Study of a Single Effect Evaporator

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    ChE 30

    Chemical engineering laboratory - II

    Experiment No. Group No. 03 (A2)

    Name of the experiment:

    STUDY OF A SINGLE EFFECT EVAPORATOR

    Submitted by:

    Md. Hasib Al Mahbub

    Student Id: 0902045

    Level: 3; Term: 2

    Section: A2

    Date of performance:28/01/2014

    Date of submission:11/02/2014

    Partners Student Id.0902041

    0902042

    0902043

    0902044

    Department of Chemical Engineering.

    Bangladesh University of engineering and technology, Dhaka.

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    Summary

    The main objective of this experiment was to study, operate and obtain characteristics, to

    perform material and energy balance and to determine steam economy which denotes the

    efficiency of the whole evaporating operation of a single effect evaporator. This process

    involved evaporation of only water in a still and steam at 10 psig is supplied to the still to heat

    the water for evaporating. The vapor produced in the column goes to condenser and in a

    condensate collected tank it was collected to find out the total amount of vapor formed with

    time. Using the observed experimental data cumulative steam economy as well as overall steam

    economy was calculated .The values of cumulative steam economy range was 0-0.19548 and

    steam economy range for each observation was 0-0.960837and the overall steam economy was

    0.1955 .The overall heat loss was 131.902 MJ. A graph between vapor condensation rates vs.

    cumulative time was plotted. The graph shows that the time required to reach steady state

    condition was high. There were some discrepancies in the experiment. The possible cause of

    other discrepancies discussed in discussions.

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    Temperature

    of Vapor

    Steam Pressure

    EvaporatorPressure

    Temperature

    of Still

    Steam In

    Feed In

    Drain

    Stream Trap

    Steam Chest

    Evaporator

    Water Level

    Entrain

    Separator

    Condenser

    CondensateDrum

    Cooling

    Water Temp.

    Figure 1: Experimental setup of a single effect evaporator

    ExperimentalSetup

    2

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    Flow Diagram

    Figure 2: Flow diagram of the system

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    Observed Data

    Steam pressure = 10 Psig

    Weight of bucket1=0.65 Kg

    Weight of bucket2= 0.70 KgTime interval = 180 Sec

    Condensate tank perimeter = 76 inch

    Cooling water flow rate = 0.23 Kg/Sec

    Cooling water inlet temperature = 74 oF

    Cooling water outlet temperature = 80 oFTable-1: Observed data for study of single effect evaporator.

    Obs.

    No.

    Vapor space

    Temperature

    ( oF )

    Still

    Temperature

    ( oF )

    Steam

    condensate

    Time (Sec)

    Level of

    vapor

    condensate

    ( cm)

    Steam

    condensate

    +

    Bucket1

    (kg)

    Steam

    condensate

    +

    Bucket2

    (kg)1 68 100 180 91.9 6.5 -

    2 72 122 180 91.9 - 5

    3 76 144 180 91.9 4.35 -

    4 84 160 180 91.9 - 3.95

    5 96 174 180 91.9 3.3 -

    6 108 180 180 91.9 - 2.87 120 186 180 91.9 2.75 -

    8 130 190 180 91.9 - 2.5

    9 146 196 180 91.9 2.3 -

    10 188 206 180 91.9 - 2.5

    11 210 206 180 91.9 2.25 -

    12 212 206 180 91.3 - 2.55

    13 212 206 180 91.1 2.45 -

    14 212 206 180 90.9 - 2.4

    15 212 206 180 90.7 2.5 -

    16 212 206 180 90.5 - 2.6

    17 212 206 180 90.3 2.3 -18 212 206 180 90.0 - 2.3

    19 212 206 180 89.8 2.6 -

    20 212 206 180 89.5 - 2.6

    21 212 206 180 89.2 2.72 -

    22 212 206 180 88.9 - 4.15

    23 212 206 180 88.6 3.5 -

    24 212 206 180 88.2 - 4

    25 212 206 180 87.9 2.6 -

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    Calculated DataTable-2: Calculated data for study of single effect evaporator.

    Obs.

    No.

    Time

    (sec)

    Cumulative

    height ofvapor

    condensate(m)

    Water

    evaporated(Kg)

    Water

    condensationrate

    Kg/Sec

    Steam

    condensate(Kg)

    Rate of steam

    condensation(Kg / Sec )

    1 180 0 0 5.85 0.0325

    2 180 0 0 0 4.30 0.0238

    3 180 0 0 0 3.70 0.0205

    4 180 0 0 0 3.25 0.0180

    5 180 0 0 0 2.65 0.0147

    6 180 0 0 0 2.10 0.0116

    7 180 0 0 0 2.10 0.0116

    8 180 0 0 0 1.80 0.01009 180 0 0 0 1.65 0.0091

    10 180 0 0 0 1.80 0.0100

    11 180 0 0 0 1.60 0.0088

    12 180 0.006 1.7775 0.0098 1.85 0.0103

    13 180 0.008 0.5925 0.0033 1.80 0.0100

    14 180 0.010 0.5925 0.0033 1.70 0.0094

    15 180 0.012 0.5925 0.0033 1.85 0.0103

    16 180 0.014 0.5925 0.0033 1.90 0.0106

    17 180 0.016 0.5925 0.0033 1.65 0.0092

    18 180 0.019 0.8887 0.0049 1.60 0.0088

    19 180 0.021 0.5925 0.0033 1.95 0.010820 180 0.024 0.8887 0.0049 1.90 0.0105

    21 180 0.027 0.8887 0.0049 2.07 0.0115

    22 180 0.030 0.8887 0.0049 3.45 0.0191

    23 180 0.033 0.8887 0.0049 2.85 0.0158

    24 180 0.037 1.1850 0.0065 3.30 0.0183

    25 180 0.040 0.8887 0.0049 1.95 0.0108

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    Table-3: Calculated data for study of single effect evaporator.

    Obs. No. Cumulative

    wt. of steam

    cond.(Kg)

    Cumulative

    Steam

    economy

    Steam

    economy

    for each

    observation

    Heat

    recovered

    by

    steam(MJ)

    Heat

    absorbed

    by

    water(MJ)

    Heat

    loss(MJ)

    1 5.850 0 0 15.789 0 15.789

    2 10.15 0 0 27.394 0 27.394

    3 13.85 0 0 37.380 0 37.380

    4 17.10 0 0 46.152 0 46.152

    5 19.75 0 0 53.304 0 53.304

    6 21.85 0 0 58.972 0 58.972

    7 23.95 0 0 64.640 0 64.640

    8 25.75 0 0 69.498 0 69.498

    9 27.40 0 0 73.952 0 73.952

    10 29.20 0 0 78.810 0 78.810

    11 30.80 0 0 83.128 0 83.128

    12 32.65 0.05444 0.960837 88.121 4.755 83.365

    13 34.45 0.06879 0.329176 92.979 6.341 86.638

    14 36.15 0.08195 0.348539 97.568 7.926 89.641

    15 38.00 0.09355 0.320279 102.56 9.511 93.049

    16 39.90 0.10395 0.311851 107.68 11.09 96.592

    17 41.55 0.11408 0.359101 112.14 12.68 99.460

    18 43.15 0.13044 0.555484 116.46 15.06 101.40

    19 45.10 0.13794 0.303854 121.72 16.64 105.07

    20 47.00 0.15128 0.467776 126.85 19.02 107.82

    21 49.07 0.16301 0.429359 132.43 21.40 111.03

    22 52.52 0.16922 0.257616 141.75 23.77 117.9723 55.37 0.17656 0.311851 149.44 26.15 123.28

    24 58.67 0.18683 0.359101 158.34 29.32 129.02

    25 60.62 0.19548 0.455782 163.61 31.70 131.90

    Table-4: Calculated data for study of single effect evaporator.

    Overall steam

    economy

    Overall heat

    released from

    steam (MJ)

    Overall heat

    recovered by

    water(MJ)

    Overall Heat loss

    (MJ)

    0.1955 163.612 31.705 131.902

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    Sample CalculationFor Observation no. 16

    Steam condensate flow rate = {(2.60.7) / 180} kg /sec= 0.011 kg /sec

    Perimeter of storage tank = 76 inch = 1.9304 m

    Inner radius of storage tank, r = {1.9304 / (2)} m

    = 0.3072 m

    Level of water vapor storage tank, h12= 90.3 cm =0.903 m

    Level of water vapor storage tank, h13= 90.0 cm =0.90 m

    Volume of water vapor condensate = r2h

    = { (0.3072)2 (0.903-0.90)} m3

    = 8.8943x 10-4m3

    Water vapor condensed in the condenser = Water evaporated in the feed tank

    From Franzini (Table: A-1)

    Density of water, = 1000 kg /m3

    Mass of water evaporated, m = (8.8943 10-41000) kg

    = 0.88943 kg

    Total mass of steam condensate, m1= 60.62 kg

    Total mass of water evaporated, m2 = 11.85 kg

    Overall steam economy = (Total mass of water evaporated / Total mass of steam consumed)

    = (11.85 / 60.62)

    = 0.1955

    Cumulative mass of water evaporate = 4.1476 kg

    Cumulative mass of steam condensate= 39.9 kg

    Cumulate steam economy= (Cumulative mass of water evaporated / Cumulative mass of

    steam)

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    Cumulate steam economy = (4.1476/39.9)

    = 0.1039

    Calculation of steam economy for Observation no. 15

    Mass of water evaporate = 0.5925 Kg

    Mass of steam condensate = 1.9 Kg

    Steam economy = (Mass of water evaporated / Mass of steam consumed)

    = (.5925/1.9)

    = 0.3118

    Enthalpy balance

    Steam pressure = 10 psig = 24.7 psia

    At 24.7 psia , Tsat= 115.203oC

    Enthalpy of evaporation, Hv1= 2698.985 KJ /Kg

    Cumulative heat released from steam, Q1= m13 Hv1

    = (39.9 x 2698.985) KJ

    = 107.69 MJ

    Overall heat released from steam, Q1,ov= mtotalHv1

    = (60.62 2698.985) KJ

    =163.612 MJ

    At, condenser pressure= 14.7 Psia , Tsat=100oC

    Enthalpy of evaporation, Hv2= 2675.57 kJ/ kg

    Cumulative heat recovered by water, Q2= m13 Hv2

    = (4.1476 2675.57) KJ

    = 11.097MJ

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    Overall heat recovered by water, Q2 ov= mtotal Hv2

    = (11.85 2675.57) KJ

    = 31.705 MJ

    Cumulative heat loss , H = Q1Q2

    = (107.6911.097) MJ

    = 96.586 MJ

    Overall heat loss, H = Q1 ovQ2 ov

    = (163.61231.705) MJ

    = 131.902 MJ

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    Results and Discussions

    Table-5: Range of result for various observation of single effect evaporator.

    Ranges of steam

    economy for

    each observation

    Range of

    cumulative heat

    loss (MJ)

    Range of

    cumulative

    steam economy

    Overall heat

    loss(MJ)

    Overall steam

    economy

    0-0.960837 15.789-131.90 0-0.19548 131.902 0.1955

    From vapor condensation rate Vs. cumulative time curve, it was observed that at beginning rate

    increases with time and go through the pick point its to a steady state condition. This state arrived after

    40 minutes.

    In this experiment, the steam economy is very low because of single effect evaporator. Steam economy

    would be greater if multiple effect evaporator was used. Heat loss is very high .The possible reasons for

    this high heat loss are discussed below

    In this experiment, we converted a double effect evaporator to a single effect evaporator byclosing some valves. The total unit of heat exchanger was too old to perform and lost its actual

    insulation. Therefore, energy could be lost in the surroundings.

    The inlet steam was collided at the steam chest and thus condensed and lost its energy. The evaporator, condenser, other apparatus used, and the internal pipe network could absorb

    some energy.

    Moreover, the result could be varied due to the error reading of the mass of condensed steamand height of condensed vapor.