STRAIN-RATE-AND-TEMPERATURE-EFFECTS- ON-THE-FLOW … · BACKGROUND...

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Austempering, A Technology for Substitution ADI DAYS 2016 6 th –7 th October Minerbe 1 STRAIN RATE AND TEMPERATURE EFFECTS ON THE FLOW STRESS OF ADI A. Ruggiero a , G. Iannitti b , E. Veneri c , F. Vettore c , N. Bonora a a University of Cassino and SL, DICeM, Cassino, Italy b TECHDYN Engineering, I00199 Rome, Italy c Zanardi Fonderie S.p.A, I37046 Minerbe (VR), Italy

Transcript of STRAIN-RATE-AND-TEMPERATURE-EFFECTS- ON-THE-FLOW … · BACKGROUND...

Page 1: STRAIN-RATE-AND-TEMPERATURE-EFFECTS- ON-THE-FLOW … · BACKGROUND Austempering,-A-Technology-for-Substitution ADI$DAYS$$2016$$ 6th$$–7 th $October$$$$$Minerbe 3 • Designers-show-lack-of-confidence-•

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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STRAIN  RATE  AND  TEMPERATURE  EFFECTS  ON  THE  FLOW  STRESS  OF  ADI

A.  Ruggieroa,  G.  Iannittib,  E.  Veneric,  F.  Vettorec  ,  N.  Bonoraa  

a  University  of  Cassino  and  SL,  DICeM,  Cassino,  Italyb  TECHDYN  Engineering,  I-­‐00199  Rome,  Italy

cZanardi  Fonderie  S.p.A,  I-­‐37046  Minerbe  (VR),  Italy

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BACKGROUND

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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• Cast  irons  are  widely  used  in  industrial  practice  mainly  for  the  production  of  components  through  the  process  of  casting  

• ADI  matrix  microstructure:  ausferrite  

• Excellent  property  combinations  of  strength,  ductility,  and  toughness  

• Valid  substitute  for  steel  for  structural  applications

References  

[1]  Böhme*  and  Reissig,  Adv.  Eng.  Mat.  2015,  17,  No.  8  

[2]  Keough  and  Hayrynen,  SAE,  2000,  paper  no  248871

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BACKGROUND

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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• Designers  show  lack  of  confidence  

• Dread  of  a  presumed  low  ductility  under  impulsive  loading  

• Charpy  impact  test  results

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AIM  OF  THE  WORK

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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• To  investigate  the  constitutive  response  of  the  ADI  1050-­‐6  under  different  conditions  of  strain  rate  and  temperature  

• To  analyze  the  strain  rate  effect  on  the  ductility  

• To  develop  a  constitutive  model  for  the  design  of  components  operating  under  both  static  and  dynamic  conditions

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MATERIALS

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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DESIGNATIONUTS   (MPa)  

YIELD  STRESS  (MPa)

ELONGATION  %

HARDNESS(BR)

ADI  1050 1050 700 6 320-­‐380ADI  1200 1200 850 3 340-­‐420HSiADI 1450 1040 8.9 40042CrMo4 1200 800 11 -­‐

[3]References  

[3]  J.  R.  Keough,  K.  L.  Hayrynen  and  G.  L.  Pioszak,  AFS  Proc.  2010,  Schaumburg,  IL  USA

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EXPERIMENTAL  CHARACTERIZATION

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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TEST STRAIN RATE TEMPERATURE

QUASI-STATIC TENSILE 0.001/s -60°C, 25°C e +70°C

Quasi-­‐static  characterization  • Instron  5586  (electromechanic)  • Local  deformation  measurements  (DIC)  • Low  temperature  (liquid  CO2)  • Induction  heating

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EXPERIMENTAL  CHARACTERIZATION

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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Characterization  at  high  strain  rate  • Direct  Tension  Split  Hopkinson  Pressure  Bar  • Low  temperature  (liquid  CO2)  • High  frame  rate  camera

TEST STRAIN RATE TEMPERATURE

DYNAMIC TENSILE 600/s -60°C e 25°C

DYNAMIC TENSILE 1200/s -60°C e 25°C

8000  mm

3000  mm 3000  mm

1000  mm

A

A

A-­‐A

1200  mm

specimenclamp

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EXPERIMENTAL  RESULTS:  local  strains

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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Local  deformation  map

Remarks  

• Uniform  strain  over  the  gage  length  up  to  failure.  No  necking

0 0.05 0.1 0.15 0.20

200

400

600

800

1000

1200

1400

1600

Deformazione

Sfor

zo (M

Pa)

T= 298 KT= 213 KT= 343 K

Stress

Strain

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EXPERIMENTAL  RESULTS:  temperature  effect

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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Remarks  

• At  low  temperatures,  the  work  hardening  rate  increases,  whereas  the  apparent  yield  strength  seems  to  decrease  slightly    

• Same  behavior  at  different  strain  rates

0 0.05 0.1 0.15 0.20

200

400

600

800

1000

1200

1400

1600

Deformazione

Sfor

zo (M

Pa)

T= 298 KT= 213 KT= 343 K

0 0.05 0.1 0.15 0.2 0.250

200

400

600

800

1000

1200

1400

1600

Deformazione

Sfor

zo (M

Pa)

HpkGS_2HpkGS_7HpkGS_11HpkGS_15

Quasistatic  test Dynamic  test

T=213  K

T=298  K

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Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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Remarks  

• Strain  rate  affects  the  material  yield  stress  

• Under  dynamic  loading,  necking  occurs  just  before  failure

T=25°C

Stress

Stress

EXPERIMENTAL  RESULTS:  strain  rate  effect  on  the  flow  stress

T=-­‐60°C

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EXPERIMENTAL  RESULTS:  strain  rate  effects  on  yield  stress  and  ductility

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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Remarks  

• Absence  of  the  knee  in  the  initial  yield  stress  vs.  strain  rate  diagram  

• As  for  the  ADI  1200,  the  failure  strain  increases  with  the  strain  rate

10-4 10-3 10-2 10-1 100 101 102 103 104600

700

800

900

1000

1100

1200

1300

1400 ADI 1050 (present work) ADI1200 (Bohmer and Reissig, 2015) Linear Fit of Sheet1 B"R02"

Yie

ld s

tres

s, R

0.2%

[MP

a]

STRAIN RATE [1/s]10-4 10-3 10-2 10-1 100 101 102 103 104

0.00

0.05

0.10

0.15

0.20

0.25

0.30

0.35

0.40 ADI1050 T=298K ADI1200 (Bohmer and Reissig, 2015) ADI1050 T=213K

FA

ILU

RE

STR

AIN

STRAIN RATE [1/s]

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EXPERIMENTAL  RESULTS:  failure  mode

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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HpkGS5  RT  1200s-­‐1

HpkGS7  RT  1200s-­‐1

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STRENGTH  MODEL

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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0 100 200 300 4000

1000

2000

3000

4000

5000

6000

7000

8000

9000

Temperatura (K)

A e

B (M

Pa)

AFit ABFit B

AS  (MPa) ma  B0  (MPa) mb n C

1207 160 10805 160 0.6 0.014 1.0

( ) ( )( ) ( )σ ε ε= + ⋅ + !nA T B T 1 Cln *

! "! "= − −$ %$ %

& '& '

! "= −$ %

& '

Sa

0b

TA A 1 exp

m

TB B exp

m

Modified  Johnson-­‐Cook

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MODEL  VERIFICATION

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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0 0.5 1 1.5 2 2.50

5000

10000

Allungamento (mm)

Forz

a (N

)

dε/dt=1E-3 s-1, T=298 KFEM

0 0.5 1 1.5 2 2.50

5000

10000

Allungamento (mm)

Forz

a (N

)

dε/dt=1E-3 s-1, T=213 KFEM

0 0.5 10

5000

10000

Allungamento (mm)

Forz

a (N

)

dε/dt=1E-3 s-1, T=313 KFEM

0 0.5 1 1.50

5000

10000

Allungamento (mm)

Forz

a (N

)

dε/dt=600 s-1, T=213 KFEM

0 0.5 10

5000

10000

Allungamento (mm)

Forz

a (N

)

dε/dt=1200 s-1, T=213 KFEM

0 0.5 1 1.50

5000

10000

Allungamento (mm)

Forz

a (N

)

dε/dt=600 s-1, T=298 KFEM

0 0.5 1 1.50

5000

10000

Allungamento (mm)

Forz

a (N

)

dε/dt=1200 s-1, T=213 KFEM

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CONCLUSIONS

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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• Experimental  results  show  an  increase  of  up  to  10%  in  ductility  with  increasing  the  strain  rate  

• Possible  differences  in  the  failure  mechanism  at  different  strain  rates  were  observed  

• Strain  rate  affects  the  initial  yield  stress  (typical  of  a  BCC  structure)  

• Absence  of  the  knee  in  the  initial  yield  stress  vs  strain  rate  diagram  (typical  of  a  FCC  structure)  

• Temperature  affects  the  work  hardening  rate  mainly  (typical  of  a  FCC  structure)  

• The  proposed  constitutive  model  describes  with  good  accuracy  the  phenomenological  behavior  that  the  ADI  1050  shows  in  the  ranges  of  strain  rate  and  temperature  analyzed

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ONGOING  WORK

Austempering,  A  Technology  for  Substitution

ADI  DAYS    2016     6th    –  7th    October                                        Minerbe

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• To  analyze  further  the  peculiar  effects  of  strain  rate  and  temperature  on  the  flow  stress

✓ Micro  mechanical  modeling  for  evaluating  the  effects  of  residual  stress    

✓ To  investigate  the  composite  structure  of  the  ausferrite

• To  analyze  the  stress  triaxiality  effect  on  the  ductility  at  different  strain  rates  and  temperatures  

• To  develop  a  damage  model0 0.5 1 1.5 2

0

0.5

1

1.5

2

2.5

3

TF

Defo

rmaz

ione

a ro

ttura

Equivalent  failure  strain

( )σ σm eqTriaxiality  factor