SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley...

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SML resist - Processing Information Introduction SML resist has been specifically designed for electron beam lithography. It is a polymer that can be processed in exactly the same way as other polymer resists such as PMMA or ZEP. Typical Processing Conditions The processes outlined below are our standard processes, given as a guide only. Pilot work should be carried out to optimise the exposure paramters for your system. Substrate preparation Solvent clean with acetone and IPA. SML has excellent adhesion to most substrates so HMDS is not generally required. Spin coating See spin curves in the product information document. Baking Hot plate at 180°C for 120 - 180 seconds. For more information or to enquire about products, please call or email us. +44 (0)1625 704465 [email protected] www.emresist.com EM Resist, Alderley Park, Alderley Edge, Cheshire, SK10 4TG Guidline exposure at 30 kV Tungsten Thermal Field Emission Single pixel line clearing dose 1000-3000 pC/cm 1000-2000 pC/cm Area clearing dose 200-500 µC/cm 2 200-500 µC/cm 2 Developer IPA:H 2 O (7:3) for 30 seconds, followed by IPA rinse for 15 seconds. Hard-bake Convection oven at 80°C for 30 minutes. Stripper Acetone Guideline exposure at 100 kV Thermal Field Emission Single pixel line clearing dose 1000-2000 pC/cm Area clearing dose 200-500 µC/cm 2

Transcript of SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley...

Page 1: SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. Phone: +44 (0) 1625 573304 Email: info@emresist.com

SML resist - Processing Information

IntroductionSML resist has been specifically designed for electron beam lithography. It is a polymer that can be processed in exactly the same way as other polymer resists such as PMMA or ZEP.

Typical Processing ConditionsThe processes outlined below are our standard processes, given as a guide only. Pilot work should be carried out to optimise the exposure paramters for your system.

Substrate preparation Solvent clean with acetone and IPA. SML has excellent adhesion to most substrates so HMDS is not generally required.

Spin coating See spin curves in the product information document.

Baking Hot plate at 180°C for 120 - 180 seconds.

For more information or to enquire about products, please call or email us.

+44 (0)1625 704465 [email protected] www.emresist.com EM Resist, Alderley Park, Alderley Edge, Cheshire, SK10 4TG

Guidline exposure at 30 kV

Tungsten Thermal Field Emission

Single pixel line clearing dose 1000-3000 pC/cm 1000-2000 pC/cm

Area clearing dose 200-500 µC/cm2 200-500 µC/cm2

Developer IPA:H2O (7:3) for 30 seconds, followed by IPA rinse for 15 seconds.

Hard-bake Convection oven at 80°C for 30 minutes.

Stripper Acetone

Guideline exposure at 100 kV

Thermal Field Emission

Single pixel line clearing dose 1000-2000 pC/cm

Area clearing dose 200-500 µC/cm2

Page 2: SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. Phone: +44 (0) 1625 573304 Email: info@emresist.com

SML50

Step size: 5nm

Current: 3.7nA

Dose: 860μC/cm2

Line width: 9nm

Pitch: 40nm

Developer: MIBK:IPA (1:3) for 30 seconds followed by IPA rinse for 15 seconds

SML50

Step size: 5nm

Current: 260pA

Dose: 1180μC/cm2

Line width: 6nm

Pitch: 35nm

Developer: IPA:H2O (7:3) for 30 seconds followed by IPA rinse for 15 seconds

www.emresist.com

100 kV Exposure Parameters

Please note that the best results (aspect ratio and resolution) are generally achieved when a relatively low beam current is used.

Resist: SML50

Instrument: Vistec EBPG 5000+Step size: 5 nmCurrent: 3.7 nADose: 860 μC/cm2

Line width: 9 nmPitch: 40 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML50

Instrument: Vistec EBPG 5000+Step size: 5 nmCurrent: 260 pADose: 1180 μC/cm2

Line width: 6 nmPitch: 35 nmDeveloper: IPA:H2O (3:7) for 30 secondsfollowed by IPA rinse for 15 seconds

www.emresist.com

100 kV Exposure Parameters

Please note that the best results (aspect ratio and resolution) are generally achieved when a relatively low beam current is used.

Resist: SML50

Instrument: Vistec EBPG 5000+Step size: 5 nmCurrent: 3.7 nADose: 860 μC/cm2

Line width: 9 nmPitch: 40 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML50

Instrument: Vistec EBPG 5000+Step size: 5 nmCurrent: 260 pADose: 1180 μC/cm2

Line width: 6 nmPitch: 35 nmDeveloper: IPA:H2O (3:7) for 30 secondsfollowed by IPA rinse for 15 seconds

For more information or to enquire about products, please call or email us.

+44 (0)1625 704465 [email protected] www.emresist.com EM Resist, Alderley Park, Alderley Edge, Cheshire, SK10 4TG

Example Exposures at 100kVAll 100kV exposures were performed by Caltech, CA, on a Vistec EPBG 5000+.

Page 3: SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. Phone: +44 (0) 1625 573304 Email: info@emresist.com

SML100

Step size: 10nm

Current: 1.6nA

Dose: 1310μC/cm2

Line width: 250nm

Pitch: 500nm

Developer: MIBK:IPA (1:3) for 30 seconds followed by IPA rinse for 15 seconds

SML2000

Step size: 10nm

Current: 10nA

Dose: 2100μC/cm2

Line width: 100nm

Pitch: 600nm

Developer: MIBK:IPA (1:3) for 30 seconds followed by IPA rinse for 15 seconds

SML2000

Step size: 10nm

Current: 239pA

Dose: 1050μC/cm2

Line width: 20 - 30nm

Pitch: 150nm

Developer: MIBK:IPA (1:3) for 30 seconds followed by IPA rinse for 15 seconds

www.emresist.com

Resist: SML100

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 1.6 nADose: 1310 μC/cm2

Write Field: 560 μm2

Line width: 250 nmPitch: 500 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML2000

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 10 nADose: 2100 μC/cm2

Write Field: 560 μm2

Line width: 100 nmPitch: 600 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML2000

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 239 pADose: 1050 μC/cm2

WriteField: 560 μm2

Line width: 20-30 nmPitch: 150 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

www.emresist.com

Resist: SML100

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 1.6 nADose: 1310 μC/cm2

Write Field: 560 μm2

Line width: 250 nmPitch: 500 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML2000

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 10 nADose: 2100 μC/cm2

Write Field: 560 μm2

Line width: 100 nmPitch: 600 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML2000

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 239 pADose: 1050 μC/cm2

WriteField: 560 μm2

Line width: 20-30 nmPitch: 150 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

www.emresist.com

Resist: SML100

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 1.6 nADose: 1310 μC/cm2

Write Field: 560 μm2

Line width: 250 nmPitch: 500 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML2000

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 10 nADose: 2100 μC/cm2

Write Field: 560 μm2

Line width: 100 nmPitch: 600 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML2000

Instrument: Vistec EBPG 5000+Step size: 10 nmCurrent: 239 pADose: 1050 μC/cm2

WriteField: 560 μm2

Line width: 20-30 nmPitch: 150 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

For more information or to enquire about products, please call or email us.

+44 (0)1625 704465 [email protected] www.emresist.com EM Resist, Alderley Park, Alderley Edge, Cheshire, SK10 4TG

Page 4: SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. Phone: +44 (0) 1625 573304 Email: info@emresist.com

For more information or to enquire about products, please call or email us.

+44 (0)1625 704465 [email protected] www.emresist.com EM Resist, Alderley Park, Alderley Edge, Cheshire, SK10 4TG

SML50

Step size: 2nm

Current: 11.67pA

Dose: 600pC/cm

Line width: 5nm

Pitch: 40nm

Developer: IPA:H2O (7:3) for 30 seconds followed by IPA rinse for 15 seconds

SML300

Step size: 2nm

Current: 12pA

Dose: 1380pC/cm

Line width: 33nm

Pitch: 300nm

Developer: IPA:H2O (7:3) for 30 seconds followed by IPA rinse for 15 seconds

www.emresist.com

30 kV Exposure Parameters

Resist: SML50

Instrument: Raith E-LiNEStep size: 2 nmCurrent : 11.67 pADose: 600 pC/cmWrite Field: 100 μm2

Line width: 5 nmPitch: 40 nmDeveloper: IPA:H20 (7:3) for 30 seconds,followed by IPA rinse for 15 seconds

Resist: SML300

Instrument: Raith E-LiNEStep size: 2 nmCurrent : 12 pADose: 1380 pC/cmLine width: 33 nmPitch: 300 nmDeveloper: IPA:H2O (7:3) for 30 seconds,followed by IPA rinse for 15 seconds

www.emresist.com

30 kV Exposure Parameters

Resist: SML50

Instrument: Raith E-LiNEStep size: 2 nmCurrent : 11.67 pADose: 600 pC/cmWrite Field: 100 μm2

Line width: 5 nmPitch: 40 nmDeveloper: IPA:H20 (7:3) for 30 seconds,followed by IPA rinse for 15 seconds

Resist: SML300

Instrument: Raith E-LiNEStep size: 2 nmCurrent : 12 pADose: 1380 pC/cmLine width: 33 nmPitch: 300 nmDeveloper: IPA:H2O (7:3) for 30 seconds,followed by IPA rinse for 15 seconds

Example Exposures at 30kVAll 30kV exposures were performed on a Raith E-line.

Page 5: SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. Phone: +44 (0) 1625 573304 Email: info@emresist.com

For more information or to enquire about products, please call or email us.

+44 (0)1625 704465 [email protected] www.emresist.com EM Resist, Alderley Park, Alderley Edge, Cheshire, SK10 4TG

Example Exposures at 25kVAll 25kV exposures were performed on a Cambridge S360 with a tungsten source and a 300kHz Elphy Quantum pattern generator.

SML600

Step size: 3.1nm

Current: 15pA

Dose: 2530pC/cm

Line width: 50nm

Pitch: 400nm

Developer: MIBK:IPA (1:3) for 30 seconds followed by IPA rinse for 15 seconds

SML300

Step size: 3.1nm

Current: 15pA

Dose: 1000pC/cm

Line width: 50nm

Pitch: 400nm

Developer: MIBK:IPA (1:3) for 30 seconds followed by IPA rinse for 15 seconds

www.emresist.com

25 kV Exposure Parameters

Resist: SML600

Instrument: Cambridge S360 tungsten source with a 300KHz Elphy Quantum pattern generator.Step size: 3.1 nmCurrent: 15 pADose: 2530 pC/cmWrite Field: 200 μm2

Line width: 50 nmPitch: 400 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML300

Instrument: Cambridge S360 tungsten source with a 300KHz Elphy Quantum pattern generator.Step size: 3.1 nmCurrent: 15 pADose: 1000 pC/cmWrite Field: 200 μm2

Line width: 50 nmPitch: 400 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. www.emresist.com Phone: +44 (0) 1625 573304 Email: [email protected]

www.emresist.com

25 kV Exposure Parameters

Resist: SML600

Instrument: Cambridge S360 tungsten source with a 300KHz Elphy Quantum pattern generator.Step size: 3.1 nmCurrent: 15 pADose: 2530 pC/cmWrite Field: 200 μm2

Line width: 50 nmPitch: 400 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

Resist: SML300

Instrument: Cambridge S360 tungsten source with a 300KHz Elphy Quantum pattern generator.Step size: 3.1 nmCurrent: 15 pADose: 1000 pC/cmWrite Field: 200 μm2

Line width: 50 nmPitch: 400 nmDeveloper: MIBK:IPA (1:3) for 30 secondsfollowed by IPA rinse for 15 seconds

EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. www.emresist.com Phone: +44 (0) 1625 573304 Email: [email protected]

Page 6: SML resist - Processing Information€¦ · EM Resist Ltd, Unit 6, Normans Hall Farm, Shrigley Road, Macclesfield, SK10 5SE, UK. Phone: +44 (0) 1625 573304 Email: info@emresist.com