id 10TR-K213125TR-K213125TR-K213125TR-K213125TR-K213125 1/16" 2-hole 0.5mm/0.5mm 0.32 mm id 10

VVVVVespelespelespelespelespelTMTMTMTMTM/Graphite Straight Fer/Graphite Straight Fer/Graphite Straight Fer/Graphite Straight Fer/Graphite Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences pkpkpkpkpkTR-K213100TR-K213100TR-K213100TR-K213100TR-K213100 1/16" 10TR-K213200TR-K213200TR-K213200TR-K213200TR-K213200 1/8" 10TR-K213400TR-K213400TR-K213400TR-K213400TR-K213400 1/4" 10

Reducing VReducing VReducing VReducing VReducing VespelespelespelespelespelTMTMTMTMTM/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213204TR-K213204TR-K213204TR-K213204TR-K213204 1/8" to 0.4 mm 0.25 mm id 10TR-K213205TR-K213205TR-K213205TR-K213205TR-K213205 1/8" to 0.5 mm 0.32 mm id 10TR-K213208TR-K213208TR-K213208TR-K213208TR-K213208 1/8" to 0.8 mm 0.53 mm id 10TR-K213210TR-K213210TR-K213210TR-K213210TR-K213210 1/8" to 1/16" 1/16" od 10TR-K213405TR-K213405TR-K213405TR-K213405TR-K213405 1/4" to 0.5 mm 0.32 mm id 10TR-K213408TR-K213408TR-K213408TR-K213408TR-K213408 1/4" to 0.8 mm 0.53 mm id 10TR-K213420TR-K213420TR-K213420TR-K213420TR-K213420 1/4" to 1/8" 1/8" od 10

2-Hole Reducing V2-Hole Reducing V2-Hole Reducing V2-Hole Reducing V2-Hole Reducing VespelespelespelespelespelTMTMTMTMTM/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213222TR-K213222TR-K213222TR-K213222TR-K213222 1/8" 2-hole 0.5mm/0.5mm 0.32 mm id 10

GC Ferrules

Standard 1/8"- Graphite/VespelTM

Standard 1/4"- Graphite VespelTM

Agilent HP- Graphite/VespelTM

Carlo Erba - Graphite/VespelTM

Standard 1/16"- Graphite/VespelTM

6 8

VespelTM Ferrules

• Upper temperature limit 350ºC• 100% high-temperature DuPont polymide• Precission-drilled id. No imperfections from molding• One-piece design requires no back ferrule• Fairly hard; tends to seal permanently to the column

VVVVVespelespelespelespelespelTMTMTMTMTM Standard Fer Standard Fer Standard Fer Standard Fer Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212103TR-K212103TR-K212103TR-K212103TR-K212103 1/16" to 0.3 mm - 10TR-K212104TR-K212104TR-K212104TR-K212104TR-K212104 1/16" to 0.4 mm 0.25 mm id 10TR-K212105TR-K212105TR-K212105TR-K212105TR-K212105 1/16" to 0.5 mm 0.32 mm id 10TR-K212108TR-K212108TR-K212108TR-K212108TR-K212108 1/16" to 0.8 mm 0.53 mm id 10TR-K212110TR-K212110TR-K212110TR-K212110TR-K212110 1/16" to 1.0 mm 0.65 mm id 10

VVVVVespelespelespelespelespelTMTMTMTMTM 2-Hole Standard Fer 2-Hole Standard Fer 2-Hole Standard Fer 2-Hole Standard Fer 2-Hole Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212124TR-K212124TR-K212124TR-K212124TR-K212124 1/16" 2-hole 0.4 mm/0.4 mm 0.25 mm id 10TR-K212125TR-K212125TR-K212125TR-K212125TR-K212125 1/16" 2-hole 0.5 mm/0.4mm 0.32 mm id 10

Reducing VReducing VReducing VReducing VReducing VespelespelespelespelespelTMTMTMTMTM Fer Fer Fer Fer Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212204TR-K212204TR-K212204TR-K212204TR-K212204 1/8" to 0.4 mm 0.25 mm id 10TR-K212205TR-K212205TR-K212205TR-K212205TR-K212205 1/8" to 0.5 mm 0.32 mm id 10TR-K212208TR-K212208TR-K212208TR-K212208TR-K212208 1/8" to 0.8 mm 0.53 mm id 10TR-K212210TR-K212210TR-K212210TR-K212210TR-K212210 1/8" to 1/16" 1/16" od 10TR-K212410TR-K212410TR-K212410TR-K212410TR-K212410 1/4" to 1/16" 1/16" od 10TR-K212420TR-K212420TR-K212420TR-K212420TR-K212420 1/4" to 1/8" 1/8" od 10

VVVVVespelespelespelespelespelTMTMTMTMTM 2-Hole Reducing Fer 2-Hole Reducing Fer 2-Hole Reducing Fer 2-Hole Reducing Fer 2-Hole Reducing Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212222TR-K212222TR-K212222TR-K212222TR-K212222 1/8" 2-hole 0.5 mm ea 0.32 mm id 10

VVVVVespelespelespelespelespelTMTMTMTMTM Straight Fer Straight Fer Straight Fer Straight Fer Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences pkpkpkpkpkTR-K212100TR-K212100TR-K212100TR-K212100TR-K212100 1/16" 10TR-K212200TR-K212200TR-K212200TR-K212200TR-K212200 1/8" 10TR-K212400TR-K212400TR-K212400TR-K212400TR-K212400 1/4" 10

GC Ferrules

VespelTM Standard Ferrules

1/16" VespelTM Ferrules: 0.5 mm id,Straight


69

TeflonTM

• Upper temperature limit 250ºC• 100% Teflon, completely inert• One-piece design requires no back ferrule

TTTTTeflonefloneflonefloneflonTMTMTMTMTM Straight Fer Straight Fer Straight Fer Straight Fer Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences pkpkpkpkpkTR-K214100TR-K214100TR-K214100TR-K214100TR-K214100 1/16" 10TR-K214200TR-K214200TR-K214200TR-K214200TR-K214200 1/8" 10TR-K214400TR-K214400TR-K214400TR-K214400TR-K214400 1/4" 10

TTTTTeflonefloneflonefloneflonTMTMTMTMTM Standard Fer Standard Fer Standard Fer Standard Fer Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K214103TR-K214103TR-K214103TR-K214103TR-K214103 1/16" to 0.3 mm - 10TR-K214104TR-K214104TR-K214104TR-K214104TR-K214104 1/16" to 0.4 mm 0.25 mm id 10TR-K214105TR-K214105TR-K214105TR-K214105TR-K214105 1/16" to 0.5 mm 0.32 mm id 10TR-K214108TR-K214108TR-K214108TR-K214108TR-K214108 1/16" to 0.8 mm 0.53 mm id 10TR-K214110TR-K214110TR-K214110TR-K214110TR-K214110 1/16" to 1.0 mm 0.65 mm id 10

Reducing TReducing TReducing TReducing TReducing Tef lonefloneflonefloneflonTMTMTMTMTM Fer Fer Fer Fer Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K214204TR-K214204TR-K214204TR-K214204TR-K214204 1/8" to 0.4 mm 0.25 mm id 10TR-K214205TR-K214205TR-K214205TR-K214205TR-K214205 1/8" to 0.5 mm 0.32 mm id 10TR-K214208TR-K214208TR-K214208TR-K214208TR-K214208 1/8" to 0.8 mm 0.53 mm id 10TR-K214210TR-K214210TR-K214210TR-K214210TR-K214210 1/8" to 1/16" 1/16" od 10TR-K214410TR-K214410TR-K214410TR-K214410TR-K214410 1/4" to 1/16" 1/16" od 10TR-K214420TR-K214420TR-K214420TR-K214420TR-K214420 1/4" to 1/8" 1/8" od 10

2-Hole Reducing T2-Hole Reducing T2-Hole Reducing T2-Hole Reducing T2-Hole Reducing Tef lonefloneflonefloneflonTMTMTMTMTM Fer Fer Fer Fer Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K214222TR-K214222TR-K214222TR-K214222TR-K214222 1/8" 2-hole 0.5 mm ea 0.32 mm id 10

Ferrule Accesories and Tools

Dry Bit set

High speed steel drills let you drill ferrules to the size you need. The set includes 0.35 mm, 0.4 mm, 0.5 mm, 0.7 mm, 0.8mm, 1.0 mm and 1.2 mm drill bits and pin vise.

DrDrDrDrDry Bit Sety Bit Sety Bit Sety Bit Sety Bit SetReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K206250TR-K206250TR-K206250TR-K206250TR-K206250 Drill Bit Set

Septa Pick

This is useful for removing small pieces of graphite ferrule from the cap and fittings of the column connectors; also removespieces of septa found in threads of the injection port.

Septa PickSepta PickSepta PickSepta PickSepta PickReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205465TR-K205465TR-K205465TR-K205465TR-K205465 Septa Pick

GC Ferrules

Teflon

Septa Pick


7 0

Injection Port LinersInjection Port Liners for Capillary GCs

• Fits original equipment• Polysiloxane deactivated borosilicate glass (quartz where noted)• Guaranteed inert phenols, organic acids and bases• Other configurations available on demand

These capillary injection port liners (sleeves) provide a clean, non adsorptivesurface for your sample. Regular replacement of liners eliminates "disappearingpeaks". They also protect your capillary column from potentially harmful non-volatiles that might otherwise deposit on your column.

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208110TR-K208110TR-K208110TR-K208110TR-K208110 2 mm splitless 79 mm 18740-80220 1TR-K208110-10TR-K208110-10TR-K208110-10TR-K208110-10TR-K208110-10 5181-8818 10TR-K208111TR-K208111TR-K208111TR-K208111TR-K208111 2 mm splitless, Quartz 79 mm 5181-8818 1TR-K208111-10TR-K208111-10TR-K208111-10TR-K208111-10TR-K208111-10 18740-80220 10TR-K208112TR-K208112TR-K208112TR-K208112TR-K208112 4 mm split/splitless 79 mm 1TR-K208112-10TR-K208112-10TR-K208112-10TR-K208112-10TR-K208112-10 10TR-K208122TR-K208122TR-K208122TR-K208122TR-K208122 4 mm split/splitless, Quartz 79 mm 1TR-K208122-10TR-K208122-10TR-K208122-10TR-K208122-10TR-K208122-10 10TR-K208113TR-K208113TR-K208113TR-K208113TR-K208113 4 mm split/splitless, with Deactivated Glass Wool 79 mm 19251-60540 1TR-K208113-10TR-K208113-10TR-K208113-10TR-K208113-10TR-K208113-10 10TR-K208114TR-K208114TR-K208114TR-K208114TR-K208114 Split Liner, 4 mm id with Cup 79 mm 18740-80190 1TR-K208114-10TR-K208114-10TR-K208114-10TR-K208114-10TR-K208114-10 10TR-K208115TR-K208115TR-K208115TR-K208115TR-K208115 As above, with OV-1/Chromosorb W-HP 80/100 79 mm 18740-60840 1TR-K208115-10TR-K208115-10TR-K208115-10TR-K208115-10TR-K208115-10 10TR-K208118TR-K208118TR-K208118TR-K208118TR-K208118 Direct Liner, 1.5 mm id 79 mm 18740-80200 1TR-K208118-10TR-K208118-10TR-K208118-10TR-K208118-10TR-K208118-10 10TR-K208129TR-K208129TR-K208129TR-K208129TR-K208129 Single Taper Liner, 2 mm id 79 mm 1TR-K208129-10TR-K208129-10TR-K208129-10TR-K208129-10TR-K208129-10 10TR-K208119TR-K208119TR-K208119TR-K208119TR-K208119 Single Taper Liner, 4 mm id 79 mm 5181-3316 1TR-K208119-10TR-K208119-10TR-K208119-10TR-K208119-10TR-K208119-10 10TR-K208120TR-K208120TR-K208120TR-K208120TR-K208120 As above, with Deactivated Wool 79 mm 5062-3587 1TR-K208120-10TR-K208120-10TR-K208120-10TR-K208120-10TR-K208120-10 10TR-K208116TR-K208116TR-K208116TR-K208116TR-K208116 Double Taper Liner, 4 mm id 79 mm 5181-3315 1TR-K208116-10TR-K208116-10TR-K208116-10TR-K208116-10TR-K208116-10 10

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208130TR-K208130TR-K208130TR-K208130TR-K208130 Universal Packed Inj. Liner, Deactivated 93 mm 5181-3382 1TR-K208130-25TR-K208130-25TR-K208130-25TR-K208130-25TR-K208130-25 10TR-K208132TR-K208132TR-K208132TR-K208132TR-K208132 Universal Packed Inj. Liner, Not Deactivated 93 mm 5080-8732 1TR-K208132-25TR-K208132-25TR-K208132-25TR-K208132-25TR-K208132-25 10

Agilent (HP) Injection Port Liners

For Agilent (HP) Packed Column GCs

I n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o r t L i n e r st L i n e r st L i n e r st L i n e r st L i n e r s

71

Injection Port LinersNote the difference..

Between a properly deactivated liner and a non-deactivated liner. Both phenol runs were performedon the same column and GC under identical conditions except for the liners.

Column:Column:Column:Column:Column: Bonded Trifluoropropyl Polysiloxane0.25 mm I.D. x 30 m x 0.2 mm film

Temp: 50ºC(7min)-270ºCInjector: 225ºCDetector: MSD, Interface temp-290ºCCarrier gas: HE, 30cm/sec

Peaks

1. Phenol2. 2-chronophenol3. 2,4-Dimethylphenol4. 24,-Dichlorophenol5. 2-Nitrophenol6. 4-Chloro-3-methylphenol7. 2,4,6-Trichlorophenol8. 4-Nitrophenol9. Pentachlorophenol10. 2,4-Dinitrophenol11. 4,6-Dinitro-2-methyl phenol

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208330TR-K208330TR-K208330TR-K208330TR-K208330 Universal Flash Injector Liner 73 mm 37-000813-00 1TR-K208330-10TR-K208330-10TR-K208330-10TR-K208330-10TR-K208330-10 10

Varian Packed Injection Port Liners

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208310TR-K208310TR-K208310TR-K208310TR-K208310 Baffle Split Liner 72 mm 01-900109-04 1TR-K208310-10TR-K208310-10TR-K208310-10TR-K208310-10TR-K208310-10 16-000829-00 10TR-K208311TR-K208311TR-K208311TR-K208311TR-K208311 4 mm Open Split Liner 72 mm 16-0008300-00 1TR-K208311-10TR-K208311-10TR-K208311-10TR-K208311-10TR-K208311-10 10TR-K208313TR-K208313TR-K208313TR-K208313TR-K208313 4 mm Open Split Liner, with Deactivated Wool 72 mm 01-900109-01 1TR-K208313-10TR-K208313-10TR-K208313-10TR-K208313-10TR-K208313-10 10TR-K208312TR-K208312TR-K208312TR-K208312TR-K208312 Frit Split Liner 72 mm 01-900109-03 1TR-K208312-10TR-K208312-10TR-K208312-10TR-K208312-10TR-K208312-10 16-000830-01 10TR-K208314TR-K208314TR-K208314TR-K208314TR-K208314 Splitless, Borosilicate Glass 74 mm 01-900109-05 1TR-K208314-10TR-K208314-10TR-K208314-10TR-K208314-10TR-K208314-10 03-949437-90 & 00 10TR-K208315TR-K208315TR-K208315TR-K208315TR-K208315 Splitless, Quartz 74 mm 1TR-K208315-10TR-K208315-10TR-K208315-10TR-K208315-10TR-K208315-10 10TR-K208316TR-K208316TR-K208316TR-K208316TR-K208316 0.5 mm SPI 54 mm 01-900109-06 1TR-K208316-10TR-K208316-10TR-K208316-10TR-K208316-10TR-K208316-10 03-918332-01 10TR-K208318TR-K208318TR-K208318TR-K208318TR-K208318 0.8 mm SPI 54 mm 01-900109-07 1TR-K208318-10TR-K208318-10TR-K208318-10TR-K208318-10TR-K208318-10 03-918332-02 10TR-K208320TR-K208320TR-K208320TR-K208320TR-K208320 Cup Splitter 72 mm 01-900109-02 1TR-K208320-10TR-K208320-10TR-K208320-10TR-K208320-10TR-K208320-10 10TR-K208346TR-K208346TR-K208346TR-K208346TR-K208346 3.4 mm ID x 5 mm OD for 1079 54 mm 1TR-K208346-10TR-K208346-10TR-K208346-10TR-K208346-10TR-K208346-10 10

Varian Capillary Injection Port Liners

I n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o r t L i n e r st L i n e r st L i n e r st L i n e r st L i n e r s

7 2 I n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o r t L i n e r st L i n e r st L i n e r st L i n e r st L i n e r s

Injection Port Liners

Carlo Erba Capillary Injection Port Liner

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208610TR-K208610TR-K208610TR-K208610TR-K208610 Splitless, 2 mm id 79 mm 453 00300 1TR-K208610-10TR-K208610-10TR-K208610-10TR-K208610-10TR-K208610-10 10

Hitachi Capillary Injection Port LinerReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208716TR-K208716TR-K208716TR-K208716TR-K208716 Double Taper Liner 68 mm 1TR-K208716-10TR-K208716-10TR-K208716-10TR-K208716-10TR-K208716-10 10

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208414TR-K208414TR-K208414TR-K208414TR-K208414 Split Liner 14A 99 mm 221-32544 1TR-K208414-10TR-K208414-10TR-K208414-10TR-K208414-10TR-K208414-10 10TR-K208416TR-K208416TR-K208416TR-K208416TR-K208416 Splitless Liner 14A 99 mm 221-32544 1TR-K208416-10TR-K208416-10TR-K208416-10TR-K208416-10TR-K208416-10 10

Shimadzu Capillary Injection Port Liners

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208240TR-K208240TR-K208240TR-K208240TR-K208240 Glass Liner for AutoSystem 112 mm N-610-1048 1TR-K208240-10TR-K208240-10TR-K208240-10TR-K208240-10TR-K208240-10 10TR-K208242TR-K208242TR-K208242TR-K208242TR-K208242 Glass Liner for 8000 Series, Sigma 2000 101 mm 0330-2221 1TR-K208242-10TR-K208242-10TR-K208242-10TR-K208242-10TR-K208242-10 10

Perkin Elmer Packed Injection Port Liners

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208232TR-K208232TR-K208232TR-K208232TR-K208232 Split Liner for Autosystem, 4mm id 92 mm N-610-1052 1TR-K208232-10TR-K208232-10TR-K208232-10TR-K208232-10TR-K208232-10 10TR-K208234TR-K208234TR-K208234TR-K208234TR-K208234 Split Liner for Autosystem, 2 mm id 92 mm N-610-1048 1TR-K208234-10TR-K208234-10TR-K208234-10TR-K208234-10TR-K208234-10 10TR-K208210TR-K208210TR-K208210TR-K208210TR-K208210 PTV Injector 88 mm N-600-2017 1TR-K208210-10TR-K208210-10TR-K208210-10TR-K208210-10TR-K208210-10 10TR-K208212TR-K208212TR-K208212TR-K208212TR-K208212 Dimple Splitter 100 mm 0330-5181 1TR-K208212-10TR-K208212-10TR-K208212-10TR-K208212-10TR-K208212-10 10TR-K208214TR-K208214TR-K208214TR-K208214TR-K208214 Splitless 100 mm 0330-5180 1TR-K208214-10TR-K208214-10TR-K208214-10TR-K208214-10TR-K208214-10 10

Perkin Elmer Capillary Injection Port Liners

Injection Liner Cleaning KitProlong the life of injection port liners and help maintain column efficiency. This kit includes four sizes of nylon brush to cleanmost of liners, and one foot of pipe cleaner for light-duty jobs. The 4 mm and 2 mm diameter brushes clean standard liners.The 1 mm and 0.5 mm diameter brushes can reach inside reversible tapered liners.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205215TR-K205215TR-K205215TR-K205215TR-K205215 Injection Sleeve Cleaning Kit

Fisons Capillary Injection Port LinerReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208612TR-K208612TR-K208612TR-K208612TR-K208612 Split, 5 mm id 105 mm 453 20030 1TR-K208612-10TR-K208612-10TR-K208612-10TR-K208612-10TR-K208612-10 10

73

Maintenance - Kits and Tools

Capillary Survival KitTM

Save 35% over items bought individuallySave 35% over items bought individuallySave 35% over items bought individuallySave 35% over items bought individuallySave 35% over items bought individually.....

Each kit includes:• Magnifier with built-in light• Slide-Lok tweezers for holding small items; "spacing" the column proper

distances into the injection port, etc.• 15 cm steel ruler• 3 column scribes, for cleanly-cut columns• 2 Universal Unions for joining broken capillary columns• Single-ended pinvise holds drill bits• 3 Drill Bits 0.4 mm, 0.5 mm and 0.8 mm• Multipurpose Septum Pick• Nylon Brushes 1/8", 3/16" and 1/4" od• Open-end wrench, 1/4" + 5/16"• High-temperature string (>400ºC) 25 ft.• Ferrule Remover• Pipecleaners 5 each 1/8" od and 1/4" od

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K-205625TR-K-205625TR-K-205625TR-K-205625TR-K-205625 Capillary Survival Kit

Packed Column Change KitThis has everything you need forhooking up columns in the GC lab. TheColumn Change Kit includes threeratchet wrenches, 7/16", 1/2" and9/16"; one ImpTM Tubing cutter, andone roll of TeflonTM tape, 1/2" x520". The ratchet wrenches are idealfor tight spaces; the ratchet tips can beopened, then snapped closed aroundfittings.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205250TR-K205250TR-K205250TR-K205250TR-K205250 Column Change Kit

Fine Wire KitThe Fine Wire Kit lets you clean manysmall items around the lab; also usefulfor bending into microhooks, other uses.The Kit contains a pin vise, and 30stainless steel wires, 10 each of thefollowing sizes: 0.006", 0.010" and0.020".

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205230TR-K205230TR-K205230TR-K205230TR-K205230 Fine Wire Kit

Needle Cleaning KitThis Kit is specifically designed forcleaning syringes and needles. Itincludes one bottle of organic,biodegradable cleaning solution, and10 each of five different diametertungsten wires, ranging in diameterfrom 0.0035" to 0.0121". Suggestedcleaning procedures are included. Thiskit is especially recommended forcleaning Hamilton Syringes.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K76620TR-K76620TR-K76620TR-K76620TR-K76620 Needle Cleaning Kit

FID Cleaning KitThe Flame Detector Cleaning Kitimproves sensibility while reducingnoise and spikes. Use it to clean boththe jet tip and collector. The FIDCleaning Kit includes everything you´llneed: three jet reamers (0.16", 0.19"and 0.024") with a unique spiraldesign that can clean without

scratching; a mini drill bit (0.0102"), two wire minibrushes, one brass and onestainless steel; and a dua-ended handle for the rearmers and brushes.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205220TR-K205220TR-K205220TR-K205220TR-K205220 FID Cleaning Kit

Injection Port Cleaning KitThis is designed for cleaning all GCInjection ports, including those inShimadzu instruments. Included are threestainless steel brushes, 5mm (forShimadzu), 1/4" and 3/8", and onescraper for removing septum residue.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K206211TR-K206211TR-K206211TR-K206211TR-K206211 Inj. Port Cleaning Kit

Utility Ring StandThis nickel-plated ring stand is usefulfor holding bubble flowmeters, as wellas wide variety of standard labequipment. The support rod is 5/16"od x 20".

Clamps are available separately. Theplastic-coated jaws hold aroundglassware from, 3/8" to 13/8" in

diameter. The small clamp is useful for securing items 3/8" in diameter and less(10 ml and less bubble flowmeters; thermometers). Rotates 360ºC. The RingStand Clamps are made from zinc-platted steel.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205570TR-K205570TR-K205570TR-K205570TR-K205570 Utility Ring StandTR-K205571TR-K205571TR-K205571TR-K205571TR-K205571 Large Ring Stand ClampTR-K205572TR-K205572TR-K205572TR-K205572TR-K205572 Small Ring Stand Clamp

M a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d T o o l so o l so o l so o l so o l s

7 4

Maintenance - Kits and ToolsGlass Tubing Cutter

For shortering glass columns or inserts;other applications involving glasstubing. The hardended steel cutingwheel scores tubing as it is turned;cuts tubing up to 1.5".

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205595TR-K205595TR-K205595TR-K205595TR-K205595 Glass Tubing CutterTR-K2055969TR-K2055969TR-K2055969TR-K2055969TR-K2055969 Spare Cutting Wheels, 5/pk

StopwatchThis 1/00th second Stopwatch hassplit/lap and normal time. It displayshours, minutes, seconds, day, date andmonth. Quartz accuracy. Useful formeasuring gas glow with bubbleflowmeters. Has alarm feauture.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205200TR-K205200TR-K205200TR-K205200TR-K205200 Stopwatch

Adjustable Wrench6 inch or 10 inch. The 6" wrench opensto 15/16" for all common Swage-lokconnectors. The 10" wrench opens to15/16" for standard CGA fittings.Chronomeplated, drop-forged steel.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205586TR-K205586TR-K205586TR-K205586TR-K205586 Adjustable Wrench 6 inchTR-K205588TR-K205588TR-K205588TR-K205588TR-K205588 Adjustable Wrench 10 inch

Ratchet WrenchThe jaws of the Ratchet Whrench open,to slip over fittings already in place.Makes tightering or loosening incramped areas easy. Three sizesavailable: 7/16", 1/2" or 9/16"

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205593TR-K205593TR-K205593TR-K205593TR-K205593 Ratchet Wrench 7/16"TR-K205592TR-K205592TR-K205592TR-K205592TR-K205592 Ratchet Wrench 1/2"TR-K205591TR-K205591TR-K205591TR-K205591TR-K205591 Ratchet Wrench 9/16"

Goose-neck FlashlightIluminates hard-to-reach areas. TheGoose-neck flashlight has a flexible neckwhich can be bent as desired. Includesbatteries.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205628TR-K205628TR-K205628TR-K205628TR-K205628 Goose-neck Flashlight

Jeweler´s ScrewDriversSix flaat-head screwdrivers whithconvenient swivel-top handles. Baldesare from 0.025" to 0.100" in width.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205676TR-K205676TR-K205676TR-K205676TR-K205676 Jeweler´s ScrewDrivers

Allen Wrench SetStandard or Metric. The standard(USA) Allen wrenches come in a set of9, from 0.050" to 3/16". The metricAllen wrenches come in a set of 7,from 1.5mm to 6mm.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205670TR-K205670TR-K205670TR-K205670TR-K205670 Allen Wrench Set StandardTR-K205671TR-K205671TR-K205671TR-K205671TR-K205671 Allen Wrench Set Metric

Micro HookThis is a multi-purpose hook used forpulling O-rings, springs, or septumfragments.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205678TR-K205678TR-K205678TR-K205678TR-K205678 Micro Hook

Magnet on a StickThis is used to pick up small objectssuch as screws and nuts frominstrumet cabinets and circuit boards.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205630TR-K205630TR-K205630TR-K205630TR-K205630 Magnet on a Stick

Threadulator Thread CutterCleans up cross-threated fittings oncolumns, etc.; use with weldedinstrumet fittings to avoide expensivereplacement. Knurled otuter handle forsecure gripping; hardless steel cutter.Available in three sizes.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205638TR-K205638TR-K205638TR-K205638TR-K205638 Threeadulator, 1/16"TR-K205640TR-K205640TR-K205640TR-K205640TR-K205640 Threeadulator, 1/8"TR-K205642TR-K205642TR-K205642TR-K205642TR-K205642 Threeadulator, 1/4"

TeflonTM TapeThis is great for leak-proofing fittings;dry-lubricating joints. Do not use overferrules. Teflon tape comes in rolls of520 inces, 1/2" wide.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205117TR-K205117TR-K205117TR-K205117TR-K205117 Teflon Tape


75

Maintenance - Kits and ToolsCapillary/HPLC Wrench Set

This set includes 4 wrenches for useon 1/32", 1/16", or 1/8" nuts. Thewrench ends are 3/16", 1/4", 5/16", 3/8" and 7/16".

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205320TR-K205320TR-K205320TR-K205320TR-K205320 Capillary/HPLC Wrench Set

Mirror on a StickThe Mirror on a Stick lets you peeraround corners or tight spaces; alsoused at the outlet of flame detectors;condensation on the mirror indicatesthe flame is lit.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205632TR-K205632TR-K205632TR-K205632TR-K205632 Mirror on a Stick

Open End WrenchesThis set fits most types of fittings.Sizes range from 5/16" to 9/16" in1/16" increments. Made fromchromeplated steel. 5 wrenches.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205622TR-K205622TR-K205622TR-K205622TR-K205622 Open End Wrenches

Lighted MagnifierThis is perfect for inspecting capillaryend cuts and syringe tips. The 11/4"x 11/4 lens magnifiers 4x; smallbifocal insert lens measures 8x. Keepone in your desk. Batteries included.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205648TR-K205648TR-K205648TR-K205648TR-K205648 Lighted Magnifier

Needle-Nose PliersThese are useful for picking up orclamping small parts. Comes with vinylgrips for sure grip.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205626TR-K205626TR-K205626TR-K205626TR-K205626 Needle-Nose Pliers

4-in-1 ScrewdriverComes with two double-ended heads,each with a flat and phillips head. Justflip the end to change the tip.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205624TR-K205624TR-K205624TR-K205624TR-K205624 4-in-1 Screwdriver

Wire Stripper/CrimperUseful for cutting or stripping wire, andcrimping on connectors. For repairs,maintenance, prototyping.

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205574TR-K205574TR-K205574TR-K205574TR-K205574 Wire Stripper/Crimper


7 6

Chart Paper

C h a rC h a rC h a rC h a rC h a r t P a p e rt P a p e rt P a p e rt P a p e rt P a p e r

Chart Paper

• High Quality Chart Papers• Available for many popular Integrators and recorders• Buy the Case for Bigger Savings

Papers for Hewlett PackardPapers for Hewlett PackardPapers for Hewlett PackardPapers for Hewlett PackardPapers for Hewlett Packard

ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....

TR-K443181TR-K443181TR-K443181TR-K443181TR-K443181 5880A, 3888A 8.5" x 184´, Z-fold blue 5/cs 5080-8778TR-K443182TR-K443182TR-K443182TR-K443182TR-K443182 8.5" x 184´, Z-fold black 5/cs 9270-0658

TR-K443192TR-K443192TR-K443192TR-K443192TR-K443192 5840A, 5880 GC, 8.5" x 184´, Z-fold blue 5/cs 5080-87353380A, 3385A Int.

TR-K443193TR-K443193TR-K443193TR-K443193TR-K443193 1082, 1084 LC 8.5" x 184´, Z-fold black 5/cs

TR-K443194TR-K443194TR-K443194TR-K443194TR-K443194 3392, 3393A Int. 4.2" x 400´, roll blue 2/cs 5080-8800TR-K443195TR-K443195TR-K443195TR-K443195TR-K443195 4.2" x 400´, roll black 2/cs

TR-K443191TR-K443191TR-K443191TR-K443191TR-K443191 3396A 9.5" x 272´, roll, ink jet 4/cs 5181-1219TR-K443179TR-K443179TR-K443179TR-K443179TR-K443179 3396A 8.5" x 230,´ Z-fold ink jet 5/cs 5062-3561

Papers for ShimadzuPapers for ShimadzuPapers for ShimadzuPapers for ShimadzuPapers for Shimadzu


TR-K441610TR-K441610TR-K441610TR-K441610TR-K441610 CR1A, CR1B 8 3/16" x 170´, roll black 1 roll 221-13391-01TR-K443612TR-K443612TR-K443612TR-K443612TR-K443612 CR3A 8 3/16" x 167´, roll black 10/cs 221-25412-00TR-K441613TR-K441613TR-K441613TR-K441613TR-K441613 CR4A 255 mm x 148", black 1 roll 223-02000-12TR-K443615TR-K443615TR-K443615TR-K443615TR-K443615 CR5A 208 mm x 148", black 10/cs 223-02037-81TR-K441617TR-K441617TR-K441617TR-K441617TR-K441617 CR7A 10 1/6" x 148´ 1 roll 200-91527

Papers for VPapers for VPapers for VPapers for VPapers for Var ianar ianar ianar ianar ian


TR-K443620TR-K443620TR-K443620TR-K443620TR-K443620 3400/3500/3600 4.3" x 150´, black 2/cs 03-917650TR-K443604TR-K443604TR-K443604TR-K443604TR-K443604 Vista 401/402 8.5" x 184´, Z-fold, black 5/cs 03-906362-0TR-K441599TR-K441599TR-K441599TR-K441599TR-K441599 4270/4290 9.4" x 183´, roll, black 1 roll 00-997096-01

Papers for WPapers for WPapers for WPapers for WPapers for Watersatersatersatersaters


TR-K441608TR-K441608TR-K441608TR-K441608TR-K441608 730 8.5" x 184´, Z-fold, blue 1 pack 74703

Thermal Paper

77C h a rC h a rC h a rC h a rC h a r t P a p e rt P a p e rt P a p e rt P a p e rt P a p e r

Papers for HitachiPapers for HitachiPapers for HitachiPapers for HitachiPapers for Hitachi


TR-K443170TR-K443170TR-K443170TR-K443170TR-K443170 234 mm x 160´, black 9/cs 661-7501

Papers for Perkin ElmerPapers for Perkin ElmerPapers for Perkin ElmerPapers for Perkin ElmerPapers for Perkin Elmer


TR-K441189TR-K441189TR-K441189TR-K441189TR-K441189 LC1-100 283 mm x 100´, Roll, black 1 roll N-625-1026

Papers for Spectra PhysicsPapers for Spectra PhysicsPapers for Spectra PhysicsPapers for Spectra PhysicsPapers for Spectra Physics


TR-K443596TR-K443596TR-K443596TR-K443596TR-K443596 SP-4000 Series 9.4" x 184´, Z-fold, black 5/cs A0022-020TR-K443598TR-K443598TR-K443598TR-K443598TR-K443598 SP-4270, SP-4290 9.4" x 167´, roll, black 10/cs A2157-020

Chromojet, CH1, CH2

Chart Paper

Recorder PaperManufacturerManufacturerManufacturerManufacturerManufacturer ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....

HoustonHoustonHoustonHoustonHouston TR-K443198TR-K443198TR-K443198TR-K443198TR-K443198 D-5000, B-5000 11" X 100´roll, 0-10 English 4/cs EC-103Kipp & ZonenKipp & ZonenKipp & ZonenKipp & ZonenKipp & Zonen TR-K441199TR-K441199TR-K441199TR-K441199TR-K441199 BD111/12, BD40/41 230 mm x 66´, 0-100 1 roll XR-9LinearLinearLinearLinearLinear TR-K441184TR-K441184TR-K441184TR-K441184TR-K441184 1201/1202/1210 230 mm x 83´, roll 1 roll 0100-0026LinearLinearLinearLinearLinear TR-K441186TR-K441186TR-K441186TR-K441186TR-K441186 142/143 120 mm x 100´, roll 1 roll 0100-0011Perkin ElmerPerkin ElmerPerkin ElmerPerkin ElmerPerkin Elmer TR-K441395TR-K441395TR-K441395TR-K441395TR-K441395 56/200/561 276 mm x 100´, roll 1 roll 056-7300

7 8

Gas & Handling Purification

Indicating Oxygen Trap

• High efficiency. Reduces O2 to less than 0,1 ppm• Changes color from bright green to brown when adsorption capacity is depleted• Non-contaminating glass tube

This safe, compact unit has a capacity of 40 cc of pure oxygen; it will removeoxygen from a full 200 ft3 cylinder of helium with purity specification of 99,995 %(assuming 20 % impurity is oxygen; or several cylinders of higher purity helium).The non contaminating, heavy-walled inner glass tube of catalyst is protected fromaccidental breakage by the outer plastic tube.

Maximum pressure is 100 psig. The indicating oxygen trap is delivered in theactive state, filled with high purity helium. It is recommended that the trap bepurged with the gas you will be using. Approximate dimensions: 1 3/8” x 10 1/4”

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202220TR-K202220TR-K202220TR-K202220TR-K202220 Indicating Oxygen Trap 1/8” fittingsTR-K202223TR-K202223TR-K202223TR-K202223TR-K202223 Indicating Oxygen Trap 1/4” fittings

Model 1000 Oxygen Trap

• High capacity, can remove 2.5 liters of O2

• Exceptional efficiency, less than 70 ppb oxygen concentration at the outlet

This is highest capacity oxygen trap, for long term protection of capillary columnstationary phases against oxidation at GC operating temperatures. It is alsorecommended for packed column carrier gases. The Model 1000 has a capacity of2,5 liters of oxygen at room temperature; its capacity is even higher at 100 ºC . Itis also effective for removing sulfur compounds, such as hydrogen sulfide andmercaptans. The Model 1000 is intended for use with non oxidizing gases such asHe, Ar, N2, H2, or CH4, containing less than 1 % oxygen. It will remove oxygen tobelow 70 ppb from these gases at flow rates normally encountered in GC .

The Model 1000 oxygen trap is a high pressure metal cylinder filled with 500 ccof active oxygen adsorbent. The adsorbent binds covalently with oxygen; no gas isgenerated from this reaction. It is delivered in the active state, filled with highpurity helium. It is ready for use, but we recommended that the trap be purgedwith the gas you will be using. Maximum flow rate for nominal pressure drop is 1liter/min; maximum pressure 1000 psig. Approximate dimensions 2” x ¼”including fitting. Weight 3 pounds.

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202200TR-K202200TR-K202200TR-K202200TR-K202200 Model 1000 Oxygen Trap 1/8” fittingsTR-K202202TR-K202202TR-K202202TR-K202202TR-K202202 Model 1000 Oxygen Trap 1/4” fittings

Moisture /Oil / Dust traps

• Recommended for FID supply gases; cleaner gas improves baseline stabilityfor more accurate analysis

• Molecular sieve 5A provide high efficiency drying• Indicating DrieriteTM warns of leaks in the gas stream• Acrylic or glass construction for low permeability; inertness

Big Trap

This removes moisture, oil and dust from wet supply gas before it flow into yourFID detector. It can also be used to purity hydrogen in flame ionization detectors.Maximum pressure is 100 psig . The Big Trap has a 400 cc total volume ofindicating DrieriteTM and molecular sieve 5 A in a clear acrylic tube. The DrieriteTM

changes from blue to pink at 5 % relative humidity to warn of leaks in the gasstream. Our unique O-ring design allows hand removal of the cartridge withoutdisconnecting the fittings from the line, while a plastic insert at each end keeps thepacking from spilling. Available with 1/8” or 1/4” fittings. Dimensions 2 1/4" x17" including fittings.

Oxygen Traps Oxygen Traps

• Recommended for all GC and GC/MS carrier gas• Reduce capillary column phase degradation

Moisture traps, Moisture/ Oil / Dust Traps

• Recommended for detector suply gases• Improves baseline stability

Hydrocarbons Traps

• Recommended for H2 and air detector supply gases• Activated charcoal adsorbent for highly efficient contaminant removal• Can also be used for purge and trap; organic analysis applications.

G a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o n

79

Gas & Handling Purification

Safe Glass Moisture Trap

This filter is designed for use with GC detectors needing very high purity gases,such as electron capture or Hall electrolytic conductivity. Gas contacts only glass,metal and the adsorbents for purity, and the trap may be used in any orientation.An internal screen at each end prevents particulate contamination. The Safe GlassTrap is enclosed in a plastic outer sheath. The outer sheath can be removed toreactivate the inner glass tube by baking under inert gas flow; instructionsincluded. It contains 55 cc total absorbents . Maximum pressure is 100 psig.Dimentions 1 3/8” x 10 1/4”.

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202260TR-K202260TR-K202260TR-K202260TR-K202260 Big Trap 1/8” fittingsTR-K202262TR-K202262TR-K202262TR-K202262TR-K202262 Big Trap 1/4” fittingsTR-K202266TR-K202266TR-K202266TR-K202266TR-K202266 Safe Glass Moisture Trap for ECD 1/8” fittingsTR-K202268TR-K202268TR-K202268TR-K202268TR-K202268 Safe Glass Moisture Trap for ECD 1/4” fittings

Hydrocarbon Trap / CO2 Trap

Model 300 High Pressure Hydrocarbon Trap

This high pressure metal cylinder filled with 500 cc of activated charcoal, one ofthe most effective adsorbents for organics and hydrocarbons. It will remove allhydrocarbons at room temperature except methane, from your FID air and H2 lines,to minimize noise and extraneous peaks in the signal. It is also recommended foruse with purge and trap apparatuses, and with GC carrier gases for trace analyses.Highest efficiency is obtained using flow rates bellow 500cc/min. Frits in each endprevent fines from entering the gas stream. The Model 300 is delivered filled withhigh purity helium; It should be purged before use with the gas you will be using.Maximum pressure is 1000 psig. The Model 300 comes with 1/8" or 1/4" fittings.Approximate dimensions 2" x 14".

Model 100 Safe Glass Hydrocarbon Trap

The Model 100 is designed to provide organics free gas, with an indicator formoisture contamination. The gas contacts only metal or glass for high purity. Itcontains indicating DrieriteTM and activated charcoal; the inner glass tube isprotected by an outer tube of clear plastic. Internal stainless steel screens at end ofthe trap protect against fines entering the gas stream. It can be used in anyorientation without gas channeling. The Trap can be regenerated by heating underinert gas flow after removing the outer plastic guard; instructions included. TheTrap should be purged before use with the gas you will be using . Maximumpressure is 100 psig. The Model 100 is supplied with 1/8" or 1/ 4" fittings.Approximate dimensions 1 3/8" x 10 1/4".

Carbon Dioxide Trap

Remove carbon dioxide from your gas stream with our carbon dioxide Trap. Highcapacity, it will irreversibly bind 100 g of carbon dioxide. Its unique design usesNaOH blended with molecular sieve to scrub out CO2. The reaction produce waterwhich is adsorbed by the molecular sieve. Not recommended for GC use. Whendrown stream water is a concern we recommended using a second moisture trap inline as a safety measure. Maximum pressure for the Carbon Dioxide, trap is 1000psig; approximate dimension 2” x 14”

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202330TR-K202330TR-K202330TR-K202330TR-K202330 Model 300 Hydrocarbon Trap 1/8" fittingsTR-K202332TR-K202332TR-K202332TR-K202332TR-K202332 Model 300 Hydrocarbon Trap 1/4" fittingsTR-K202340TR-K202340TR-K202340TR-K202340TR-K202340 Model 100 Safe Glass Hydrocarbon Trap 1/8" fittingsTR-K202342TR-K202342TR-K202342TR-K202342TR-K202342 Model 100 Safe Glass Hydrocarbon Trap 1/4" fittingsTR-K202350TR-K202350TR-K202350TR-K202350TR-K202350 Carbon Dioxide Trap 1/8" fittingsTR-K202352TR-K202352TR-K202352TR-K202352TR-K202352 Carbon Dioxide Trap 1/4" fittings

G a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o n

8 0

Super-Clean Gas Filters

A revolution in gas purifying of GC and GC/MS gases

Unique «POINT-OF-USE» and «SEMI IN-LINE» glass/metal, diffusionproof Super-Clean Gas Filters, purify the delicate carrier and burner gases for your GC and GC/MS system for Hydrocarbons, Oxygen (colour indicated) and Moisture (colourindicated) to better-as 6.0 gas (99,9999%) quality, independent of the originalgas quality.

Analytical advantages of SGT Super-Clean Gas Filters

• Longer lifetime of analytical columns, avoids bleeding, espec. important forMS and ECD.

• Better sensitivity, decreases baseline noise, eliminates spikes.

• Filter-change during analysis within seconds, system stays online.

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S u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r s

81

Spec’s on SGT Super-Clean Gas Filters

• The specified lifetimes are strongly depending of the quality of the incominggas.

• Effectivity: <0.1 ppm at a flowrate of 2 liters/minute

Benefits of the “quick-fit” system:

• Filter replacement within seconds.- El iminates GC downtime.- El iminates GC downtime.- El iminates GC downtime.- El iminates GC downtime.- El iminates GC downtime.

• Tool-less filter replacement.- Easy handling- Easy handling- Easy handling- Easy handling- Easy handling

• Diffusion-proof Baseplate (also during filter replacement).- El iminates analytical disturbance.- El iminates analytical disturbance.- El iminates analytical disturbance.- El iminates analytical disturbance.- El iminates analytical disturbance.

• Baseplates can be wall-mounted.- Convenient posit ioning- Convenient posit ioning- Convenient posit ioning- Convenient posit ioning- Convenient posit ioning

Standard Configurations

P U R I F I C A T I O N O F C A R R I E R G A S

• Removal of Oxygen, moisture and hydrocarbons for longer column lifetime andcleaner baseline.

• Use a Triple filter on 1-position baseplate.

• Excelent for Carrier gas and ECD, MS applications

SG-F0301SG-F0301SG-F0301SG-F0301SG-F0301 Filter,Triple (O2/Moisture/Hydrocarbons)SG-B0010SG-B0010SG-B0010SG-B0010SG-B0010 Baseplate for 1 Super Clean Gasfilter

Super-Clean Gas FiltersP U R I F I C A T I O N O F G A S E S F O R F I D

• Removal of moisture and hydrocarbons in the gases of the FID for a betterbaseline.

• 2 Combi filter (Hydrocarbons/moisture) (One for Air & one for Hydrogen)

2u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F0201 Filter,Combi, high capacity, (Hydrocarbons/moisture).

2u. of SG-B00102u. of SG-B00102u. of SG-B00102u. of SG-B00102u. of SG-B0010 Baseplate for 1 Super Clean Gasfilter

P U R I F I C A T I O N F O R C A R R I E R A N D F I D G A S E S

• The full solution for your GC/FID system

• Use a Triple + 2 Combi filter (One for Air & one for Hydrogen)

1u. of SG-F03011u. of SG-F03011u. of SG-F03011u. of SG-F03011u. of SG-F0301 Filter,Triple (O2/Moisture/Hydrocarbons)

2u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F0201 Filter,Combi, high capacity, (Hydrocarbons/moisture).


H I G H C A P A C I T Y P U R I F I E R S F O R C A R R I E R A N D F I D G A S E S

• Recomended for low quality gases

• Use Ultra Capacity Moisture and Oxygen filters for carrier + 2 Ultra CapacityHydroCarbon filter (One for Air & one for Hydrogen)

1u. of SG-F01011u. of SG-F01011u. of SG-F01011u. of SG-F01011u. of SG-F0101 Moisture filter, standard, ultra capacity

1u. of SG-F01021u. of SG-F01021u. of SG-F01021u. of SG-F01021u. of SG-F0102 Oxygen filter,standard, ultra capacity

2u. of SG-F01032u. of SG-F01032u. of SG-F01032u. of SG-F01032u. of SG-F0103 Hydrocarbons filter,standard, ultra capacity


ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionSG-B0010SG-B0010SG-B0010SG-B0010SG-B0010 Baseplate for 1 Super Clean GasfilterSG-B0020SG-B0020SG-B0020SG-B0020SG-B0020 Baseplate for 2 filtersSG-B0030SG-B0030SG-B0030SG-B0030SG-B0030 Baseplate for 3 filtersSG-F0101SG-F0101SG-F0101SG-F0101SG-F0101 Moisture filter, standard, ultra capacitySG-F0102SG-F0102SG-F0102SG-F0102SG-F0102 Oxygen filter,standard, ultra capacitySG-F0103SG-F0103SG-F0103SG-F0103SG-F0103 Hydrocarbons filter,standard, ultra capacitySG-F0301SG-F0301SG-F0301SG-F0301SG-F0301 Filter,Triple (O2/Moisture/Hydrocarbons)SG-F0201SG-F0201SG-F0201SG-F0201SG-F0201 Filter,Combi, high capacity, (Hydrocarbons/moisture)SG-F0730SG-F0730SG-F0730SG-F0730SG-F0730 Filter bundle of 3 (Triple + 2x Hydrocarbons/ moisture

Combi)SG-F0740SG-F0740SG-F0740SG-F0740SG-F0740 Filter bundle of 4 (standard : oxygen, moisture +

2x Hydrocarbons)

One position platform

Quick-Fit System

S u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r s

8 2

Helium Gas Leak Check

H e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c k

Helium Gas Leak Check

• Pipe fittings• Welding parts• Pressure regulators

Specifications

Detection Method: Thermal Conductivity DetectorTarget gas: HeliumRange: High/LowSensibility: Minimum Detection Limit 0.01 mL/minDisplay: LCDPower Supply: Rechargeable BatteryOperation Temp: 10-35ºCDimensions: 65 (W) x 37 (D) x 143 (H) mmWeight: 330g approx.Accesories: Recharger AC 100 - 220v

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionGL-2702-1941GL-2702-1941GL-2702-1941GL-2702-1941GL-2702-1941 Helium Gas Leak Detector LD 229GL-XXXXXGL-XXXXXGL-XXXXXGL-XXXXXGL-XXXXX Recharger AC 100 - 220v

83

Teknokroma 2t Head Space Sampler

The Teknokroma 2t Head Space Sampler for Head Space techniquewithin your reach with a low cost and high precision level

The 2t sampler is the first manual system for Static Head Space which allows theapplication of this technique in a quantitative, economical and precise manner.

Now it is possible to use the Static Head Space technique with a manualequipment. the Teknokroma 2t sampler is a low cost, high versatility and easyoperations system. For this reason the Static Head Space technique is beingsuccesfully introduced to laboratories.

The new 2t sampler makes the Head Space technique available to all GasChromatography users.

It complies with all the European CE requirements.

Applications

• Volatiles in pharmaceuticals

• Flavours analysis in food and cosmetic products

• Alcohol and other toxic compounds in blood

• Screening of volatiles in all type of environmental samples (soils, waters,plastics, polymers, etc.)

It is according the Pharmacopeia test:

European Pharmacopeia 4th. (2002). "Gas Chromatography will static head-spaceinjection 2.2.28". "It is possible to use airtight syringes and a conventionalchromatograph".

USP 26(2003 <467> Organic Volatile Impurities: "Proceed as direct underMethod V, except to inject, using a heated gas-tight syringe, 1 ml. of theheadspace".

Technical specifications

Heating temperature Range: up to 120ºC.Variable injection: up to 2,5 ml.Temperature accuracy: +/- 0,5ºCHolds up to 6 vials of: 2, 4, 6, 9, 10, 12, 20, 22 and 27 ml.Sampling time control with accoustic alarm: 1 to 99 secondsEquilibrium time control with accoustic alarm: 1 to 99 minutesStabilization time from 25ºC to 70ºC with1 ml syringe and 6 empty 20 ml vials: 8 minutesSafety temperature: 150ºCPower: 220 +/- 10% VAC.

The F irst Manual SystemFor Stat ic Head Space

TTTTT e k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e r

8 4 TTTTT e k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e r


a. Insert the syringe holder into the heating block.b. Set the temperature and the equilibrium time with the keyboard.c. Press the start.

3

Insert the closed vials with the sample into the heating block.

2

Inject the sample into the GC.Repeat this sequence for the additional samples.

5

Put the syringe into the black holder.

1

After the equilibrium time is achieved, move the syringe holder intovial number 1, and aspirate the sample by moving the plunger upuntil the prefixed volume is reached.

4

85


Retention time (min.)Benzene 1.45Toulene 2.85

Chromatographic parametersChromatographic parametersChromatographic parametersChromatographic parametersChromatographic parametersColumn: TRB-1TRB-1TRB-1TRB-1TRB-1, P/N TR-113015Dimensions: 15m x 0,53mm x 3µmInjection: 0,7 ml, head space, (split 1:2), 150ºCCarrier gas: He, 4psi (27.6 kPa)Oven temperature: 60ºC (10 min.)Detector: FID, 250ºCSample: 5ml in 10ml vials (25ppm benzene/toulene in water)

Headspace condit ionsHeadspace condit ionsHeadspace condit ionsHeadspace condit ionsHeadspace condit ions10ml vials, P/N CC-10-CVCap with blue silicone/PTFE seal P/N CC-20-ST3Healting block temperature: 75ºCEquilibrium time: 30 minutesSampling time: 30 secondsSyringe used: 1ml (1001 LTN, pst 5, P/N HA-81343)Sampled volume: 0,7ml

Performance qualification

To check the Head Space sampler, proper performance, the followingreproductibility test is recommended. In this test, we check not only the equipmentperformance but we also evaluate:

• The vials are correctly sealed.• The sampling procedure followed by the analyst is correct• The Gas Chromatograph works properly• The data-aquisition system works properly

Sample preparation

Add 2.5 µl of benzene and 2.5 µl mof toulene to 100 ml of water (25ppm), stirup until it is completely dissolved.

Adjust headspace sample conditions and inject. Integrate the benzene and toluenepeacks of the 6 chromatograms obtained. The Relative Standard Deviation of thearea quotients must be lower than 5%.

Benzene areaBenzene areaBenzene areaBenzene areaBenzene area TTTTToulene areaoulene areaoulene areaoulene areaoulene area Area RatioArea RatioArea RatioArea RatioArea Ratio3418.4613418.4613418.4613418.4613418.461 5441.008 0.6283466.1253466.1253466.1253466.1253466.125 5449.905 0.6253359.1763359.1763359.1763359.1763359.176 5381.354 0.6243316.6463316.6463316.6463316.6463316.646 5374.388 0.6243782.4043782.4043782.4043782.4043782.404 6035.683 0.6273794.0263794.0263794.0263794.0263794.026 6063.646 0.626

Mean VMean VMean VMean VMean Valuealuealuealuealue 0.626Standard deviation (SD)Standard deviation (SD)Standard deviation (SD)Standard deviation (SD)Standard deviation (SD) 0.00163Relative standard deviation (RSD)Relative standard deviation (RSD)Relative standard deviation (RSD)Relative standard deviation (RSD)Relative standard deviation (RSD) 0.26%

ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-132110TR-132110TR-132110TR-132110TR-132110 2t Sampler for Static Head Space mod. 5060

(syringe not included)HA-81343HA-81343HA-81343HA-81343HA-81343 Syringe Hamilton 1 ml.1001 LTN point style 5HA-81443HA-81443HA-81443HA-81443HA-81443 Syringe Hamilton 2,5 ml. 1002 LTN point style 5

TTTTT e k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e r

8 6

Headspace Vials & AccesoriesHeadspace Vials• 20 mm crimp finish is beveled for a tigher seal.• Borosilicate glass• Flat bottom vials feature a slightly longer neck - custom fit for Carlo Erba

and Agilent.• Rounded bottom vials are specifically designed for Pekin-Elmer; also use with

Tekmar and Varian.

Reference 100/pkReference 100/pkReference 100/pkReference 100/pkReference 100/pk Ref. 1000/csRef. 1000/csRef. 1000/csRef. 1000/csRef. 1000/cs VVVVVia lia lia lia lia l VVVVVolumeolumeolumeolumeolume DimmensionsDimmensionsDimmensionsDimmensionsDimmensionsCC-C4020-20/PCC-C4020-20/PCC-C4020-20/PCC-C4020-20/PCC-C4020-20/P CC-C4020-20CC-C4020-20CC-C4020-20CC-C4020-20CC-C4020-20 Flat Bottom 20 ml 23 x 75 mmCC-C4020-10/PCC-C4020-10/PCC-C4020-10/PCC-C4020-10/PCC-C4020-10/P CC-C4020-10CC-C4020-10CC-C4020-10CC-C4020-10CC-C4020-10 Flat Bottom 10 ml 23 x 46 mmCC-C4020-2/PCC-C4020-2/PCC-C4020-2/PCC-C4020-2/PCC-C4020-2/P CC-C4020-2CC-C4020-2CC-C4020-2CC-C4020-2CC-C4020-2 Rounded Bottom 20 ml 23 x 75 mmCC-C4020-210/PCC-C4020-210/PCC-C4020-210/PCC-C4020-210/PCC-C4020-210/P CC-C4020-210CC-C4020-210CC-C4020-210CC-C4020-210CC-C4020-210 Rounded Bottom 10 ml 23 x 46 mm

Headspace 20 mm Crimp Seals• Use with all Headspace vials

References 1000/csReferences 1000/csReferences 1000/csReferences 1000/csReferences 1000/cs Seal DescriptionSeal DescriptionSeal DescriptionSeal DescriptionSeal DescriptionCC-C4020-3ACC-C4020-3ACC-C4020-3ACC-C4020-3ACC-C4020-3A One-Piece unlined 20 mm aluminium crimp seals onlyCC-C4020-6ACC-C4020-6ACC-C4020-6ACC-C4020-6ACC-C4020-6A One-Piece pressure release unlined 20 mm crimp seals only. Pressure will vent

when a 3 bar +/- 0.5 rating is exceeded within the vial

Headspace 20 mm Crimp Seals with Septa• Pre-assembled 20 mm crimp seals with septa• Ready-to-use with any Headspace vials

Reference 100/pkReference 100/pkReference 100/pkReference 100/pkReference 100/pk Ref. 1000/csRef. 1000/csRef. 1000/csRef. 1000/csRef. 1000/cs VVVVVia lia lia lia lia l VVVVVolumeolumeolumeolumeolume DimmensionsDimmensionsDimmensionsDimmensionsDimmensionsCC-C4020-32A/PCC-C4020-32A/PCC-C4020-32A/PCC-C4020-32A/PCC-C4020-32A/P CC-C4020-32ACC-C4020-32ACC-C4020-32ACC-C4020-32ACC-C4020-32A Tan PTFE/White Silicone Regular - 60 to 125ªCCC-C4020-32AP/PCC-C4020-32AP/PCC-C4020-32AP/PCC-C4020-32AP/PCC-C4020-32AP/P CC-C4020-32APCC-C4020-32APCC-C4020-32APCC-C4020-32APCC-C4020-32AP Tan PTFE/White Silicone Pressure Release - 60 to 125ªCCC-C4020-34A/PCC-C4020-34A/PCC-C4020-34A/PCC-C4020-34A/PCC-C4020-34A/P CC-C4020-34ACC-C4020-34ACC-C4020-34ACC-C4020-34ACC-C4020-34A Ivory PTFE/Red Rubber Regular - 40 to 100ªCCC-C4020-34AP/PCC-C4020-34AP/PCC-C4020-34AP/PCC-C4020-34AP/PCC-C4020-34AP/P CC-C4020-34APCC-C4020-34APCC-C4020-34APCC-C4020-34APCC-C4020-34AP Ivory PTFE/Red Rubber Pressure Release - 40 to 100ªCCC-C4020-36A/PCC-C4020-36A/PCC-C4020-36A/PCC-C4020-36A/PCC-C4020-36A/P CC-C4020-36ACC-C4020-36ACC-C4020-36ACC-C4020-36ACC-C4020-36A Gray PTFE/Black Butyl Molded Septa Regular - 40 to 125ªCCC-C4020-36AP/PCC-C4020-36AP/PCC-C4020-36AP/PCC-C4020-36AP/PCC-C4020-36AP/P CC-C4020-36APCC-C4020-36APCC-C4020-36APCC-C4020-36APCC-C4020-36AP Gray PTFE/Black Butyl Molded Septa Pressure Release - 40 to 125ªC

Headspace 20 mm Septa

Reference 100/pkReference 100/pkReference 100/pkReference 100/pkReference 100/pk Ref. 1000/csRef. 1000/csRef. 1000/csRef. 1000/csRef. 1000/cs SeptaSeptaSeptaSeptaSepta TTTTTemp. Rangeemp. Rangeemp. Rangeemp. Rangeemp. RangeCC-C4020-30/PCC-C4020-30/PCC-C4020-30/PCC-C4020-30/PCC-C4020-30/P CC-C4020-30CC-C4020-30CC-C4020-30CC-C4020-30CC-C4020-30 Gray Butyl Stopper -20 to 120ªCCC-C4020-32/PCC-C4020-32/PCC-C4020-32/PCC-C4020-32/PCC-C4020-32/P CC-C4020-32CC-C4020-32CC-C4020-32CC-C4020-32CC-C4020-32 Tan PTFE/White Silicone -60 to 125ªCCC-C4020-34/PCC-C4020-34/PCC-C4020-34/PCC-C4020-34/PCC-C4020-34/P CC-C4020-34CC-C4020-34CC-C4020-34CC-C4020-34CC-C4020-34 Ivory PTFE/Red Rubber -40 to 100ªCCC-C4020-36/PCC-C4020-36/PCC-C4020-36/PCC-C4020-36/PCC-C4020-36/P CC-C4020-36CC-C4020-36CC-C4020-36CC-C4020-36CC-C4020-36 Gray PTFE Black Butyl Molded Septa -40 to 125ªC

20 mm Crimping & Decapping Tools• For Headspace vials and any 20 mm crimp seals

ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription PkPkPkPkPkCC-C4020-100CC-C4020-100CC-C4020-100CC-C4020-100CC-C4020-100 Manual Crimper, 20 mm 1CC-C4020-101CC-C4020-101CC-C4020-101CC-C4020-101CC-C4020-101 Decapping Pliers, 20 mm 1CC-C4020-102CC-C4020-102CC-C4020-102CC-C4020-102CC-C4020-102 Manual Decrimper, 20 mm 1

CC-C4020-210 CC-C4020-2

H e a d S p a c e VH e a d S p a c e VH e a d S p a c e VH e a d S p a c e VH e a d S p a c e V i a l s & A c c e s o r i e si a l s & A c c e s o r i e si a l s & A c c e s o r i e si a l s & A c c e s o r i e si a l s & A c c e s o r i e s

Teknokroma Capillary Columns

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