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NATAS Symposia, October 2000

Plenary Lecturers

Mettler Award Lecturers

1. Characterization of Polymers by Thermal Analysis and Rheology

Paper Title Author(s)

High Performance DSC - High Scanning Rate DSC: Applications to Polymers (Invited

Lecturer)

Professor Vincent B. F. Mathot,Katholieke Universiteit v

Leuven

Dynamics of Reversible Melting Revealed from Frequency Dependent Heat Capacity Schick, C., A. Wurm, S. Adamovsky

Structure-Property Relationships in High-Strain P (VDF-TrFE) Electrostrictors as Revealed

by Thermal Analysis

Ramotowski, T., A. Amin, G. Kavarnos, R. Ting

Advances in Polymer On-line Capillary Rheology Nelson, B.

A Study of the Impact of Blend Composition on the Bound Rubber Formed in Elastomer

Blend Systems by Thermogravimetric Analysis

Woolard, C.

Use of Several Thermal Analysis Techniques on a Hypalon Paint Coating for the Solid Rocket

Booster (SRB) of the Space Shuttle

Wingard, C.

Measuring the Fiber Shrinkage Using DMTA Suwardie, J.

Thermophysical Properties of a Thermal Interface Material He, Y.

High Quality Heat Capacity Measurements at Different Frequencies of Temperature

Modulation

Wunderlich, B.

Torque and Normal Force Measurements to Characterize the Rheological Response of

Concentrated Polymer Solutions

McKenna, G., V. Soulivong, X. Shi

Method for Analysis of Dynamic Mechanical Thermal Analysis Data Using the Havriliak-

Negami Model

Szabo, J., I. Keough

Verification of Crystallization and Crystal Perfection Processes Seen in PET by MDSC Thomas, L., S. Aubuchon

Characterization of Polymer Blends by MDSC Thomas, L., S. Aubuchon

Ionic Aggregation Effect on the Crystallisation Behavior of Ionomeric Systems Gao, Y., N.Choudhury, N. Dutta, J. Matisons

Thermal Laser-Interferometric Creep Rate Spectroscopy: High Resolution Analysis of

Relaxations in Polymeric Materials and Brittle Solids

Bershtein, V., N. Peschanskaya, P. Yakushev

The Anomalies of Segmental Dynamics in Complex Polymer Systems as Studied via

Combined CRS/DSC Approach

Bershtein, V., V. Egorov, L. Egorova, A. Fainleib, P. Pi

P. Sysel, P. Yakushev

Thermal Transitions in the PVDF Observed by DRS, DSC, DMA and TSDC Techniques Korzhenko, A., F. Beaume, B., Ernst

Generalized and Localized Heating in Micro-Thermal Anaysis Reading, M., D. Price, T. Lever`

Problem Solving with Mico-Thermal Analysis Lever, T., D. Price, M. Reading

Rheological and Dielectric Thermal Analysis of Failed Engine Oils Riga, A.

Application of Micro-Thermal Analysis on Polymer Blend Xie, W., Z. Gao, W. Pan

Phase Transformations in Nano-Confined Environments Cheng, S., L. Zhu, Q. Ge, R. Quirk, E. Thomas, B. Hisao

Yeh, B. Lotz

Temperature Modulated Dynamic Load TMA of Fibers Foreman, J., R. Riesen

Enhanced Characterization of Polymeric StepScan DSC Sichina, W.

Surface Finish of Injection Molded Materials by Micro-Thermal Analysis Provotas, M., S. Edwards, N.R. Choudhury, J. Matisons

Z.D. Cheng, The University of Akron

2000 To Be Announced

1999 The Role of Metastable States in Polymers: Concepts, Principles, and Experimental Observations, Professor Stephen

The Role of Thermal Methods in the Characterisation of Pyrotechnic Systems, Professor Ted Charsley, University of Huddersfield

Temperature-Modulated DSC: Applications and Interpretation, Professor Sindee Simon, Texas Tech University

Decomposition of Solids Accompanied by Melting-Bawn Kinetics, Professor Michael Brown, Rhodes University

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2. Hazard Evaluation by Thermoanalysis and Rheology


Introduction of the New DRC Differential Reaction Calorimeter Le Parlouer, P., C. Mathonat, J.L. Daudon, X. Le Tacon

The Versatile VSP2: A Tool for Adiabatic Thermal Analysis and Vent Sizing Applications Askonas, C., J. Burelbach, J. Leung

Advanced Reactive System Screening Tool Burelbach, J.

Phenomenon of Autocatalysis in Decomposition of Energetic Chemicals Chervin, S., G. Bodman

Thermal Analysis of Polymer Flammability Lyon, R., R. WaltersSafe Process Development from Reaction Hazards Testing Using Thermoanalytical

Techniques

Leggett, D.

DSC Hazard Evaluation of Thermally Unstable Materials Blaine, R., G. Dallas, T. Kelly

Understanding the Large Scale Chemistry of Ethyl Diazoacetate Via Reaction Calorimetry Clark, J., A. Shah, J. Peterson

The Interpretation of Thermal Analytical Data in the Determination of a Safe Operating

Envelope for the Pilot Plant Scale-Up of Chemical Processes

Tuma, L.

Thermal Hazard Assessment of Emulsion Explosives Jones, D., P. Lightfoot, R. Fouchard

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3. Polyolefin Characterization by Thermal Analysis and Rheology


Analytic Rheology of Polymer Melts (Invited Lecturer) Professor Ron Larson, University of Michigan

The Thermodynamic and Structural Properties of Metallocene-Type Random Ethylene

Copolymers

Simanke, A., R. Alamo

Kinetic and Morphological Studies of a Series of Narrow Propylene-Ethylene Copolymers Chatterjee, J., A. Little, R.G. Alamo

Phase Behavior of Injection Molded B- Nucleated Polypropylenes Varma-Nair, M., R. Kolb, P. Meka, A. Faldi

Melting and Crystallization of Low Molecular Weight Polyethylene by Calorimetry Pak, J., B. WunderlichDetermination of the Processing History of PP Fibers by Thermal Analysis Bhat, G., A. Saraf

Reversible and Irreversible Heat Capacities of Poly{Carbonyl(Ethylene-Co-Propylene)} by

Temperature-Modulated Differntial Scanning Calorimetry, TMDSC

Pyda, M., B. Wunderlich

Thermal Decomposition of Base Oils by Conventional, Isothermal and Modulated TGA. Gamlin, C., N. Choudhury, N. Dutta, J. Matisons

Crystallization, Melting and Morphology at Ambient and High Pressures of Homogeneous

Ethylene Copolymers with High Comonomer Contents

Eynde, S., V. Mathot, G. Hohne, H. Reynaers

Structure and Properties of Polypropylene Polymers in a Spunbonding Process Bhat, G., R. Nanjundappa, R. Kotra, M. Kannadaguli

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4. Pharmaceutical Applications of Thermal Analysis


Recent Advances in Pharmaceutical Thermal Analysis (Invited Lecturer) Professor Duncan Craig, The Queen's University of Belf

Utilization of Differential Scanning Calorimetry for Pharmaceutical Crystal Form

Quantitation

Vitez, I.

TG,TG/MS: Applications to Determination of Residual Moisture in Pertussis Vaccine and

Other Freeze-Dried Biological Products

May, J.

Volatization, Evaporation & Vapor Pressure Studies Using a Thermobalance Price, D.A Comparative Method for Developing Vapor Pressure Curves Based on Evaporation Data

Obtained From a Simultaneous TGA-DTA Unit

Phang, P., D. Dollimore, S. Evans

The Use of Benzoic Acid as a Calibration Material in Thermal Analysis Wright, S., P.Phang, D. Dollimore, K. Alexander

Kinetic Study of the Drug Acetazolamide Using Thermogravimetry Burnham, L., D. Dollimore, K. Alexander

A Study of the Evaporation of Pentadecanoic Acid Using Simultaneous TG/DTA Shen, L., K. Alexander, D. Dollimore

A Study of the Evaporation of a Fragrance Component Using a Simultaneous TG/DTA Unit Sorokina, T., K. Alexander, D. Dollimore

A Stability Study of Drug Excipients and Their Effect on the Drug Salsalate Using Different

Physical Methods

Shulga, O., D. Dollimore, D. Alexander

Thermal Analysis of the Evaporation of Compounds used in Aromatherapy Hazra, A., D. Dollimore, K. Alexander

Tableting of Nicotinic Acid in the Presence of Spray Dried Lactose, Pregelatinized Corn

Starch and Magnesium Stearate

Menon, D., D. Dollimore, K., Alexander

Calculation of Vapor Pressure Curves for Hydroxy Benzoic Acid Compounds UsingThermogravimetry

Chatterjee, K., D. Dollimore, K. Alexander

The Kinetics of Decomposition of Magnesium Carbonate Hydroxide Hydrate Khan, N., D. Dollimore, K. Alexander

Study of Protein Stability and Denaturation Kinetics by Differential Scanning Calorimetry Young, P., P. Phang, D. Dollimore, C. Schall

Thermal Stability of Folic Acid and Associated Excipients Vora, A., M. Samtani, D. Dollimore, K. Alexander

A Study of the Dehydration of Magnesium Sulfate Heptahydrate MgSO4.7H2O Using a

Simultaneous TG/DTA Unit

Khan, F., D. Dollimore, K. Alexander

Factors Affecting the Stability of Ascorbic Acid Delineated Using Thermal Analysis

Techniques

Alexander, K., C. Gu, D. Dollimore

New Enhancements in the Area of High Resolution Differential Scanning Calorimetery (DSC) Ferrara, J., V. Reddy, R. Byrne, N. Nakamura, R. Kinos

Studies of Cimetidine Pre-Formulated and Tablets for TG and DSC Coupled to the

Photovisual System

Macedo, R.O., F. dos Santos Sousa

Thermal Characterization of the Quercetin and Rutin Flavonoids Macedo, R.O., F. dos Santos Sousa

Quality Control of the Thiabendazole Pre-Formulated and Tablets for TG and DSC Coupled

to the Photovisual System

Macedo, R.O., F. dos Santos Sousa

Freeze Drying Modeled by MDSC Aubuchon, S., L. Thomas

Characterisation of Spray Dried and Micronised Salbutamol Sulphate by Modulated

Temperature DSC

Murphy, J., D. Craig, A. Hasnain, M. Vemuri

Quality and Disintegration Properties of Drugs and Excipients by Thermal Analytical

Techniques

Riga, A., H. Griffith, Z. Gao, WP Pan, R. Collins

The Effect of Annealing on the Glass Transition Region of Sucrose Solutions Kett, V., D. Craig, D. Deutsch

A Calorimetric Study of Modified Soy Proteins via Enzyme Catalyzed Reactions. Effect of

Protease Specificity.

Briones-Martinez, R., C. Fernandez and M. I. Cortes-

Vazquez

Thermal Studies of Albizia inopinnataCrude Extract in the Presence of Cyclodextrin and

Aerosil by TG and DSC Coupled to the Photovisual System

Dantas de Medeiros, A.C., I. Almeida de Medeiros, R. O

MacedoCharacterization of Pharmaceutical Materials by Thermal Analysis Sichina, W.

A Novel Technique for Characterizing Polymorphs by DSC Drayton, R.A.

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5. Thermal Analysis in Environmental Applications


Utility of MDSC in Monitoring Solvent-Based Coating Cure Thomas, L., S. Aubuchon

Analysis of Crystallinity in Polyolefin Underground Storage Tanks by MDSC Aubuchon, S., L. Thomas

Thermal Reduction of Steel-Making Secondary Materials II. Electric-Arc-Furnace Dust Mikhail, S., A.M. Turcotte

Kinetic Parameters of Regeneration of Coked Alumina by TG Fernandes, V.J., Araujo, A.S., Fernandes, G.J.T.

Characterization of Engine Oil Volatilities Using the TGA Noack Test Sichina, W.

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6. Modern Applications of Solutions Calorimetry


Thermal Characterization of Second Tier Configurational Excitations in Glassforming Liquids

(Invited Lecturer)

Professor Austin Angell, Arizona State University

Measuring Solubility Data of Cycloalkanes by Differential Scanning Calorimetry Young, P., D. Dollimore, C. Schall

Single Seed Calorimetry Analysis of Corn Flour Aggarwal, P.

Recent Advances in Calorimetry for Intra- and Inter-Molecular Analysis of Biomolecules Chellani, M .

Calorimetric Studies of Molecular Recognition Flowers, R.

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7. Thermal Analysis of Explosives, Propelants and Pyrotechnics


Isoconversional Kinetic Analysis of the Thermal Decomposition of the High Explosive NTO Long, G., B. Brems, C. Wight

A Competition Between Vaporization and Liquid State Decomposition for the High

Explosive RDX

Long, G., S. Vyazovkin, B. Brems, C. Wight

Thermal Decomposition of Composite HMX/HTPB Propellant Peterson, J., C. Wight

Kinetic Analysis of TA Data: Getting the Error Bars Right Wight, C., S. Vyazovkin

The Use of TA Data in Combustion Simulations: Does the Choice of Reaction Model Makeany Difference?

Wight, C., J. Wang

Characterization of a Microencapsulated Marking Agent for Explosives by TGA Mintz, K.

A Comparison of the Thermal Decomposition of Nitramines and Difluoroamines Oxley, J., J. Smith, J. Zhang

Critical Ignition Termperature Pickard, J.

Thermal Characterization of Passivated Aluminium Nanopowder Jones, D., P. Brousseau, R. Fouchard, A.M. Turcotte, Q

Kwok, P. Lightfoot

Thermal Properties of KDNBF, A Primer for Explosives Jones, D., R. Fouchard, A.M. Turcotte, P. Lightfoot, Q.

Kwok

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10. Applications of Thermal Conductivity Techniques


Thermal Conductivity of PTFE and PTFE composites Price, D.M., M. Jarratt

Thermal Conductivity Imaging Using the Atomic Force Microscope Price, D.M., M. Reading, A. Hammiche, H.M. Pollock

Cure Monitoring by Thermal Conductivity and Correlations to DSC Chandler, C., Mathis, N.

Thermal Effusivity as a Predictive Delamination Measurement Chandler, C., Mathis, N., Scholl, R.

Transient Plane Source Technique - Applications in Electronic Materials Dixon, C.

Laser Flash Diffusivity Measurements of Filled Adhesive Effective Thermal Conductivity and

Contact Resistance Using Multilayer Methods Campbell, R.C., S.E. SmithRelationship of Dielectric Cure State to Thermal Conductivity and Thermal Diffusivity of

Epoxy Resin

Shephard, D.D., S.E. Smith

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11. Polymer Degradation by Thermal Analysis


Use of a Simple CCD Camera for Simultaneous DSC - Chemiluminescence and Multiple

Sample Degradation Studies

Woo, L., C. Sandford, H. Blom, M. Ling, S. Ding

Kinetic Study of Stabilizing Effect of Oxygen on Thermal Degradation of Poly(methyl

methacrylate)

Peterson, J., S. Vyazovkin, C. Wight

Evolved Gas Collection from a Thermogravimetric Analyser and Identification by Gas

Chromatography - Mass Spectrometry

Lever, T., D. Price

Interpretation of Isothermal TGA: Modeling the Effects of Diffusion Rdissi, A., S. SimonImpact of Initiator Characteristics on the Thermal Stability of Vinylidene Chloride

Copolymers

Howell, B.A., Plover, D.E., Hahnfield, L.J., Kling, S.M.

Mounts, M.L.

Kinetic Parameters of Polymer Degradation by SAPO-37 Fernandes, V.J., Aranjo, A.S., Fernandes, G.J.T., Matos

J.R., Ionashiro, M.

Thermal Stability of Vinyldene Chloride Polymers Produced by Suspension and Emulsion

Techniques

Howell, B.A., Plover, D.E., Hahnfield, L.J., Kling, S.M.

Mounts, M.L.

The Utility of Kinetic Analysis in the Determination of Reaction Mechanism Howell, B.A.

Monomers on the Thermal Stability of Vilyldene Chloride Polymers Howell, B.A.

Thermal Decomposition of Cycloadducts of Vinylnaphthalenes with Electron-Deficient

Dienophiles

Howell, B.A., Powers, J.J., Priddy, D.B.

Thermal Decomposition Characteristics of Structurally Diverse Polystyrenes Howell, B.A., Cui, Y., Priddy, D.B.

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12. Practical Use of ASTM Protocols in Thermal Methods


TGA Noack Method for Lubricating Oils Reddy, V., R. Byrne, O. Sakamoto

An "ASTM-like" Standard Test Method for the Composition and Wear of Cellulose-Based

Automatic Transmission Plates by Thermogravimetric Analysis and X-Ray Diffraction

Analysis

Riga, A.

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14. General Session


Portable Thermal Analyser: A New Calorimetric Concept Le Parlouer, P., L. Benoist, I. Chan

Characterizing Solid-Solid Interactions of Cycloalkanes by Differential Scanning Calorimetry

and X-Ray Powder Diffraction

Young, P., D. Dollimore, C. Schall

Concept of Variable Activation Energy: Why it just can't stay put? Vyazovkin, S.

Lead-Tin Solder Characterization by Differential Scanning Calorimetry Fleszar, M.

Recent Developments in DSC Software: Determining Kinetics and Thermodynamic

Parameters of Recycled Polyethylene Terephthalate

Cassel, R., L. Li

Micro Thermal Analysis Calibration and Repeatability Blaine, R., D. Slough, D. Price

Multi Frequency Heat Capacity Measurement by Different Types of Termperature Modulation Kamasa, P., M. Pyda, M. Merzlyakov, C. Schick, B.

Wunderlich

Advances to Dynamic Mechanical Analysis Foreman, J.

Tg and Cp Measurements on Perfluoropolyethers Siemens, R., R. Karis

High Scanning Rate DSC: A New Standard? Pijpers, T., E. van der Vegte, V. Mathot, B. Cassel

Thermogravimetric Evaluation of Flame Retardancy of Polyester/Sisal Composite Fernandes, V.J., Silva, D.R., Fonseca, V.M.

Thermal Techniques for Elucidating Polymorphic Information Drayton, R.A.

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15. Poster Session


Multi Frequency TMDSC Studies of Polymers - Benefits and Limitations Merzlyakov, M., C. Schick

Thermal Decomposition Properties of Polymer Fibers Lee, J., C. Hsu, K Cheng

A Study on the Thermal Behaviors of Uncalcined Ca(HP04)2PH20 and CaCO3 Mixture Lee, J., C. Hsu, K. Cheng

Thermal Properties and Firing Characteristics of the Zr/KCI04/Viton A Priming

Compositions

Lee, J., C. Hsu, K. Cheng

A Study on Devitrification and Nucleation of Calcium Phosphate Glass with Si3N4 Additive Lee, J., C. Hsu, K. Cheng

Estimated Shelf Life for Some Explosives Lee, J., C. Hsu, K. Cheng

Use of Several Thermal Analysis Techniques to Study the Cracking of Nitrile Butadiene

Rubber (NBR) Insulator on the Booster Separation Motor (BSM) of the Space Shuttle

Wingard, C.

Center for Thermal Analysis Vyazovkin, S.

Applications of DSC and RADEX on Thermal Hazard Analysis - Examples on Cumene

Hydorperoxide

Peng, D.J., Y.J. Yang, P.J. Wen, P.Y. Yeh, H.Y Hou and

C.M Shu

Emergency Relief System Design for A Reactor Contining Phthalic Anhydride Shu, C.M., K.H.Hu, P.J. Wen, P.Y Yeh, Y.J.Yang, H.Y

Hou, D.J. Peng

Thermal Decomposition of Cumene Hydroperoxide by Isothermal Microcalorimeter Hou, H.Y., C.M. Shu, Y.S Duh, D.J. Peng, Y.J. Yang

A New Instrument for Photo-Thermal Analysis Foreman, J., M. Zemo

Thermal Stability of Tobacco Using TG/DTG and DTA Longanezi, T., M. Campos, C. MotheThermal Analysis of Granite and Marble Industry Residue Filho, H., H. Polivanov, Em Barroso, C. Mothe

Thermal Characterization of DMNB, a Detection Agent for Explosives Jones, D., R. Fouchard, Q. Kwok, P. Lightfoot

Using an Adiabatic Calorimeter to Separate Catalytic and Self-Decomposition Reactions for

Hydrogen Peroxide in the Presence of Hydrochloric Acid

Yang, Y.J. et al.

Kinetic Study of Cashew Gum and Pine Gum by DSC Araujo, C., H. Mothe, C. Mothe

Deformation Calorimetric Studies of Polyolefin Adhesives and Polymers Gibson, M.T., V.V. Kolpe

Thermal Characterization of Eutectic Explosives Containing HNIW Yeh, T-F, H-P Liu

Thermal Behavior and Stability of UV Curable Adhesives for Microelectronics Assembly Tsang, Chito

Characterization of Thermal and Mechanical Behavior of Polyimide Films - A Product

Performance Evaluation

Tsang, Chito

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16. Cure and Properties of Thermosetting Materials


A Scalable Methodology for Thermal Analysis from Micro-to Macro-TA Using Thermoset

Composites (Invited Lecturer)

Professor James Seferis, University of Washington

Modulated Temperature DSC for the Characterisation of Cure and Properties of

Thermosetting Materials and Reacting Multi-phase Polymer Systems (Invited Lecturer)

Professor Bruno van Mele, Vrije Universiteit Brussel

Evaluation of Interphase Thermal Properties on Glass Fiber Composites Using Scanning

Thermal Microscopy

Tillman, M., B. Hayes, J. Seferis

Development and Characterization of a Thermosetting Resin for Universal Composite

Systems Using Thermal Analysis

Hayes, B., J. Seferis

Evaluation of High Performance Fibrous Systems in Honeycomb Applications Wu, Y., J. Seferis

New TMA Method for the Measurement of Polymerization-induced Shrinkage in

Photopolymers

Bair, H., M. Schilling, V. Colvin, A. Hale and N. Levino

Evolution of Viscoelastic Properties and Residual Stresses During Thermoset Cure Prasatya, P., G. McKenna, S. Simon

Thermal Analysis of Thermosetting Adhesives for Wood Riedl, B., B Park, Y. Bedard

Characterization of a Dielectric Thin Film for Flip Chip Packaging He, Y.

Evaluation of Adhesives for Pressure Sensor Applications Adhihetty, I., D. White, S. Petrovic

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