Table of Content Introduction of heat exchanger. Design of Coolers.
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Transcript of Table of Content Introduction of heat exchanger. Design of Coolers.
Table of Content
• Introduction of heat exchanger.
• Design of Coolers.
Continue
• Introduction of fixed bed reactors.
• Design of reactors.
Heat exchanger
• Heat exchanger is a device designed to transfer heat from one fluid (liquid or gases) to another where the two fluids are physically separated.
• In our design we assumed that the cooler which used is a shell and tube heat exchanger.
• The advantages of shell and tube heat exchanger are:
1. The configuration gives a large surface area in a small volume.
2. Can be constructed from a wide range of materials.3. Easily cleaned.
Assumptions:
1- Use shell and tube heat exchanger, two shell and four tube passes.
2- Assume the outer, the inner diameter and the length of the tube.
Design procedure of shell and tube heat exchanger:
1. Heat load ,(kW)
2. Log mean Temperature, (˚C)
Where - Inlet shell side fluid temperature (˚C). - Outlet shell side fluid temperature (˚C). - Inlet tube side temperature (˚C).- Outlet tube temperature (˚C).
)(
)(ln
)()(
12
21
1221
tT
tTtTtT
Tlm
TmCQ ph
3.Provisional Area, (m2)
Where - True temperature difference.
- ( Temperature correction factor)
4. Area of one tube, m2. Where-Outer diameter (do), (mm)
-Length of tube (L), (mm)
- Number of tubes = provisional area / area of one tube
mTU
QA
mT
lmtm TFT tF
LdA o
5. Overall heat transfer coefficient, W/m2 oC.
Where- Outside coefficient (fouling factor).- Inside coefficient (fouling factor).
6. Bundle diameter.
Where- Outside diameter (mm).- Number of tubes.-K1 & n1 are constant.
ii
o
id
oi
o
odo hd
d
hdi
d
kw
d
dLNd
hhU
11
2
1110
0
odh
idh
0d
tN
7. Shell diameter.
8. Shell thickness.
Where- t: shell thickness (in).
- P: internal pressure (psig).
- ri: internal radius of shell (in).
- EJ: efficiency of joints.
- S: working stress (psi).
- Cc: allowance for corrosion (in).
ClearanceDD bs
cJ
i CPSE
t
6.0
Pr
Results
Equipment name Cooler
Objective To cool the feed stream and prepare
it to inter the separator Equipment Number E-103
Type Shell and tube heat exchanger Location After the reactor (CRV-100)
Utility Sea water
Material of construction Carbon steel
Insulation Quartz wool – Glass wool Shell Side Inlet temperature (oC) 200
Shell Side Outlet temperature (oC) 40
Tube Side Inlet temperature (oC) 35
Tube Side Outlet temperature (oC) 94.439
Heat load (kW) 1169.316
Overall heat transfer coefficient (W/m2 oC) 300
LMTD (oC) 32.972
Number of tubes 470
Tube length (m) 4.88
Tube diameter (m) 0.63354
Heat Exchanger area (m2) 144.161
Thickness (mm) 18.5
Shell diameter (m) 0.69554
Number of tube Rows 4
Cost $ $93,200
Reactors• In our plant, the reactor used is catalytic fixed bed reactor.
• catalytic fixed bed reactor is a cylindrical tube, randomly filled with catalyst particles which may be spheres or cylindrical pellets to optimize flow distribution patterns and to alternate the speed of reaction.
• It is used very commonly in industry because it has many valuable features such as:
1. It gives the highest conversion.2. Efficient heat transfer.3. Temperature uniformity.4. Less severe pressure drop.
Design Procedure of Catalytic Fixed Bed Reactor
For CH4+CO22CO+2H2
1. Get reaction rate constant (k).
2. Calculate the concentration for carbon dioxide.
3. Calculate the rate of reaction.
4. Calculate the weight of catalyst.
AA kCr
0A
A
F
r
dW
dx
5. Calculate the volume of reactor.
6. Assume the ratio of length to diameter of reactor (L / D).
7. Calculate the height of reactor.8. Calculate the flow rate of heating the
reactor. 9. Calculate the thickness of reactor.10. Calculate the cost.
*)1()(
WcolumnV
ResultsEquipment name reactor
Objective To convert CO2 and CH4 to CO
Equipment Number ERV-100 (flow sheet 1)
Type Catalytic fixed bed reactor
Location After Furnace F-100
Material of construction Carbon steel
Insulation Quartz wool – Glass wool
Operating temperature (oC) 800
Operating pressure (psia) 14.696
Feed Flow Rate (mole/s) 52.174
Conversion 92.22
Results
Weight of Catalyst (Kg) 1000
Height of Bed/s (m) 1.9409
Volume of reactor (m3) 0.4187
Catalyst Type Ni-Al2O3
Catalyst Density (Kg/m3) 3980
Reactor Height (m) 3.4261
Reactor Diameter (m) 0.4852
Reactor thickness (m) 10
CO2 Flow rate for heating reactor kg/h 13631.388
Cost $ $32300
ResultsEquipment name reactor
Objective To convert CO2 and CH4 to CO
Equipment Number ERV-100 (flow sheet 2)
Type Catalytic fixed bed reactor
Location After Furnace F-100
Material of construction Carbon steel
Insulation Quartz wool – Glass wool
Operating temperature (oC) 800
Operating pressure (psia) 14.696
Feed Flow Rate (mole/s) 52.735
Conversion 91.58
Results
Weight of Catalyst (Kg) 1000
Height of Bed/s (m) 1.9409
Volume of reactor (m3) 0.4187
Catalyst Type Ni-Al2O3
Catalyst Density (Kg/m3) 3980
Reactor Height (m) 3.4261
Reactor Diameter (m) 0.4852
Reactor thickness (m) 10
CO2 Flow rate for heating reactor kg/h 13792.75
Cost $ $32300
Equilibrium Reactor 2 (flow sheet 2)
CO+2H2CH3OHAssumption:
• Set Hydrogen as a limiting reactant.
• The porosity of the catalyst Φ=0.3
• the ratio of length to diameter (L/D)=4
Design Procedure of Catalytic Fixed Bed Reactor
1. Get reaction rate constant (k).
2. Calculate the concentration.
3. Calculate the rate of reaction.
4. Calculate the weight of catalyst.
0A
A
F
r
dW
dx
)(AB
CAA CKeqC
CCkr
5. Calculate the volume of reactor.
6. Assume the ratio of length to diameter of reactor (L / D).
7. Calculate the height of reactor.8. Calculate the flow rate of cooling the
reactor. 9. Calculate the thickness of reactor.10. Calculate the cost.
*)1()(
WcolumnV
ResultsEquipment name reactor
Objective To convert CO and H2 to methanol
Equipment Number ERV-101 (flow shee2)
Type Catalytic fixed bed reactor
Location After cooler E-101
Material of construction Carbon steel
Insulation Quartz wool – Glass wool
Operating temperature (oC) 250
Operating pressure (psia) 1469.6
Feed Flow Rate (mole/s) 229.34
Conversion 30.11
Results
Weight of Catalyst (Kg) 2323.88
Height of Bed/s (m) 3.24459
Volume of reactor (m3) 1.956128
Catalyst Type CuO/ZnO/Al2O3
Catalyst Density (Kg/m3) 1980
Reactor Height (m) 5.055742
Reactor Diameter (m) 0.811148
Reactor thickness (m) 57.9
H2 Flow rate for cooling reactor kg/h 13792.75
Cost $ $95,300
Design Procedure of Catalytic Fixed Bed Reactor
CO+CH3OHCH3COOH1. Get reaction rate constant (k).
2. Calculate the partial pressure for CO and CH3OH.
3. Calculate the rate of reaction.
4. Calculate the weight of catalyst.
0A
A
F
r
dW
dx
BAA PkPr
5. Calculate the volume of reactor.
6. Assume the ratio of length to diameter of reactor (L / D).
7. Calculate the height of reactor.8. Calculate the flow rate of cooling the
reactor. 9. Calculate the thickness of reactor.10. Calculate the cost.
*)1()(
WcolumnV
ResultsEquipment name reactor
Objective To convert CO and CH3OH to CH3COOH
Equipment Number CRV-101 (flow sheet 1)
Type Catalytic fixed bed reactor
Location After cooler E-100
Material of construction Carbon steel
Insulation Quartz wool – Glass wool
Operating temperature (oC) 200
Operating pressure (psia) 517
Feed Flow Rate (mole/s) 152.7
Conversion 90
Results
Weight of Catalyst (Kg) 451.0188
Height of Bed/s (m) 1.7925
Volume of reactor (m3) 0.3298
Catalyst Type CH3I
Catalyst Density (Kg/m3) 2278.9
Reactor Height (m) 3.24066
Reactor Diameter (m) 0.4481
Reactor thickness (m) 13.1
H2 Flow rate for cooling reactor kg/h 7999.6617
Cost $ $12,800
ResultsEquipment name reactor
Objective To convert CO and CH3OH to CH3COOH
Equipment Number CRV-100 (flow sheet 2)
Type Catalytic fixed bed reactor
Location After cooler E-102
Material of construction Carbon steel
Insulation Quartz wool – Glass wool
Operating temperature (oC) 200
Operating pressure (psia) 515
Feed Flow Rate (mole/s) 185.26
Conversion 90
Results
Weight of Catalyst (Kg) 350.8217
Height of Bed/s (m) 1.6485
Volume of reactor (m3) 0.08382
Catalyst Type CH3I
Catalyst Density (Kg/m3) 2278.9
Reactor Height (m) 3.06067
Reactor Diameter (m) 0.41213
Reactor thickness (m) 12.3
H2 Flow rate for cooling reactor kg/h 4102.094
Cost $ $11,200
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