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Elevated temperature material properties of cold-formed steel hollow sections Finian McCann a , Leroy Gardner b , Sophie Kirk c Abstract Elevated temperature material tests on cold-formed steel coupons cut from circular, rectangular and square hollow sections have been conducted, including both steady-state and transient-state tests. The experimental apparatus, methods of testing and results obtained are fully described. Temperature dependent retention factors for stiffness, strength and ductility were determined and compared to those provided in the European Standard EN 1993-1-2:2005 and the Australian Standard AS 4100:1998. It was found that the codified retention factors, despite being derived on the basis of tests on hot-finished material, are also applicable to cold-formed hollow sections. A design proposal from the literature for the

Transcript of Statistical Analysis - LSBU Open Research · Web viewCold-formed, elevated temperatures, fire...

Statistical Analysis

Elevated temperature material properties of cold-formed steel hollow sections

Finian McCanna, Leroy Gardnerb, Sophie Kirkc

Abstract

Elevated temperature material tests on cold-formed steel coupons cut from circular, rectangular and square hollow sections have been conducted, including both steady-state and transient-state tests. The experimental apparatus, methods of testing and results obtained are fully described. Temperature dependent retention factors for stiffness, strength and ductility were determined and compared to those provided in the European Standard EN 1993-1-2:2005 and the Australian Standard AS 4100:1998. It was found that the codified retention factors, despite being derived on the basis of tests on hot-finished material, are also applicable to cold-formed hollow sections. A design proposal from the literature for the prediction of ultimate strain has been also shown to be suitable for application to cold-formed hollow sections. A new expression for predicting strain at fracture has been proposed that provides a lower bound estimate of the test results derived in the current study.

Keywords: Cold-formed, elevated temperatures, fire design, hollow sections, material properties, steel, structural engineering, tensile testing, tubular sections

a Corresponding author. Department of Civil and Environmental Engineering, Imperial College London, SW7 2AZ, UK. Phone: +44 7943525139. Email: [email protected]

b Department of Civil and Environmental Engineering, Imperial College London, SW7 2AZ, UK. Email: [email protected],

c Department of Civil and Environmental Engineering, Imperial College London, SW7 2AZ, UK. Email: [email protected]

Symbols

Latin script symbols

Aooriginal cross-sectional area

Emodulus of elasticity at temperature

f0.2,0.2% proof stress at temperature

f2.0,stress at 2% strain at temperature

fu,ultimate tensile strength at temperature

Lgauge length

kXretention factor for material property X

Greek script symbols

f,fracture strain at temperature

u,ultimate strain at temperature

temperature

Introduction

In recent years, a significant amount of research has been conducted into the behaviour and performance of steel structures in fire conditions. Reviews have been carried out of fire engineering research on columns and beams [1], composite structures [2], connections [3] and design approaches [4]. Findings arising from the research have been used to formulate and extend design codes such as the European Standard EN 1993-1-2 [5] and the Australian Standard AS 4100 [6].

Fire is now generally treated as a specific limit state for which a structure must be designed, as opposed to simply applying a prescribed level of fire protection [7]. A key effect that must be gauged when conducting analysis and design of steel, or composite steel-concrete, structures in fire is the loss of stiffness and strength of the material with increasing temperature, along with changes in ductility. Accurate assessment of elevated temperature material properties is essential for use in numerical parametric studies and in underpinning the development of fire design codes. In the present study, the full-range elevated temperature stress–strain response of cold-formed steel hollow sections is studied. In particular, although it is known that the mechanical properties of steel at room temperature are influenced by cold-work [8], it is not clear whether the elevated temperature properties of typical cold-formed steel hollow sections can still be presented as constant proportions of the room temperature values using the same retention factors as for hot-finished material. This will be explored for all key mechanical properties (i.e. relating to strength, stiffness and ductility).

There is extensive literature concerning the elevated temperature testing of steel material and structural elements. A variety of cold-formed steel products and grades, including S355 circular hollow sections (CHS) and rectangular hollow sections (RHS) were tested by [9, 10]. Tests on cold-formed specimens of grades G450 and G550 steel were conducted by [11, 12], while high-strength steel (S690) specimens were examined by [13]. A study [14] of the effects of elevated temperature on cold-formed Q345 steel provided empirical equations for retention factors for modulus of elasticity, yield strength and ultimate strength. A comparison between the results of the test programmes conducted by [9] and [12], together with the predictive models provided in EN 1993-1-2 [5], the ASCE manual [15] and proposed by [16], was made by [17]. A significant spread of experimental results, as well as some differences between the models themselves, was observed. In the present study, comparisons are made with the results of [9–11] since these tests were also performed on cold-formed material.

Experimental study

2.1 Introduction

In this section, an experimental study is described in which coupons cut from cold-formed S355 steel circular, square and rectangular hollow section (CHS, SHS and RHS, respectively) members have been tested at elevated temperatures. Two testing methods were employed – steady-state (isothermal) and transient-state (anisothermal). In the steady-state tests, the coupons were heated to a target temperature that was held constant while the coupon was subjected to an increasing axial tensile load until fracture. In the transient-state tests, the coupons were loaded with a tensile stress that was maintained constant while the coupon was heated until fracture. Steady-state tests enable stress-strain curves, which are suitable for use in numerical models, to be obtained directly, while transient-state tests more closely mimic the conditions to which material would be subjected to in a structure under fire conditions, i.e. static load followed by increasing temperature. Values were obtained for the following temperature-dependent material properties, where is temperature,

· Modulus of elasticity, E

· Yield strength (0.2% proof strength), f0.2,

· Strength at 2% strain, f2.0,

· Ultimate stress, fu,

· Ultimate strain, u,

· Strain at fracture, f,

These properties are illustrated in Figure 1. From the test results, temperature-dependent retention factors were calculated for each of the material properties, which are compared later in Section 5 with existing experimental results, code provisions and predictive models from the literature.

2.2 Test apparatus

The test apparatus, located in the Structures Laboratory of the Department of Civil and Environmental Engineering at Imperial College London, is shown in Figure 2. It comprised an Instron 750 hydraulic testing machine, an electric furnace capable of heating to temperatures up to 1100°C, a heat control unit with temperature probes which were inserted into the furnace, thermocouples attached to the test specimens, rock-wool insulation at either end of the furnace and an extensometer. The extensometer, shown in Figure 3, comprised two clamps fixed to the specimen with pointed bolts, two invar rods, a contact plate and a linear variable differential transducer (LVDT). The machine load, machine displacement, LVDT displacement and thermocouple readings were recorded using the DATASCAN data acquisition equipment and logged using the DSLOG computer package at a frequency of 1 Hz.

2.3 Test specimens

The test specimens were all extracted from cold-formed grade S355J2H steel hollow section members produced according to EN 10219-1 [18]. The cross-sections of the members and the number of tests conducted are summarised in Table 1.

Each coupon had an overall length of 800 mm, with the central 600 mm having a nominal width of 20 mm. In order to ensure that the coupons failed within the gauge length (thus providing full stress-strain curves up to fracture), the test pieces were narrowed by a further 2 mm in this region. The extensometer was aligned with the centre of the furnace to ensure that the length of coupon being measured coincided with the region of the furnace at the target test temperature. Standard gauge lengths of , where Ao is the original cross-sectional area of the coupons in the narrowed region, were also marked onto the specimens for the calculation of the fracture strain after testing.

2.4 Testing methods

As mentioned in Section 2.1 and described in the following sub-sections, two complementary elevated temperature material testing methods were employed in the programme. All tests were conducted in accordance with ISO 6892 parts 1 and 2 [19, 20], following the prescribed heating rates and loading rates.

2.4.1 Steady-state (isothermal) tests

In the steady-state tests, the specimens were heated up to the target temperature at a rate of 10°C/min. Typically, a period of 10 to 15 minutes was allowed after the heating phase for the temperature to settle. The target temperatures ranged from room temperature to 1000°C in increments of 100°C. The testing machine was set to load control for the heating phase so that the upper jaw of the machine could displace to accommodate the thermal expansion of the specimen, thus ensuring no load was induced. The tensile coupons were then tested until fracture under displacement control at a displacement rate of 0.05 mm/s, in keeping with the strain rates set out in [19, 20]. The results of the steady-state tests are presented in Section 3.

2.4.2 Transient-state (anisothermal) tests

The transient-state test specimens were loaded in tension to a particular level and then subjected to increasing temperature until failure. The applied stress levels ranged from 10% to 90% of the ultimate strength at room temperature fu,20°C for the RHS specimens and from 20% to 80% for the SHS specimens. While maintaining the loads at these levels with the testing machine set to load control, the furnace was activated and the temperature increased at a rate of 10°C/min until failure. The heating rate of 10˚C/min was reported by [21] to be similar to the rate of temperature increase of protected steelwork during a fire, and thus provides a good representation of typical fire conditions. Since the strength of the steel decreases with increasing temperature, the higher the applied stress level, the lower the failure temperature. The results of the transient-state tests are presented in Section 4.

The displacement readings from the extensometer comprised components relating to the mechanical tensile strain of the coupons, the thermal strain of the coupons and also some thermal strains associated with the extensometer apparatus itself. For the steady-state tests, once the target temperature was achieved, the extensometer reading was zeroed and thus only the mechanical strain was measured. For the transient-state tests, however, both mechanical and thermal strains arise with increasing temperature. To isolate the thermal strains, extensometer readings were taken during the heating phase of an unloaded coupon up to 1000°C. The resulting thermal strains were then deducted from the total temperature-strain plots to give the mechanical strains induced from the effect of the applied load alone.

By examining the full set of transient-state temperature-strain curves, of which there were one for each applied stress level, stress-strain curves were derived by extracting strains corresponding to a specific temperature from each curve, and plotting these against the respective applied stresses, as demonstrated in Figure 4, resulting in a set of isothermal stress-strain curves. For higher temperatures, for example at 2 in Figure 4, fewer data points are available since for transient-state tests performed at the higher applied stress levels (f3 in the example) the failure temperature is lower than the temperature in question.

Steady-state test results

In this section, the results of the steady-state tests are presented. A total of 27 steady-state tests were conducted across the three cross-sections, yielding stress-strain curves for a series of distinct temperatures. The key mechanical properties at each temperature were then extracted from these curves.

3.1 Determination of mechanical properties

Mechanical properties were determined from each steady-state test and normalised by the respective property at room temperature in order to compare with retention factors given in EN 1993-1-2 [5], AS 4100 [6] and derived from previous tests [9, 11]. The retention factors derived from the steady-state test results are presented in Section 5, along with retention factors derived from the transient-state test results.

The modulus of elasticity was determined from the experimental stress-strain data by means of a best fit through the initial linear portion of the curve. The range of linear elastic behaviour decreased for higher temperatures due to the reducing strength and the increasingly nonlinear response of the material. In addition to the limited linear elastic range at higher temperatures, cold-formed steel material in general does not possess a well-defined yield point. Hence, the 0.2% proof strength was taken as an effective yield strength of the material [22]. The strength at 2% strain was also extracted from the stress-strain curves, as this strength is typically employed in the design of steel elements in fire [23], due to a greater tolerance for larger deformations in this design scenario [24]. The ultimate strength fu, was taken as the maximum stress observed during the tensile tests, with the ultimate strain εu, being the corresponding strain. The fracture strain εf, was determined by measuring the extension across two half-gauge lengths marked on the specimen either side of the fracture location and dividing by the original gauge length.

3.2 Stress-strain curves

The isothermal stress-strain curves recorded for the CHS, RHS and SHS specimens are shown in Figures 5 to 7, respectively. As expected, overall trends of reduced strength and stiffness, earlier and more pronounced nonlinearity and increased ductility are observed with increasing temperature. Also, particularly at lower temperatures, the CHS material exhibits a more rounded stress–strain response with higher ultimate strain values than the RHS and SHS materials, but lower ultimate strength values. This may be attributed to the higher level of cold-work experienced by the RHS and SHS specimens during forming [8, 25].

3.3 Elastic modulus and 0.2% proof strength

Values of modulus of elasticity obtained from the steady-state tests across the three cross-sections are presented in Table 2 and Figure 8. The results show the anticipated trend of reducing modulus of elasticity with increasing temperature, albeit with some scatter present. This reflects the sensitivity of the values obtained from the tests to small variations in the test setup and the measurement method, and has been observed previously [9, 10, 17]. Comparisons with the transient-state test results are described in Section 4.2.

The measured values of 0.2% proof strength at elevated temperature are presented in Table 3 and Figure 9. It can be seen that the 0.2% proof strength is maintained approximately at its room temperature level for temperatures up to 400°C for all cross-sections. For temperatures higher than 400°C, the strength begins to decrease noticeably. At lower temperatures, the RHS and SHS material may be seen to possess higher 0.2% proof strengths than the CHS material, which may be due to the additional cold-work experienced during forming, although the benefit of cold-work seems to disappear after about 700°C.

3.4 Strength at 2% strain and ultimate strength

The measured values of strength at 2% strain from the steady-state tests are provided in Table 4 and are shown in Figure 10, while the ultimate tensile strengths are given in Table 5 and Figure 11. As was observed for the 0.2% proof strength, for temperatures up to approximately 400°C, there is little to no reduction in both the strength at 2% strain and the ultimate strength of the cold-formed steel material. For higher temperatures, there is again a noticeable loss of strength with increasing temperature. Comparisons with the transient-state test results are described in Section 4.3.

3.5 Ultimate strain and fracture strain

The values of ultimate strain derived from the steady-state results are presented in Table 6 and shown in Figure 12. It may be observed that although a clear trend is not immediately apparent, the ultimate strain generally decreases with increasing temperature up to 800°C. This may also be seen in the shape of the stress-strain curves (see Figures 5 to 7) where the ultimate strength is attained sooner after yielding as the temperature increases. This is then followed by an extended period of necking before final fracture of the coupon. For temperatures above 800°C, the ultimate strain increases again.

Values of fracture strain recorded from the steady-state tests are presented in Table 7 and shown in Figure 13. It can be seen that there is a general trend of increasing ductility as the temperature increases up to 800°C, where the fracture strain is at a maximum. For temperatures higher than 800°C, the trend is reversed and the fracture strain decreases. It has been explained by [26] that this effect is related to the phase change that steel undergoes at temperatures of about 800°C. It appears that there are opposing trends in ultimate strain and fracture strain with increasing temperature, suggesting that greater overall ductility, indicated by increased fracture strain, is associated with the ultimate strength being attained at lower strains. Comparisons with the transient-state test results are described in Section 4.4.

Transient-state test results

In this section, the results of the transient-state results are presented. A total of 13 transient-state tests were conducted – nine on RHS specimens and four on SHS specimens.

4.1 Determination of mechanical properties

In the transient-state tests, a constant load was applied to the specimens and then the temperature was increased until fracture. The stresses corresponding to the constant applied loads were specified as fixed percentages of the ultimate strength of the material at room temperature, and are given in Table 8. Predicted failure temperature ranges, based on the ultimate strengths of the material obtained from the steady-state tests are also shown. It can be seen that the actual failure temperatures generally fell within the predicted ranges.

Stress–strain curves were derived from the temperature–strain data using the method described in Section 2.4.2. Since the number of applied stress levels was limited, the production of full stress-strain curves was restricted and the post-yield behaviour was often not captured, especially for the SHS curves where the highest stress level was 80% of fu,20°C. It was thus not possible to extract values for 0.2% proof strength from the transient-state stress-strain curves; however, values for the strength at 2% strain were extracted by determining the temperature at which the 2% strain was achieved for a particular stress level.

It was also not possible to extract results for ultimate strain since the ultimate strength for a particular transient-state test was taken as the constant stress applied during that test, and thus the concept of a particular strain corresponding to the ultimate strength is not applicable. As was carried out for the steady-state tests, results for fracture strain were obtained manually through measurement of the specimens after the tests.

4.2 Modulus of elasticity

The results for modulus of elasticity from the steady-state tests and the transient-state tests are compared in Figure 8. It can be seen that the results obtained from the two testing methods are generally in good agreement. In keeping with the results from the steady-state tests, a general trend of decreasing stiffness with increasing temperature is observed.

4.3 Strength at 2% strain and ultimate strength

The steady-state results and the transient-state results for strength at 2% strain are compared in Figure 10. As can be seen, the results are in close agreement, with the transient-state test results being slightly lower than those from the steady-state tests.

Results for ultimate strength obtained from the transient-state tests are compared with those obtained from the steady-state tests in Figure 11. It is observed that ultimate strength values from transient-state testing tend to be slightly higher than their steady-state counterparts.

4.4 Fracture strain

The results for fracture strain are compared between the steady-state and transient-state tests in Figure 13. Despite there being some scatter present at temperatures between 500–700°C, it can be seen that the trends displayed in the steady-state data and the transient-state data agree reasonably well, with ductility increasing with temperature up to a peak value at 800°C. For higher temperatures, ductility decreases again.

5. Retention factors

In this section, retention factors derived from both the steady-state and transient-state test results are presented and compared with those provided in EN 1993-1-2 [5] and AS 4100 [6] and those reported in [9, 11]. The retention factor kX for a particular material property X of the steel is defined as kX = XX20°C, i.e., the values are normalised by the respective value at room temperature. In EN 1993-1-2 [5], retention factors are provided for the modulus of elasticity E, 0.2% proof strength (yield strength) f0.2,, strength at 2% strain f2.0, and ultimate strength fu,. The Australian Standard AS 4100 [6] provides retention factors for the modulus of elasticity and 0.2% proof strength. Comparison of retention factors given in EN 1993-1-2 [5] with those set out in BS 5950-8 [27], which provides separate factors for hot-finished and cold-formed material, show that the EN 1993-1-2 [5] factors are the same as the BS 5950-8 [27] values for hot-finished steel. It is therefore assumed that the EN 1993-1-2 [5] values are intended for application to hot-finished steel, as was also assumed by [11]. Where possible, comparison is also made between the results of the present study and the BS 5950-8 [27] retention factors for cold-formed steel material.

5.1 Modulus of elasticity and 0.2% proof strength

Retention factors for modulus of elasticity kE are presented in Table 9 and shown in Figure 14. Comparison is made with EN 1993-1-2 [5], AS 4100 [6] and the results of [11, 12]. Comparison is not made with the results of [9, 10] as the values reported therein are identical to the EN 1993-1-2 [5] retention factors. It can be seen that, while there is some scatter observed in the values obtained from certain steady-state tests, the retention factors follow a clear trend of decreasing stiffness with temperature. Overall, it appears that AS 4100 [6] over-predicts the retention factors for modulus of elasticity, especially for temperatures higher than 400°C, while the EN 1993-1-2 [5] values tend to agree more closely with the results of the present study. It can also be seen that the results of the present study, especially those derived from tests on RHS and SHS specimens, agree well with those found by [11] for plated samples.

The retention factors for the 0.2% proof strength k0.2 are presented in Table 10 and Figure 15. For temperatures up to 600°C, the values of k0.2 determined from the results of the present study are slightly below the EN 1993-1-2 curve [5], while for temperatures higher than 600°C, the results of the present study are marginally above the code provisions. The retention factors set out in AS 4100 [6] generally provide a lower bound to the test results between 300–600°C and align well for temperatures above this level. The additional test results from the literature on cold-formed material (S355 [9] and G450 [11] steel) follow similar trends to the results of the present study, though are lower at higher temperatures. Overall, the values proposed by EN 1993-1-2 [5] for hot-rolled sections are deemed suitable for application to cold-formed material. Overall, there is good agreement across the tested temperature range between the results of the present study and the results of [9] for grade S355J2H steel and [11] for grade G450 steel.

5.2 Strength at 2% strain and ultimate strength

Since retention factors for strength at 2% strain k2.0 are not provided by AS 4100 [6], comparison of k2.0 is made with the results of [11], the provisions EN 1993-1-2 [5] and the provisions of BS 5950-8 [27], which specifies distinct retention factors for the strength of steel at 0.5%, 1.5% and 2.0% strain for cold-formed steel material. The retention factors for strength at 2% strain derived from the steady-state and transient-state tests are presented in Table 11 and Figure 16. As was found for k0.2, for temperatures up to 400°C, the retention factors for strength at 2% strain are slightly below the EN 1993-1-2 [5] and BS 5950-8 [27] curves. For temperatures above 400°C, the retention factors from BS 5950-8 [27] provide a lower bound to the results of the present study, while the EN 1993-1-2 [5] curve slightly over-predict the retention factors. However, overall, the values for k2.0 from EN 1993-1-2 [5] agree satisfactorily with the results of the present study. It can be seen that the results of [11] for plated grade G450 material, which align well with EN 1993-1-2 [5], are also in good agreement with the results of the present study.

Retention factors for ultimate strength ku are shown in Table 12 and are compared in Figure 17 with those from Appendix A of EN 1993-1-2 [5] and a fitted formula for ultimate strength proposed by [11] of the form

where a, b, c and n are constants derived from regression, with values recommended by [11] based on their tests on cold-formed material of a = 1.0, b = 22°C, c = 5.6 × 108 and n = 3 for 22°C ≤ < 450°C, and a = 0.043, b = 1000°C, c = -1.12 × 1011 and n = 4 for 450°C ≤ ≤ 1000°C. Retention factors for ultimate strength are not provided in AS 4100 [6]. For temperatures up to approximately 400°C, the results for ku are over-predicted by the EN 1993-1-2 [5] curve, but for higher temperatures the curve provides a lower bound to the results of the present study. Overall, there is good agreement between the EN 1993-1-2 [5] curve and the retention factors of the present study. It can also be seen that for temperatures above 400°C, the design curve of [11] provides a lower bound for the retention factors of the present study, while for lower temperatures the retention factors are slightly over-predicted by the design curve.

5.3 Ultimate strain and fracture strain

Retention factors for ultimate strain ku derived from the steady-state tests are presented in Table 13 and Figure 18, with comparison made with a design curve proposed by [11]. Although the experimental data exhibit significant scatter, it can be seen that the design curve provides a lower bound for the retention factors for ultimate strain across almost all of the tested temperature range. The curve is rather conservative at lower temperatures when compared with the retention factors of the present study. Similar conservatism was reported by [11] when compared with the results of tests on G450 and G550 plate materials.

The retention factors for fracture strain kf are shown in Table 14 and Figure 19. Owing to an absence of predictive expressions for the fracture strain of cold-formed steel material at elevated temperatures in the literature, a design curve for kf is proposed herein, which is also shown in Figure 19. The curve is described by the expression

As can be seen from Figure 19, the design curve provides a reasonable approximation for kf across the tested temperature range.

6.Conclusions

Tensile tests have been performed at elevated temperatures on a total of 40 coupons cut from cold-formed grade S355J2H steel hollow sections. 27 steady-state tests and 13 transient-state tests were carried out. The temperatures at which the tests were conducted ranged from room temperature to 1000°C. The test coupons were cut from three different cross-section shapes, namely circular, rectangular and square hollow sections. The results obtained for modulus of elasticity, ultimate tensile strength, strength at 2% strain and strain at fracture from the two testing methods (steady-state and transient-state) were compared and found to be generally in good agreement. Results for 0.2% proof stress and ultimate strain were extracted from the steady-state tests only. Retention factors were derived for all the mechanical properties by normalising the values recorded at elevated temperatures by the respective values of the properties at room temperature.

Some scatter was observed in the results for modulus of elasticity from both the steady-state and the transient-state tests. The retention factors derived from them were found to agree well with the provisions of EN 1993-1-2 [5]. Less scatter was observed in the results for the strength and ductility of the specimens. It was found that for temperatures up to 400°C, the retention factors derived from the results of the present study for 0.2% proof strength, strength at 2% strain and ultimate strength were slightly lower than those given in EN 1993-1-2 [5], but for higher temperatures, the results align very closely with the provisions of EN 1993-1-2 [5]. Overall, it is recommended that the retention factors set out in EN 1993-1-2 [5] for modulus of elasticity, 0.2% proof strength (yield strength), strength at 2% strain and ultimate strength are suitable for use in the design of cold-formed CHS, SHS and RHS elements.

A design formula proposed by [11] for the retention factor for ultimate strain was compared with the results of the present study and was found to provide appropriate lower bound predictions, with some conservatism at lower temperatures. A formula for the prediction of the fracture strain of cold-formed steel material at elevated temperatures was proposed in the present study, which was shown to provide generally conservative results across the tested temperature range.

Further work is recommended to increase the pool of available experimental results for the mechanical properties of cold-formed steel sections at elevated temperatures. Such data can to be used to determine parameters for elevated temperature stress-strain models, such as those of the form proposed by [28].

7.Acknowledgements

The authors would like to express their sincere gratitude to the European Union for the help provided through the Project RFSR-CT-2012-00025, carried out with a financial grant from the Research Programme of the Research Fund for Coal and Steel.

The authors would also like to thank the technical staff of the Structures Laboratory at the Department of Civil and Environmental Engineering at Imperial College London, in particular Gordon Herbert and Leslie Clark, for their expertise, guidance and assistance in conducting this research.

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Figure 1 Definition of measured elevated temperature material properties

Figure 2 Elevated temperature testing apparatus

Figure 3 Extensometer components used to record strain

Figure 4 Derivation of isothermal stress-strain curves from transient-state test temperature-strain data

Figure 5 Stress-strain curves for circular hollow sections from steady-state tests

Figure 6 Stress-strain curves for rectangular hollow sections from steady-state tests

Figure 7 Stress-strain curves for square hollow sections from steady-state tests

Figure 8 Measured values of modulus of elasticity from steady-state and transient-state tests

Figure 9 Measured values of 0.2% proof strength from steady-state tests

Figure 10 Measured values of strength at 2% strain results from steady-state and transient-state tests

Figure 11 Measured values of ultimate strength from steady-state and transient-state tests

Figure 12 Measured values of ultimate strain from steady-state tests

Figure 13 Measured values of fracture strain from steady-state and transient-state tests

Figure 14 Comparison of retention factors for modulus of elasticity

Figure 15 Comparison of retention factors for 0.2% proof strength

Figure 16 Comparison of retention factors for strength at 2% strain

Figure 17 Comparison of retention factors for ultimate strength

Figure 18 Retention factors for ultimate strain, compared with the proposal of Chen and Young (2007)

Figure 19 Retention factors for fracture strain compared with design proposal

Figure 1

Figure 2

Figure 3

Figure 4

Figure 5

Figure 6

Figure 7

Figure 8

Figure 9

Figure 10

Figure 11

Figure 12

Figure 13

Figure 14

Figure 15

Figure 16

Figure 17

Figure 18

Figure 19

Table 1 Summary of specimen cross-sections and number of tensile coupon tests conducted

Section

Steady-state tests

Transient-state tests

CHS 193.7×8

11

-

RHS 250×150×10

11

9

SHS 150×150×8

5

4

Table 2 Measured values of modulus of elasticity from steady-state tests

Temperature (°C)

Modulus of elasticity (MPa)

CHS

RHS

SHS

20

198600

198600

205000

100

200300

181300

-

200

126800

163000

196500

300

123000

160700

-

400

102200

159600

163500

500

114200

92700

-

600

46800

54000

27900

700

11200

23700

-

800

34000

20800

4700

900

7900

6000

-

1000

9700

850

-

Table 3 Measured values of 0.2% proof strength from steady-state tests

Temperature (°C)

0.2% proof strength (MPa)

CHS

RHS

SHS

20

404

537

531

100

367

482

-

200

373

493

510

300

360

444

-

400

385

448

511

500

265

357

-

600

115

219

224

700

107

139

-

800

57

69

84

900

45

54

-

1000

26

36

-

Table 4 Measured values of strength at 2% strain from steady-state tests

Temperature (°C)

Strength at 2% strain (MPa)

CHS

RHS

SHS

20

443

541

558

100

417

485

-

200

425

501

526

300

396

467

-

400

435

451

529

500

318

367

-

600

204

234

263

700

107

153

-

800

66

75

84

900

45

54

-

1000

31

36

-

Table 5 Measured values of ultimate strength from steady-state tests

Temperature (°C)

Ultimate strength (MPa)

CHS

RHS

SHS

20

480

541

559

100

453

489

-

200

435

519

529

300

438

482

-

400

475

460

532

500

330

367

-

600

205

235

263

700

107

157

-

800

68

77

84

900

49

54

-

1000

33

36

-

Table 6 Measured values of ultimate strain from steady-state tests

Temperature (°C)

Ultimate strain (%)

CHS

RHS

SHS

20

10.400

1.496

2.540

100

7.392

6.883

-

200

2.660

12.801

4.087

300

6.971

8.067

-

400

7.460

2.661

2.894

500

5.300

1.997

-

600

3.071

1.756

1.980

700

1.389

1.463

-

800

4.566

1.061

2.207

900

8.194

2.577

-

1000

7.507

3.671

-

Table 7 Measured values of fracture strain from steady-state tests

Temperature (°C)

Strain at fracture (%)

CHS

RHS

SHS

20

13.2

24.3

22.3

100

7.1

24.3

-

200

2.4

28.6

14.2

300

14.3

31.4

-

400

21.4

31.4

18.2

500

35.7

-

600

27.8

35.7

33.2

700

45.7

35.7

-

800

89.9

47.1

51.6

900

44.3

31.4

-

1000

36.4

38.6

Table 8 Tensile stresses applied in transient-state tests, predicted failure temperature ranges and actual failure temperatures

RHS

SHS

% of fu,20°C

Applied stress (MPa)

Predicted failure temperature (°C)

Actual failure temperature (°C)

Applied stress (MPa)

Predicted failure temperature (°C)

Actual failure temperature (°C)

100%

541

559

90%

495

20 – 300

94

-

-

-

80%

441

400 – 500

394

458

400 – 600

484

70%

402

400 – 500

456

-

-

-

60%

332

500 – 600

503

346

400 – 600

558

50%

275

500 – 600

572

-

-

-

40%

231

500 – 700

554

194

600 – 800

659

30%

168

600 – 700

660

-

-

-

20%

114

700 – 800

767

88

600 – 800

756

10%

54

800 – 1000

791

-

 -

-

Table 9 Experimentally-derived retention factors for modulus of elasticity

Temperature (°C)

kE

CHS steady-state

RHS steady-state

SHS steady-state

RHS transient-state

SHS transient-state

20

1.000

1.000

0.596

1.000

1.000

100

1.009

0.913

-

0.969

-

200

0.639

0.820

0.936

0.906

0.817

300

0.619

0.809

-

0.831

0.725

400

0.515

0.804

0.779

0.769

0.690

500

0.575

0.466

-

0.598

0.509

600

0.236

0.272

0.133

0.280

0.081

700

0.057

0.120

-

0.049

-

800

0.171

0.105

0.022

-

-

900

0.040

0.030

-

-

-

1000

0.049

0.004

-

-

-

Table 10 Experimentally-derived retention factors for 0.2% proof strength

Temperature (°C)

k0.2

CHS steady-state

RHS steady-state

SHS steady-state

20

1.000

1.000

1.000

100

0.908

0.898

-

200

0.923

0.919

0.960

300

0.890

0.827

-

400

0.953

0.834

0.962

500

0.656

0.665

-

600

0.285

0.408

0.422

700

0.264

0.258

-

800

0.140

0.129

0.158

900

0.111

0.100

-

1000

0.065

0.067

-

Table 11 Experimentally-derived retention factors for stress at 2% strain

Temperature (°C)

k2.0

CHS steady-state

RHS steady-state

SHS steady-state

RHS transient-state

SHS transient-state

20

1.000

1.000

1.000

1.000

1.000

100

0.941

0.896

-

-

-

200

0.958

0.927

0.943

-

-

300

0.893

0.864

-

0.815

-

400

0.980

0.834

0.948

-

-

450

-

-

-

0.685

0.821

500

0.717

0.679

-

0.537

-

550

-

-

-

0.500

0.620

600

0.459

0.432

0.471

-

-

650

-

-

-

0.241

0.348

700

0.240

0.283

-

-

-

712

-

-

-

-

0.158

750

-

-

-

0.083

-

800

0.150

0.138

0.151

-

-

900

0.102

0.100

-

-

-

1000

0.069

0.066

-

-

-

Table 12 Experimentally-derived retention factors for ultimate strength

Temperature (°C)

ku

CHS steady-state

RHS steady-state

SHS steady-state

RHS transient-state

SHS transient-state

20

1.000

1.000

1.000

1.000

1.000

100

0.945

0.904

-

-

-

200

0.905

0.959

0.947

-

-

300

0.912

0.891

-

-

-

400

0.989

0.850

0.953

-

-

450

-

-

-

0.913

-

480

-

-

-

-

0.821

500

0.688

0.679

-

-

-

550

-

-

-

0.713

-

560

-

-

-

-

0.620

600

0.428

0.435

0.471

0.608

-

650

-

-

-

0.508

0.348

700

0.223

0.291

-

0.416

-

750

-

-

-

0.311

0.158

800

0.141

0.143

0.150

-

-

900

0.102

0.100

-

-

-

1000

0.068

0.067

-

-

-

Table 13 Experimentally-derived retention factors for ultimate strain

Temperature (°C)

ku

CHS steady-state

RHS steady-state

SHS steady-state

20

1.000

1.000

1.000

100

0.711

4.602

-

200

0.256

8.559

1.609

300

0.670

5.394

-

400

0.717

1.779

1.139

500

0.510

1.335

-

600

0.295

1.174

0.780

700

0.134

0.978

-

800

0.439

0.710

0.869

900

0.788

1.723

-

1000

0.722

2.455

-

Table 14 Experimentally-derived retention factors for fracture strain

Temperature (°C)

kf

CHS steady-state

RHS steady-state

SHS steady-state

RHS transient-state

SHS transient-state

20

1.000

1.000

1.000

1.000

1.000

94

-

-

-

1.059

-

100

0.536

1.000

-

-

-

200

0.179

1.176

0.638

-

-

300

1.085

1.294

-

-

-

390

-

-

-

1.235

-

400

1.623

1.294

0.815

-

-

455

-

-

-

1.294

-

480

-

-

-

-

3.022

500

-

1.471

-

1.235

-

560

-

-

-

1.294

2.853

600

2.109

1.471

1.491

-

-

613

-

-

-

1.412

-

659

-

-

-

-

3.053

700

3.466

1.471

-

-

-

746

-

-

-

-

3.060

800

6.826

1.941

2.318

-

-

900

3.360

1.294

-

-

-

1000

2.758

1.588

-

-

-

CHS steady-state201002003004005006007008009001000181000180323.512681412300010219811421146832112253395479429700RHS steady-state201002003004005006007008009001000198630181334162975160748159604926605403323746.84621352699820788.8278058098116014.4950474532925845.67042618974074SHS steady-state201002003004005006007008009001000205000196537163540278914667RHS transient-state201002003004005006007008009001000198630192500180000.0000000007165108.69565217389152797.24048722661118821.2180746553655588.235294117689667.5191815856742SHS transient-state201002003004005006007008009001000210000171612.90322580628152226.79326076951144926.22595110664106954.9549549559317112.412673770395

Temperature (°C)

Modulus of elasticity (MPa)

CHS201002003004005006007008009001000404367373359.5385265115106.656.54526.17RHS201002003004005006007008009001000536.71171261660209482493444447.84357219138.6507096572715369.01694134814994253.61635174878705436.168750000000003SHS20100200300400500600700800900100054051052322484

Temperature (°C)

0.2% proof strength (MPa)

CHS steady-state201002003004005006007008009001000443.27500000000003417.17634907697192424.85944088708425395.9736842105263434.50972782214541317.70753414147617203.5137503004365106.5608127456310166.27322602447486645.4173147185230830.500525270227886RHS steady-state201002003004005006007008009001000540.84510788736611484.85495967474304501.44866432048451467.49840511842348451.1669650913858367.24554378713509233.87909194691923152.9938646308812974.66449016049855954.20426880154705935.943750000000001SHS steady-state20100200300400500600700800900100055852652926384RHS transient-state20300450500550650750541440.81481481481478370.68518518518522290.53703703703707270.5130.2407407407407345.083333333333329SHS transient-state2046654564271255845834619488

Temperature (°C)

Strength at 2% strain (MPa)

CHS steady-state201002003004005006007008009001000479.95625000000001453.44416722145837434.54240199906303437.80263157894734474.72757576850535330.26699401565139205.18844152924117107.2181805354393267.69293505963911248.86080919819496432.741014393897899RHS steady-state201002003004005006007008009001000540.95732676349553489.19043326903255518.6308021619468482.17875706232877459.86892997598824367.24554378713509235.14662827053374157.416712967214177.27924034626180154.33506092121392336.187500000000007SHS steady-state201002003004005006007008009001000558.70000000000005529.29999999999995532.29999999999995263.384RHS transient-state20450550600650700750541493.93299999999999385.733328.928274.82800000000003225.05599999999998168.251SHS transient-state20480559.6658.574655845834619488

Temperature (°C)

Ultimate strength (MPa)

CHS20100200300400500600700800900100010.47.39149999999999972.666.97142999999999987.465.33.07142999999999991.3885714.56599999999999988.19400000000000087.5069999999999997RHS2010020030040050060070080090010001.49571428571428566.882857142857142612.801428571428578.06714285714285672.66142857142857151.99714285714285731.75571428571428581.46285714285714311.06142857142857162.57714285714285653.6714285714285717SHS2010020030040050060070080090010002.544.08699999999999972.89400000000000011.982.2069999999999999

Temperature (°C)

Ultimate strain (%)

CHS steady-state20100200300400500600700800900100013.18470897.07313760000000082.365714285714286114.321.427.845.79044.336.363636363636367RHS steady-state20100200300400500600700800900100024.28571428571428524.28571428571428528.57142857142857331.42857142857142731.42857142857142735.71428571428571535.71428571428571535.71428571428571547.14285714285714631.42857142857142738.571428571428569SHS steady-state20100200300400500600700800900100022.27428571428571414.21285714285714318.15571428571428633.20571428571429451.637142857142869RHS transient-state209439045550056061324.28571000000000225.71428117647058929.99999470588235831.42856588235294529.99999470588235831.42856588235294534.285708235294123SHS transient-state20480559.6658.57462266.49142857142857162.76142857142856767.1728571428571467.320000000000007

Temperature (°C)

Fracture strain (%)

CHS steady-state20100200300400500600700800900100011.00855991943605240.6385397784491440.619335347432024120.514592145015105750.575080563947633410.235810674723061445.6520644511581064E-20.170966767371601213.998992950654582E-24.8841893252769386E-2RHS steady-state20100200300400500600700800900100010.912923526154155950.820495393445098920.809283592609374210.803524140361476120.466495494134823550.272028394502341010.119553170284080940.104661067340330323.0279892500897611E-24.2575161163456712E-3SHS steady-state20100200300400500600700800900100010.958717073170731740.797756097560975650.136053658536585352.2765853658536585E-2RHS transient-state2010020030040050060010.969138599405930610.906207521522432110.831237454826430520.769255603318867220.598203786309496890.279858205176044324.8670992204529397E-2SHS transient-state2010020030040050060010.817204301075267980.724889491717950030.690124885481460230.509309309309313958.1487679398906651E-2Chen and Young (2007) - G450225010015020025030035040045050055060065010.977600000000000020.937599999999999990.897599999999999950.857600000000000030.817599999999999990.777600000000000070.737600000000000030.69760.654090909090909060.479090909090909010.326818181818181790.197272727272727279.045454545454544E-2EN 1993-1-2201002003004005006007008009001000110.90.80.70.60.310.130.096.7500000000000004E-24.4999999999999998E-2AS41002010020030040050060070080090010000.997504574853707910.979148380428787710.941340306843403090.884551709033263520.802293574777276810.682925149072742380.505061409946561460.3201856148491880.184862692565304718.1512108682811557E-20

Temperature (°C)

kE

CHS steady-state20100200300400500600700800900100010.908415841584158450.923267326732673310.889851485148514860.952970297029702930.655940594059405970.284653465346534630.263861386138613870.139851485148514860.111386138613861396.4777227722772279E-2RHS steady-state20100200300400500600700800900100010.898061265795991330.918556439911667470.827259755214564630.834414434178582410.66516155993603510.408040284666643380.258333675971621880.128592202714703789.9897860412611644E-26.7389529890578351E-2SHS steady-state20100200300400500600700800900100010.960451977401129970.962335216572504760.421845574387947290.15819209039548024Chen and Young (2007) - G450228018032032040045045050055055066066097010.986999999999999990.970999999999999970.968999999999999970.986999999999999990.933000000000000050.850999999999999980.822999999999999950.726999999999999980.532000000000000030.606999999999999980.1070.1110.04Outinen and Mäkeläinen (2002) - S355J2H201002003004005006007007508008509001.0121.0120.956999999999999960.8710.761000000000000010.514000000000000010.238999999999999990.1087.8E-24.7E-23.5000000000000003E-22.1999999999999999E-2EN 1993-1-2201002003004004505005506006507007127508009001000111110.890.780.6250.470.350.230.215600000000000010.170.110.060.04AS41002010020030040050060070080090010001110.876811594202898560.731884057971014520.586956521739130490.44202898550724640.297101449275362310.152173913043478277.246376811594203E-30

Temperature (°C)

k0.2

CHS steady-state20100200300400450500550600650700712750800900100010.941123115621164910.958455678499992580.893291262107103410.98022610754530570.716727841952458760.45911398184070040.240394366354139080.14950815187970190.102458552182106096.8807230884276996E-2RHS steady-state20100200300400450500550600650700712750800900100010.896476556048865450.927157622409175760.864385012087014240.834188862045404210.679021661528305680.432432666092684330.282879261362835640.138051521723383750.100221427560430836.6458491490109739E-2SHS steady-state20100200300400450500550600650700712750800900100010.942652329749103960.948028673835125460.471326164874551980.15053763440860216RHS transient-state20100200300400450500550600650700712750800900100010.814814814814814770.685185185185185230.537037037037037090.50.240740740740740738.3333333333333329E-2SHS transient-state20100200300400450500550600650700712750800900100010.820788530465949790.620071684587813590.347670250896057350.15770609318996415Chen and Young (2007) - G450228018032032040045045050055055066066097010.9980.993999999999999991.01499999999999991.0541.050.936000000000000050.8770.774000000000000020.557000000000000050.647000000000000020.147999999999999990.147999999999999994.4999999999999998E-2EN 1993-1-2201002003004004505005506006507007127508009001000111110.890.780.6250.470.350.230.215600000000000010.170.110.060.04BS 5950-82002503003504004505005506001110.935000000000000050.866999999999999990.730.590.490.39

Temperature (°C)

k2.0

CHS steady-state20100200300400450480500550560600650700750800900100010.944761459448560940.905379192372352760.912171956462588640.98910593573582040.688118956708348660.427514886053137480.223391570659699330.141039803231313490.101802631381912346.8216664318670503E-2RHS steady-state20100200300400450480500550560600650700750800900100010.904305033071314160.958727752639701670.891343426194383450.850102045437386540.678880801900467510.434686095624949250.290996544790373230.142856444534391140.100442416126048716.6895295080865114E-2SHS steady-state20100200300400450480500550560600650700750800900100010.947377841417576310.952747449436191050.471272597100411640.15034902452120993RHS transient-state20100200300400450480500550560600650700750800900100010.913000000000000030.712999999999999970.607999999999999980.508000000000000010.415999999999999980.311SHS transient-state20100200300400450480500550560600650700750800900100010.820788530465949790.620071684587813590.347670250896057350.15770609318996415EN 1993-1-220100200300400450480500550560600650700750800900100011110.80.712000000000000080.659200000000000120.624000000000000110.50.475200000000000070.3760.280000000000000030.184000000000000020.136000000000000018.8000000000000009E-24.8000000000000001E-23.2000000000000001E-2Chen and Young (2007) - G450228014018022032040045050055066080097010.99965158571428570.997066014285714290.992956585714285690.98613858571428570.952743585714285750.90355330.805552083333333390.563833333333333410.384718750.154361333333333355.6333333333333332E-24.3006749999999996E-2

Temperature (°C)

ku

CHS steady-state20100200300400500600700800900100010.710721153846153750.255769230769230750.670329807692307660.717307692307692310.509615384615384580.295329807692307660.13351644230769230.439038461538461490.787884615384615410.72182692307692298RHS steady-state20100200300400500600700800900100014.60171919770773658.55873925501432715.39350525310410771.77936962750716351.33524355300859621.17382999044890180.978032473734479770.709646609360076621.72301814708691482.4546322827125122SHS steady-state20100200300400500600700800900100011.60905511811023621.13937007874015750.779527559055118060.86889763779527551Chen and Young (2007) - G450228014018022032040045050055066080097010001.00347027027027020.847027027027027040.704324324324324350.620.544324324324324320.392972972972972960.31081081081081080.277027027027027030.256756756756756740.250.219444444444444440.180555555555555550.133333333333333330.125

Temperature (°C)

keu

CHS steady-state2094100200300390400455480500560600613659700746800900100010.536465207813575650.179428632338957891.08458974016483591.62309233842849572.10850313122954123.46613644234496526.82608927376470123.35995283141973642.7580158681877585RHS steady-state20941002003003904004554805005606006136597007468009001000111.17647058823529421.29411764705882361.29411764705882361.47058823529411781.47058823529411781.47058823529411781.94117647058823551.29411764705882361.588235294117647SHS steady-state2094100200300390400455480500560600613659700746800900100010.638083632632118980.815097485890200151.49076449461262222.3182401231400722RHS transient-state2094100200300390400455480500560600613659700746800900100011.05882352941176471.23529411764705891.29411764705882361.23529411764705891.29411764705882361.411764705882353SHS transient-state2094100200300390400455480500560600613659700746800900100013.02233766233766232.85279220779220743.0533116883116883.0600000000000005Proposal2094100200300390400455480500560600613659700746800900100011.00766641.00896000000000011.04536000000000011.10976000000000011.19165999999999991.20215999999999991.2649151.29624000000000011.322561.40823999999999991.470961.49230859999999991.57164940000000011.64735999999999991.73790641.85176000000000012.08415999999999982.34456

Temperature (°C)

kef

20

o

A

L

65

.

5

=