,rjorie McLaugh!in -, Whittaker waste manifest activities · 2012. 11. 30. · ANALYTICAL. REPORT...
Transcript of ,rjorie McLaugh!in -, Whittaker waste manifest activities · 2012. 11. 30. · ANALYTICAL. REPORT...
,rjorie McLaugh!in -, Whittaker waste manifest activities "Ip a g e 1 ý
From: "Kevin Taylor" <[email protected]>To: <[email protected]>Date: Mon, Nov 14, 2005 2:44 PMSubject: Whittaker waste manifest activities
Marjorie:
To address the last open issue from your site inspection, I haveattached a copy of the spreadsheet and laboratory report used tocalculate the activity values placed on the Whittaker waste manifests.However, minor mathematical errors were identified and the calculationsshow activity values slightly higher than what were on the manifest.The correct thorium value is 85.1 comparedto 83.9 pCi/g and the correcturanium activity is 16.7 compared to 16.2 pCi/g.
The methodology for determining the activity estimate for the manifestswas as follows:
1 - Eight representative slag samples (high, medium, and low activitysamples) were collected and pulverized on-site using the excavatorbucket.
2 - Samples were analyzed by STL for thorium and uranium isotopes usingalphaspectroscopy. See attached data report..
3 - The sums of the reported concentrations plus the 2-sigma analyticalerror were used to determine the average activity of the data set. Seeattached spreadsheet.
4 - To provide a level of conservatism, the average value was increasedby the standard deviation of the data set. This value (mean + 1 sigma)was placed on the waste manifest. See attached spreadsheet.
It is important to note that while only 8 samples were used for thedetermining the values to put on the manifest, the range of the data isconsistent with surveys of large (1.7 cubic yard) composite samples,including on-site gamma spectroscopy analyses.
We are sending out our reply to your comments on the Section 2 FFSP thisweek.
Information in this record was deletedin accordance with the Freedom of InformlatonAct, exemptions ti n . ..'FOIA - . . ,= -00 6 J ..
3rjorie McLaughlin - Whittaker waste manifest activities .Page 21
Pat is demobilizing from the site this week. I will include a copy forthe final fenceline survey with the groundwater sample results. Let meknow if you have any additional questions.
Kevin E. Taylor, PE, CHPSr. Health PhysicistEnvirocare of Utah, LLC17 College St., Suite D
p Greenville, SC 29601, 864-235-3695 - office
Ktaylorg)Denvllccom
CC: "Kenneth Kasper" <[email protected]>, "Richard Moss" <[email protected]>,"Stewart Smith" <[email protected]>, "Lee Penney" <[email protected]>,<[email protected]>
\temp\GW)OOOO1 .TMP - - Pagell\temp\GW)0000J.TMP Page 11
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Whittaker waste manifest activitiesMon, Nov 14, 2005 2:41 PM"Kevin Taylor" <ktaylorpenvllc.com>
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Recipientsnrc.govkplpo.KPDOMMM3 (Marjorie McLaughlin)
scientech.comphorkman CC
envllc.comlpenney CC (Lee Penney)ssmith CC (Stewart Smith)rmoss CC (Richard Moss).kkasper CC (Kenneth Kasper)
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Date & TimeMonday, November 14, 2005 2:41 PM
SEVERN
--T-R'E STLI
STL St. Louls13715 Rider Trail NorthEarth City, MO 63045
Tel; 314 298 8566 Fax: 314 298 8757www,stl-inucom
ANALYTICAL. REPORT
PROJECT NO. 23535
Whittaker, Transfer, PA
Lot #: F5G070301
Rich Moss
Scientech Inc143 West Street
New Milford, CT 06776
SEVERN TRENT LABORATORIES, INC.
Chet ScheibelProject Manager
July 20, 2005
ro a e ting.-Ud ers.in Emi' iirý 5 Severn Trent Laboratorle4, Inc.
Case NarrativeLOT NUMBER: F5G070301
This report contains the analytical results for the eight samples received under chain of custody bySTL St. Louis on July 7, 2005. These samples are associated with your Whittaker, Transfer, PAproject.
The analytical results included in this report meet all applicable quality control procedurerequirements except as noted on the following page.
The test results in this report meet all NELAP requirements for parameters in which accreditationsare held by STL St. Louis. Any exceptions to NELAP requirements are noted in the case narrative.The case narrative is an integral part of this report.
All chemical analysis results are based upon sample as received, wet weight, unless noted otherwise.All radiochemistry results are based upon sample as dried and ground with the exception of tritium,unless requested wet weight by the client.
Observations/Nonconformances
Reference the chain of custody and condition upon receipt report for any variations on receiptconditions and temperature of samples on receipt.
Iso topic Thorium by A-01-R MOD
The Thorium spectrum are smeared due to a matrix interference. Samples to re-extract with areduced aliquot to minimize this interference. The re-extract results provided better qualityspectrnur and will be reported, F5G070301-007 and -007X were stopped during counting to mrnimizetailing.
Affected Samples:F5G070301 (1): 6-30-05 S-1F5(070301 (2): 6-30-05 S-2F5070301 (3):-6-30-05S-3F5G070301 (4): 6-30-05 S-4F5G070301 (5): 6-30-05 S-5F5G070301 (6): 6-30-05 S-6F5G070301 (7): 6-30-05 S-7F5G070301 (8): 6-30-05 S-8
METHODS SUMMARY
FSG070301
ANALYTICAL PREPARATIONMETHOD METHODPARAMETER
Inductively Coupled Plasma (ICP) MetalsIsotopic Thorium by Alpha SpectroscopyIsotopic Uranium by Alpha SpectroscopyMercury in Liquid Waste (Manual Cold-Vapor)
SW846 6010BEML A-01-R MODEML A-01-R MODSW846 7470A
SW846 1311/3010
SW846 1311/7470
References;
EML "ENVIRONMENTAL MEASUREMENTS LABORATORY PROCEDURES MANUAL"HASL-300 28TH EDITION, VOLUME I and II DEPARTMENT OF ENERGY
SW846 "Test Methods for Evaluating Solid Waste, Physical/ChemicalMethods"' Third Edition, November 1986 and its updates.
I,
SAMPLE SUMMARY
PSG070301
SAMPLED SAMP
WO # SAMPLE# CLIENT SAMPLE iD DATE TIME
HE2LG 001 6-30-05 S-I 06/30/05 13:00HE2L4 002 6-30-05 S-2 06/30/05 13:05HE2L6 003 6-30-05 S-3 06/30/05 13:10HE2LB 004 6-30-05 S-4 06/30/05 13:15HE2MC 005 6-30-05 S-5 06/30/05 i3:20HE2MG 006 6-30-05 S-6 06/30/05 13:25HE2Mfl 007 6-30-05 S-7 06/30/05 13:30HE2MJ 008 6-30-05 S-8 06/30/05 13:35
NOTE(S)--The analytical results of the samples listed above are presented on the following pages.
- All calculations art performed before rounding to avoid round-off errors in calculated results.
- Resulit noted as 'ND' were not detected at or above the stated limit.
* This report must not be reproduced, except In full, without the written approval of the laboratory.
- Results for the following parameters are never teporEed on a dry weight basis: color, corrossviry, density, flsxpoim, ignitabIlity, layers, odor,
palin, Ailte test, pH, porosity pressure, reactivity. redox potential, specific gravity, spot tests, solids, solubltity, temperature, viscosity, and weight.
SCIEITECH INC
Client Sawple ID: 6-30-05 S-I
TCLP Metals
Lot-Sample #. : F5G070301-001
Date Sampled. .: 06/30/05 13:00 Date Received..:. 07/07/05
Leach Date ....... 07/11/05 Leach Batch #..: P519204
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Matrix ....... : SOLID
Prep Batch #...: 5193423
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Selenium
Antimony
Beryllium
Nickel
Thallium
zinc
ND
4650 J
ND
ND
ND
ND
ND
ND
ND
124 B
ND
11.8 B,J
500Dilution
500Dilution
25.0
Dilution
50.0Dilution
250Dilution
50.0Dilution
500Dilution
375Dilution
62.5Dilution
250Dilution
1250
Dilution
150Dilution
ug/LFactor: 2.5
ug/LFactor: 2.5
ug/L
Factor: 2.5
Factor: 2.5
ug/LFactor: 2.5
ug/LFactor: 2.5
ug/LFactor: 2.5
uq/LFactor: 2.5
ug/LFactor: 2.5
ug/L
Factor: 2.5
ug/L
Factor: 2.5
SW846 6010B
Analysis Time..
SW846 6010BAnalysis Time.:
SW846 6010BAnalysis Time..
SW846 6010BAnalysis Time.
SW846 6010BAnalysis Time...,
SW846 6010BAnalysis Time...
SW846 6010BAnalysis Time.
SW846 6010BAnalysis Time..:
SW846 6010B.AnalyaAs. Time,.:
SW846 60103Analysis Time..
SW846 6010BAnalysis Time.
SW846 60103Analysis Time..
13 :56
13:56
13:56
13-,56
13 55
13 56
13:56
13;56
)j1: 56
13:56
13:56
13; :6
PREPARATION-
ANALYSIS DATE
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/OS
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
WORKORDER #
HE2LG1AA
EZ2LGIAC
HE2LG1AD
HE2LGIAE
HE2LGIAF
HE2LGiAG
HE2LGIAH
HE2LG1AJ
HE2LGIAK
H•2LGIAL
H{E2 LGlAM
HE2LGIAN>
Prep Batch #...: 5194097
Mercury ND 10.0 ug/L SW846 7470A
Analysis Time..: 14:2707/15/O5 "HE2LGIAP
Dilution Factor: 5
((Continued on next page)
SCIENTECH INC
Client Sample ID: 6-30-05 S-i
TCLP Metals
Lot-Sample #...: F5G070301-001 Matrix ......... : SOLID
NOTE (S) :
Analysis performned In accordance wirh USEPA Toxicity Charactcristic Leachrir Procedure Method 1311
I Method blank contamination. The alsoclaled method blamnk con(arns thre arget analyie at a reportable level.
B EgImaled rMlL •e•rlt Is lets than RL.
SCIENTECH INC
Client Sample ID: 6-30-05 S-2
TCLP Metals
Lot-Sample #...: F5G070301-002
Date Sampled...: 06/30/05 13:05 Date Received..: 07/07/05Leach Date......: 07/11/05 Leach Batch #..: P519204
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Matrix ....... : SOLID
PREPARATION- WORKANALYSIS DATE ORDER #
07/12-07/13/05 HE2L41AAPrep Batch #...: 5193423Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Selenium
Antimony
Beryllium
Nickel
Thallium
Zinc
ND
4740 J
ND
ND
ND
ND
ND
ND
ND
1170
ND
11.3 B,J
5194097ND
500 ug/LDilution Factor: 2.5
500 ug/LDilution Factor: 2.5
25.0 ug/LDilution Factor: 2.5
50.0 ug/LDilution Factor: 2,5
250 ug/LDilution Factor: 2.5
50.0 ug/LDilution Factor: 2.5
500 ug/LDilution Factor: 2.5
375 ug/LDilution Factor: 2.5
62.5 ug/LDilutaon _act.or 2.5 5
250 ug/LDilution Factor: 2.5
1250 ug/LDilution Factor: 2.5
15O ug/LDilution Factor: 2.5
1010 uq/LDilution Factor: 5
SW846 6010BAnalysis Time..:
SW846 6010B
Analysis Time..
SW846 6010B
Analysis Time..
SW846 6010BAnalysis Time.-
SW846 GO1OB
Analysis Time,.
SW846 6010B
Analysis Time..
SW846 6010BAnalysis Time.
SW846 6010B
Analysis Time..:
SW846 6010B_.... An~a.!ysi!s Tim• ,.
SW846 6010BAnalysis Time..
SW846 6010B
Analysis Time..:
SW84S 6010BAnalysis Time,.:
14:20
14:20
14.20
14:20
14z20
14:20
14:20
14 :20
14:20
14,20
14120
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/o5
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/os
07/12-07/13/05
07/12-07/13/OS
BE2LA1AC
HE21,41AD
HE2L41AE
HE2L41AF
HE2L4 lAG
HE2L41AH
HE2L41AJ
HE2L,41AK
BER2L4IAL
HB2L4lAM
HE2L41AN
Prep Batch #.
Mercury
K
SW846 7470A
Analysis Time.. % 14:3507/15/05 HE2L41AP
(Continued on next page)
SCIENTECH INC
Client Sample ID: 6-30-05 S-2
TCLP Metals
Lot-Sample # .. : F5G070301-002 Matrix .......... : SOLID
NOTE (S):Analysis performed in accordance with USEPA Toxicity Charactcristic Leaching Procedurc Method 1311
J Method blank contamination. The associated mechod blank contains the targeo ana(yte at a reportable level.
8 Fstimated reult. Rensul Is less than RL
SCIENTECH INC
Client Sample ID: 6-30-05 S-3
TCLP Metals
Lot-Sample #...: F5G070301-003Date Sampled... 06/30/05 13:10 Date Received..: 07/07/05Leach Date ..... .. 07/11/05 Leach Batch #..: P519204
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Matrix ....... : SOLID
PREPARATION- WORKANALYSIS DATE ORDER #
07/12-07/13/0S HE2L61AA
Prep Batch #...; 5193423Arsenic ND
Barium 7740 J
Cadmium ND
Chromium ND
Lead ND
Silver ND
Selenium ND
Antimony ND
Beryllium ND
Nickel 6550
Thallium ND
Zinc 19.6 B,J
500 ug/LDilution Factori 2.5
500 ug/LDilution Factor: 2.5
25.0 ug/LDilution Factor: 2.5
50.0 ug/LDilution Factor: 2.5
250 ug/LDilution Factor: 2.5
50.0 ug/LDilution Factor. 2.5
500 ug/LDilution Factor: 2.5
375 ug/LDilution Factor: 2.5
62.5 ug/L_Dilution Factor .. 2..5
250 ug/LDilution Factor: 2.5
1250 ug/LDilution Factor, 2.5
150 ug/LDilution Factor: 2.5
SW846 6010B 'Analysis Time.
,SW846 6010BAnalysis Time..
SW846 6010BAnalysis Time..-
SW846 60108Analysis Time..:
SW846 6010BAnalysis Time.,.
SW846 6010BAnalysis Time,.:
SW846 6010BAnalysis Time.. i
SW846 6010BAnalysis Time..:
SW846 6010BAnalysis-Time...
SW846 6010BAnalysis Time.
SW846 6010BAnalysis Time..
SW846 6010BAnalysis Time..-
14:25
14:25
14t25
14:25
14:25
14:25
14:25
14 :25
14.t25
14:25
14:25
14:25
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/O5
07/12-07/13/05
07/12-07/13/05
HE2L61AC
HE2L61AD
HE2L61AE
HE2L61AF
HE2L61AG
HE2L61AH
HE2L61AJ
HE2L61AK
IM2L61AL
HE2L61AM
BE2L61AN
Prep Batch #...: 5194097Mercury ND 10.0 ug/L SW846 7470A
Analysis Time.., 14:38
07/15/05 HE2L61APDilution Factor: 5
(Continued on next page)
SCIENTECH INC
Client Sample ID: 6-30-05 S-3
TCLP Metals
Lot-Sample #...: FSG070301-003 Matrix .......... .SOLID
NOTE (S) :Analysls performed in accordance with USEPA Toxicity Charcteristic Leach•ng Procedur Method 13.1
J MVIIod blank contamsnallon. The associated method blank contains the jorget analyte at a reporable level.
B Elsimated esult. Result Is loss than RL.
SCIENTECH INC
Client Sample ID; 6-30-05 S-4
TCLP Metals
Lot-Sample # ... : F5G070301-004
Date Sampled...: 06/30/05 13:15 Date Received..: 07/07/05
Leach Date ..... : 07/11/05 Leach Batch #..: P519204
REPORTING
Matrix ....... : SOLID
PREPARATION-PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE
Prep Batch #....: 5193423
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Selenium
Antimony
Beryllium
Nickel
Thallium
Zinc
ND 500 usg/L SW846 6010B
Dilution Factor: 2.5
5590 J 5o0 ug/LDilution Factor: 2.5
ND 25.0 ý ug/LDilution Factor: 2,5
ND 50.0 ug/LDilution Factor: 2,5
ND 250 ug/LDilution Factor: 2.5
ND 50.0 ug/LDilution Factor: 2.5
ND 500 ug/LDilution Factor: 2.5
ND 375 ug/LDilution Factor; 2.5
ND 62.5 ug/L- Dilution FactOr: 2.5
1780 250 ug/LDilution Factor: 2.5
ND 1250 ug/LDilution FactOr: 2.5
25,0 B,J 150 ug/LDilution Factor: 2.5
Analysis
SW846Analysis
SW846
Analysis
SW846
Analysis
SW846
Analysis
SW846
Analysis
SW846Analysis
SW646
Analysis
SW846AnaiySis
SW846
Analysis
SWB46Analysis
SW846Analysis
Time.. 14:41
6010B
Time..: 14:41
6010B
Time,, 14:41
6010BTime,. 14:41
6010BTime. - 14:41
6010B
Time..: 14:41
6010B
Time..: 14:41
6010B
Time..: 14:41
6010BTime..:_14:4l
GOlOB
Time..: 14:41
6010B
Time..: 14:41
6010B
Time-..: 14:41
0'7/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07113/05
07/12-07/13/05
07/12-07/13/OS
WORKORDER #
HE2L81AA
IIE21,8XAC
HE2LBIAD
HE2L8 lAE
RE2LB1AF
}IE2L81AG
HE2L81AH
HE2L81AJ
IiE2LS1AX
BB2LBIAL
1E2LB1AM
8B2L83AN
Prep Batch #...: 5194097Mercury ND 10 .0 ug/L SW846 7470A
Analysis Time..: 14:4007/15/05 HE2LS1AP
Dilution Factor: S
(Continued on next page)
SCIENECH INC
Client Sample ID: 6-30-05 S-4
TCLP Metals
Lot-Sample # ... : F5G070301-004 Matrix ......... ; SOLID
NOTE (S) :Ana)ysis performeu In accordance with USEPA Toxicity Charactristic LeachIng Procedure Method 1311
I Method blank contamination. The associated method blank contains tht targOt analytc at a reportable level.
B Estimated result. Result is less than RL,
SCIENTECH LNC
Client Sample ID: 6-30-05 S-5
TCLP Metals
Lot-Sample #...: FSG070301-005
Date Sampled...; 06/30/05 13:20 Date Received..: 07/07/05
Leach Date ..... .. 07/11/05 Leach Batch #..: P519204
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Matrix ....... .SOLID
Prep Batch i...: 5193423Arsenic ND
Barium 4340 J
Cadmium ND
Chromium ND
Lead ND
Silver ND
Selenium ND
Antimony ND
Beryllium ND
Nickel 591
Thallium ND
Zinc 10.5 BJ
500 ug/LDilution Factor: 2.5
500 ug/LDilution Factor: 2.5
25.0 ug/L
Dilution Factor: 2.5
o 50,0 ug/LDilution Factor: 2.5
250 ug/L
Dilution Factor: 2,5
50.0 ug/L
Dilution Factor: 2.5
500 ug/L
Dilution Factor, 2.5
375 ug/L
Dilution Factor: 2.5
62.5 ug/L
Dilution Factor: 2.5
250 ug/LDilution Factor; 2.5
1250 ug/L
Dilution Factor; 2.5
150 ug/L
Dilution Factor: 2.5
SW846 6010BAnalysis Time..: 14:46
SW846 6010B
Analysis Time..: 14:46
SW846 60103
Analysis Time..- 14.46
SW846 6010B
Analysis Time..; 14.46
SW846 6010B
Analysis Time..; 14:46
SW846 6010B
Analysis Time.. : 14:46
SW846 6010BAnalysis Time,.- 14:46
SW846 6010BAnalysis Time..: 14:46
SW046 6010B
Analysis Time..: 14:46
SW846 6010B
Analysis Time..: 14:46
SW846 6010B
Analysis Time..: 14:46
SW846 6010B
Analysis Time..: 14:46
SW846 7470A
Analysis Time,._ 14:43
PREPARATION-ANALYSIS DATE
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/os
071/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/OS
07/12-07/13/05
07/12-07/13/05
WORKORDER #
H82MCIAA
HE2MCIAC
HE 2MClAD
HE2MCIAE
HE82MCAF
HE2MCIAG
HE2MClAR
HE2MC1AJ
HE2MCIAK
HE2MCIAL
EE2MC1AM
HB2MC1AN
Prep Batch #...: 5194097Mercury ND 10,0 ug/L 07/15/05 HE2MCIAP
Dilution Factor: 5
(Continued on next page)
I SCIENTECH INC
Client Sample ID: 6-30-05 S-5
TCLP Metals
Lot-Sample #...: FSG070301-005 Matrix ......... : SOLID
NOTE (S):Analysls performed In ccordarnce with USEPA Toxlcity COarocleriStu I..Laching Procedure Method 1311
J• Method blank contamination. The associated method blank contains the target ana.lyce at a reportable level.
B Estimaterd rciuL Rea.lt Is les than RL.
k
I'
SCIENTECH INC
Client Sample ID: 6-30-05 S-6
TCLP Metals
Lot-Sample #...: F5G070301-006
Date SamplJed...: 06/30/05 13:25 Date Received..: 07/07/05Leach Date._.: 07/11/05 Leach Batch j..: P519204
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Prep Batch #...: 5193423
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Selenium
Antimony
Beryllium
Nickel
Thallium
Zinc
ND
4460 J
WD
ND
ND
ND
ND
ND
ND
1030
ND
6.8 B,J
500
Dilution Factor: 2.5
500 ug/LDilution Factor: 2.5
25.0 uq/L
Dilution Factor: 2.5
5o.0 ug/L
Dilution Factor: 2.5
250 uS/L
Dilution Factor: 2.5
50.0 ug/L
Dilution Factor: 2.5
500 uq/L
Dilution Factor: 2.5
375 ug/L
Dilution Factor: 2.5
62.5 ug/L
Dilution Factor: 2.5
250 Ug/LDilution Factor: 2.5
1250 ug/L
Dilution Factor: 2.5
ISO ug/LDilution Factor; 2.5
ug/L SW846 6010B
Analysis Time..
SW846 6010B
Analysis Time..:
SW846 6010B
Analysis Time.-
SW846 6010BAnalysis Time.
SW846 6010BAnalysis Time..
SW846 6010B
Analysis Time..;
SW846 6010B"Analysis Time..t
SW846 6010B
Analysis Time..:
SW846 6010BAnalysis Time..:
SW846 6010B
Analysis Time.
SW846 6010BAnalysis Time.:
SW846 6010B
Analysis Time..:
14:51
14:51
14:51
14:51
14:51
14:51
14,51
14:51
14:51
14:51
14:51.
14:51
Matrix ........ SOLID
PREPARATION- WORK
ANALYSIS DATE ORDER #
07/12-07/13/05 EE2MGIAA
07/12-07/13/05 HE2MG1AC
07/12-07/13/05 HE2MG1AD
07/12-07/13/05 HE2MG4IA
07/12-07/13/05 HE2MGIAF
07/12-07/13/05 HE2MG1AG
07/12-07/13/0S HE2MGIAH
07/12-07/13/05 HE2MGIAJ
07/12-07/13/05 HE2MG1AK
07/12-07/13/05 HE2MGIAL
07/12-07/13/05 HE2MGIAM
07/12-07/13/05 HE2MGIAN
Prep Batch #...: 5194097Mercury ND 10.0 ug/L SW846 7470A 07/15/05 HE2MG1AP
Dilution Factor: 5 Analysis T:
(Continued on next page)
ime.,: 14:44
4
SCIENTECH INC
Client Sample ID: 6-30-05 S-6
TCLP Metals
Lot-Sample #,...: FSG070301-006 Matrix ......... : SOLID
NOTE (S) :Analysis performed In accordance with I•SEPA Toxicity Characterislic Larhing Piocedure Method 1311
1 Method blank contamination. The assoctited method blank contains the target anatytc at a reportable level.
B Eslmatcd re-it. Reshlt is loss than RL.
SCIENTECH INC
Client Sample ID: 6-30-OS S-7
TCLP Metals
Lot-Sample #..: FSG070301-007
Date Sampled... : 06/30/05 13:30 Date Received..: 07/07/05
Leach Date ..... : 07/11/05 Leach Batch #..: P519204
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Matrix ........ SOLID
Prep Batch i...: 5193423Arsenic ND
Barium J14600
Cadmium ND
Chromium ND
Lead ND
Silver ND
Selenium ND
Antimony ND
Beryllium ND
Nickel 8360
Thallium ND
Zinc 13.8 B,J
500 ug/L
Dilution Factor: 2.5
500 ug/LDilution Factor: 2.S
25.0 ug/LDilut'ion Factor: 2.5
50.0 ug/LDilution Factor: 2.5
250 • ug/LDilution Factor: 2.5
50.0 ug/LDilution Factor: 2.5
500 ug/LDilution Factor: 2.5
375 ug/L
Dilution Factors 2.5
62.5 ug/LDilution Factor: 2.5
250 ug/LDilution Factor: 2.5
1250 ug/LDilution Factor: 2.5
150 ug/LDilution Factor: 2.5
Analysis
SW846
Analysis
SW846
Analysis
SW846
Ahalysia
SW846
Analysis
SW846
Analysis
SW846
Analysis
SW846
Analysis
SW846
Analysis
SW846Analysis
SW846
Analysis
SW846
Analysis
Time..
6010B3
Time..
6010B3
Time..,6010BTime. .601013Time..:
6010BTime..:
6010BTime..:
6010BTime..:
6010BTime. .:
6010BTime,..:
601013Time..
60101BTime..:
601DBTime. .
14:56
14:56
14:56
14:56
14:56
14:56
14:56
14:56
14:56
14:56
14:56
14:"56
SW846 6010B
PREPARATION-ANALYSIS DATE
07/12-07/13/05
07/12-07/13/os
07/12-07/13/OS
07/12-07/13/o5
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/1.2-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
WORKORDER #
HE2MHIAA'
HE2MHIAC
HE2MH1AD
HE2MH1AR
HE2MHIAF
HE2MH1AG
HE2MH1AH
HE2MHIAJ
HE2MH1AK
EE2MH13AL
HE2MH1AM
BE2MHIAN
Prep Batch #...: 5194097
Mercury ND 10,0 SW846 7470A 07/15/05 HE2MHlAPDilution Factor: S Analysis T:
(Continued on next page)
iCe, , : 14:47
1.-.
SCIE=ThCH INC
Client Sample ID: 6-30-05 S-7
TCLP Metals
Lot-Samuple # ... : F5G070301-007 Matrix ......... : SOLID
NOTE (S) :Analysis perforated In accordance with USSPA Toxicity Charcteristic Leaching Procedure Method )3] 1
J1 Method blankc contamination. The "elocated method blank contains the target analyte at a reportable level.B Estimateed resule. Reasutl is less Eln RL
7}
--..o
SCIENTECH INC
Client Sample ID: 6-30-05 S-8
TCLP Metals
Lot-Sample I...: F5G070301-008Date Sampled...: 06/30/05 13:35 Date Received..: 07/07/05Leach Date_..: 07/11/05 Leach Batch #.-: P519204
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Matrix ....... : SOLID
PREPARATION- WORKANALYSIS DATE ORDER #
07/12-07/13/05 HE2MJIAAPrep Batch #...: 5193423
Arsenic
BaXium
Cadmium
Chromium
Lead
Silver
Selenium
Antimony
Beryllium
Nickel
Thallium
Zinc
ND
11000 J
ND
ND
ND
NU
ND
ND
ND
3290
ND
8.0 B,J
500 ug/LDilution Factor7 2.5
500 uq/LDilution Factor: 2,5
25.0 uq/LDilution Factor: 2.5
50.0 ug/LDilution Factor: 2.5
250 uq/LDilution Factor: 2,5
50.0 ug/LDilution Factor: 2.5
500 ug/LDilution Factor, 2.5
375 ug/LDilution Factor% 2.5
62.5 ug/LDilution Factor: 2.5
250 . ug/LDilution Factor: 2.5
1250 ug/LDilution Factor: 2.5
15O uq/L
Dilution Factor: 2.5
Analysis
SW846Analysis
SW846Analysis
SW846Analysis
SW846Analysis
SW84GAnalysis
SW846Analysis
SW846Analysis
SW846Analysis
SW846Analysis
SW846Analysis
SW846Analysis
Time..: 15:02
6010B
Time..: 15:02
6010B
Time..: 25:02
6010B
Time..: 15:02
6010BTime..: 25:02
6010BTime..: 15:02
602.0B
Time..: 15:02
6010B
Time..; 15:02
6010BTime..: 15:02
Time..: 15:02
6010B
Time,.: 15:02
GOiOBTime.. 15:02
SW846 6010B
07/12-07/13/05
07/12-07/13/os
07/12-07/13/os
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/05
07/12-07/13/os
07/12-07/13/05
HE2MJIJAC
HE2MJIAD
HE2MJIAE
HE2MJIAF
HE2MJIAG
HE2MJIAH
HE2MJIAJ
HE2MJIAK
EF2MfJIAL
HE2MJ1AM
HE2MJ.AN
Prep Batch #...: 5194097
Mercury ND 10.0 ug/L SW846 7470AAnalysis Time..: 14:53
07/1•I5/ HE2MJIAPDilution Factor: 5
(Continued on next page)
(..t
SCIE=TECH INC
Client Sample ID: 6-30-05 S-8
TCLP Metals
Lot-Sample #...: F5G070301-008 Matrix ......... : SOLID
NOTE (S) :Analysis performed in accordance with USEPA T'oxilcity Characteritic Leliching Procedure Method 1311
1 Method blank contamination. The associated method blank contains the target analyle at a reportaibe level.
B .stnmated result. Result is less than RL.
,
M•-)EOD BLANK REPORT
TCLP Metals
Client Lot #...: FSG070301 Matrix ..........- SOLID
PREPARATION- WORKREPORTINGPARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER #
MB Lot-Sample #: F5Gll0000-412 Prep Batch #...: 5193423Leach Date.....;. 07/11/05 Leach Batch #..: P519204
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Selenium
Antimony
Beryllium
Nickel
ND
18.2 B
ND
ND
ND
ND
ND
ND
ND
ND
500 ug/LDilution Factor: 2.5
Analysis Time.. 13:46
500 ug/LDilution Factor: 2.5
Analysis Time..; 13:46,
25.0 ug/LDilution Factor: 2.5
Analysis Time..: 13:46
50.0 ug/LDilution Factor: 2,5
Analysia Time..: 13:46
25o uq/LDilution Factor: 2.5
Analysis Time..: 13:46
50.0 ug/LDilution Factor: 2.5
Analysis Time..: 13:46
5oo uqg/LDilution Factor: 2.5
Analysis Time..: 13:46
375 ug/LDilution Factor: 2.5
Analysis Time..: 13:46
62.5 ug/LDilution Factor: 2.5
Analysis Time..: 13:46
250 ug/L
Dilution Factorz 2.5
Analysis Time..: 13:46
SWB46
SK846
SW846
SW846
SW846
SW846
SW846
SWMS4 6
SW846
SW846
6010B
60103
6010B
6010B
6010B
6010B
6010B
6010B
60108
6010B
07/12-07/13/05 HE8FQIAA
07/12-07/13/05 81E8FQ1AC
07/12-07/13/05 HE8FQ1AD
07/12-07/13/05 HESFQIAE
07/12-07/13/05 HRBFQ1AF
07/12-07/13/05 HE8FQIAG
07/12-07/13/05 HEBFQlAH
07/12-07/13/05 HE8FQlAJ
07/12-07/13/05 HE8FQlAK
07/12-07/13/05 HE8FQ1AL
(Continued on next page)
"( ...
METHOD BLANK REPORT
TCLP Metals
Client Lot #...: F5G070301 Matrix ......... : SOLID
REPORTING PREPARATION- WORKPARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER #
MB Lot-Sample #: F5GI10000-412 Prep Batch #...:Leach Date.....- 07/11/05 Leach Batch V..:Mercury ND 10.0 ug/L
Dilution Pactor: 5Analysis Time.. 14;18
5194097P519204
SW846 7470A 07/15/05 HE8FQIAP
MB Lot-Sample #. F5GII0000-412 Prep Batch #. . :
Leach Date ..... ; 07/11/05 Leach Batch #..:
Thallium ND 1250 ug/LDilution Factors 2.5
Analysis Time..; 13:46
5193423P519204
SW846 6010B
SW846 6010B
07/12-07/13/05 HEBFQIAM
07/12-07/13/05 BEBFQlANZinc 11.6 B 150 ug/LDilution Factor: 2.5
Analysis Timre..: 13:46
NOTE (S):
Calculations are istrfortned before rounding to avoid round-off erors ift calculated r'enut.. E.stm ated resu'l. R s.ult Is len. than RL.
K.
LABORATORY CONTROL SAMPLE EVALUATION REPORT
TCLP Metals
Client Lot #...:
PARAMETER
F5G070301
PERCENT RECOVERY
RECOVERY LIMITS METHOD
Matrix ........ .. SOLID
PREPARATION-ANALYSIS DATE WORK ORDER #
07/12-07/13/05 HFA251AALCS Lot-Sample#: F5G120000-423 Prep Batch #...: 5193423Arsenic
'Barium
Cadmium
Chromium
Lead
Silver
Selenium
Antimony
Beryllium
Nickel
Thallium
Zinc
106
103
99
95
96
100
109
101
105
95
96
104
Dilution Factor: 2.5
(80 - 120) SW846 601;Dilution Factor: 2.5
(80 - 120) SW846 601Dilution Factor; 2.5
(80 - 120) SW846 601
Dilution Factor: 2.5
i80 - 120) SW846 '601
Dilution Factor; 2.5
(80 - 120) SW846 601Dilution Factor; 2.5
(80 - 120) SW846 601Dilution Factor; 2.5
(80 - 120) SW846 601
Dilution Factor: 2.5
(80 - 120) SW846 601
Dilution Factor: 2.5
(80 - 120) SW846 601
Dilution Factor: 2.5
(80 - 120) SW846 601
Dilution Factor: 2.5
(80 - 120) SW846 601
C
C
C
C
C
(
(80 - 120) SW846 6010BAnalysis Time..: 13:5l
OB 07/12-07/13/05Analysis Time..: 13!51
OB 07/12-07/13/05
Analysis Time-. 13:51
0a 07/12-07/13/05
Analysis Time.-. 13:5S
0B 07/12-07/13/05Analysis Time..- 13,51
OB 07/12-07/13/05
Analysis Time..; 13:51
0B 07/12-07/13/05
Analysis Time.- . 13:51
OB 07/12-07/13/OSAnalysis Time..: 13:51
OB 07/12-07/13/05
Analysis Time.. ; 13:51
0B 07/12-07/13/05
HFA251AC
HFA25!AD
HFA251AE
HFA251AF
HFA2S1AG
HFA251AH
HFA251AJ
HFA251AK
HFA251ALAnalysis Time..: 13:51
0B 07/12-07/13/05 HFA251AMAnalysis Time.. ; 13%51
0B 07/12-07/13/05 RFA251AN
Analysis Time..; 13:51Dilution Factor; 2.5
LCS Lot-Sample#:Mercury
F5G130000-097 Prep Batch # ... : 5194097
99 (82 - 125) SW846 7470A 07/15/05
Dilution Factor: 5 Analysis Time..; l4t20
(Continued on next page)
HFCNMIAA
(s'.
LABORATORY CONTROL SAMPLE EVALUATION REPORT
TCLP Metals
Client Lot ... FSG070301 Matrix ......... .. SOLID
PERCENT RECOVERY PREPARATION-PARAMETER RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER #
NOTE(S):Caik.lL3tiOS are performed before roundin, to avoid round-off errors in calculaled results.
(
MATRIX SPIKE SAMPLE EVALUATION REPORT
TCLP Metals
Client Lot #...: F50070301Date Sampled... 06/30/05 13:00.Date Received..: 07/07/05
Matrix ......... : SOLID
I PERCENT RECOVERY RPD PREPARATION- WORK
PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE ORDER #
MS Lot-Sample #: F5G070301-001 Prep Batch ... : 5193423Leach Date ..... : 07/11/05 Leach Batch *..: P519204
Arsenic
Barium
Cadmium
105104
(83(83
- 111)- 111) 1.0 (0-20)
Dilution Factor: 2.5
Analysis Time..: 14:02
9898
9594
(79 - 1.1)(79- 111) 0.18 (0-20)
Dilution Factor: 2.5
Analysis Time.. 14:02
(65 - 122)
(65 - 122) 0.48 (0-20)Dilution Factor% 2.5
Analysis Time..Cl14:02
(74 - 114)
(74 - 114) 0.56 (0-20)
Dilution Factor; 2,5
Analysis Time.-. 14:02
SW846 6010BSW846 6010B
SW846 6010BSW846 6010B
SW846 6010BSW846 6010B
SW846 6010BSW846 6010B
Chromium 9292
07/12-07/13/05 HE2LGIAT07/12-07/13/05 HE2LGIAU
07/12-07/13/05 HE2LGIAV07/12-07/13/05 HE2LG1AW
07/12-07/13/05 HE2LGIAX07/12-07/13/05 HE2LG1A0
07/12-07/13/05 HE2LGIAI07/12-07/13/05 HE2LGIA2
07/12-07/13/05 HE2LGIA307/12-07/13/05 RE2LGIA4
07/12-07/13/05 HE2LGIA5
07/12-07/13/05 HE2LG1A6
07/12-07/13/05 HE2LGIA707/12-07/13/05 HE2LG1A8
07/12-07/13/05 HE2LGIA9
07/12-07/13/05 HE2LGICA
Lead 9191
9089
(65 - 121) SW846 6010B
(65 - 121) 0.25 (0-20) SW846 6010B
Dilution Factor: 2.5
.Analysis Time-. 14:02
Silver (70 - 123)(70 -- 123) 1.6 (0-.20)
Dilution Factor; 2.5Analysis Time. 14:02
(76 - 124)(76 - 124) 0.74 (0-20)
Dilution Factor! 2.5Analysis Time.. 14:02
Selenium 107206
Antimony 9595
SW846 6010BSW846 60.10B
SW846 6010BSW846 6010B
SW846 6010BSW846 6010B
(68(68
- 129)- 129) 0.38 (0-20)
Dilution Factor: 2.5
Analysis Time..ý 14:02
(Continued on next page)
MATRIX SPIKE SAMPLE EVALUATION REPORT
TCLP Metals
Client Lot #,...: F51070301Date Sampled...: 06/30/05 13:00 Date Received..: 07/07/05
Matrix ......... : SOLID
PARAMETERBeryllium
PERCENTRECOVERY104103
Nickel 91
90
RECOVERY RPDLIMITS RPD LIMITS(82 - 113)
(82 - 113) 0.34 (0-20)Dilution Factorz 2.5
Analysis Time-. 14:02
(75 - 109)
(75 - 109) 0.42 (0-20)
Dilution Factor: 2.5
Analysis Time..: 14!02
(78 - 110)
(78 - 110) 0.23 (0-20)
Dilution Factor: 2.5
Analysis Time-. 14i02
METHODSW846 6010BSW846 6010B
PREPARATION- WORKANALYSIS DATE ORDER #07/12-07/13/05 HE2LGICC07/12-07/13/05 HE2LGICD
07/12-07/13/05 HE2LGICE07/12-07/13/05 HE2LGICF
Thallium 9393
SW846 6010BSW846 6010B
SW846 6010BSW846 6010B
SW846 6010BSW846 6010B
07/12-07/13/05 HE2LG1CG07/12-07/13/OS HE2LGIC{
07/12-07/13/05 HE2LG1CJ07/12-07/13/05 HE2LGICK
Zinc 101
101(10
(10- 15o)- 150) 0.18 (0-30)
Dilution Factor: 2.5
Analysis Time.. 1 14 : 02
MS Lot-Sanple #:Leach Date ..... :Mercury 100
98
FSG070301-001 Prep Batch #...: 5194097
07/11/05 Leach Batch I..: P519204(64 - 122) SW846 7470A(64 - 122) 2.0 (0-20) SW846 7470A
Dilution Factort 5Analysis Time. : 14,29
07/15/05 HE2LGICL07/15/05 HE2LGICM
NOTE (S) :CalculaLions are performcd before rounding to avoid round-off erors In calculated remisui.
K-.
SCIENTECH INC
Client SamDle ID: 6-30-05 S-i
Severn Trent Laboratories - Radiochamistry
Lab Sample ID: F5G070301-001
Work Order: HE2LGDate Collected:Date Received:
06/30/05 130007/07/05 0900
Matrix: SOLID
TotalUncert. Prep Aaaly&ia
PaKa.tr aegult QuaL 12 +/) MDC Date Date Batch 4 lOd
Xeo URANIKU (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD
Uranium 23419.9 2'1 0.05 07/11/05 07/14/05 5192451 85Uranium 235 0.96 J 0.25 0.07 07/11/05 Q7/14/0S 5192451 85
Uranium 238 19.8 2.1 0.05 07111/05 07/14/05 5192451 85
ISO THORIUM (SHORT CT) DOE .- 01-R MOD pCi/p A-01-R MOD
Thorium 228 55.4 5.2 0.2 07/15/05 07/18/05 5196204 86
Thorium 230 12.8 1.5 0.09 07/15/05 07/18/05 5196204 .86Thorium 232 56.0 5.2 0.06 07/15/05 07/18/D5 5196204 85
NOTE(S)
Data are incomplete without the case narrative.
k iCia determined by instrument performance only.,,.jold results are greater than the MDC
J Result is greater than sample detection limit but leas than stated reporting limit.
SCIENTECH INC
Client Sample ID: 6-30-05 S-2
Severn Trent Laboratories - Radiochemistry
Lab Sample ID:Work Order:;Matrix:
FSC070301-002HE2L4SOLID
Date Collected:Date Received:
06/30/05 130507/07/05 0900
TotalVncert. Prep Analysis
Parameter Result Qual (2 a+/-) mc Date Date Batch y Xld s
Iso. URANIUM (SHORT CT) DOE A-01-R M0D pCi/g A-01-R MOD
Uranium 234 8.09 0.93 0.08. 07/11/05 07/14/05 5192451 86
Uranium 235S 0.39 3 0.15 0.07 07/11/05 07/14/05 5192451 86
Uranium 238 9.0 1.0 0.09 07/11/05 07/14/05 5192451 86
ISO THORIUM (SHORT CT) DOEIA-01"x MOD pCi/g A-01-R MODThorium 228 4 1 400715 0 5 6
Thorium 228 43.3 4.0 0.2 07/15/05 07/18/05 5196204 92
Thorium 230 11.2 1.3 0.0 07/15/05 07/18/05 5196204 92Thorium 232 41.9 3.9 0.09 07/15/05 07/18/05 5196204 92
NOTE (S)Data are incouplete without the case narrative.
)C is determined by instrument performance only.
-4old results are greater than the HDC
J Result is greater than sample detection limit but less than stated reporting limit.
SCIENTECH INC
Client Sample ID: 6-30-05 S-3
Severn Trent Laboratories - Radiochemistry
Lab Sample ID;Work Order:
Matrix:
F5G070301-003
HE2L6
SOLID
Date Collected:Date Received:
06/30/05 131007/07/05 0900
TotalUncert. prop Analysia
Parameter ResUlt QUal (2 0/-) MDC Date Dats Batch 0 Yld
Iso URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODUranium 234 10.3 2 1.2 0.09 07/11/G5 07/14/05 5192451 81
Uranium 235 0.64 J 0.20 0.09 07/11/05 07/14/05 5192451 81
Uranium 238 9.9 1.1 0.05 07/11/05 07/14/05 5192451 81
Iso THORIUM (SHORT CT) DOEiA-01-R MOD pCi/g A-01-R MODThorium 228 40.7 3.8 0.1 07/15/05 07/18/05 5196204 91Thorium 230 11.8 -1.4 0.05 07/15/05 07/18/05 5196204 91
Thorium 232 39.2 3.7 0.1 07/15/05 07/18/05 5196204 91
('V
-i
NOTE (S)
Data are incomplete without the case narrative.
DC is determined by instrument performance only..- Sold results are greater than the PMC
J Result is 'greater than sample detection limit but loss than stated reporting limit.
SCIENTECH INC
Client SamnDle ID: 6-30-05 S-4
Severn Trent Laboratories - Radiochemistry
Lab Sample ID: F5G070301-004Work Order: HE2L8
Date Collected:Date Received:
06/30/05 131507/07/05 0900
Matrix: SOLID
Tot.aOncert. Prep Analysis
PRsamutlr AsQua1 (2 o0/-) ImC Date Date Batch Yld Is
Tao URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD
Uranium 234 9.29 1.0 0.04 07/11/05 07/14/05 5192451 83
Uranium 235 0.39k J 0.15 0.03 07/11/05 07/14/05 5192451 83
Uranium 238 9.5 1.0 0.03 07/11/05 07/14/05 S192L.51 83
Iso THORIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD
Thorium 228 76.6 7.6 0.3 07/15/05 07/18/05 5196204 69
Thorium 230 16.9 2.0 0.2 07/15/05 07/18/05 5196204 69
Thorium 232 75.2 7.5 0.2 07/15/05 07/18/05 5196204 69
NOTE (S)Data are iecccplate without the case narrative,
1DC is determined by instrument performance only.told results are greater than the KDC
J Result is greeter than sample detection limit but lees than stated reporting limit.
SCIENTECH INC
Client SalnDle ID: 6-30-05 S-5
Severn Trent Laboratories - Radiochemistry
Lab Sample ID:Work Order:Matrix:
F5G070301-005HE2MCSOLID
Date Collected:Date Received:
06/30/05 132007/07/05 0900
TotalUncert. Prep Analysis
Parameter Iesult Qual (2 a+/-) MDc Date Data Batch # Yld %
Iso URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD-Uranium 234 10.2- 1.2 0.09 07/11/05 07/14/05 5192451 87
Uranium 235 0.78 j 0.24 0.08 07/11/05 07/14/05 5192451 87
Uranium 238 10.3 1.2 0.07 07/11/05 07/14/05 5192451 87
Iso THORIUM (SHORT CT) DOE A-01-R MOD pCi/5 A-01-R MOD
Thorium 228 28.5f 2.9 0.2 07/15/05 07/18/05 5196204 89
Thorium 230 7.4 -' 1.0 0.06 07/15/05 07/18/05 5196204 89
Thorium 232 29.5 3.0 0.09 07/15/05 07/18/05 5196204 89
NOTH (S)
Data are incomplete without the case narrativo.
DC is determined by instrument performance only.ý"'-Bold reaults are greator than the 4DC
J Result is greator than sample detection limit but less than stated reporting limit.
SCIENTECH INC
Client Sainnle ID: 6-30-05 S-6
Severn Trent Laboratories - Radiochemistry
Lab Sample ID:Work Order:Matrix:
FSG070301-006
HE2MG
SOLID
Date Collected:Date Received:
06/30/05 132507/07/05 0900
Totaluncert.
Prop Analysis
Parameter Result ual (2 a+/-) 1DC vat. Date Batch # Yld %
Iso URANIUTM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODGranium% 234 9.'2 1.0 0.05 07/11/05 07/14/05 5192451 88Uranium 23S 0.41 1 0.15 0.06 07/11/05 07/14/05 S192451 so
Uranium 238 9.4• 1.0 0.05 07/11/05 07/14/05 5192451 88
Iso THORIU M (SHORT CT) D0 A-01-R MOD pCi/g A-01R MODThorium 228 37.9 3.6 0.2 07/15/05 07/18/05 5196204 "90Thorium 230 1 0_5. 1.3 0.1 07/15/05 07/18/05 S196204 90
Thorium. 232 37.8 3.5 0.1 07/15/05 07/18/05 5196204 90
* NOTE(S)
Data are incomplete without thn case narrative.
( DC is determined by instrument performance only.( 8old results ara greater than the MDC
J Result is greater than sample deto•tion limit but less than stated reporting limit.
SCIENTECH INC
Client Sample ID: 6-30-05 S-7
Severn Trent Laboratories - Radiochemistry
Lab Sample ID: F5G070301-007
Work Order: HE2MH
Matrix; SOLID
Date Collected:Date Received:
06/30/05 133007/07/05 0o00
TotalUneart, Prep Analysis
Parameter Result Qual (2 o+/-) MDC Date Data Batch 0 Yld %
ISO URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD
Uranium 234 14.3 | 1.6 0.08 07/11/05 07/14/05 5192451 88
Uranium 235 0.70 J 0.21 0.06 07/11/05 07/14/05 5192451 88
Uranium 238 14.4 1.6 0.06 07/11/05 07/14/05 5192451 88
ISO THORIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD
Thorium 228 90 16 0.4 07/15/05 07/19/05 5196204 84
Thorium 230 17.3 3.6 0.4 07/15/05 07/19/05 5196204 84
Thorium 232 83 14 0.4 07/15/05 07/19/05 5196204 84
NOTE (S)
Data are incomplete without the caae narrative.
DC in determined by instrument performance only.
results are greater Chan the MDC
J Result is greater than sample detection limit but less than stated reporting limit.
SCIENTECH INC
Client, Samole ID: 6-30-05 S-7 DUP
Severn Trent Laboratories -. Radiochemistry
Lab Sample ID:
Work Order:
Matrix;
F5G070301-007X
HE2MH
SOLID
Date Collected:Date Received:
06/30/05 133007/07/05 0900
TotalUncert. Prep Analysis
Parameter Result Qual (2 a+/-) MDC Date Date Batch # Yld %
ISo URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD
Uranium 234 12.7 1.5 0.1 07/11/05 07/14/05 5192451 77
Uranium 235 0.613 J 0.21 0.09 07/11/05 07/14/05 5192451 77
Uranium 238 12.6 1.5 0.07 07/11/05 07/14/05 5192451 77
Iso THORIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODThorium 228 77 14 0.5 07/15/05 07/19/05 5196204 84
Thorium 230 14.8 3.3 0.4 07/15/05 07/19/05 5196204 84
Thorium 232 74 13 0.3 07/15/05 07/19/05 5196204 84
NOTE (S)
Data are inoemplete without the cave narrative.
)C is determined by instrument performance only..... old results are greater than the MDC
iJ Result is greater than Sample detection limit but less than stated reporting limit.
SCIENTECH INC
Client Sample ID: 6-30-05 S-8
Severn Trent Laboratories - Radiochemistry
Lab Sample ID:
Work Order;
Matrix:
FSG070301-008HE2MJSOLID
Date Collected:Date Received:
06/30/05 133507/07/05 0900
TotalVacert. Prop Analysis
Parameter Reauit Qual (2 o+/-) XDC Date Date Batch # Yld .
Iso URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODUranium 23,4 9.2 1.I1 0.1 07/11/05 07 /14/05 5192451 90Uranium 235 0.41• J 0.16 0.09 07/11/05 07/14/05 5192451 90
Uranium 23 8 9.0I 1.0 0.08 07/11/05 07/14/05 5192451 90
ISO THORIUM (SHORT CT) DO A-01-R MOD pCi/g A-01-R MOD
Thorium 222 309.9 3.3 0.2 07/15/05 07/18/05 5196204 69Thorium 230 7.3 12 .1 0.1 07/15/05 07/18/D5 5196204 69
Thoritum 232 29.9 3.3 0.i 07/15/05 07/18/D5 5196204 69
NOTE(S)
Data are iucompletO without the case narrative.
(\ 'iDC is determined by instrument performance only..Bold results are greater than the MDC
J Result is greater than sample detection lim:it but less than stated reporting limit.
Uranium Decay Chain
28U t, 234Th :
100%
Thorium Decay Chain
234pa * 234u
234 u 230Th * 226Ra * 222Rn *'
218po * 214
pb C 214Bi
232Th r> 22Ra * 22Ac -
2 28Th • 2 24
Ra *2 2 0
Rn c* 2 16
po =:> 212 Pb * 2 1 2Bi
Note: All sample values include stated +2a lab variance. No background was subtracted.
Sample#S-1S-2S-3S-4S-5S-6S-7
S-7[Dup]S-8
Average =
232Th
61.245.842.982.732.541.4
9787
33.2
2 8Th
60.647.344.584.231.441.5106
9133.9
ThE60.9046.5543.7083.4531.9541.45
101.5089.0033.55
238u
21.91011
10.511.510.4
1614.1
10
234u 230Th
pCi< DJm
22 14.39.02 12.511.5 13.210.2 18.911.4 8.410.2 11.815.9 20.914.2 18.110.3 8.4
2 35U
1.21 19.400.54 10.510.84 11.900.54 13.201.02 10.430.56 10.800.91 17.600.82 15.470.57 9.57
13.21 pCl"'gu
3.51 pCi'9m u
16.7 pCi 9'mu
Standard deviation of data set =59.12 pCi"gn Th
25.94 pCiO Tn
85.1 pCi-'mT