TABLE OF CONTENTS - Analytics CorpCustomer Service – x0 4. How to Use This Directory This...

TABLE OF CONTENTS

I. GENERAL INFORMATION

1. Introduction 3

2. Mailing/shipping address 3

3. Contact information 3

4. How to use this directory 4

5. Discount program 4

II. INDUSTRIAL HYGIENE SERVICES AND FEES

1. General information and Policies 5

1.1. Standard Turnaround Time 5

1.2. Shipping, Billing and Rush Multipliers 5

1.3. Discounts for Multiple Analytes on Single Media 6

1.4. Blanks and Charges 6

1.5. Method Development 6

1.6. Media 6

1.7. Sampling Instructions 7

1.8. Analytical Reports 9

1.9. No Charge Loaner Pump Program 10

1.10. Laboratory Test Request (Chain of Custody) 12

2. Industrial Hygiene Test Catalog 13

2.1. How to Use the Test Catalog 13

2.2. Alphabetical Listing of Test Methods 16

2.3. Profiles 107

2.4. Media Table 110

III. PHARMACEUTICAL TESTING SERVICES 117

1

IV. ENVIRONMENTAL SERVICES AND FEES 119

1. Introduction 119

2. Standard Turnaround Time 119

3. Billing and Rush Multipliers 119

4. Deliverable Multipliers 119

5. Certifications 119

6. Sample Containers/Shipping Kits 120

7. Sample Kit/Cooler Return Policy 120

8. Sample Kit/Cooler Temperatures 120

9. Sample Collection and Preservation Guidelines 120

10. How to Submit a Sample 121

11. Reports and Deliverables 122

12. Alphabetical Listing of Methods 125

V. MISCELLANEOUS SERVICES AND FEES 147

1. Introduction 147

2. Microbiology: Bacteria in Air 148

3. Microbiology: Bacteria in Water 148

4. Microbiology: Fungal 149

5. Air Quality Testing 150

VI. SERVICE GUIDE SUMMARY 150

1. Standard Terms and Conditions 150

2

I. General Information

1. IntroductionAnalytics has been a major supplier of industrial hygiene and environmental testing servicesto Fortune 500 companies, government agencies, and engineering firms since 1977. Thisexperience allows us to provide services that are both high in quality and cost effective.

Analytics is proud of the reputation we have earned over the last 30 years as a result ofproviding our customers the best quality analytical data available in the U.S. and more than30 countries abroad. We have over 1800 active clients and have done business with mostof them for over 10 years.

Analytics’ facility is one of the finest industrial hygiene and environmental laboratories in thecountry. We have in place the certifications, SOPs, insurance, and state-of-the art- instrumentation required to meet OSHA, NIOSH, and EPA analytical requirements.

Our standard turnaround time is 3 days for Industrial Hygiene samples, and 5 days forenvironmental samples. Analytics has no difficulty in meeting 24-hour turnaround time asmay be required.

2. Mailing/Shipping Addresses

Main Office & Laboratory

Analytics Corporation

10329 Stony Run Lane Ashland, VA 23005

800-888-8061 804-365-3000

804-365-3002 (Fax)

Remittance Address Analytics Corporation

PO Box 25249 Richmond, VA 23260

Website www.analyticscorp.com

Federal Tax ID #36-4359432 DUNS

#151052102

3. Contact Information

All personnel can be reached via our toll free number – 800-888-8061.

James McCarthy, President –5201 Jeffrey Spink, CEO – x5004

Andrew Teague, CIH, Industrial Hygiene Technical Laboratory Director – x5226 Dawn Casto, Environmental Technical Director – x5208

Jack Simila, Sales & No Charge Loaner Pumps – x5108 Customer Service – x0

3

http://www.analyticscorp.com/

4. How to Use This Directory

This directory has been designed so you can find individual industrial hygiene analytes alphabetically and within profiles. Environmental analytes are sorted alphabetically and by regulation. Pharmaceutical APIs and surrogates are sorted alphabetically.

The following information is included in the alphabetical listings:

Industrial Hygiene: Analyte, CAS #, Recommended Media, Suggested Volume, Sampling Rate, LOQ, Analytical Method, Analytical Technique, Lab Code, and Comments.

Environmental: Analyte, Method, Sample Container and Volume Requirements, Preservation, Holding Times, and Limits of Quantitation.

Pharmaceutical: Compound, Media, Reporting Limit, Method.

Please refer to the Data Deliverables Section at the end of both the IH and Environmental Services and Fees sections for a complete listing of our data package options. We can provide your data via fax, e-mail, or CD-ROM. Our data package turnaround time is contingent upon the data package level required.

5. Discount Program

Please note that all prices listed in this Directory of Services are our list/non-discounted prices. Client discounts may be available and are based on your annual volume of business. Please contact our Sales personnel to discuss volume related discounting.

4

II. Industrial Hygiene Services and Fees

1. General Information and Policies As you know, an industrial hygiene laboratory analyzes samples taken in the workplace environment. Since results of these analyses are used to determine the magnitude or presence of a problem in the workplace environment, it is vital that the laboratory analyzing the samples be proficient in producing high quality data on which important health decisions will be based. Our accreditation from AIHA is a mark of that capability. The AIHA accreditation shows that the laboratory has met defined standards for performance based on examination of a variety of criteria. When an IH laboratory is accredited by AIHA, it becomes part of a select group that have proven a high level of professional performance can be achieved and maintained.

1.1 Standard Turnaround Time

Analytics standard turnaround time for most industrial hygiene analyses is 3 business days from sample receipt at the laboratory. Faxed, e-mail, or verbal results are available by the close of business on the due date. A hard copy of the report will follow by mail.

1.2 Shipping, Billing and Rush Multipliers

Analytics will cover the cost of STANDARD OVERNIGHT FedEx return shipment to the laboratory of six (6) or more samples shipped within the United States. All other overnight delivery services charged on Analytics’ accounts will be billed at the courier’s published rate.

Clients may request monthly billing or individual invoices by sample group. Pricing is subject to change based on the current state of the economy. Billing by sample group is assumed unless otherwise requested. Billing terms are payable net 30. Acceptable forms

of payment include check, money order, wire transfer, VisaTM, MasterCardTM, DiscoverTM

or American ExpressTM.

Samples requiring rush or priority turnaround time must be scheduled prior to sample submission. The following charges will apply:

2 Day Turnaround Time 1.75 x price 1 Day Turnaround Time 2.00 x price Same Day Turnaround Time 3.00 x price Weekend Analysis 3.00 x price + $300 Holiday Analysis 3.00 x price + $300

5

1.3 Discounts for Multiple Analytes on Single Media

Analysis of multiple compatible analytes captured on one medium is available at a discounted fee. The higher priced analyte is billed at the published fee with additional analytes discounted as follows:

Organics by GC 50% of the published fee Inorganics by ICP 50% of the published fee Inorganics by ICP/MS 50% of the published fee Inorganics by GFAA 50% of the published fee Analytes by IC/HPLC 50% of the published fee

Other discounts may apply based on the volume and types of samples.

1.4 Blanks and Charges

Blanks act as a control for analysis by accounting for contamination that can occur during handling, storage or shipment of samples. Therefore, they are recommended as standard industrial hygiene practice. Please handle them the same as samples, but draw no air through them. Submit one blank with each sample group of 10 or less, two blanks with 11-20 samples, etc. (i.e., 10% blanks). Since blanks are analyzed as any other sample in the laboratory, they are priced according to the analysis requested. Additional support documentation, including instrument calibration, chromatograms, etc. is available at a preparation charge of 20% of the total analytical cost.

Analytics reserves the right to refuse to process any sample, which is deemed by the laboratory to be non-compliant with the quality assurance requirements. In such cases, client services will notify the client. If sample issues cannot be resolved, the client may be billed a sample-handling fee for costs incurred up to that point.

1.5 Method Development

Analytics has over 500 methods currently in service. It has always been our policy to develop new routine methods at no charge, assuming adequate demand. In addition, we can develop very specific/one of a kind methods for a standard fee plus expenses.

1.6 Media

Standard filter cassettes, sorbent tubes, specialized filters and tubes are supplied free if the samples are returned for analysis. Fees for organics are based on small charcoal tube analysis – there is an additional charge of $8.00 for large charcoal tubes. Diffusive (passive) monitor fees are not included in the analytical unit price and are billed at the time of shipment. Media can be shipped via ground service at no charge. A purchase order or credit card authorization may be required prior to the shipment of media. Media that has been supplied free and not returned for analysis to our laboratory after thirty days will be billed at current manufacturer published prices. See Section 2.4 - Media Table, which provides part numbers, descriptions and pricing for sampling media.

6

1.7 Sampling Instructions

The Analytics technical staff is available to discuss sampling strategies, sample requirements, and laboratory capabilities. Please direct inquiries through client services.

The volume of air to be collected for your samples is based on a number of factors, including:

• Threshold Limit Value (TLV) or Permissible Exposure Limit (PEL)• Sensitivity of the analytical procedure• Capacity of the collection device• Concentration range to be measured

The recommendations for air volumes, sampling rates and suggested media within this directory are provided for your convenience and are intended only as a guide to sample collection. With few exceptions, these air volumes enable the laboratory to report one-tenth of the TLV as the detection limit.

Fees for analyses of samples submitted on sorbent tubes include separate desorption, analysis, and reporting of both front and back sections.

Clearly label every tube, badge, vial, or sample container with your sample field number or your identification number. This number should also be printed on the chain of custody.

To facilitate testing and reporting, please type or clearly print all required information on the Laboratory Test Request/Chain of Custody (COC) form (an example immediately follows this section or our website www.analyticscorp.com). To initiate the COC, fill out and sign the appropriate sections designating time, date, and requested analysis. Submit the original with your samples and retain the copy for your records. The COC form should be submitted with each group of samples using a separate form for each sample type.

1.7.1 Solid Sorbent Tube Sampling Solid sorbent tubes include large and small charcoal tubes, porous polymer tubes such as XAD and XAD-7, large and small silica gel tubes, DNPH (dinitrophenyl hydrazine) tubes, Orbo tubes, Porapak Q, Tenax tubes, Firebrick tubes, Hydrar tubes and Florisil tubes. Sampling should be performed in the following manner:

1. Calibrate each pump at the recommended flow rate for the analyte of interest, using arepresentative solid-sorbent tube in-line. Calibrate each pump with a bubble meter orequivalent flow measuring device.

2. Break the ends of the solid sorbent tube immediately before sampling. The openingsshould be at least ½ of the internal diameter of the tube. Use a tube tip breaker or file.

3. Connect the solid sorbent tube to the tube holder, making sure the smaller sorbentsection (backup section) is nearest the pump. The air that is being sampled should notpass through any hose or tubing before entering the solid sorbent tube. To avoidchanneling and premature breakthrough, position the tube vertically during sampling.

4. Prepare field blanks by breaking the ends of tubes from the same lot as the tubes thatare being used for sampling. Handle the blanks in the same manner as the samples, but

7

do not draw air through the blanks. 5. Sample at an accurately known flow rate for the length of time necessary to obtain the

specified air volume. Check the pump periodically during sampling to detect any changes in flow rate. If the accurate measurement of volume cannot be determined due to inconsistent flow rates, discard the sample.

6. Be sure to keep an accurate record of sampling data including sample location, beginning and ending times of air sampling, temperature, relative humidity, atmospheric pressure or

7. elevation above sea level, and name of employee. 8. Seal the ends of the tubes with plastic caps immediately after sampling. Clearly label

each sample with an appropriate identification number. Label each blank tube as a blank.

9. Pack the tubes tightly for shipment to the laboratory, with adequate packing to minimize the possibility of breakage. Enclose a completed sample analytical request form (chain of custody) with each batch.

10. Bulk samples are recommended when sampling chemical mixtures such as fuel oil, kerosene, etc. When it is necessary to ship a bulk sample along with the air samples, the bulk sample must be shipped in a separate package to avoid possible cross contamination.

1.7.2 Sampling Using Filters Filters include glass fiber filters, Teflon filters, mixed cellulose ester membranes, polyvinyl chloride filters, and treated filters and pads.

Sampling with filters can be done open or closed faced. Open-faced sampling is done with three (3) piece cassettes with just the top of the cassette removed. Closed-faced sampling is performed with only the buttons removed from the cassette. Open-faced sampling is used in situations where even dispersal of the analyte over the filter is desired, such as in asbestos sampling or on certain coated filters such as for isocyanate sampling. Closed-faced sampling is performed in most cases of particulate sampling, which deposits the analyte near the center of the cassette.

Sampling should be performed in the following manner:

1. Calibrate the sampling pump at the recommended flow rate with a representative filter

in line using a bubble meter or equivalent flow measuring device.

2. Remove the cassette buttons (closed faced sampling) or cassette top (open faced sampling). Air being sampled should not pass through any hose or tubing before entering the cassette.

3. Attach the cassette to the sampling pump using flexible tubing or a cassette holder, making sure the filter pad end of the cassette is closest to the pump.

4. Prepare field blanks using cassettes from the same lot by briefly removing and replacing cassette buttons and handling these blanks in the same manner as the samples, without drawing air through the blanks.

5. Sample at a known flow rate for the length of time necessary to obtain the specified air volume, or until there is evidence of excessive filter loading. Check the pump during sampling to detect any changes in flow rate. If the accurate measurement of volume cannot be determined due to inconsistent flow rates, discard the sample.

6. Disconnect the filter after sampling. Replace the buttons (or top) and properly label the

8

sample and blanks. Be sure to keep an accurate record of sample data including sample location, beginning and ending times or air sampling, temperature, relative humidity, atmospheric pressure or elevation above sea level, and name of employee or area.

7. Ship the samples to the laboratory as soon as possible in a container designed to prevent damage in shipment. Enclose a completed chain of custody with each batch.

1.7.3 Sampling for Respirable Aerosols Respirable aerosol sampling is performed using a cyclone and filter sampler. Sampling for respirable aerosols should be performed in the same manner as sampling a filter except:

1. Calibrate each pump at the flow designated by the type of cyclone being used with a

representative cyclone and filter in line. Note that the filter is mounted upside down with the cyclone in place.

2. Inspect the interior of the cyclone. If there is visible scoring or damage inside, discard the cyclone since the dust separation characteristics may have been altered. Clean the interior of the cyclone.

3. Attach the cyclone to the filter according to the manufacturer’s instructions. Connect the assembly to the sampling pump. During sampling, make sure the cyclone hangs vertically and that the assembly does not get inverted during sampling. If an accurate and consistent flow rate cannot be maintained, discard the sample.

1.7.4 Sampling for Inhalable Aerosols We can provide pre-weighing of inhalable samplers, as well as post-weighing. Contact the laboratory for details on this relatively new technique.

1.8 Analytical Reports

Most clients have their data reported on our standard report, which includes total mass of analyte on each collector section, limits of quantitation, method reference and calculated air concentration. If you need additional data or would like a different format, please contact our customer service department at 800-888-8061, x0 and they will be able to assist you with your request. All laboratory reports, sample data and client proprietary information are held in confidence. Raw data for all analytical results will be retained for a period of 5 years. If data needs to be retained for a longer period, contact client services.

9

1.9 No Charge Loaner Pump Program

Analytics offers a No Charge Loaner Pump Program. This program will provide you with everything you need for air sampling analysis–pumps, sample media, all accessories, and instructions, custom packaged to your requirements, shipped to you as you need it. You pay only for shipping and, of course, the analysis – there is absolutely no cost to use the pumps and accessories.

To order your pumps, all you need to do is contact Jack Simila at 800-888-8061, x5108.

Your order will include the pumps (as many as you need, all fully charged and pre-calibrated), tubing, sample media, sample media holders, pumps, chargers, instructions, cyclones, splitters, low flow regulators, tube breaker, tool kit, chain of custody form and calibrated field rotameter, all packed in a sturdy carrying case. Pumps are normally sent out the same day. Please keep in mind the more notice you provide, the less expensive shipping charges will be. Typical shipping costs for a sampling set that includes five pumps and is shipped across the country (VA to CA) with 2nd day delivery is about $40.

We use primarily SKC AirCheck 52 sampling pumps, which handle flows in the range of 25 to 3000 ml/min with a backpressure of 25" water at 2 liters per minute. They weigh 20 ounces and have a timer, flow fault feature and NiCad or NiMH battery with a battery-check feature. Other pumps are available on request. The pumps arrive fully charged and calibrated versus a primary standard, with a record of calibration in the shipment. A field rotameter, calibrated against a primary standard, is included in the sampling kit. Post calibration can be performed and reported if you request it on your chain of custody when you return the samples and pumps.

The pumps and all accessories can be kept for the duration of your sampling project. As long as you are collecting and submitting for analysis daily samples, you may use the pumps indefinitely. If your project is postponed, you will need to call to confirm availability. Depending on the length of the time delay, you may need to return everything to us, but we will re-ship the entire sampling kit to you for your new scheduled date.

10

1.10 Laboratory Test Request (Chain of Custody)

Sample Custody is a set of procedures used to provide an accurate written record that can be used to trace the possession of a sample from the time of collection through its introduction into a data set. The Laboratory Test Request/Chain of Custody is used to record the transfer, possession, and custody of samples to ensure their integrity from collection through data reporting. Until you relinquish custody, you are responsible to ensure no one tampers with your samples. Custody is a critical part of the process because data reported without a complete and accurate chain of custody will not withstand legal challenge. The following items must be completed on the chain in order to ensure sample integrity and accurate analysis/reporting:

1. Date Shipping Samples

2. Total Number of Samples

3. Type of Media

4. Project Name or Number

5. PO or Release Number

6. Contact – Who the Report Will be Sent to

7. Telephone Number

8. Turnaround Time Required

9. Special Instructions, if needed

10. Where to fax/e-mail results

11. Sample ID or Sample Number

12. Sample Date

13. Sample volume

14. Analysis

15. Initiate COC

16. Laboratory Receipt Information (for laboratory use)

11

LABORATORY TEST REQUESTACCOUNT NUMBER, NAME AND ADDRESS

10329 Stony Run Lane

Ashland, VA 23005

(804) 365-3000

TOLL FREE (800) 888-8061

FAX (804) 365-3002

SAMPLE DATE

SIGN HERE TO INITIATE CHAIN OF CUSTODY

CARRIER IF "ANALYTICS COURIER" SIGN HERE DATE

PLEASE RETAIN A COPY FOR YOUR RECORDS

SIGNATURE(SAMPLE RECEIVING)

SIGNATURE(SAMPLE ADMINISTRATION)

SIGNATURE(LAB)

SIGNATURE(LAB)

SAMPLES RECEIVED BY: SAMPLES RELEASED BY:

SIGNATURE(SAMPLE RECEIVING)

SIGNATURE(SAMPLE ADMINISTRATION)

SIGNATURE(LAB)

SIGNATURE(LAB)

DATE/TIME CONDITION OF SAMPLE

PURCHASE ORDER NO.

DATE SHIPPED

* o SAME DAY

* o 1 DAY

* oCALL FOR AVAILABILITY

SPECIAL INSTRUCTIONS AND/OR UNUSUAL CONDITIONS:TURN AROUND TIME

CONTACT

CHAIN OF CUSTODY RECORD

FOR LABORATORY USE ONLY

SAMPLES HAVE VEEN SEALED FOR TRANSPORT AND

DELIVERED TO LABORATORY VIA:

ANALYSS REQUESTED - PLEASE USE SEPARATE

LABORATORY TEST REQUEST FOR EACH SAMPLE TYPE

o FAX RESULTS FAX NUMBER:

( ) __________________

o EMAIL RESULTS - EMAIL:________________________

SAMPLE # OR SAMPLE AREASAMPLE

VOLUME/LITERS

*o2 DAY

oSTANDARD

*EXTRA CHARGE

PROJECT NAME OR NUMBER

TELEPHONE NUMBER

# OF SAMPLES SAMPLE TYPE/MEDIA

V01 06.2017 Toll Free: 800-888-8061 Find more info at www.analyticscorp.com

12

ccatlynLine

2. Industrial Hygiene Test Catalog

2.1 How to Use the Test Catalog

This section is composed of several categories of information that allows the user to access the necessary parameters for industrial hygiene air sampling. The guide has been arranged to make it as easy as possible for the user. For many categories, abbreviations are used to facilitate a concise format. The following descriptions give the relevant information pertaining to each category in order of appearance in the guide.

Analyte & CAS# This category will give the name of the compound to be analyzed and the corresponding CAS#. In cases where there are other names for a compound, there may be a redirection to another place in the guide.

Recommended Media This category specifies the method recommended collection media for air sampling of the particular compound. Abbreviations used in this category are defined in the Section 2.4 Media Table.

Suggested Volume, L This category specifies the method recommended air volume to be sampled in liters. In many cases, this recommended volume can be at least doubled before breakthrough occurs. In high relative humidity locations or with very high volatile compounds, this recommended volume should not be exceeded.

Sampling Rate, LPM This sampling range indicates the minimum and maximum flow rate of the sampling pumps used in liters per minute.

LOQ (Limit of Quantitation) This category lists the lowest quantifiable sampling media loading (also known as Reporting Limit, RL) that will be reported (typically in micrograms) per sample. Samples measured below this loading will be reported as “

Lab Code (Compatibility) This category gives the option to the user of sampling more than one compound on a specific sampling media. In order to do so, not only must the same sampling media be specified for each compound, but the Compatibility letter designations given in this category must match for each test compound to be sampled. Particular attention must be given to other parameters of the individual compounds such as sample volume and flow rate in order to ensure sample validity. Care must be taken to make sure that no flow rate or air volume parameter for an individual compound is exceeded when sampling for two or more compounds. The exception to the Lab Code list is NC, which means the analyte is not compatible with other compounds.

Due to the frequency of questions on substance compatibility (analytes or compounds that can be sampled on the same collection media), we have included a compatibility code in this edition of the sampling guide. Please see the “Lab Code” column in the list of individual air contaminants for information on individual analytes and compounds. Listed below is the compatibility code key. When two or more substances have the same Recommended Media and same the Lab Code, they can be sampled together and are eligible for a discounted price (see terms and conditions section for details).

Code A

Desorbing Solution Carbon disulfide (CS2)

Code AA

Desorbing Solution Sodium Thiosulfate

B C

CS2 + 1% 2-Butanol CS2 + 1% 2-Propanol

CC EE

Toluene OSHA ID125G Acid Digestion

D CS2 + 5% 2-Propanol FF 0.1N Potassium Hydroxide E Methylene Chloride + 5% HH Acetone

Methanol F CS2 + 1% Dimethylformamide II Methylene Chloride + 15%

Methanol H CS2 + 1% Methanol JJ 50% Methanol + 50% Water I Methylene Chloride KK 50% Isopropanol + 50%

Toluene J Water-soluble Metals Prep LL CS2 + 2% Acetone K Methanol MM Benzene M Ethanol NN Di-n-Butylamine

Derivatization N Acetonitrile OO Aqua Regia Acid digestion O Acetonitrile + 10%

Dimethylsulfoxide P Isooctane Q Methanol + 20% water NC Prep Not Compatible With

Additional Tests S Hexane T NIOSH 7300M Acid Digestion U Bicarbonate/carbonate Eluent V Sodium borate Eluent W Tetrahydrofuran X 0.01N Sodium Hydroxide Y Methanesulfonic Acid Eluent

14

2.2 Alphabetical Listing of Test Methods

Analytics is pleased to offer an extensive array of Industrial Hygiene analyses, including most OSHA, NIOSH, ASTM, and EPA methods and also numerous proprietary methods. Specific analytical tests are listed in the following sections. Lists of tests are presented in the Sections that follow here; Section 2.2 provides an alphabetical list by analyte, and Section 2.3 provides a listing of our profiles. Please note that for most tests Analytics does not require a minimum sample fee. Volume discounts are available depending on the annual volume or scope of your project. Please contact our sales department or your project manager for details.

15

Alphabetical Listing

of

Industrial Hygiene Tests

V01 06.2017 Toll Free: 800-888-8061 Find more info at www.analyticscorp.com 16

Analyte CAS # Recommended Media

Suggested

(minutes for passive

samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Acenapthene

83-32-9 K-06PTFE + ORBO 43

200-1000 2 3NIOSH 5506

HPLCN $116

Wrap cassettes with foil if sampling in bright sunlight.

Transfer filter to glass vial immediately after sampling, and

wrap tube and vial with aluminum foil to protect from light.

Store samples cold and ship samples cold for overnight

delivery.

Acenapthylene

208-96-8 K-06PTFE + ORBO 43

200-1000 2 3NIOSH 5506

HPLCN $116





delivery.

Acetaldehyde

75-07-0T-119

DNPH-Treated Silica Gel,

226-119

2 - 15 0.2 - 1.0 0.2EPA TO-11

HPLCN $116

Any ketone or aldehyde will react with the DNPH and is a

potential interference. Large concentrations of acetone or

MEK will compete with aldehyde and are therefore

potential negative interferences. Refrigerate media before

and after sampling and ship cold overnight. High ozone

level may necessitate ozone scrubber.

UMEX-100

SKC UMEX

Aldehyde PM 500-100

Up to 8 hours 0.0231 0.2EPA TO-11

HPLCN $116

Any ketone or aldehyde will react with the DNPH and is a

potential interference. Large concentrations of acetone or

MEK will compete with aldehyde and are therefore

potential negative interferences. Refrigerate media before

and after sampling and ship cold overnight. High ozone

level may necessitate ozone scrubber.

Acetic Acid

64-19-7T-01

Charcoal, 226-015 - 48 0.2 Max 5

OSHA ID 186SG M

ICV $69

Preferred method. Use PTFE prefilter (PN C-29) to remove

particulate acetates, if present. Particulate acetates can be

measured on filter, otherwise discard after sampling.

Formic Acid can also be determined but must be stored and

shipped cold overnight.

T-10-03

Prewashed Silica Gel,

226-10-03

1 - 24 0.05 - 0.2 5NIOSH 2011M

ICV $69

Use PTFE prefilter (PN C-29) to remove particulate acetates,

if present. Particulate acetates can be measured on filter,

otherwise discard after sampling. Formic Acid can also be

determined.

Acetic Anhydride

108-24-7

C-28

GFFs (2), amine-treated,

37mm, 4PC

TWA 15 Max

STEL 7.5 Max

0.050 Max

0.50 Max10

OSHA 102M

HPLC/UVKK $100

Open face sampling. Interference from ketene and acetyl

chloride. Limited shelf life media; store cold. Ship samples

cold overnight to the lab.

Acetoin

573-86-0 T-183(2 in Series) Custom Silica

Gel, 226-183

TWA 9 Max

STEL 3 Max

0.050 Max

0.20 Max0.4

OSHA Method 1012

GC-ECDNC $110

Protect from light during sampling and storage (wrap with

foil). Store and ship samples cold. Ship overnight. May be

sampled on same tube with diacetyl. Filter built into tube

faces incoming air streams. Samples stable at least 17 days.

A three (3) sample minimum charge will be applied.

V01 06.2017

Toll Free: 800-888-8061

Find more info at www.analyticscorp.com17


Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Acetone

67-64-1

T-01

Charcoal, 226-010.5 - 3 0.01 - 0.2 20

NIOSH 1300

GC/FIDA $56

O-91

Carbosieve S-III, Orbo 913 Max 0.05 Max 20

OSHA 69

GC/FIDF $56

M-3520

3M POVM 3520,

2-stage

2 Hours Max (at PEL) 0.0401 30NIOSH 1300M

GC/FIDA $56

Keep samples cold and expedite analysis for optimum

results.

M-02

SKC POVM, 575-0028 hours Max 0.0152 20

Proprietary,

IHGC-P029

GC/FID

A $77

T-09

Charcoal, 226-093 - 25 0.01 - 0.2 20

NIOSH 1606

GC/FIDII $56

M-01

SKC POVM, 575-00115 min - 8 hours 0.0224 10

NIOSH 1606M

GC/FIDII $56

M-3520

3M POVM 3520,

2-stage

2 Hours Max 0.0482 30NIOSH 1606M

GC/FIDII $56

Acetylene Tetrabromide

79-27-6 $-

See 1,1,2,2-Tetrabromoethane.

Acetylacetone

123-54-6

T-95

XAD-7, 226-95

TWA 24

STEL 3

TWA 0.05-0.1

CEIL 0.2 5

OSHA 7M

GC/FIDHH $77

Also known as 2,4-Pentandione.

Acid Mist (Inorganic Acid

Profile) See Inorganic Acid

Profile in Section 2.3

Profile includes Hydrobromic Acid, Hydrochloric Acid,

Hydrofluoric Acid, Nitric Acid, Phosphoric Acid, Sulfuric

Acid. Also see individual acids.

Acrolein

107-02-8T-119


226-119

2 - 30 0.2 - 1.0 0.25EPA TO-11M

HPLC/UVN $116

Result may be biased low due to instability of acrolein-

DNPH derivative. Any ketone or aldehyde will react with

the DNPH and is a potential interference. Large

concentrations of acetone or MEK will compete with

aldehyde and are therefore potential negative

interferences. Refrigerate media before and after sampling

and ship overnight.

T-117

HMP XAD-2,

226-117

TWA 48

STEL 3

TWA 0.1

STEL 0.2 1

OSHA 52

GC/NPDCC $102

Preferred method for compound stability. Not sensitive

enough to reach ACGIH TLV CEILING. Can also be analyzed

for formaldehyde. Store media cold be use.

UMEX-100

SKC UMEX Aldehyde

PM 500-100

Up to 8 hours 21.2 0.2EPA TO-11M

HPLC/UVN $116

Result may be biased low due to instability of acrolein-

DNPH derivative. Any ketone or aldehyde will react with


concentrations of acetone or MEK will compete with


interferences. Refrigerate media before and after sampling

and ship overnight.

Acetonitrile

75-05-8

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Acrylamide

79-06-1

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0 0.40

Proprietary,

IHHPLC-P003

HPLC/UV

NC $160

Methylolacrylamide may also be tested along with

acrylamide.

T-57

GFF/XAD-7 OVS,

226-57

120 Max 1.0 Max 0.4OSHA PV2004

HPLC/UVNC $116

Acrylic Acid

79-10-7T-30-08 (2)

Anasorb 708, 226-30-08,

2 tubes in series

24 0.1 2OSHA PV2005

HPLC/UVK $116

Two identical tubes sampled in series. Low results due to

polymerization of acrylic acid on the sampling tube may

result from the presence of initiators collected. Methacrylic

acid may also be tested along with acrylic acid.

T-49-108

Chromosorb 108,

226-49-108

TWA 20

STEL 4.5

TWA 0.03-0.3

STEL 0.3 3

Proprietary,

IHHPLC-P005

HPLC/UV

JJ $160

Methacrylic acid can be collected and analyzed along with

acrylic acid using this sampling protocol (see lower

recommended sampling volume for methacrylic acid).

Acrylonitrile

107-13-1

T-01

Charcoal, 226-016 - 20 0.2 1

OSHA 37

GC/NPDHH $100

Preferred method.

M-3500

3M POVM, 350015 min - 8 hours 0.04 1.5

OSHA 37M

GC/NPDHH $100

M-02

SKC POVM, 575-002Up to 8 hours 0.0204 2.5

Proprietary,

IHGC-P029

GC/FID

A $77

T-81

Anasorb 747,

226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.25

Proprietary,

IHGC-P029

GC/FID

A $77

Aldehyde Profile See

Aldehyde Profile in

Section 2.3

T-119


226-119

16 - 30 0.2 - 1Varies with

compound

EPA TO-11

HPLC/UVN $254

Profile includes Acetaldehyde, Acrolein, Butyraldehyde,

Formaldehyde, Glutaraldehyde, and Isovaleraldehyde. For

STEL sampling, collect a 15-minute sample at 1 LPM. Ozone

may interfere - use ozone scrubber in known ozone

contaminated areas. Any ketone or aldehyde will react with


concentrations of acetone or MEK will compete with the


interferences. Refrigerate before and after sampling and

ship overnight. Media contains residual acetonitrile which

could interfere with acetonitrile monitoring.

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Alkaline Dust

(as NaOH, KOH, other)

N/A

C-66

PTFE, 1um, 37mm, 2PC70 - 1000 1.0 - 4.0

40 NaOH,

56 KOH

NIOSH 7401

TitrationNC $69

This test provides a single cumulative measure of all

alkaline aerosols present in the exposure; e.g., sodium

hydroxide, potassium hydroxide, sodium bicarbonate,

calcium carbonate, etc. The acid-base titration test is not

compound-specific, but the result will be expressed in

terms of the alkaline compound identified on the test

request form. Acid compounds present in the sampling

environment will be negative interferences in the

measurement.

T-01

Charcoal, 226-014 - 50 0.01 - 0.2 5

NIOSH 1402

GC/FIDD $56

Also known as 2-Propenol.

M-3500

3M POVM, 3500Up to 8 hours 0.0404 7.5

NIOSH 1402M

GC/FIDI $56

Also known as 2-Propenol.

Allyl Chloride

107-05-1

T-01

Charcoal, 226-0116-100 0.01 - 1 5

NIOSH 1000

GC/FIDMM $77

Allyl Chloroformate

2937-50-0

T-153

Amine-treated XAD-2,

226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 5

AIHAJ 12/1986,

pp.742-746

GC/FID

NN $77

Store media and samples cold, ship samples cold overnight.

Samples must arrive at lab within 10 days of sampling.

Allyl Methacrylate

96-05-9

T-81

Anasorb 747,

226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.3

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min 0.012 2.6

Proprietary,

IHGC-P029

GC/FID

A $77

Aluminum

(metal dust and fume)

7429-90-5C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 2

NIOSH 7300M

ICP-OEST $40

Also see Welding Fume Profile. This analysis method is not

sufficient for analysis of the alpha-alumina form of

aluminum oxide which is commonly used in abrasives and

refractory materials (also known as corundum).

Ammonia

7664-41-7

T-10-06

H2SO4-Treated Silica Gel,

226-10-06

7.5 - 96 0.2 Max 2.5 NIOSH 6016 IC NC $69

Capacity reduced at high humidity. Prefilter (C-50) required

in presence of ammonium salt particulates.

T-29

Anasorb 747,

226-29

7 - 24 0.1 - 0.5 5.0

OSHA ID 188/

NIOSH 6015M

IC

NC $69

Sampling per OSHA ID188, analysis by NIOSH 6015M.

Capacity reduced at low humidity. Prefilter (C-50) required

in presence of ammonium salt particulates.

M-N584

Assay Ammonia PM,

AT N584

TWA Up to 8 hours

STEL 15 minutes0.0288 2.5

NIOSH 6016M

ICNC $69

Ship at ambient temperature to arrive at lab within 2 days.

Must be received by lab within 2 weeks of sampling. Store

unused samplers in refrigeration for maximum shelf life.

Ammonium Chloride

12125-02-9C-05

MCEF, 37mm, 0.8um, 3PC960 Max 2 Max 10

OSHA ID188M

ICNC $69

Sampling is for particulate ammonium salts, with analysis

for ammonium ion; ammonium chloride equivalent is

determined by calculation.

Allyl Alcohol

107-18-6

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Ammonium Persulfate, as

Persulfate

7727-54-0C-10

PVC, 37mm, 5um, 3PC

TWA 480-960

STEL 60

TWA 1-4

STEL 4 2.7

NIOSH 6016M

ICNC $69

When submitting samples, “Ammonium Persulfate, AS

PERSULFATE” needs to be specified on the Analysis Request

Form in order to have results reported correctly as

persulfate. Analysis is for ammonium ion with “ammonium

persulfate, as persulfate” determined by calculation.

n-Amyl Acetate

628-63-7

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0260 30

NIOSH 1450M

GC/FIDA $56

M-01

SKC POVM, 575-01Up to 8 hours 0.0118 40

NIOSH 1450M

GC/FIDA $56

sec-Amyl Acetate

626-38-0

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

n-Amyl Alcohol

71-41-0

T-09

Charcoal, 226-093 - 48 0.05 - 0.2 3.3

OSHA 7

GC/FIDA $56

t-Amyl Methyl Ether

994-05-8

T-09

(2 in series) Charcoal,

226-09

96 Max 0.1-0.2 20NIOSH 1615M

GC/FIDA $56

Aniline

62-53-3

T-10

Silica Gel, 226-105 - 30 0.02 - 0.2 10

NIOSH 2002

GC/FIDM $56

C-15

GFFs (2), H2SO4-treated,

37mm, 3PC

5 - 50 0.1 - 0.2 20NIOSH 2017

GC/FIDM $102

This arrangement allows for collection of o-toluidine on the

same cassette, and a silica gel tube (226-15) may be

included downstream of the cassette to trap and include

nitro benzene in the analysis.

Anthracene

120-12-7 K-06PTFE + ORBO 43

200-1000 2 3NIOSH 5506

HPLCN $116





delivery.

Antimony and Compounds,

as Sb

7440-36-0

C-05

MCEF, 37mm, 0.8um, 3PC40 - 1000 1.0 - 3.0 2.0

OSHA ID 125

ICPEE $40

Also See Welding Fume Profile

Antimony - ICP-MS

7440-36-0C-05

MCEF, 37mm, 0.8um, 3PC2000 Max 1 - 4 0.05

NIOSH 7300M

ICP-MST $51

Antimony Trioxide,

as Sb

1309-64-4

C-05

MCEF, 37mm, 0.8um, 3PC240 0.5-3.0 1

OSHA ID-125

ICPEE $40

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Aromatic 100

N/A T-01Charcoal, 226-01

TWA 5-20

STEL 3

TWA 0.01-0.2

STEL 0.2 50

NIOSH 1550

GC/FIDA $77

Ship 5 ml pure distillate in separate shipment for reference,

and note separate shipment of the bulk sample on the test

request form. Also known as High Flash Aromatic Naphtha.

Aromatic 150

N/AT-01

Charcoal, 226-01

TWA 5-20

STEL 3 0.01-0.2 50

NIOSH 1550

GC/FIDA $77



request form.

Aromatic 200

N/AT-01

Charcoal, 226-01

TWA 5-20

STEL 3 0.01-0.2 50

NIOSH 1550

GC/FIDA $77



request form.

Arsenic

7440-38-2C-05

MCEF, 37mm, 0.8um, 3PC800 - 1000 1.0 - 3.0 2

NIOSH 7300

ICPT $40

C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 0.05

NIOSH 7300M

ICP/MST $46

Arsenic Trioxide

(as Arsenic)

1327-53-3

C-18

MCEF/Treated Backup,

37mm, 3PC

30 - 1000 1.0 - 3.0 0.05OSHA ID105M

GFAANC $51

Particulate arsenic collects on the MCE filter, and arsenic

trioxide vapor collects on the treated pad. Particulate

arsenic may be tested from the MCE filter if needed.

C-18

MCEF/Treated Backup,

37mm, 3PC

30 - 1000 1.0 - 3.0 0.05OSHA ID105M

ICP-MSNC $51

Particulate arsenic collects on the MCE filter, and arsenic

trioxide vapor collects on the treated pad. Particulate

arsenic may be tested from the MCE filter if needed.

Arsine

(as Arsenic)

7784-42-1 T-01Charcoal, 226-01

10 Max 0.2 Max 0.01NIOSH 6001M

GFAANC $51

Precede tube with arsenic trioxide cassette (see above) if

particulate arsenic and/or arsenic trioxide are present. This

treated filter/tube train can be tested for particulate

arsenic, arsenic trioxide vapor, and arsine if needed.

Samples are stable for at least 6 days at ambient

temperature.

T-09

Charcoal, 226-09120 - 240 0.5 Max 0.04

NIOSH 6001M

GFAANC $51

If particulate arsenic is present, precede tube with arsenic

trioxide cassette (see above) to trap particulate arsenic and

arsenic trioxide. This treated filter/tube train can be tested

for particulate arsenic, arsenic trioxide vapor, and arsine if

needed. The recommended sampling rate and maximum

volume included here are those described in the similar

method OSHA ID105. Samples are stable for at least 6 days

at ambient temperature.

Bulk sample, approx.

1 - 3 cubic inch volumeN/A 1.0%

EPA/600/M4- 82-

020, Dec. 1982

PLM

NC $17

Sample is assumed to be homogeneous

Bulk sample, approx.

1 - 3 cubic inch volumeN/A 1.0%

EPA- 600/R-93/116,

July 1993

PLM

NC $17

Price per layer

Asbestos Bulk ID

N/A

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Asbestos Bulk Point Count

N/ABulk sample, approx.

1 - 3 cubic inch volumeN/A


Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Benzene

71-43-2

T-01

Charcoal, 226-012 - 30 0.01 - 0.2 2

NIOSH 1501

GC/FIDA $56

M-01

SKC POVM, 575-00115 - 240 Min. 0.016 4.0

NIOSH 1501M

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0355 3

NIOSH 1501M

GC/FIDA $56

T-81

Anasorb 747, 226-81

TWA 30

STEL 3 0.03-0.2 1.1

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-00215 - 240 Min. 0.0171 2.2

Proprietary,

IHGC-P029

GC/FID

A $77

M-N521

Assay Technology POVM,

N521

15 - 480 Min. 0.073 2.0 A $56

Benzene Soluble

Fraction N/AC-06

GFF, 37mm, 1um, 3PC960 1 - 2 30

OSHA 58

Gravimetric with

extraction

MM $116

This is the same test as Coal Tar Pitch Volatiles by OSHA 58.

Transfer filter into glass vial using tweezers immediately

after sampling; wrap vial in foil to protect from light.

Additional specific PAH analysis is available as follow-up if

needed for samples with BSF exceeding 0.2 mg/M3.

C-09

PTFE, Pre-weighed, 37mm,

2um, 3PC

28 - 400 1 - 4 30

NIOSH 5042

Gravimetric with

extraction

MM $116

Test includes measurement of Total Particulates and

Benzene Soluble Fraction. This is the NIOSH approach for

both Coal Tar Pitch Volatiles and Asphalt Fumes. Protect

samples from light if follow-up PAH analysis is needed.

Benzidine

92-87-5C-07

GFF, 13mm, 1um, 2PC

Swinnex

20 - 100 0.2 0.2NIOSH 5509

HPLCNC $116

Transfer filter and Teflon ring to vial after sampling. Store in

freezer, ship on dry ice for overnight delivery. Stable at

least 11 days at -15° C.

1,2-Benzisothiazolin-3-one

(BIT)

2634-33-5

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0 0.3

IHO- HPLC-070

HPLC/UVK $160

Samples stable up to 21 days at ambient temperature.

Benzo(a)anthracene

56-55-3 K-06PTFE + ORBO 43

200-1000 2 3NIOSH 5506

HPLCN $116





delivery.

Benzo(b)fluoranthene

205-99-2 K-06PTFE + ORBO 43

200-1000 2 3NIOSH 5506

HPLCN $116





delivery.

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Benzo(k)fluoranthene

207-8-9 K-06PTFE + ORBO 43

200-1000 2 3NIOSH 5506

HPLCN $116





delivery.

Benzo(g,h,i)perylene

191-24-1 K-06PTFE + ORBO 43

200-1000 2 3NIOSH 5506

HPLCN $116





delivery.

Benzo (a) pyrene

50-32-8 C-06GFF, 37mm, 1um, 3PC

960 2.0 3OSHA 58

HPLC/FLMM $116

Place filter into glass vial using tweezers and wrap with foil

to protect from light. Ship refrigerated by overnight

delivery. Also see selected PNA Profile.

K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

Benzophenone

119-61-9

T-110

Chromosorb 106,

226-110

48 Max 0.2 Max 1.6OSHA PV2130

GC/FIDNC $56

Samples are stable at ambient temperature for at least 14

days.

Benzoyl Chloride

98-88-4T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 5

AIHAJ 12/1986,

pp.742-746

GC-FID

NN $77

Other chloroformates/acid chlorides may be tested from

the same sample. Store media and samples cold, ship

samples cold overnight. Samples must arrive at lab within

10 days of collection.

Benzoyl Peroxide

94-36-0C-05

MCEF, 37mm, 0.8um, 3PC40 - 400 1 - 3 1

NIOSH 5009

HPLC/UVNC $116

Ship refrigerated for overnight delivery.

Synonym: Dibenzoyl peroxide.

Benzoyl Peroxide

Inhalable

94-36-0

Call lab 960 Max 2.0 1NIOSH 5009M

HPLCNC $116

Important Note: 1. The IOM sampler should be operated

at 2 Lpm in order to correctly collect the particle size range

(up to 100 um) which comprises inhalable particles. 2. This

listing modifies NIOSH method 5009, which does not take

into account monitoring of inhalable particulates. The

maximum air volume of 400 L recommended in method

5009 has been increased to 960 L in this listing in order to

allow for a full-shift sample at the 2 Lpm sampling rate

required for the IOM sampler. However, if analytical results

show a filter loading of 1 to 2 milligrams or greater,

consider resampling for a shorter time period. 3. If

available, ship samples by overnight delivery to the lab in

an insulated container with cold pack (9% loss of material

from filter has been measured after 1 week @ 25 C).

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Benzyl Acetate

140-11-4

T-01

Charcoal, 226-0110 - 50 0.1 - 0.2 20

OSHA CSI

GC/FIDA $56

Benzyl Alcohol

100-51-6

T-01

Charcoal, 226-0110 - 24 0.01 - 0.2 20

NIOSH 1402M

GC/FIDD $56

T-95

XAD-7, 226-95

TWA 24

STEL 4.5

TWA 0.02- 0.1

STEL 0.3 2

OSHA 32M

HPLCK $116

Benzyl Chloride

100-44-7

T-01

Charcoal, 226-016 - 50 0.01 - 0.2 5

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0272 7.5

NIOSH 1003M

GC/FIDA $56

Benzylchloroformate

501-53-1

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 5

AIHAJ 12/1986,

pp.742-746

GC/FID

NN $77

Store media and samples cold, ship samples cold overnight.

Samples must arrive at lab within 10 days of sampling.

Beryllium

7440-41-7

C-05

MCEF, 37mm, 0.8um, 3PC200 - 2000 1.0 - 4.0 0.005

NIOSH 7300M

ICP/MST $46

Not appropriate for monitoring “high-fired” beryllium

oxide. When monitoring “high-fired” beryllium oxide (such

as manufactured for use in ceramics in electronic

Applications, and in lasers), contact the lab prior to

sampling. The combination of digestion

technique/analytical technique/ method sensitivity must

be carefully chosen to obtain accurate results. Contact lab

for further information.

C-05

MCEF, 37mm, 0.8um, 3PC200 - 2000 1.0 - 4.0 0.05

OSHA ID125M

ICPEE $40

This approach is suitable for analysis of high-fired beryllium

oxide.

Beryllium

Wipe

7440-41-7

K-07

Ghost Wipe Kit100 cm2 - 0.01

NIOSH 7102M

GFAAT $51

This approach is NOT suitable for analysis of high-fired

beryllium oxide.

K-07

Ghost Wipe Kit100 cm2 - 0.1

OSHA ID125M

ICPEE $40

This approach is suitable for analysis of high-fired beryllium

oxide.

Biphenyl

92-52-4$-

See Diphenyl.

Bis (Chloromethyl) Ether

(BCME)

542-88-1

T-89

TCP-treated XAD- 4,

226-89

TWA 20

STEL 4.5 0.05-0.3 0.014

Proprietary,

IHGC-P011

GC/ECD

NC $153

Immediately after sampling heat treat tube(s) at 75°C for 45

minutes. Wrap in aluminum foil to protect from light.

Chloromethyl Methyl Ether can be determined on same

tube.

Bismuth

1304-82-1C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 2

NIOSH 7300M

ICPT $40

Bisphenol A

80-05-7

C-06

GFF, 37mm, 1um, 3PC300 1.6 2

NIOSH PCAM 333

HPLCN $116

Store samples in freezer. Ship cold overnight.

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Boric Acid

(measured as Boron)

10043-35-3

C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 12

NIOSH 7300M

ICP-OEST $40

Samples are acid digested and tested for boron; equivalent

H3BO3 is calculated mathematically. Test is not specific for

boric acid.

Boron

7440-42-8C-05

MCEF, 37mm, 0.8um, 3PC50 - 500 1.0 - 3.0 2

NIOSH 7300M

ICPT $40

Bromine

7726-95-6

IMP-09

Impinger,

NaH- CO3/ Na2CO3

80 - 240 0.5 7.5OSHA ID 108

ICNC $69

Impinger solution available from laboratory.

C-16

Ag/PTFE, Cl2/Br2 Sampler,

25mm, 3PC

15 - 360 0.3 - 1.0 5.0NIOSH 6011

ICAA $69

Preferred method. Precleaning of filter required prior to

shipment. Cassette has short shelf life. Avoid direct sunlight

on filter during or after sampling. Chlorine can also be

measured as well as bromine.

Bromoethane

74-96-4- $-

See Ethyl Bromide

Bromoform

75-25-2

T-01

Charcoal, 226-014 - 70 0.01 - 0.2 20

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0293 30

NIOSH 1003M

GC/FIDA $56

Bromomethane

74-83-9$-

See Ethyl Bromide

1-Bromopropane

106-94-5T-01

Charcoal, 226-0112 Max 0.2 Max 0.5

NIOSH 1011M

GC/FIDA $56

The larger charcoal tube 226-09 may be used for greater

capacity at higher concentrations.

Synonym: n-Propyl bromide

M-3500

3M POVM, 3500Up to 8 hours 0.032 1.5

NIOSH 1011M

GC/FIDA $56

3M 3520 is recommended for 8-hour samples collected at

high humidity (>80%).

BTEX Profile

N/A T-01Charcoal, 226-01

5 - 15 0.05 - 0.2See

comments

NIOSH 1501

GC/FIDA $127

Profile includes Benzene (LOQ = 2 ug), Ethyl Benzene (LOQ

= 5 ug), Toluene (LOQ = 5 ug), Xylene (LOQ = 5 ug), Total

Hydrocarbons as Hexane (LOQ = 20 ug).

M-01 SKC POVM,

575-001Up to 8 hours Various

See

comments

NIOSH 1501M

GC/FIDA $127


= 10 ug), Toluene (LOQ = 10 ug), Xylene (LOQ = 10 ug), Total

Hydrocarbons as Hexane (LOQ = 40 ug).

M-3500

3M POVM, 3500Up to 8 hours Various

See

comments

NIOSH 1501M

GC/FIDA $127


= 7.5 ug), Toluene (LOQ = 7.5 ug), Xylene (LOQ = 7.5 ug),

Total Hydrocarbons as Hexane (LOQ = 30 ug).

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1,3-Butadiene

106-99-0

T-73

TBC-Treated charcoal,

226-73

3 Max 0.01 - 0.05 2OSHA 56

GC/FIDA $56

Preferred method. Store collected samples under

refrigeration, and ship refrigerated overnight. Samples are

stable at least 17 days if stored cold.

T-09

(2) Charcoal, 226-095 - 25 0.01 - 0.5 8

NIOSH 1024

GC/FIDI $56

Two 226-09 tubes in series; cap separately after sampling.

Ship cold overnight, store in freezer after sampling.

M-3520

3M POVM 3520, 2-stageUp to 8 hours 0.0428 3

NIOSH 1024M

GC/FIDI $56

1,3-Butanediol

107-88-0- $-

See 1,3-Butylene Glycol

1,4-Butanediol

110-63-4- $-

See 1,4-Butylene Glycol

n-Butanol

71-36-3- $-

See n-Butyl alcohol

Sec-Butanol

78-92-2- $-

See sec-Butyl Alcohol.

t-Butanol

75-65-0- $-

See tert-Butyl alcohol.

2-Butanone

78-93-3- $-

See Methyl Ethyl Ketone.

2-Butoxyethanol

111-76-2

T-01

Charcoal, 226-011 - 10 0.01 - 0.1 20

NIOSH 1403M

GC/FIDE $56

Also known as Butyl Cellosolve, Ethylene Glycol Monobutyl

Ether, and Dowanol EB

M-3500

3M POVM, 3500Up to 8 hours 0.0282 30

NIOSH 1403M

GC/FIDE $56

Also known as Butyl Cellosolve, Ethylene Glycol Monobutyl

Ether, and Dowanol EB

2-Butoxyethyl Acetate

112-07-2

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

OSHA 83

GC/FIDE $56

Also known as Butyl Cellosolve Acetate and Ethylene Glycol

Monobutyl Ether Acetate

M-3500

3M POVM, 3500Up to 8 hours 0.0243 30

OSHA 83M

GC/FIDE $56

Also known as Butyl Cellosolve Acetate and Ethylene Glycol

Monobutyl Ether Acetate

1-Butoxy-2-Propanol

5131-66-8-

See Propylene Glycol n-Butyl Ether

n-Butyl Acetate

123-86-4

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

T-81

Anasorb 747, 226-8110 0.03-0.2 1.1

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min 0.013 2.2

Proprietary,

IHGC-P029

GC/FID

A $77

M-3500

3M POVM, 3500Up to 8 hours 0.0316 30

NIOSH 1450M

GC/FIDA $56

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

s-Butyl Acetate

105-46-4

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0286 30

NIOSH 1450M

GC/FIDA $56

t-Butyl Acetate

540-88-5

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0294 30

NIOSH 1450M

GC/FIDA $56

n-Butyl Acrylate

141-32-2

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450M

GC/FIDA $56

Also see Acrylate Monomer Profile.

M-3500

3M POVM, 3500Up to 8 hours 0.0273 30

NIOSH 1450M

GC/FIDA $56

T-73

TBC-Treated charcoal,

226-73

1 - 12 0.01 - 0.05 20OSHA CSI

GC/FIDA $56

M-02

SKC POVM, 575-00230 min - 8 hours 0.012 2.5

Proprietary,

IHGC-P029

GC/FID

A $77

Recommended passive sampling method.

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.3

Proprietary,

IHGC-P029

GC/FID

A $77

n-Butyl Alcohol

71-36-3

T-01

Charcoal, 226-012 - 10 0.01 - 0.2 20

NIOSH 1401

GC/FIDC & A $56

M-3500

3M POVM, 3500Up to 8 hours 0.0343 30

NIOSH 1401M

GC/FIDC $56

sec-Butyl Alcohol

78-92-2

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.01-0.2

STEL 0.2 20

NIOSH 1401

GC/FIDC $56

M-3500

3M POVM, 3500Up to 8 hours 0.0348 30

NIOSH 1401M

GC/FIDC $56

t-Butyl Alcohol

75-65-0

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.01-0.2

STEL 0.2 20

NIOSH 1400

GC/FIDC $56

M-3500

3M POVM, 3500Up to 8 hours 0.0352 30

NIOSH 1400M

GC/FIDB $56

Butyl Carbitol

112-34-5- $-

See Diethylene Glycol Monobutyl Ether.

Butyl Carbitol Acetate

124-17-4- $-

See Diethylene Glycol Monobutyl Ether Acetate

Butyl Cellosolve

111-76-2- $-

See 2-Butoxyethanol.

Butyl Cellosolve Acetate

112-07-2- $-

See 2-Butoxyethyl Acetate.

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

n-Butyl Glycidyl Ether

2426-08-6

T-01

Charcoal, 226-0115 - 30 0.01 - 0.2 20

NIOSH 1616

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0270 30

NIOSH 1616M

GC/FIDA $56

t-Butyl Glycidyl Ether

7665-72-7

T-01

Charcoal, 226-0115 - 30 0.01 - 0.2 20

NIOSH 1616M

GC/FIDA $56

tert-Butyl Hydrazine

Hydrochloride, as

Particulate

7400-27-3

C-11

PVC, Preweighed, 37mm,

5um, 2PC

TWA 960

STEL 60 1-4 50

NIOSH 0500

Gravimetric$21

Not chemical specific.

tert-Butyl Hydroperoxide

75-91-2

…BHP

T-47-01

Silica Gel, 226-47-01

TWA 10

STEL 3

TWA 0.05-0.2

STEL 0.22

IN-HOUSE

GC/MSK $160

Samples are stable at least 9 days. Three (3) sample

minimum.

Butyl Isocyanate

111-36-4

K-20

GFF, 2PP-treated, C-1415-30 1.0 Max 0.4

OSHA Stopgap

HPLC/UVO $116

Sample open faced. Refrigerate media before and after

sampling. Ship cold by overnight delivery. Testing is for

both 2,4- and 2,6-TDI isomers. Media has 2-month shelf life

(stored cold). OSHA National Emphasis Program specifies

field desorption immediately after sampling; the K-20 kit

includes C-14 cassette, V-04 vial with 3mL 90/10 (v/v)

acetonitrile/dimethyl sulfoxide, tweezers(2), rack,

instruction set, SDS for solution. Contact lab for more

specifics.

N-Butyl Lactate

138-22-7

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.02-0.2

STEL 0.21

OSHA PV2080

GC/FIDE $77

Butyl Mercaptan

109-79-5

C-48

GFF, Hg Acetate-Treated,

37mm, 2PC,

SKC PN 225-9007

TWA 20

STEL 3 - 150 Max0.2 Max -

NIOSH 2542

GC/FPDNC

Call for

pricing

Store media cold before use. Protect samples from light.

Subcontracted to an outside laboratory. Samples stable at

least 3 weeks at 25ºC.

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Butyl Methacrylate

97-88-1

T-30-04

XAD-2, 226-30-041 - 8 0.05 - 0.1 20

NIOSH 2537M

GC/FIDDD $56 Also see Acrylate Monomer Profile.

T-81

Anasorb 747, 226-81TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.3

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002TWA 8 hr (Max)

STEL 15 min 0.01 2.6

Proprietary,

IHGC-P029

GC/FID

A $77 Recommended passive sampling method.

n-Butyl Phthalate

84-74-2- $- See Dibutyl Phthalate.

n-Butylamine

109-73-9

T-30-18

NITC-Treated XAD-2,

226-30-18

3 - 30 0.01 - 1.0 4NIOSH 2540M

HPLCN $116

Store media cold before sampling. Samples stable at

ambient temperature for at least 15 days.

1,3-Butylene Glycol

107-88-0T-57

GFF/XAD-7 OVS, 226-571 - 20 0.01 - 0.10 20

NIOSH 5523

GC/FIDK $77 Also see Glycol Profile.

1,4-Butylene Glycol

110-63-4T-57

GFF/XAD-7 OVS, 226-5760 - 1000 0.5 - 1.0 80

NIOSH 5523M

GC/FIDK $77

Butyraldehyde

123-72-8

T-119


226-119

2 - 30 0.2 - 1.0 0.8TO-11

HPLCN $116

Refrigerate before and after sampling and ship overnight.

Ozone may interfere - use ozone scrubber in known ozone

contaminated areas. Any ketone or aldehyde will react with


concentrations of acetone or MEK will compete with the


interferences. Media contains residual acetonitrile which

could interfere with acetonitrile monitoring.

gamma- Butyrolactone

96-48-0

T-01

Charcoal, 226-0110 Max 1 Max 20

OSHA Stopgap

GC-FIDE $56

Cadmium

7440-43-9

C-05

MCEF, 37mm, 0.8um, 3PC 800 - 1000 1.0 - 3.0 0.5NIOSH 7300

ICPT $40

C-05

MCEF, 37mm, 0.8um, 3PC 800 - 1000 1.0 - 3.0 0.025NIOSH 7300M

ICP/MST $46

Calcium

7440-70-2C-05

MCEF, 37mm, 0.8um, 3PC100 - 1000 1.0 - 3.0 2

NIOSH 7300

ICPT $40 Consult TLV booklet for form of analyte.

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Camphor

76-22-2

T-01

Charcoal, 226-011 - 25 0.01 - 0.2 10

NIOSH 1301

GC/FIDH $56

M-3500

3M POVM, 3500Up to 8 hours 0.0214 15

NIOSH 1301M

GC/FIDH $56

Caprolactam

Vapor

105-60-2

T-57

GFF/XAD-7 OVS,

226-57

100 1 Max 10OSHA PV2012

HPLCK $116 Vapor analysis only.

Caprolactam

Vapor + Particulate

105-60-2

T-57

GFF/XAD-7 OVS,

226-57

100 1 Max 10OSHA PV2012

HPLCK $160

Filter (particulate) and sorbent beds (vapor) are all tested

and reported separately; a cumulative result for all three

sections is also reported.

Carbitol (DGMEE)

111-90-0- $- See Diethylene Glycol Monoethyl Ether

Carbitol Acetate

112-15-2- $- See Diethlylene Glycol Ethyl Ether Acetate

Carbon Black

(as Total Particulate)

1333-86-4

C-11

PVC, Preweighed, 37mm,

5um, 2PC

100 - 960 1.0 - 2.0 50NIOSH 0500

GravimetricNC $21

Any and all other particulates will be a positive interference

with the gravimetric analysis. More specific analysis for

Carbon Black by OSHA ID196 is available as a subcontracted

analysis. Also see the entry for Elemental Carbon.

Carbon Dioxide

124-38-9Call Lab 3.5 - 500

OSHA ID172

GC/TCDNC $- Analysis is subcontracted.

Carbon Disulfide

75-15-0

T-44 & T-01

in series Drying Tube,

226-44, preceding

Charcoal, 226-01

25 Max 0.2 MaxNIOSH 1600

GC/FPDNC

Call for

pricing

Precede the charcoal tube with a drying tube (PN 226-44).

Store and ship cold, with drying tube still attached.

Subcontracted to outside laboratory.

Carbon Tetrabromide

558-13-4T-93

XAD-4, 226-93

TWA 10

STEL 3

TWA 0.02-0.2

STEL 0.2

OSHA Stopgap

GC/ECDNC

Call for

pricing

Important Note: Contact the laboratory before sampling in

order to allow time for set up. Subcontracted to outside

laboratory.

Tetrachloromethane

56-23-5

T-01

Charcoal, 226-013 - 150 0.01 - 0.2 20

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0302 30

NIOSH 1003M

GC/FIDA $56

Carbonyl Chloride

75-44-5- $- See Phosgene

Catechol

575-001

T-95

XAD-7, 226-9524 Max 0.1 Max 30

OSHA Stopgap

GC/FIDA $56

Cellosolve

110-80-5- $- See 2-Ethoxyethanol

V01 06.2017

Toll Free: 800-888-8061



Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Cellosolve Acetate

111-15-9- $- See 2-Ethoxyethyl Acetate

Cerium Oxide

1306-38-3 C-05 MCEF, 37mm, 0.8um, 3PC

960-1920 2-4 2.5 ICP T $77Call to schedule analysis to ensure standard is in stock.

Three (3) sample minimum. Testing is for elemental cerium,

with mathematical calculation of cerian oxide.

Chlordane

57-74-9

T-30-16

GFF/XAD-2 OVS,

TABLE OF CONTENTS - Analytics CorpCustomer Service – x0 4. How to Use This Directory This...

Documents

Transcript of TABLE OF CONTENTS - Analytics CorpCustomer Service – x0 4. How to Use This Directory This...