SEY of MgO and Al 2 O 3 as deposited by ALD
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Transcript of SEY of MgO and Al 2 O 3 as deposited by ALD
SEY of MgO and Al2O3 as deposited by ALD
Slade Jokela, Igor Veryovkin, Alex Zinovev
Film Properties
• MgO– Thickness – 6nm
– ALD-deposited
– 12 at.% C
• Al2O3
– Thickness – 9nm
– ALD-deposited
– 12 at.% C
0 200 400 600 800
0
1
2
3
4
5
6
SEY
(se
cond
arie
s pe
r pr
imar
y)
Primary Electron Energy (eV)
Al2O
3 Scan 1
Al2O
3 Scan 2
MgO Scan 1 MgO Scan 2
SEY of Al2O3
• Significantly decreased electron beam current– Decreased from ~6A to 0.01A– Dose effect seems to have diminished
0 200 400 600 800
0
1
2
3
4
5
SEY
(se
cond
arie
s pe
r pr
imar
y)
Primary Electron Energy (eV)
Al2O
3 - 9nm ALD
Scan 1 Scan 2 Scan 3
UPS of Al2O3 and MgO
• Spectra have decreased sensitivity to low energy electrons
– Small magnetic fields can deflect electrons away from detector
– Will apply bias voltage to sample
0 5 10 15 20-20000
0
20000
40000
60000
80000
100000
120000
140000
Ele
ctro
n C
ount
Electron Kinetic Energy (eV)
UPS of Al2O
3 (21.2 eV He)
0 5 10 15 20-20000
0
20000
40000
60000
80000
100000
120000
140000
Cou
nts
Electron Kinetic Energy (eV)
UPS of MgO (21.2eV He)
Future Plans
• Apply voltage bias to sample– This will overcome detector’s “insensitivity” to
low kinetic energy electrons
• Install electron gun that can be defocused– This will allow us to cover a large area of the
sample with electrons– Desorption of surface species may then be
detectable by XPS