Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort...

47

Transcript of Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort...

Page 1: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080634 Page Number: 1 of 2Summary ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX 79901 Report Date: August 12, 2009Work Order: 9080634�9080634�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split Sampling Date Time DateSample Des ription Matrix Taken Taken Re eived204898 EP-62 (GW) water 2009-08-04 08:07 2009-08-04204899 EP-66 (GW) water 2009-08-04 08:41 2009-08-04204900 EP-5 (GW) water 2009-08-04 09:04 2009-08-04204901 EP-6 (GW) water 2009-08-04 10:01 2009-08-04204902 EP-7 (GW) water 2009-08-04 10:16 2009-08-04204903 SEP-4 (SW) water 2009-08-04 10:52 2009-08-04Sample: 204898 - EP-62 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204899 - EP-66 (GW)Param Flag Result Units RLHexavalent Chromium 0.0110 mg/L 0.0100Sample: 204900 - EP-5 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 2: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080634 Page Number: 2 of 2Sample: 204901 - EP-6 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204902 - EP-7 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204903 - SEP-4 (SW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100

Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 3: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080635 Page Number: 1 of 2Summary ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX 79901 Report Date: August 12, 2009Work Order: 9080635�9080635�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split Sampling Date Time DateSample Des ription Matrix Taken Taken Re eived204904 SEP-9 (SW) water 2009-08-04 13:10 2009-08-06204905 SEP-7 (SW) water 2009-08-04 13:40 2009-08-06204906 EP-111 (SW) water 2009-08-04 14:20 2009-08-06204907 EP-112 (SW) water 2009-08-04 14:50 2009-08-06204908 SEP-11 (SW) water 2009-08-04 15:10 2009-08-06204909 SEP-3 (SW) water 2009-08-04 15:35 2009-08-06204910 FD-2 water 2009-08-04 11:40 2009-08-06Sample: 204904 - SEP-9 (SW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204905 - SEP-7 (SW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204906 - EP-111 (SW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 4: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080635 Page Number: 2 of 2Sample: 204907 - EP-112 (SW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204908 - SEP-11 (SW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204909 - SEP-3 (SW)Param Flag Result Units RLHexavalent Chromium 0.0140 mg/L 0.0100Sample: 204910 - FD-2Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100

Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 5: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080637 Page Number: 1 of 2Summary ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX 79901 Report Date: August 12, 2009Work Order: 9080637�9080637�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split Sampling Date Time DateSample Des ription Matrix Taken Taken Re eived204915 FD-3 (GW) water 2009-08-05 06:30 2009-08-05204916 EP-20 (GW) water 2009-08-05 07:55 2009-08-05204917 EP-35 (GW) water 2009-08-05 08:30 2009-08-05204918 EP-29 (GW) water 2009-08-05 09:04 2009-08-05Sample: 204915 - FD-3 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204916 - EP-20 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204917 - EP-35 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204918 - EP-29 (GW)Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 6: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080637 Page Number: 2 of 2Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100

Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 7: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080418 Page Number: 1 of 2Summary ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX 79901 Report Date: August 12, 2009Work Order: 9080418�9080418�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split Sampling Date Time DateSample Des ription Matrix Taken Taken Re eived204592 EP-110 (GW) water 2009-08-03 08:00 2009-08-03204593 EP-126 (GW) water 2009-08-03 08:55 2009-08-03204594 EP-129 (GW) water 2009-08-03 09:41 2009-08-03204595 EP-94(GW) water 2009-08-03 10:41 2009-08-03204596 EP-49(GW) water 2009-08-03 11:26 2009-08-03Sample: 204592 - EP-110 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204593 - EP-126 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204594 - EP-129 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204595 - EP-94(GW)Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 8: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080418 Page Number: 2 of 2Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204596 - EP-49(GW)Param Flag Result Units RLHexavalent Chromium 0.0200 mg/L 0.0100

Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 9: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080419 Page Number: 1 of 2Summary ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX 79901 Report Date: August 12, 2009Work Order: 9080419�9080419�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split Sampling Date Time DateSample Des ription Matrix Taken Taken Re eived204597 EP-71 (GW) water 2009-08-03 13:17 2009-08-03204598 EP-51 (GW) water 2009-08-03 13:55 2009-08-03204599 EP-81 (GW) water 2009-08-03 14:35 2009-08-03204600 EP-80 (GW) water 2009-08-03 14:57 2009-08-03204601 FD-1 water 2009-08-03 06:00 2009-08-03Sample: 204597 - EP-71 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204598 - EP-51 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204599 - EP-81 (GW)Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204600 - EP-80 (GW)Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 10: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080419 Page Number: 2 of 2Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100Sample: 204601 - FD-1Param Flag Result Units RLHexavalent Chromium <0.0100 mg/L 0.0100

Tra eAnalysis, In . � 6701 Aberdeen Ave., Suite 9 � Lubbo k, TX 79424-1515 � (806) 794-1296This is only a summary. Please, refer to the omplete report pa kage for quality ontrol data.

Page 11: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Certi� ationsWBENC: 237019 HUB: 1752439743100-86536 DBE: VN 20657NCTRCA WFWB38444Y0909NELAP Certi� ationsLubbo k: T104704219-08-TX El Paso: T104704221-08-TX Midland: T104704392-08-TXLELAP-02003 LELAP-02002Kansas E-10317Analyti al and Quality Control ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX, 79901 Report Date: August 12, 2009Work Order: 9080634�9080634�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split SamplingProje t Number: 2009 Split SamplingEn losed are the Analyti al Report and Quality Control Report for the following sample(s) submitted to Tra eAnalysis, In .Date Time DateSample Des ription Matrix Taken Taken Re eived204898 EP-62 (GW) water 2009-08-04 08:07 2009-08-04204899 EP-66 (GW) water 2009-08-04 08:41 2009-08-04204900 EP-5 (GW) water 2009-08-04 09:04 2009-08-04204901 EP-6 (GW) water 2009-08-04 10:01 2009-08-04204902 EP-7 (GW) water 2009-08-04 10:16 2009-08-04204903 SEP-4 (SW) water 2009-08-04 10:52 2009-08-04These results represent only the samples re eived in the laboratory. The Quality Control Report is generated on a bat hbasis. All information ontained in this report is for the analyti al bat h(es) in whi h your sample(s) were analyzed.

Page 12: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

This report onsists of a total of 6 pages and shall not be reprodu ed ex ept in its entirety, without written approval ofTra eAnalysis, In .Dr. Blair Leftwi h, Dire torDr. Mi hael Abel, Proje t ManagerStandard FlagsB - The sample ontains less than ten times the on entration found in the method blank.

Page 2 of 6

Page 13: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Case NarrativeSamples for proje t 2009 Split Sampling were re eived by Tra eAnalysis, In . on 2009-08-04 and assigned to work order9080634. Samples for work order 9080634 were re eived inta t at a temperature of 4.0 deg. C.Samples were analyzed for the following tests using their respe tive methods.Prep Prep QC AnalysisTest Method Bat h Date Bat h DateChromium, Hexavalent SM 3500-Cr B 53193 2009-08-04 at 12:03 62354 2009-08-04 at 12:03Results for these samples are reported on a wet weight basis unless data pa kage indi ates otherwise.A matrix spike (MS) and matrix spike dupli ate (MSD) sample is hosen at random from ea h preparation bat h. The MSand MSD will indi ate if a site spe i� matrix problem is o urring, however, it may not pertain to the samples for work order9080634 sin e the sample was hosen at random. Therefore, the validity of the analyti al data reported has been determinedby the laboratory ontrol sample (LCS) and the method blank (MB). These quality ontrol measures are performed withea h preparation bat h to ensure data integrity.All other ex eptions asso iated with this report have been footnoted on the appropriate analyti al page to assist in generaldata omprehension. Please onta t the laboratory dire tly if there are any questions regarding this proje t.

Page 3 of 6

Page 14: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080634 Page Number: 4 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasAnalyti al ReportSample: 204898 - EP-62 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204899 - EP-66 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium 0.0110 mg/L 1 0.0100Sample: 204900 - EP-5 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204901 - EP-6 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 Sample Preparation: 2009-08-04 Prepared By: JR

Page 15: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080634 Page Number: 5 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204902 - EP-7 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204903 - SEP-4 (SW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Method Blank (1) QC Bat h: 62354QC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 QC Preparation: 2009-08-04 Prepared By: MDMDLParameter Flag Result Units RLHexavalent Chromium <0.00594 mg/L 0.01Laboratory Control Spike (LCS-1)QC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 QC Preparation: 2009-08-04 Prepared By: MD

Page 16: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080634 Page Number: 6 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasLCS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.498 mg/L 1 0.500 <0.00594 100 95.4 - 105Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.LCSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.491 mg/L 1 0.500 <0.00594 98 95.4 - 105 1 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Matrix Spike (MS-1) Spiked Sample: 204899QC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53193 QC Preparation: 2009-08-04 Prepared By: MDMS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.562 mg/L 1.11 0.556 0.011 99 80.1 - 118Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.MSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.572 mg/L 1.11 0.556 0.011 101 80.1 - 118 2 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Standard (CCV-1)QC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.507 101 90 - 110 2009-08-04Standard (CCV-2)QC Bat h: 62354 Date Analyzed: 2009-08-04 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.495 99 90 - 110 2009-08-04

Page 17: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:
Page 18: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Certi� ationsWBENC: 237019 HUB: 1752439743100-86536 DBE: VN 20657NCTRCA WFWB38444Y0909NELAP Certi� ationsLubbo k: T104704219-08-TX El Paso: T104704221-08-TX Midland: T104704392-08-TXLELAP-02003 LELAP-02002Kansas E-10317Analyti al and Quality Control ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX, 79901 Report Date: August 12, 2009Work Order: 9080635�9080635�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split SamplingProje t Number: 2009 Split SamplingEn losed are the Analyti al Report and Quality Control Report for the following sample(s) submitted to Tra eAnalysis, In .Date Time DateSample Des ription Matrix Taken Taken Re eived204904 SEP-9 (SW) water 2009-08-04 13:10 2009-08-06204905 SEP-7 (SW) water 2009-08-04 13:40 2009-08-06204906 EP-111 (SW) water 2009-08-04 14:20 2009-08-06204907 EP-112 (SW) water 2009-08-04 14:50 2009-08-06204908 SEP-11 (SW) water 2009-08-04 15:10 2009-08-06204909 SEP-3 (SW) water 2009-08-04 15:35 2009-08-06204910 FD-2 water 2009-08-04 11:40 2009-08-06These results represent only the samples re eived in the laboratory. The Quality Control Report is generated on a bat h

Page 19: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

basis. All information ontained in this report is for the analyti al bat h(es) in whi h your sample(s) were analyzed.This report onsists of a total of 8 pages and shall not be reprodu ed ex ept in its entirety, without written approval ofTra eAnalysis, In .Dr. Blair Leftwi h, Dire torDr. Mi hael Abel, Proje t ManagerStandard FlagsB - The sample ontains less than ten times the on entration found in the method blank.

Page 2 of 8

Page 20: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Case NarrativeSamples for proje t 2009 Split Sampling were re eived by Tra eAnalysis, In . on 2009-08-06 and assigned to work order9080635. Samples for work order 9080635 were re eived inta t at a temperature of 4.0 deg. C.Samples were analyzed for the following tests using their respe tive methods.Prep Prep QC AnalysisTest Method Bat h Date Bat h DateChromium, Hexavalent SM 3500-Cr B 53197 2009-08-04 at 16:20 62359 2009-08-04 at 16:20Chromium, Hexavalent SM 3500-Cr B 53198 2009-08-05 at 11:35 62360 2009-08-05 at 11:35Results for these samples are reported on a wet weight basis unless data pa kage indi ates otherwise.A matrix spike (MS) and matrix spike dupli ate (MSD) sample is hosen at random from ea h preparation bat h. The MSand MSD will indi ate if a site spe i� matrix problem is o urring, however, it may not pertain to the samples for work order9080635 sin e the sample was hosen at random. Therefore, the validity of the analyti al data reported has been determinedby the laboratory ontrol sample (LCS) and the method blank (MB). These quality ontrol measures are performed withea h preparation bat h to ensure data integrity.All other ex eptions asso iated with this report have been footnoted on the appropriate analyti al page to assist in generaldata omprehension. Please onta t the laboratory dire tly if there are any questions regarding this proje t.

Page 3 of 8

Page 21: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080635 Page Number: 4 of 82009 Split Sampling 2009 Split Sampling El Paso, TexasAnalyti al ReportSample: 204904 - SEP-9 (SW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53197 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204905 - SEP-7 (SW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53197 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204906 - EP-111 (SW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204907 - EP-112 (SW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JR

Page 22: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080635 Page Number: 5 of 82009 Split Sampling 2009 Split Sampling El Paso, TexasRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204908 - SEP-11 (SW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204909 - SEP-3 (SW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium 0.0140 mg/L 1 0.0100Sample: 204910 - FD-2Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53197 Sample Preparation: 2009-08-04 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Method Blank (1) QC Bat h: 62359QC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53197 QC Preparation: 2009-08-04 Prepared By: MD

Page 23: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080635 Page Number: 6 of 82009 Split Sampling 2009 Split Sampling El Paso, TexasMDLParameter Flag Result Units RLHexavalent Chromium <0.00594 mg/L 0.01Method Blank (1) QC Bat h: 62360QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 QC Preparation: 2009-08-05 Prepared By: MDMDLParameter Flag Result Units RLHexavalent Chromium <0.00594 mg/L 0.01Laboratory Control Spike (LCS-1)QC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53197 QC Preparation: 2009-08-04 Prepared By: MDLCS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.497 mg/L 1 0.500 <0.00594 99 95.4 - 105Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.LCSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.499 mg/L 1 0.500 <0.00594 100 95.4 - 105 0 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Laboratory Control Spike (LCS-1)QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 QC Preparation: 2009-08-05 Prepared By: MDLCS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.489 mg/L 1 0.500 <0.00594 98 95.4 - 105Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.LCSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.483 mg/L 1 0.500 <0.00594 97 95.4 - 105 1 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.

Page 24: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080635 Page Number: 7 of 82009 Split Sampling 2009 Split Sampling El Paso, TexasMatrix Spike (MS-1) Spiked Sample: 204904QC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MDPrep Bat h: 53197 QC Preparation: 2009-08-04 Prepared By: MDMS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.687 mg/L 1.11 0.556 0.148 97 80.1 - 118Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.MSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.680 mg/L 1.11 0.556 0.148 96 80.1 - 118 1 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Matrix Spike (MS-1) Spiked Sample: 204907QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 QC Preparation: 2009-08-05 Prepared By: MDMS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.492 mg/L 1.11 0.556 <0.00659 88 80.1 - 118Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.MSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.488 mg/L 1.11 0.556 <0.00659 88 80.1 - 118 1 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Standard (CCV-1)QC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.496 99 90 - 110 2009-08-04Standard (CCV-2)QC Bat h: 62359 Date Analyzed: 2009-08-04 Analyzed By: MD

Page 25: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080635 Page Number: 8 of 82009 Split Sampling 2009 Split Sampling El Paso, TexasCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.496 99 90 - 110 2009-08-04Standard (CCV-1)QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.489 98 90 - 110 2009-08-05Standard (CCV-2)QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.501 100 90 - 110 2009-08-05

Page 26: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:
Page 27: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Certi� ationsWBENC: 237019 HUB: 1752439743100-86536 DBE: VN 20657NCTRCA WFWB38444Y0909NELAP Certi� ationsLubbo k: T104704219-08-TX El Paso: T104704221-08-TX Midland: T104704392-08-TXLELAP-02003 LELAP-02002Kansas E-10317Analyti al and Quality Control ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX, 79901 Report Date: August 12, 2009Work Order: 9080637�9080637�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split SamplingProje t Number: 2009 Split SamplingEn losed are the Analyti al Report and Quality Control Report for the following sample(s) submitted to Tra eAnalysis, In .Date Time DateSample Des ription Matrix Taken Taken Re eived204915 FD-3 (GW) water 2009-08-05 06:30 2009-08-05204916 EP-20 (GW) water 2009-08-05 07:55 2009-08-05204917 EP-35 (GW) water 2009-08-05 08:30 2009-08-05204918 EP-29 (GW) water 2009-08-05 09:04 2009-08-05These results represent only the samples re eived in the laboratory. The Quality Control Report is generated on a bat hbasis. All information ontained in this report is for the analyti al bat h(es) in whi h your sample(s) were analyzed.This report onsists of a total of 6 pages and shall not be reprodu ed ex ept in its entirety, without written approval of

Page 28: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Tra eAnalysis, In .Dr. Blair Leftwi h, Dire torDr. Mi hael Abel, Proje t ManagerStandard FlagsB - The sample ontains less than ten times the on entration found in the method blank.

Page 2 of 6

Page 29: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Case NarrativeSamples for proje t 2009 Split Sampling were re eived by Tra eAnalysis, In . on 2009-08-05 and assigned to work order9080637. Samples for work order 9080637 were re eived inta t at a temperature of 8.0 deg. C.Samples were analyzed for the following tests using their respe tive methods.Prep Prep QC AnalysisTest Method Bat h Date Bat h DateChromium, Hexavalent SM 3500-Cr B 53198 2009-08-05 at 11:35 62360 2009-08-05 at 11:35Results for these samples are reported on a wet weight basis unless data pa kage indi ates otherwise.A matrix spike (MS) and matrix spike dupli ate (MSD) sample is hosen at random from ea h preparation bat h. The MSand MSD will indi ate if a site spe i� matrix problem is o urring, however, it may not pertain to the samples for work order9080637 sin e the sample was hosen at random. Therefore, the validity of the analyti al data reported has been determinedby the laboratory ontrol sample (LCS) and the method blank (MB). These quality ontrol measures are performed withea h preparation bat h to ensure data integrity.All other ex eptions asso iated with this report have been footnoted on the appropriate analyti al page to assist in generaldata omprehension. Please onta t the laboratory dire tly if there are any questions regarding this proje t.

Page 3 of 6

Page 30: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080637 Page Number: 4 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasAnalyti al ReportSample: 204915 - FD-3 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204916 - EP-20 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204917 - EP-35 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204918 - EP-29 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 Sample Preparation: 2009-08-05 Prepared By: JR

Page 31: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080637 Page Number: 5 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Method Blank (1) QC Bat h: 62360QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 QC Preparation: 2009-08-05 Prepared By: MDMDLParameter Flag Result Units RLHexavalent Chromium <0.00594 mg/L 0.01Laboratory Control Spike (LCS-1)QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 QC Preparation: 2009-08-05 Prepared By: MDLCS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.489 mg/L 1 0.500 <0.00594 98 95.4 - 105Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.LCSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.483 mg/L 1 0.500 <0.00594 97 95.4 - 105 1 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Matrix Spike (MS-1) Spiked Sample: 204907QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDPrep Bat h: 53198 QC Preparation: 2009-08-05 Prepared By: MDMS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.492 mg/L 1.11 0.556 <0.00659 88 80.1 - 118Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.MSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.488 mg/L 1.11 0.556 <0.00659 88 80.1 - 118 1 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.

Page 32: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080637 Page Number: 6 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasStandard (CCV-1)QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.489 98 90 - 110 2009-08-05Standard (CCV-2)QC Bat h: 62360 Date Analyzed: 2009-08-05 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.501 100 90 - 110 2009-08-05

Page 33: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:
Page 34: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Certi� ationsWBENC: 237019 HUB: 1752439743100-86536 DBE: VN 20657NCTRCA WFWB38444Y0909NELAP Certi� ationsLubbo k: T104704219-08-TX El Paso: T104704221-08-TX Midland: T104704392-08-TXLELAP-02003 LELAP-02002Kansas E-10317Analyti al and Quality Control ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX, 79901 Report Date: August 12, 2009Work Order: 9080418�9080418�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split SamplingProje t Number: 2009 Split SamplingEn losed are the Analyti al Report and Quality Control Report for the following sample(s) submitted to Tra eAnalysis, In .Date Time DateSample Des ription Matrix Taken Taken Re eived204592 EP-110 (GW) water 2009-08-03 08:00 2009-08-03204593 EP-126 (GW) water 2009-08-03 08:55 2009-08-03204594 EP-129 (GW) water 2009-08-03 09:41 2009-08-03204595 EP-94(GW) water 2009-08-03 10:41 2009-08-03204596 EP-49(GW) water 2009-08-03 11:26 2009-08-03These results represent only the samples re eived in the laboratory. The Quality Control Report is generated on a bat hbasis. All information ontained in this report is for the analyti al bat h(es) in whi h your sample(s) were analyzed.

Page 35: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

This report onsists of a total of 6 pages and shall not be reprodu ed ex ept in its entirety, without written approval ofTra eAnalysis, In .Dr. Blair Leftwi h, Dire torDr. Mi hael Abel, Proje t ManagerStandard FlagsB - The sample ontains less than ten times the on entration found in the method blank.

Page 2 of 6

Page 36: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Case NarrativeSamples for proje t 2009 Split Sampling were re eived by Tra eAnalysis, In . on 2009-08-03 and assigned to work order9080418. Samples for work order 9080418 were re eived inta t at a temperature of 3.0 deg. C.Samples were analyzed for the following tests using their respe tive methods.Prep Prep QC AnalysisTest Method Bat h Date Bat h DateChromium, Hexavalent SM 3500-Cr B 53187 2009-08-03 at 14:40 62347 2009-08-03 at 14:40Results for these samples are reported on a wet weight basis unless data pa kage indi ates otherwise.A matrix spike (MS) and matrix spike dupli ate (MSD) sample is hosen at random from ea h preparation bat h. The MSand MSD will indi ate if a site spe i� matrix problem is o urring, however, it may not pertain to the samples for work order9080418 sin e the sample was hosen at random. Therefore, the validity of the analyti al data reported has been determinedby the laboratory ontrol sample (LCS) and the method blank (MB). These quality ontrol measures are performed withea h preparation bat h to ensure data integrity.All other ex eptions asso iated with this report have been footnoted on the appropriate analyti al page to assist in generaldata omprehension. Please onta t the laboratory dire tly if there are any questions regarding this proje t.

Page 3 of 6

Page 37: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080418 Page Number: 4 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasAnalyti al ReportSample: 204592 - EP-110 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204593 - EP-126 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204594 - EP-129 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204595 - EP-94(GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 Sample Preparation: 2009-08-03 Prepared By: JR

Page 38: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080418 Page Number: 5 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204596 - EP-49(GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium 0.0200 mg/L 1 0.0100Method Blank (1) QC Bat h: 62347QC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 QC Preparation: 2009-08-03 Prepared By: MDMDLParameter Flag Result Units RLHexavalent Chromium <0.00594 mg/L 0.01Laboratory Control Spike (LCS-1)QC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 QC Preparation: 2009-08-03 Prepared By: MDLCS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.501 mg/L 1 0.500 <0.00594 100 95.4 - 105Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.LCSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.498 mg/L 1 0.500 <0.00594 100 95.4 - 105 1 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.

Page 39: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080418 Page Number: 6 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasMatrix Spike (MS-1) Spiked Sample: 204592QC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDPrep Bat h: 53187 QC Preparation: 2009-08-03 Prepared By: MDMS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.565 mg/L 1.11 0.556 <0.00659 102 80.1 - 118Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.MSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.578 mg/L 1.11 0.556 <0.00659 104 80.1 - 118 2 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Standard (CCV-1)QC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.498 100 90 - 110 2009-08-03Standard (CCV-2)QC Bat h: 62347 Date Analyzed: 2009-08-03 Analyzed By: MDCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.506 101 90 - 110 2009-08-03

Page 40: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:
Page 41: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Certi� ationsWBENC: 237019 HUB: 1752439743100-86536 DBE: VN 20657NCTRCA WFWB38444Y0909NELAP Certi� ationsLubbo k: T104704219-08-TX El Paso: T104704221-08-TX Midland: T104704392-08-TXLELAP-02003 LELAP-02002Kansas E-10317Analyti al and Quality Control ReportJose OjedaTCEQ Region 6401 E. FranklinSuite 560El Paso, TX, 79901 Report Date: August 12, 2009Work Order: 9080419�9080419�Proje t Lo ation: El Paso, TexasProje t Name: 2009 Split SamplingProje t Number: 2009 Split SamplingEn losed are the Analyti al Report and Quality Control Report for the following sample(s) submitted to Tra eAnalysis, In .Date Time DateSample Des ription Matrix Taken Taken Re eived204597 EP-71 (GW) water 2009-08-03 13:17 2009-08-03204598 EP-51 (GW) water 2009-08-03 13:55 2009-08-03204599 EP-81 (GW) water 2009-08-03 14:35 2009-08-03204600 EP-80 (GW) water 2009-08-03 14:57 2009-08-03204601 FD-1 water 2009-08-03 06:00 2009-08-03These results represent only the samples re eived in the laboratory. The Quality Control Report is generated on a bat hbasis. All information ontained in this report is for the analyti al bat h(es) in whi h your sample(s) were analyzed.

Page 42: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

This report onsists of a total of 6 pages and shall not be reprodu ed ex ept in its entirety, without written approval ofTra eAnalysis, In .Dr. Blair Leftwi h, Dire torDr. Mi hael Abel, Proje t ManagerStandard FlagsB - The sample ontains less than ten times the on entration found in the method blank.

Page 2 of 6

Page 43: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Case NarrativeSamples for proje t 2009 Split Sampling were re eived by Tra eAnalysis, In . on 2009-08-03 and assigned to work order9080419. Samples for work order 9080419 were re eived inta t at a temperature of 3.0 deg. C.Samples were analyzed for the following tests using their respe tive methods.Prep Prep QC AnalysisTest Method Bat h Date Bat h DateChromium, Hexavalent SM 3500-Cr B 53189 2009-08-03 at 17:50 62349 2009-08-03 at 17:50Results for these samples are reported on a wet weight basis unless data pa kage indi ates otherwise.A matrix spike (MS) and matrix spike dupli ate (MSD) sample is hosen at random from ea h preparation bat h. The MSand MSD will indi ate if a site spe i� matrix problem is o urring, however, it may not pertain to the samples for work order9080419 sin e the sample was hosen at random. Therefore, the validity of the analyti al data reported has been determinedby the laboratory ontrol sample (LCS) and the method blank (MB). These quality ontrol measures are performed withea h preparation bat h to ensure data integrity.All other ex eptions asso iated with this report have been footnoted on the appropriate analyti al page to assist in generaldata omprehension. Please onta t the laboratory dire tly if there are any questions regarding this proje t.

Page 3 of 6

Page 44: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080419 Page Number: 4 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasAnalyti al ReportSample: 204597 - EP-71 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204598 - EP-51 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204599 - EP-81 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204600 - EP-80 (GW)Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 Sample Preparation: 2009-08-03 Prepared By: JR

Page 45: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080419 Page Number: 5 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Sample: 204601 - FD-1Laboratory: El PasoAnalysis: Chromium, Hexavalent Analyti al Method: SM 3500-Cr B Prep Method: N/AQC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 Sample Preparation: 2009-08-03 Prepared By: JRRLParameter Flag Result Units Dilution RLHexavalent Chromium <0.0100 mg/L 1 0.0100Method Blank (1) QC Bat h: 62349QC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 QC Preparation: 2009-08-03 Prepared By: JRMDLParameter Flag Result Units RLHexavalent Chromium <0.00594 mg/L 0.01Laboratory Control Spike (LCS-1)QC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 QC Preparation: 2009-08-03 Prepared By: JRLCS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.503 mg/L 1 0.500 <0.00594 101 95.4 - 105Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.LCSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.505 mg/L 1 0.500 <0.00594 101 95.4 - 105 0 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.

Page 46: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date:

Report Date: August 12, 2009 Work Order: 9080419 Page Number: 6 of 62009 Split Sampling 2009 Split Sampling El Paso, TexasMatrix Spike (MS-1) Spiked Sample: 204597QC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRPrep Bat h: 53189 QC Preparation: 2009-08-03 Prepared By: JRMS Spike Matrix Re .Param Result Units Dil. Amount Result Re . LimitHexavalent Chromium 0.570 mg/L 1.11 0.556 0.047 94 80.1 - 118Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.MSD Spike Matrix Re . RPDParam Result Units Dil. Amount Result Re . Limit RPD LimitHexavalent Chromium 0.567 mg/L 1.11 0.556 0.047 94 80.1 - 118 0 20Per ent re overy is based on the spike result. RPD is based on the spike and spike dupli ate result.Standard (CCV-1)QC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.506 101 90 - 110 2009-08-03Standard (CCV-2)QC Bat h: 62349 Date Analyzed: 2009-08-03 Analyzed By: JRCCVs CCVs CCVs Per entTrue Found Per ent Re overy DateParam Flag Units Con . Con . Re overy Limits AnalyzedHexavalent Chromium mg/L 0.500 0.505 101 90 - 110 2009-08-03

Page 47: Rep ort Date: August 12, 2009 W ork Order: 9080634 P age ...€¦ · b er: 1 of 2 Summary Rep ort Jose Ojeda TCEQ Region 6 401 E. F ranklin Suite 560 El P aso, TX 79901 Rep ort Date: