SATL Results from Crystal City Water Testing

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    KSAT-12

    RE: Crystal City Water

    San Antonio, TX 78215

    1408 N. St.Mary's

    Pilar Arias

    SATL received 1 Sample(s) on 02/23/2016 for analyses identified on the chain of custody. The analyses were

    performed using methods indicated on the laboratory report. Any deviations observed at sample receiving are

    notated on the Sample Receipt Checklist and/or Chain of Custody documents attached as part of this analytical

    report.

    There were no problems in the sample analyses unless otherwise noted. Sample data and associated QC are

    presented in the attached laboratory report. QC sample data were within laboratory acceptance limits except where

    noted on the report.

    Sincerely,

    For San Antonio Testing Laboratory, Inc.

    February 25, 2016

    1602357SATL Report No.:

    Dear Pilar Arias

  • 7/24/2019 SATL Results from Crystal City Water Testing

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Sample ID Laboratory ID Matrix Date Sampled

    SAMPLE SUMMARY

    Date Received

    Total Samples received in this work order: 1

    Sampling Method

    The following samples were requested for analysis as per the CoC. Any re-runs or re-analyses requested are identified as such.

    Crystal City Water 1602357-01 02/17/16 22:00 02/23/16 14:02Liquid Grab

    All quality control samples and checks are within acceptance limits unless otherwise indicated.

    Test results pertain only to those items tested.

    All samples were in good condition when received by the laboratory unless otherwise noted.

    Notes

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Sample Matrix: Liquid

    Sample ID #: Crystal City Water Lab Sample ID #: 1602357-01Sampling Method: Grab

    Date/Time Collected: 02/17/16 22:00

    Analyte Result PQL Batch Analyzed MethodUnits Analyst NotesPrep Method

    Total Metals By ICP-OES

    02/24/16 14:050.050 B609085 EPA 200.70.940 mg/L XEAluminum * EPA 200.7

    02/24/16 14:050.010 B609085 EPA 200.7

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Sample Matrix: Liquid

    Sample ID #: Crystal City Water Lab Sample ID #: 1602357-01Sampling Method: Grab

    Date/Time Collected: 02/17/16 22:00

    Analyte Result PQL Batch Analyzed MethodUnits Analyst NotesPrep Method

    Volatile Organic Compounds by GC/MS

    02/24/16 12:310.010 B609087 EPA 8260C

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Sample Matrix: Liquid

    Sample ID #: Crystal City Water Lab Sample ID #: 1602357-01Sampling Method: Grab

    Date/Time Collected: 02/17/16 22:00

    Analyte Result PQL Batch Analyzed MethodUnits Analyst NotesPrep Method

    Volatile Organic Compounds by GC/MS

    02/24/16 12:310.005 B609087 EPA 8260C

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Total Metals By ICP-OES - Quality Control

    Batch B609081 - EPA 245.1

    Blank (B609081-BLK1) Prepared: 02/24/16 09:10 Analyzed: 02/24/16 14:12

    Mercury 0.0002 mg/L

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Total Metals By ICP-OES - Quality Control

    Batch B609085 - EPA 200.7

    Blank (B609085-BLK1) Prepared: 02/24/16 08:48 Analyzed: 02/24/16 10:48

    Thallium 0.010 mg/L

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Total Metals By ICP-OES - Quality Control

    Batch B609085 - EPA 200.7

    LCS Dup (B609085-BSD1) Prepared: 02/24/16 08:48 Analyzed: 02/24/16 10:59

    Arsenic 0.010 2.00 2085-115100 0.3mg/L1.99Barium 0.010 2.00 2085-115101 0.7mg/L2.03

    Beryllium 0.004 2.00 2085-11599 0.3mg/L1.98

    Boron 0.010 2.00 2085-115100 0.2mg/L2.00

    Cadmium 0.005 2.00 2085-11599 0.1mg/L1.98

    Calcium 1.00 2.00 2085-115100 0.05mg/L1.99

    Chromium 0.010 2.00 2085-115100 0.4mg/L1.99

    Cobalt 0.010 2.00 2085-11599 0.2mg/L1.99

    Copper 0.010 2.00 2085-11599 0.1mg/L1.98

    Iron 0.050 2.00 2085-11599 0.4mg/L1.99

    Lead 0.010 2.00 2085-11599 0mg/L1.98

    Magnesium 0.050 2.00 2085-11599 0.1mg/L1.98

    Manganese 0.010 2.00 2085-115100 0.1mg/L1.99

    Molybdenum 0.010 2.00 2085-115100 0.3mg/L2.00

    Nickel 0.010 2.00 2085-115100 0mg/L1.99

    Potassium 1.00 20.0 2085-11599 0.4mg/L19.8

    Selenium 0.010 2.00 2085-115100 0.05mg/L2.00

    Silver 0.010 1.00 2085-115110 0.5mg/L1.10

    Sodium 1.00 2.00 2085-115100 2mg/L1.99

    Strontium 0.010 2.00 2085-11599 0.2mg/L1.98Thallium 0.010 2.00 2085-115100 0.05mg/L2.00

    Tin 0.010 2.00 2085-11599 0.2mg/L1.98

    Titanium 0.010 2.00 2085-115100 0.5mg/L2.00

    Vanadium 0.010 2.00 2085-11599 0.2mg/L1.98

    Zinc 0.010 2.00 2085-11599 0.2mg/L1.98

    Duplicate (B609085-DUP1) Source: 1602335-01 Prepared: 02/24/16 08:48 Analyzed: 02/24/16 13:49

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Total Metals By ICP-OES - Quality Control

    Batch B609085 - EPA 200.7

    Duplicate (B609085-DUP1) Source: 1602335-01 Prepared: 02/24/16 08:48 Analyzed: 02/24/16 13:49

    Iron 0.050 206mg/L0.218 0.204Lead 0.010 200mg/L0.00250 0.00250

    Magnesium 0.050 201mg/L3.76 3.71

    Manganese 0.010 202mg/L0.0321 0.0315

    Molybdenum 0.010 201mg/L2.08 2.06

    Nickel 0.010 205mg/L0.00630 0.00600

    Potassium 1.00 201mg/L9.52 9.43

    Selenium 0.010 20mg/L

  • 7/24/2019 SATL Results from Crystal City Water Testing

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Total Metals By ICP-OES - Quality Control

    Batch B609085 - EPA 200.7

    Matrix Spike (B609085-MS1) Source: 1602335-01 Prepared: 02/24/16 08:48 Analyzed: 02/24/16 13:54

    Silver 0.010 1.00 75-125120mg/L1.21 0.00590Sodium 1.00 2.00 75-12577mg/L17.9 16.4

    Strontium 0.010 2.00 75-125104mg/L2.19 0.106

    Thallium 0.010 2.00 75-125111mg/L2.22

  • 7/24/2019 SATL Results from Crystal City Water Testing

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    Blank (B609087-BLK1) Prepared: 02/24/16 09:30 Analyzed: 02/24/16 10:22

    2-Chlorotoluene 0.005 mg/L

  • 7/24/2019 SATL Results from Crystal City Water Testing

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    Blank (B609087-BLK1) Prepared: 02/24/16 09:30 Analyzed: 02/24/16 10:22

    Naphthalene 0.005 mg/L

  • 7/24/2019 SATL Results from Crystal City Water Testing

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    LCS (B609087-BS1) Prepared: 02/24/16 09:30 Analyzed: 02/24/16 10:54

    Carbon Tetrachloride 0.005 0.0500 63.7-121102mg/L0.0512Chlorobenzene 0.005 0.0500 70.7-138100mg/L0.0500

    Chloroethane 0.005 0.0500 30.6-174107mg/L0.0536

    2-Chloroethyl Vinyl Ether 0.005 0.0500 25.2-13657mg/L0.0285

    Chloroform 0.005 0.0500 73.2-125105mg/L0.0525

    Chloromethane 0.005 0.0500 51.7-193103mg/L0.0516

    2-Chlorotoluene 0.005 0.0500 60.9-13699mg/L0.0493

    4-Chlorotoluene 0.005 0.0500 60.9-13699mg/L0.0494

    Dibromochloromethane 0.005 0.0500 65.2-12699mg/L0.0494

    1,2-Dibromo-3-chloropropane 0.005 0.0500 58.8-11892mg/L0.0462

    1,2-Dibromoethane 0.005 0.0500 71.6-12499mg/L0.0494

    Dibromomethane 0.005 0.0500 76.7-124103mg/L0.0513

    1,2-Dichlorobenzene 0.005 0.0500 56.8-13796mg/L0.0482

    1,3-Dichlorobenzene 0.005 0.0500 49.9-14598mg/L0.0490

    1,4-Dichlorobenzene 0.005 0.0500 51.7-13897mg/L0.0485

    rans-1,4-Dichloro-2-butene 0.005 0.0500 43-13798mg/L0.0489

    cis-1,4-Dichloro-2-butene 0.005 0.0500 39.8-13195mg/L0.0474

    Dichlorodifluoromethane 0.005 0.0500 27.9-25090mg/L0.0451

    1,1-Dichloroethane 0.005 0.0500 59.9-136104mg/L0.0518

    1,2-Dichloroethane 0.005 0.0500 67.5-129104mg/L0.0521

    1,1-Dichloroethene 0.005 0.0500 67.1-138105mg/L0.0524

    cis-1,2-Dichloroethylene 0.005 0.0500 63.1-136105mg/L0.0523

    rans-1,2-Dichloroethylene 0.005 0.0500 62.6-138106mg/L0.0530

    1,2-Dichloropropane 0.005 0.0500 75.2-125105mg/L0.0525

    1,3-Dichloropropane 0.005 0.0500 79.9-123102mg/L0.0508

    2,2-Dichloropropane 0.005 0.0500 56.4-153102mg/L0.0512

    1 1 Di hl l 0 005 0 0500 60 4 136105/L0 0527

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    LCS (B609087-BS1) Prepared: 02/24/16 09:30 Analyzed: 02/24/16 10:54

    Acetonitrile 0.005 0.0500 44-149108mg/L0.0539Methyl Iodide 0.005 0.0500 48.6-13688mg/L0.0442

    Methyl Methacrylate 0.005 0.0500 66.2-121104mg/L0.0521

    Methyl-tert-Butyl Ether 0.005 0.0500 16.3-183102mg/L0.0510

    Methylene Chloride 0.005 0.0500 61.3-148104mg/L0.0519

    Naphthalene 0.005 0.0500 5.3-15288mg/L0.0439

    Propylbenzene 0.005 0.0500 60.2-139102mg/L0.0508

    Styrene 0.005 0.0500 62.3-146102mg/L0.0508

    1,1,1,2-Tetrachloroethane 0.005 0.0500 72.4-13099mg/L0.0495

    1,1,2,2-Tetrachloroethane 0.005 0.0500 63.3-115100mg/L0.0498

    Toluene 0.005 0.0500 66-130102mg/L0.0512

    1,2,3-Trichlorobenzene 0.005 0.0500 6.55-14489mg/L0.0447

    1,2,4-Trichlorobenzene 0.005 0.0500 21.8-15591mg/L0.0456

    1,1,1-Trichloroethane 0.005 0.0500 66.9-126102mg/L0.0511

    1,1,2-Trichloroethane 0.005 0.0500 76.5-123101mg/L0.0504

    Trichlorofluoromethane 0.005 0.0500 60.5-160107mg/L0.0534

    1,2,3-Trichloropropane 0.005 0.0500 58.7-122100mg/L0.0502

    1,2,4-Trimethylbenzene 0.005 0.0500 60.7-138100mg/L0.0502

    1,3,5-Trimethylbenzene 0.005 0.0500 60.9-13999mg/L0.0494

    Vinyl acetate 0.005 0.0500 29.6-14399mg/L0.0495

    Vinyl chloride 0.005 0.0500 45.8-190106mg/L0.0532

    ,p-Xylenes 0.005 0.100 27.4-146103mg/L0.103

    o-Xylene 0.005 0.0500 64.9-129100mg/L0.0502

    0.0500 87.4-109Surrogate: Toluene-d8 1020.0509 mg/L

    0.0500 65.7-120Surrogate: 4-Bromofluorobenzene 1020.0510 mg/L

    0.0500 81.2-126 Surrogate: Dibromofluoromethane 1050.0526 mg/L

  • 7/24/2019 SATL Results from Crystal City Water Testing

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    LCS Dup (B609087-BSD1) Prepared: 02/24/16 09:30 Analyzed: 02/24/16 11:26

    Trichloroethene 0.005 0.0500 17.571.1-136100 1mg/L0.0502Butylbenzene 0.005 0.0500 27.442.8-155102 2mg/L0.0512

    sec-Butylbenzene 0.005 0.0500 25.256.8-143103 2mg/L0.0513

    ert-Butylbenzene 0.005 0.0500 25.361.6-138101 2mg/L0.0503

    Carbon disulfide 0.005 0.0500 27.653.9-166106 3mg/L0.0532

    Carbon Tetrachloride 0.005 0.0500 18.663.7-121104 2mg/L0.0521

    Chlorobenzene 0.005 0.0500 18.470.7-138101 0.9mg/L0.0505

    Chloroethane 0.005 0.0500 2030.6-174106 0.7mg/L0.0532

    2-Chloroethyl Vinyl Ether 0.005 0.0500 34.825.2-13660 6mg/L0.0302

    Chloroform 0.005 0.0500 17.873.2-125108 3mg/L0.0539

    Chloromethane 0.005 0.0500 26.951.7-193106 2mg/L0.0528

    2-Chlorotoluene 0.005 0.0500 24.760.9-136103 4mg/L0.0514

    4-Chlorotoluene 0.005 0.0500 23.560.9-136101 2mg/L0.0506

    Dibromochloromethane 0.005 0.0500 19.865.2-126100 0.7mg/L0.0498

    1,2-Dibromo-3-chloropropane 0.005 0.0500 27.358.8-11895 3mg/L0.0477

    1,2-Dibromoethane 0.005 0.0500 20.371.6-124100 0.9mg/L0.0498

    Dibromomethane 0.005 0.0500 22.476.7-124103 0.8mg/L0.0517

    1,2-Dichlorobenzene 0.005 0.0500 20.756.8-137100 4mg/L0.0502

    1,3-Dichlorobenzene 0.005 0.0500 20.749.9-145101 3mg/L0.0504

    1,4-Dichlorobenzene 0.005 0.0500 19.451.7-138100 3mg/L0.0500

    rans-1,4-Dichloro-2-butene 0.005 0.0500 32.443-137100 2mg/L0.0500

    cis-1,4-Dichloro-2-butene 0.005 0.0500 38.339.8-13197 2mg/L0.0485

    Dichlorodifluoromethane 0.005 0.0500 16.627.9-25094 4mg/L0.0469

    1,1-Dichloroethane 0.005 0.0500 20.759.9-136107 3mg/L0.0535

    1,2-Dichloroethane 0.005 0.0500 16.567.5-129105 0.2mg/L0.0523

    1,1-Dichloroethene 0.005 0.0500 17.667.1-138108 3mg/L0.0538

    i 1 2 Di hl h l 0 005 0 0500 23 563 1 136108 3/L0 0538

  • 7/24/2019 SATL Results from Crystal City Water Testing

    16/25

    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    LCS Dup (B609087-BSD1) Prepared: 02/24/16 09:30 Analyzed: 02/24/16 11:26

    Isopropylbenzene (Cumene) 0.005 0.0500 25.164.8-130103 1mg/L0.05164-Isopropyltoluene 0.005 0.0500 25.854.2-144103 3mg/L0.0513

    Methacrylonitrile 0.005 0.0500 23.755.4-136110 2mg/L0.0550

    Methyl Butyl Ketone (2-Hexanone) 0.005 0.0500 23.770.5-130113 1mg/L0.0563

    Methyl Ethyl Ketone (2-Butanone) 0.005 0.0500 30.756.5-136119 2mg/L0.0597

    Acetonitrile 0.005 0.0500 30.144-149110 2mg/L0.0552

    Methyl Iodide 0.005 0.0500 28.548.6-13694 6mg/L0.0471

    Methyl Methacrylate 0.005 0.0500 28.866.2-121105 1mg/L0.0526

    Methyl-tert-Butyl Ether 0.005 0.0500 25.816.3-183105 3mg/L0.0526

    Methylene Chloride 0.005 0.0500 21.561.3-148105 1mg/L0.0524

    Naphthalene 0.005 0.0500 305.3-15292 4mg/L0.0458

    Propylbenzene 0.005 0.0500 25.260.2-139104 2mg/L0.0521

    Styrene 0.005 0.0500 23.462.3-146103 1mg/L0.0515

    1,1,1,2-Tetrachloroethane 0.005 0.0500 21.672.4-130100 0.6mg/L0.0498

    1,1,2,2-Tetrachloroethane 0.005 0.0500 20.563.3-115102 3mg/L0.0511

    Toluene 0.005 0.0500 15.666-130103 0.6mg/L0.0515

    1,2,3-Trichlorobenzene 0.005 0.0500 29.76.55-14493 4mg/L0.0465

    1,2,4-Trichlorobenzene 0.005 0.0500 27.221.8-15593 3mg/L0.0467

    1,1,1-Trichloroethane 0.005 0.0500 20.466.9-126104 2mg/L0.0522

    1,1,2-Trichloroethane 0.005 0.0500 18.776.5-123101 0.3mg/L0.0506

    Trichlorofluoromethane 0.005 0.0500 16.160.5-160109 2mg/L0.0545

    1,2,3-Trichloropropane 0.005 0.0500 24.758.7-122101 1mg/L0.0507

    1,2,4-Trimethylbenzene 0.005 0.0500 24.160.7-138102 2mg/L0.0512

    1,3,5-Trimethylbenzene 0.005 0.0500 25.660.9-139102 3mg/L0.0511

    Vinyl acetate 0.005 0.0500 27.129.6-143105 5mg/L0.0523

    Vinyl chloride 0.005 0.0500 32.445.8-190108 2mg/L0.0541

    X l 0 005 0 100 24 527 4 146103 0 2/L0 103

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    Matrix Spike (B609087-MS1) Source: 1602357-01 Prepared: 02/24/16 09:30 Analyzed: 02/24/16 13:03

    Bromochloromethane 0.005 0.0500 68.4-140101mg/L0.0504

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    Matrix Spike (B609087-MS1) Source: 1602357-01 Prepared: 02/24/16 09:30 Analyzed: 02/24/16 13:03

    cis-1,3-Dichloropropylene 0.005 0.0500 44.6-14699mg/L0.0497

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    Acetone 0.010 0.0500 10.319.5-259111 5mg/L0.0553

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    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    Matrix Spike Dup (B609087-MSD1) Source: 1602357-01 Prepared: 02/24/16 09:30 Analyzed: 02/24/16 13:35

    2,2-Dichloropropane 0.005 0.0500 39.979-14899 7mg/L0.0496

  • 7/24/2019 SATL Results from Crystal City Water Testing

    21/25

    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Result Limit

    Reporting

    Units Level

    Spike

    Result

    Source

    %REC

    %REC

    Limits RPD

    RPD

    LimitAnalyte

    Volatile Organic Compounds by GC/MS - Quality Control

    Batch B609087 - 5030B

    Matrix Spike Dup (B609087-MSD1) Source: 1602357-01 Prepared: 02/24/16 09:30 Analyzed: 02/24/16 13:35

    0.0500 81.2-126 Surrogate: Dibromofluoromethane 106 0.0532 mg/L

    Milligrams per Kilogram (Parts per Million)mg/Kg

    Practical Quantitation LimitPQL

    Milligrams per Liter (Parts per Million)mg/L

    Parts per MillionPPM

    TNI / NELAC accredited analyte*

    RMCCL Recommended Maximum Concentration of Contaminants Level

    Maximum Contaminant LevelMCL

    MicroRoentgens per hour (Measure of Radioactivity Level)R/hr

    DEFINITIONS

    LCS recovery is outside QC acceptance limits, the results may have a slight bias.L

    MS recovery is outside QC limits, the results may have a slight bias due to possible matrix interferences.M

    Surrogate recovery is outside QC limits due to matrix interferences.Surr L

    Surr H Surrogate recovery is high due to contribution from hydrocarbon interferences.

    Standard Methods for the Examination of Water and Wastewater, 21st Edition 2005

    Methods for Chemical Analysis of Water and Wastes, EPA 600/4-79-020, Rev. March 1983

    EPA SW Test Methods for the Examination of Solid Waste, SW-846, 1996

    Test Methods followed by the laboratory are referenced in the following approved methodology, unless otherwise specified.

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    22/25

    Project: Crystal City Water

    Project Number: [none]

    Project Manager: Pilar Arias

    Reported:KSAT-12

    1408 N. St.Mary's 02/25/16 09:48

    San Antonio TX, 78215

    Report No. 1602357

    NELAC Cert. No.:

    Received:

    02/23/16 14:02

    LABORATORY REPORT

    Additional Notes:

    T104704360-16-12

    Aimee Landon For Marcela Gracia Hawk, President For The results in this report apply to the samples analyzed in accordance with the chain ofcustody document. This analytical report must be reproduced in its entirety.

    Richard Hawk, General Manager

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    1610 S. Laredo Street, San Antonio, Texas 78207-7029 (210) 229-9920 Fax (210) 229-9921

    KSAT 12 Crystal City Water/Sediment Sample

    ContaminantResult

    (ppm)*

    EPA DW Limit

    (ppm)1Times Higher Potential Health Effects from Long-term exposure above MCL2

    Aluminum 0.94 0.2 4.7 XSecondary Contaminant may cause cosmetic effects (such as skin or tooth

    discoloration) or aesthetic effects (such as taste, odor, or color)

    Beryllium 0.008 0.004 2 X Intestinal Lesions

    Iron 171 0.3 570 XSecondary Contaminant may cause cosmetic effects (such as skin or toothdiscoloration) or aesthetic effects (such as taste, odor, or color)

    Manganese 6.98 0.05 139 XSecondary Contaminant may cause cosmetic effects (such as skin or tooth

    discoloration) or aesthetic effects (such as taste, odor, or color)

    Lead 0.098 0.015 6.5 X

    Infants & Children: Delays in physical or mental development;

    Children could show deficits in attention span and learning abilities;

    Adults: Kidney problems, high blood pressure.

    1PPM = Parts Per Million2Reference EPA National Primary & Secondary Drinking Water Regulations

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