Release Abatement Measure Status Report No. 2 Site ... · disposal site, identified as 50 Fordham...

AECOM •LOCKHEED MARTIN FORMER GE FACILITY, RELEASE ABATEMENT MEASURE STATUS REPORT NO. 2

Release Abatement Measure Status Report No. 2

Site Improvement Activities Former General Electric Facility

50 Fordham Road, Wilmington, MA RTN 3-0518

Prepared for:

Lockheed Martin Corporation/Wilmington Realty Trust

Prepared by:

AECOM

April 27, 2018

_________________________________

Prepared By: Nicole Callahan

_________________________________

Reviewed By: Scott Olson

____________________________

Reviewed by Daniel W. Folan, PhD, PG, LSP

AECOM •LOCKHEED MARTIN FORMER GE FACILITY, RELEASE ABATEMENT MEASURE STATUS REPORT NO. 2 Page i

DOCUMENT CHANGE HISTORY

Revision Number

Prepared By/Approved By

Release Date

Change Description

Section Narrative of

Items Affected

0 N. Callahan/

D. Folan/S. Olson

April 27, 2018

AECOM •LOCKHEED MARTIN FORMER GE FACILITY, RELEASE ABATEMENT MEASURE STATUS REPORT NO. 2 Page i

TABLE OF CONTENTS

1 INTRODUCTION ............................................................................................... 1-1

1.1 CONTACT INFORMATION ....................................................................................... 1-2

1.2 DISPOSAL SITE AND RAM BACKGROUND .......................................................... 1-3

2 RAM STATUS ................................................................................................... 2-1

2.1 SOIL MANAGEMENT ................................................................................................ 2-1

2.1.1 Island and Light Pole Excavations – Stockpile 11 ............................................ 2-2

2.1.2 Northern EPL Drainage Swale Excavation- Stockpile 12 ................................. 2-2

2.2 AIR MONITORING ...................................................................................................... 2-3

2.3 GROUNDWATER MANAGEMENT .......................................................................... 2-3

3 REMEDIATION WASTE ................................................................................... 3-1

4 FUTURE RAM ACTIVITIES .............................................................................. 4-1

4.1 FUTURE RAM ACTIVITIES ....................................................................................... 4-1

4.2 FUTURE MCP SUBMITTALS .................................................................................... 4-1

5 LSP OPINION AND CERTIFICATION ............................................................. 5-1

6 REFERENCES .......................................................................................................... 6-1

LIST OF APPENDICES

APPENDIX A LABORATORY ANALYTICAL REPORTS

APPENDIX B WASTE DISPOSAL DOCUMENTATION

LIST OF FIGURES

Figure 1-1 Site Location Map

Figure 1-2 Site Plan

Figure 2-1 Soil Excavation, Grading, and Reuse Areas

Figure 2-2 Soil Stockpile Generation Areas

AECOM •LOCKHEED MARTIN FORMER GE FACILITY, RELEASE ABATEMENT MEASURE STATUS REPORT NO. 2 Page ii

LIST OF TABLES

Table 2-1 Stockpile Summary and Tracking Sheet

Table 2-2 Summary of Soil Analtyical Results – RAM Stockpile Sampling

AECOM •LOCKHEED MARTIN FORMER GE FACILITY, RELEASE ABATEMENT MEASURE STATUS REPORT NO. 2 Page 1-1

Section 1

1 Introduction

Pursuant to the Massachusetts Contingency Plan (MCP) 310 CMR 40.0445, AECOM Technical

Services, Inc. (AECOM), on behalf of Lockheed Martin Corporation (Lockheed Martin) and for

Wilmington Realty Trust (WRT), has prepared the following Release Abatement Measure (RAM)

Status Report No. 2 for the former General Electric Company (GE) Facility located at 50 Fordham

Road, Wilmington, Massachusetts (site). This report is being submitted within six months of the

submittal of the initial RAM Status Report (No. 1) for the site, which was submitted to the

Massachusetts Department of Environmental Protection (MassDEP) on November 3, 2017. The

RAM Plan was submitted to the MassDEP on July 3, 2017. Within this report, “property” pertains

to the address (40-50 Fordham Road) of the former GE Facility, and “site” refers to the MCP

disposal site, identified as 50 Fordham Road and release tracking number (RTN) 3-0518.

A Tier Classification Extension submittal was provided to MassDEP on July 7, 2017 prior to

RAM activities beginning. In addition, no issues were identified by MassDEP as part of their

screening level review of the RAM Plan.

In accordance with the MCP, 310 CMR 40.0445(2), this RAM Status Report contains the

following:

(a) the status of response operations;

(b) any significant new site information or data;

(c) details of and/or plans for the management of Remediation Waste, Remediation

Wastewater and/or Remedial Additives;

(d) any other information that MassDEP determines to be necessary to complete during its

review and evaluation of a Status Report; and,


(e) a Licensed Site Professional (LSP) Opinion as to whether the RAM is being conducted in

conformance with the RAM Plan and any conditions of approval established by

MassDEP.

The MassDEP Bureau of Waste Site Cleanup (BWSC) Transmittal Form BWSC-106 is being

submitted electronically to MassDEP concurrently with this status report via eDEP. Refer to the

July 3, 2017 RAM Plan and the November 3, 2017 RAM Status Report No. 1 completed by

AECOM (AECOM, 2017a & 2017b) for additional details regarding release history, proposed

RAM activities, and RAM activities completed during the first 120-days of implementation.

1.1 CONTACT INFORMATION

The following site-specific information is provided.

Person Conducting RAM

And Property Owner: Wilmington Realty Trust

Gary Stanieich

424 Broadway

Somerville, MA 02145

(603) 860-5508

Telephone: 978-905-2100

Person Completing RAM Submittals: Lockheed Martin Corporation

Paul E. Calligan

6801 Rockledge Drive

MP CCT 246

Bethesda, MD 20817

(240) 687-1813

LSP for the RAM: Daniel W. Folan, PhD, PG, LSP

LSP # 1736

AECOM

250 Apollo Drive

Chelmsford, MA 01824

(978) 905-2114


The RAM activities outlined herein and related to the property improvement and re-development

activities were conducted by WRT, with AECOM observing and documenting the work for MCP

submittals and completing the submittals on behalf of WRT and Lockheed Martin.

1.2 DISPOSAL SITE AND RAM BACKGROUND

The WRT property is designated as 50 Fordham Road in Wilmington, Massachusetts, as shown on

Figure 1-1, Site Location Map, though it consists of buildings identified as 40 and 50 Fordham

Road. The property consists of a 13-acre parcel east of Fordham Road and north of Concord

Street, within a mixed commercial industrial area. The 13-acre parcel is located both in the towns

of Wilmington and North Reading, in Middlesex County, Massachusetts.

The property is located in a mixed commercial, industrial area, and near residential areas. It is

bounded by wooded wetland to the east and north, beyond which are residential properties.

Fordham Road is located along the western property boundary with commercial/industrial parcels

further west and north along Fordham Road. The former Converse, Inc. property and other

commercial/industrial properties are located to the south along Concord Street.

The property contains a number of former industrial buildings, paved parking areas, and an active

sewage and wastewater treatment plant for the facility. The buildings are identified as Building 1

and 1A, which are attached, and Building 2. A Treatment Shed that houses an inactive

groundwater treatment system is still present. Building 3, the Oil House, the concrete ramp to the

former Oil House, the Guard Shack, the former Pump House/Vault, the former Tank Farm, and the

original Tank Farm area groundwater treatment building have been removed. The current site

plan is included as Figure 1-2.

WRT, formerly the Barbo Realty Trust (BRT), is the current property owner and has owned the

property at least since the property was developed in the late 1960s.

A RAM Plan was submitted to the MassDEP for WRT on behalf of Lockheed Martin on July 3,

2017 detailing the proposed redevelopment and construction work and associated monitoring

activities to be completed at the site by WRT. The objective of the RAM is to ensure that

potentially impacted soil, groundwater, or soil gas encountered during construction activities at the

property are managed in accordance with the requirements set forth in the MCP as well as the


Notice of Activity and Use Limitation (AUL) for the property signed July 2015 and recorded on

September 28, 2015 at the Middlesex North Registry of Deeds, the MCP 310 CMR 40.0000, and

Policy #WSC-00-425. Based upon the MassDEP’s WSC-00-425 policy, “construction activities at

a disposal site meet the regulatory definition of a remedial action, to the extent that such activities

involve the potential removal, disposal and relocation of released oil or hazardous material.”

An initial RAM Status Report No. 1 was submitted to the MassDEP for WRT on behalf of

Lockheed Martin on November 3, 2017, detailing RAM activities completed during the 120-day

period following the submittal of the RAM Plan. WRT initiated excavation activities related to

the redevelopment of the site under the RAM in July 2017. Prior to the submittal of the RAM

Plan, limited site work was completed, including site preparation, demolition of various above-

grade and sub-grade structures, the removal of surface concrete and asphalt paving from areas

throughout the site, and exploratory test pits adjacent to select excavation areas. After the

submittal of the RAM Plan and Tier Classification Extension, subsurface excavation was

completed in the following planned construction areas as detailed in the RAM Status Report No.

1: wastewater tight tank and associated trenching, drainage swale excavations, and utility, hydrant,

and curbing excavations. During these excavations, AECOM personnel observed and field

screened soils using a photoionization detector (PID) for the purposes of providing input relative

to the segregation, management, and sampling of soils. Excavated soils were segregated into

stockpiles and sampled for site constituents of concern (COCs). Analytical results were reviewed

to determine if the soil could be re-used on-site or if it was necessary to transport the stockpiled

soil off-site for either disposal or recycling at an appropriate facility. During the initial RAM

activities discussed in the RAM Status Report No. 1, all soil was able to be re-used on-site with

the exception of one stockpile (Stockpile 10). The transportation of this soil off-site for recycling

was completed during this reporting period and is discussed in Section 2 below.


Section 2

2 RAM Status

WRT initiated excavation activities related to the redevelopment of the site under a RAM in July

2017. The majority of the first phase of site work was completed prior to and documented in the

first RAM Status Report submitted in November 2017. Since then, limited excavation and site

work under the RAM has been completed during the month of October 2017. This work included

small excavations related to ongoing site redevelopment activities, including parking lot islands,

light poles and drainage swales. The second and final phase of site work is anticipated to be

completed in spring/summer of 2018. The three areas (light poles, islands, and northern drainage

swale) where soil excavation, grading, staging, and re-use of soils with levels less than Method 1

S-1 risk standards occurred on-site in accordance with the RAM Plan to date are depicted on

Figure 2-1. Information related to the limited excavation completed during this reporting period,

including, field observations, amount and size of stockpiles generated, and laboratory analytical

data and re-use options for the stockpiles generated are detailed in the soil management section

below.

2.1 SOIL MANAGEMENT

During the minimal excavation activities completed during this reporting period (October 2017

through March 2018), AECOM personnel observed multiple excavations for the purposes of

providing input relative to the segregation, management, and sampling of soils. All excavated

soils were segregated into stockpiles based on discreet excavation area. After excavation of each

area was complete, the generated soil stockpile was sampled for analysis of site COCs including:

volatile organic compounds (VOCs), extractable petroleum hydrocarbons (EPH), volatile

petroleum hydrocarbons (VPH), and total arsenic, chromium, copper, lead, zinc, and cyanide.

Analytical results were reviewed to determine if the soil could be re-used on-site within the site

boundaries (concentrations all below Method 1 S-1 Soil Standards) or if it is necessary to transport

the stockpile off-site for either disposal or recycling at an appropriate facility (concentrations

above Method 1 S-1 Soil Standards).


Stockpiled soil was staged in the parking area to the north of Building 1A (eastern parking lot

area), as shown on Figure 2-1. Soil was stockpiled on 6 mil poly sheeting and covered with 6 mil

poly sheeting at the end of each day. Soils that were excavated and temporarily stored in the

stockpiles for screening are described below and presented in Figure 2-2. Currently, less than the

4,500 cubic yards noted in the RAM Plan have been managed under this RAM.

2.1.1 Island and Light Pole Excavations – Stockpile 11

Excavation for the removal and re-location of two light poles and the excavation of several small

islands located in the eastern parking lot (EPL) were completed on October 9 and 10, 2017,

respectively. Excavation related to the light pole re-location extended to a maximum depth of

three feet below ground surface (ft bgs). Excavation for the small islands extended only to a depth

of two inches bgs. No odors or stained soil were observed during these activities. The soils

removed during excavation of these areas were placed into Stockpile 11, which totaled

approximately 40 cubic yards. A composite soil sample was collected from multiple locations

within the stockpile and submitted to Eurofins Spectrum Analytical, Inc. of Agawam, MA

(Eurofins) for analysis of site COCs in accordance with the RAM Plan. Laboratory analytical

results from Stockpile 11 did not identify concentrations of COCs above Method 1 S-1 Soil

Standards. Based on the analytical results, it was determined that soil from Stockpile 11 could be

re-used within the boundaries of the site. A minor amount of soil from the relocation of the two

light poles was not stockpiled for re-use but was backfilled to its original location after site

improvements.

Additional details related to the stockpiles are included on Table 2-1. Laboratory analytical

results from the stockpile samples are summarized on Table 2-2 and copies of the laboratory

analytical report is included as Appendix A.

2.1.2 Northern EPL Drainage Swale Excavation- Stockpile 12

Excavation was completed from October 24 through October 31, 2017 in accordance with the

approved storm water management plan to form the final drainage swale located in the northern

portion of the EPL.


Excavation for the swale extended to a maximum depth of one foot bgs. No odors or staining

were observed within the soils. Excavated soils were accumulated into Stockpile 12, which

totaled approximately 10 cubic yards when complete. A composite soil sample was collected from

multiple locations within the stockpile and submitted to Eurofins for analysis of site COCs in

accordance with the RAM Plan. Laboratory analytical results from Stockpile 12 did not identify

concentrations of COCs above Method 1 S-1 Soil Standards. Based on the analytical results, it

was determined that soil from this stockpile could be re-used within the boundaries of the site.

On-site re-use areas are shown on Figure 2-1.

Additional details related to the stockpiles are included on Table 2-1. Laboratory analytical

results from the stockpile samples are summarized on Table 2-2 and copies of the laboratory

analytical report is included as Appendix A.

2.2 AIR MONITORING

Based on the limited nature (small areas and shallow depths) of the excavation activities

completed during this reporting period, quantitative air monitoring was not completed.

AECOM did not observe excessive visible dust during excavation activities. Additionally, access

to the work zones was limited, and passage of trespassers/workers through the work zones during

excavation was observed to be minimal. Exposure to dust by potential receptors was further

limited as site workers (other than construction workers) within the RAM area consisted mostly of

people within cars driving through the exterior parking areas.

2.3 GROUNDWATER MANAGEMENT

Groundwater was not encountered during RAM activities completed during this reporting period.

To date, the management of groundwater has not been necessary as part of this RAM.


Section 3

3 Remediation Waste

Impacted soil (concentrations of COCs above Method 1 S-1 Standards) was not identified during

RAM activities completed to date, with the exception of approximately 20 cubic yards of soil

(Stockpile 10). Results from this stockpile identified one EPH fraction at concentrations above

Method 1 S-1, S-2, and S-3 Soil Standards. Stockpile 10 (20 cubic yards weighing approximately

40.5 tons) was transported off-site on December 19, 2017 under a MassDEP Bill of Lading to

Aggregate Recycling Corp (ARC) of Eliot, ME for asphalt batching in accordance with 310 CRM

40.0030. Waste disposal documentation is included in Appendix B. All other stockpiles

generated under the RAM to date (Stockpiles 1 through 9, 11 and 12) have been distributed to

designated re-use areas on-site (Figure 2-1), as allowed based on laboratory analytical results

below S-1 Soil Standards. The generation and management of Stockpiles 1 through 10 is

described in RAM Status Report #1. Dewatering has not been required to facilitate excavation

activities completed to date.


Section 4

4 Future RAM Activities

Additional activities related to the implementation of the RAM and the approximate timeline for

these activities are discussed below.

4.1 FUTURE RAM ACTIVITIES

The initial phase of excavation and grading activities at the site is complete. Additional phases of

work are scheduled to take place within the next six months. Any additional excavation work

within the site boundaries will be conducted in accordance with the RAM Plan, submitted in July

2017. Additional activities associated with this RAM will be documented in a RAM Completion

Report, or RAM Status Report, if not completed within six months of this report.

4.2 FUTURE MCP SUBMITTALS

In accordance with the MCP, specifically 310 CMR 40.0446, AECOM will submit a RAM

Completion Report within 60 days following completion of the RAM. Otherwise, RAM Status

Reports will be submitted in compliance with the MCP, every six months until a RAM

Completion Report is submitted.


Section 5

5 LSP Opinion and Certification

The seal and signature of Daniel W. Folan, the LSP of this RAM Status Report No. 2, is included

in the RAM Transmittal Form (BWSC 106) filed via eDEP. It is the opinion of the LSP-of-

Record, Daniel W. Folan, that to the best of his knowledge, information and belief, the response

actions that are the subject of this RAM (i) are being implemented in accordance with the

applicable provision of M.G.L. c.21E and 310 CMR 40.000, (ii) are appropriate and reasonable to

accomplish the purposes of such response actions as set forth in the applicable provisions of

M.G.L. c. 21E and 310 CMR40.0000, and (iii) comply with the identified provisions of all orders,

permits, and approvals identified in this submittal.


Section 6

6 References

1. AECOM, 2017a. Release Abatement Measure Plan, Former General Electric Facility, 50

Fordham Road, Wilmington, MA, RTN 3-0518. July 2017.

2. AECOM, 2017b. Release Abatement Measure Status Report No. 1, Former General

Electric Facility, 50 Fordham Road, Wilmington, MA, RTN 3-0518. November 2017.

3. MassDEP, 2014. Massachusetts Contingency Plan, 310 CMR 40.0000,

December 31, 2007, Amended April 25, 2014 and June 20, 2014.


FIGURES

Site Location

Former GE Facility 50 Fordham Road, Wilmington, MA

DATE: 01/25/2017

SITE LOCATION MAP

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TABLES

Table 2‐1Summary of Soil Analytical Results ‐ RAM Stockpile Sampling

Former GE Facility, 50 Fordham Rd, Wilmington, MA

Stockpile ID

RAM Status Report Soil Excavation Location Stockpile Generation

Date(s)

Approx. Volume

(cy)

Stockpile Sample Date

Sample Results

Received

Stockpile Sample ID

Sample Results Soil End Use Final Soil Location

Stockpile Discrete Sample Screening

(ranges in ppm)1 1 Swale near GZA-102 wells 7/6/17-7/10/17 240 7/10/2017 7/15/2017 SP1_071017-1 All < S1 Re-use on-site Southern re-use area 5 samples: (0.0 - 0.2)2 1 Drainage trench by loading dock 7/10/2017 12 7/10/2017 7/15/2017 SP2_071017-1 All < S1 Re-use on-site Southern re-use area 5 samples: (0.2 - 2.3)3 1 Southern area of swales east of EPL 7/11/17 - 7/18/17 200 7/18/2017 7/24/2017 SP3_071817-1 All < S1 Re-use on-site Northern re-use area 5 samples: (0.0 - 0.1)4 1 Tight tank soils 0-5 ft bgs 7/12/2017 20 7/12/2017 7/19/2017 SP4_071217-1 All < S1 Re-use on-site Northern re-use area 5 samples: (0.0 - 0.1)5 1 Tight tank soils 5-8.5 ft bgs 7/12/2017 20 7/12/2017 7/19/2017 SP5_071217-1 All < S1 Re-use on-site Northern re-use area 5 samples: (13.2 - 335.8)

6 1 Southern middle area of swales east of EPL 7/18/17-7/26/17 200 7/26/2017 8/2/2017 SP6_072617-1 All < S1 Re-use on-site Southern re-use area and lot

east of Building 1 5 samples: (all 0.0)

7 1 Northern area of swales north of EPL 7/20/2017 120 7/20/2017 7/26/2017 SP7_072017-1 All < S1 Re-use on-site Re-use area east of Bulding 1 5 samples: (0.0 - 0.2)

8 1 Northern area of swales north and east of EPL 7/21/17-7/31/17 240 7/31/2017 8/7/2017 SP8_073117-1 All < S1 Re-use on-site Re-use area east of Bulding 1 6 samples: (all 0.0)

9 1 Northeastern area of swales northeastern corner of EPL; swale in center of EPL 7/31/17-8/3/17 150 8/3/2017 8/10/2017 SP9_080317-1 All < S1 Re-use on-site Re-use area east of Bulding 1 5 samples: (0.0 - 0.1)

10 1 & 2 Curbing trench soils from 0-1.5 ft bgs 8/10/17-8/11/17 20 8/11/2017 8/15/2017 SP10_081117-1 EPH >S1 Off site recycling or disposal Recycling at an offsite facility (ARC, Eliot, ME) Not measured

11 2Islands in EPL from 0-2 inches bgs and

relocation of lightpoles in EPL from 0-3 ft bgs

10/9/17-10/11/17 40 10/11/2017 10/17/2017 SP11_101117-1 All < S1 Re-use on-site Re-use in original excavation or area east of Bulding 1 Not measured

12 2 Northern swale in the EPL soils from 0-1 ft bgs 10/24/17-10/31/17 10 11/1/2017 11/6/2017 SP12_110117-1 All < S1 Re-use on-site Re-use area east of Bulding 1 5 samples: (all 0.0)

1 of 1

Table 2-2Summary of Soil Analytical Results - RAM Stockpile Sampling

Former GE Facility, 50 Fordham Rd, Wilmington, MA

Client ID: SP1_071017-1 SP2_071017-1 SP3_071817-1 SP4_071217-1 SP5_071217-1 SP6_072617-1 SP7_072017-1 SP8_073117-1 SP8_073117-2 SP9_080317-1 SP10_081117-1 SP11_101117-1 SP12_110117-1Lab ID: SC36812-03 SC36812-02 SC37123-02 SC36934-02 SC36934-03 SC37220-02 SC37220-02 SC37605-02 SC37605-03 (DUP) SC37797-02 SC38055-02 SC40242-01 SC40987-02Matrix: Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil SoilSample Date: 10-Jul-17 10-Jul-17 18-Jul-17 12-Jul-17 12-Jul-17 26-Jul-17 20-Jul-17 20-Jul-17 20-Jul-17 3-Aug-17 11-Aug-17 11-Oct-17 1-Nov-17MADEP EPH 5/2004 R (mg/kg dry)C9-C18 Aliphatic Hydrocarbons 1000 3000 1000 3000 5000 < 10.4 < 10.4 <10.7 < 10.4 < 10.8 < 10.9 < 11.1 < 10.6 < 10.7 < 10.8 < 104 < 10.5 < 10.5C19-C36 Aliphatic Hydrocarbons 3000 5000 3000 5000 5000 19.5 <10.4 <10.7 51.2 18 33.4 < 11.1 < 10.6 < 10.7 < 10.8 5,460 < 10.5 98C11-C22 Aromatic Hydrocarbons 1000 3000 1000 1000 1000 16.9 <10.4 11.3 35.4 18.4 23.3 < 11.1 < 10.6 < 10.7 < 10.8 < 104 < 10.5 20.8MADEP VPH 5/2004 Rev. 1.1 (mg/kg)C5-C8 Aliphatic Hydrocarbons 100 500 100 500 500 < 5.22 < 4.92 < 1.02 < 1.77 3.4 < 0.740 < 0.863 < 0.722 < 0.752 < 0.802 < 0.703 < 1.29 < 0.723C9-C12 Aliphatic Hydrocarbons 1000 3000 1000 3000 5000 1.58 < 0.328 < 0.342 < 0.591 20 < 0.247 < 0.288 < 0.241 < 0.251 < 0.428 < 0.234 < 0.311 < 0.386C9-C10 Aromatic Hydrocarbons 100 500 100 300 300 0.994 < 0.328 < 0.342 < 0.591 19 < 0.543 < 0.288 0.275 < 0.251 < 0.428 < 0.234 < 0.311 < 0.386Total Metals SW846 6010C (mg/kg)Arsenic 20 20 20 20 50 7.44 8.16 8.34 7.2 7.72 10.2 11.8 11.1 12.8 11.8 7.41 10.4 12.8Chromium 100 200 100 200 200 9.89 10.9 13 17.7 12.3 10.7 21.1 16.3 11.7 14.2 12.6 11.5 13.2Copper 1000 10000 NE NE NE 6.09 6.25 7.16 11.9 10.9 9.27 8.52 7.6 8.21 7.3 7.47 8.37 < 13.7Lead 200 600 200 600 600 11.8 6.17 10.8 10.1 10.4 15 7.56 8.85 7.93 7.46 8.73 8.35 8.59Zinc 1000 3000 1000 3000 5000 34.5 19.5 21.9 44.8 25.4 20.4 20.9 17.7 15 19.2 26.1 16.5 22.9Total Cyanide SW9010CCyanide 30 100 30 100 500 < 0.54 < 0.53 <0.54 <0.53 <0.46 <0.55 <0.56 <0.477 <0.412 < 0.369 < 0.437 < 0.281 < 0.281VOC SW846 8260C (µg/kg)1,1,2-Trichlorotrifluoroethane (Freon 113) NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Acetone 6000 50000 6000 6000 6000 < 46.4 < 48.2 < 50.0 < 76.6 < 66.8 < 49.0 < 55.1 < 49.9 < 48.9 < 48.5 < 47.9 < 484 < 46.1Benzene 2000 200000 2000 2000 2000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Bromobenzene 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Bromochloromethane NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Bromodichloromethane 100 100 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Bromoform 100 1000 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Bromomethane 500 500 500 500 500 < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.212-Butanone (MEK) 4000 50000 4000 4000 4000 < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21n-Butylbenzene NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61sec-Butylbenzene NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61tert-Butylbenzene 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Carbon disulfide 100000 1000000 NE NE NE < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21Carbon tetrachloride 5000 5000 10000 10000 10000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Chlorobenzene 1000 3000 1000 1000 1000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Chloroethane 100000 1000000 NE NE NE < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21Chloroform 200 200 400 400 400 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Chloromethane 100000 1000000 NE NE NE < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.212-Chlorotoluene 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.614-Chlorotoluene NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2-Dibromo-3-chloropropane 10000 100000 NE NE NE < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21Dibromochloromethane 5 30 5 5 5 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2-Dibromoethane (EDB) 100 100 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Dibromomethane 500000 5000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2-Dichlorobenzene 9000 100000 9000 9000 9000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,3-Dichlorobenzene 3000 200000 3000 3000 3000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,4-Dichlorobenzene 700 1000 700 700 700 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Dichlorodifluoromethane (Freon12) 1000000 10000000 NE NE NE < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.211,1-Dichloroethane 400 9000 400 400 400 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2-Dichloroethane 100 100 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,1-Dichloroethene 3000 40000 3000 3000 3000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61cis-1,2-Dichloroethene 300 400 300 300 300 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61trans-1,2-Dichloroethene 1000 1000 1000 1000 1000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2-Dichloropropane 100 100 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,3-Dichloropropane 500000 5000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.612,2-Dichloropropane NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,1-Dichloropropene NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61cis-1,3-Dichloropropene 10 100 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61trans-1,3-Dichloropropene 10 100 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Ethylbenzene 40000 1000000 40000 40000 40000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Hexachlorobutadiene 30000 100000 30000 100000 100000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.612-Hexanone (MBK) 100000 1000000 NE NE NE < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21Isopropylbenzene 1000000 10000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.614-Isopropyltoluene 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Methyl tert-butyl ether 100 100000 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.614-Methyl-2-pentanone (MIBK) 400 50000 400 400 400 < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21Methylene chloride 100 4000 100 100 100 < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21Naphthalene 4000 20000 4000 4000 4000 < 4.64 11.9 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61n-Propylbenzene 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Styrene 3000 4000 3000 3000 3000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,1,1,2-Tetrachloroethane 100 100 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,1,2,2-Tetrachloroethane 5 20 5 5 5 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Tetrachloroethene 1000 10000 1000 1000 1000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Toluene 30000 1000000 30000 30000 30000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2,3-Trichlorobenzene NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2,4-Trichlorobenzene 2000 6000 2000 2000 2000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,1,1-Trichloroethane 30000 600000 30000 30000 30000 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,1,2-Trichloroethane 100 2000 100 100 100 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Trichloroethene 300 300 300 300 300 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Trichlorofluoromethane (Freon 11) 1000000 10000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2,3-Trichloropropane 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,2,4-Trimethylbenzene 1000000 10000000 NE NE NE < 4.64 18.6 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,3,5-Trimethylbenzene 10000 100000 NE NE NE < 4.64 5.02 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Vinyl chloride 700 700 900 900 900 < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61m,p-Xylene 300000 300000 < 9.29 11.6 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21o-Xylene 500000 500000 < 4.64 6.32 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Tetrahydrofuran 500000 5000000 NE NE NE < 9.29 < 9.64 < 10.0 < 15.3 < 13.4 < 9.80 < 11.0 < 9.98 < 9.78 < 9.71 < 9.59 < 96.8 < 9.21Ethyl ether 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Tert-amyl methyl ether NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Ethyl tert-butyl ether NE NE NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.61Di-isopropyl ether 100000 1000000 NE NE NE < 4.64 < 4.82 < 5.00 < 7.66 < 6.68 < 4.90 < 5.51 < 4.99 < 4.89 < 4.85 < 4.79 < 48.4 < 4.611,4-Dioxane 200 6000 200 200 200 < 92.9 < 96.4 < 100 < 153 < 134 < 98.0 < 110 < 99.8 < 97.8 < 97.1 < 95.9 < 968 < 92.1Notes:SP: Excavated Soil Stock Pile< - Non-detect at laboratory detection limit (detection limit shown after < J = Estimated Value, J+ = biased high, J- = biased low, R = rejectedSample Type N = normal sample, FD = duplicate samplemg/kg - milligrams per kilograms NE = not establishedDetections are boldedMCP - Massachusetts Contingency Plan Exceedance of Method 1 S1 Standards are yellow highlighted

MA Method 1S-3 Soil &

GW-1

400000 400000 400000

MassDEP RCS-2 Reportable

Concentations

MassDEP RCS-1 Reportable

Concentrations


GW-1


GW-1

1 of 1


APPENDIX A – LABORATORY ANALYTICAL REPORTS

Report Date:

17-Oct-17 17:45

ü Final Report

Revised Report

Laboratory Report

SC40242

AECOM Environment

250 Apollo Drive


Attn: Art Taddeo

Project:

Project #:

LMC-Wilmington- 40 Fordham Rd. - MA

60478638.5.01

I attest that the information contained within the report has been reviewed for accuracy and checked against the quality control

requirements for each method. These results relate only to the sample(s) as received.

All applicable NELAC requirements have been met.

Massachusetts # M-MA138/MA1110

Connecticut # PH-0777

Florida # E87936

Maine # MA138

New Hampshire # 2972/2538

New Jersey # MA011

New York # 11393

Pennsylvania # 68-04426/68-02924

Rhode Island # LAO00348

USDA # P330-15-00375

Vermont # VT-11393

Eurofins Spectrum Analytical holds primary certification in the State of Massachusetts for the analytes as indicated with an X in the

"Cert." column within this report. Please note that the State of Massachusetts does not offer certification for all analytes. Please refer to

our website for specific certification holdings in each state.

Please note that this report contains 30 pages of analytical data plus Chain of Custody document(s). When the Laboratory Report is

indicated as revised, this report supersedes any previously dated reports for the laboratory ID(s) referenced above. Where this report

identifies subcontracted analyses, copies of the subcontractor's test report are available upon request. This report may not be

reproduced, except in full, without written approval from Eurofins Spectrum Analytical, Inc.

Eurofins Spectrum Analytical, Inc. is a NELAC accredited laboratory organization and meets NELAC testing standards. Use of the NELAC logo

however does not insure that Eurofins Spectrum Analytical, Inc. is currently accredited for the specific method or analyte indicated. Please refer to

our "Quality" web page at www.spectrum-analytical.com for a full listing of our current certifications and fields of accreditation. States in which

Eurofins Spectrum Analytical, Inc. holds NELAC certification are New York, New Hampshire, New Jersey, Pennsylvania and Florida. All analytical

work for Volatile Organic and Air analysis are transferred to and conducted at our 830 Silver Street location (PA-68-04426).

Please contact the Laboratory or Technical Director at 800-789-9115 with any questions regarding the data contained in this laboratory report.

Eurofins Spectrum Analytical, Inc. 830 Silver Street T | 413-789-9018

Agawam, MA 01001 F | 413-789-4076

www.EurofinsUS.com/Spectrum Page 1 of 30

Authorized by:

Dawn WojcikLaboratory Director

Sample Summary

Work Order:

Project:

Project Number:

SC40242


60478638.5.01

Laboratory ID Client Sample ID Matrix Date Sampled Date Received

SC40242-01 SP11_101117-1 Soil 11-Oct-17 10:30 11-Oct-17 18:31

SC40242-02 TB_101117-1 Methanol/Deionized Water 11-Oct-17 10:25 11-Oct-17 18:31

This laboratory report is not valid without an authorized signature on the cover page .

Page 2 of 3017-Oct-17 17:45

The following outlines the condition of all VPH samples contained within this report upon laboratory receipt .

Matrices Soil

Containers Satisfactoryü

Sample

Preservative

Aqueous

(acid preserved)

N/A pH<2 pH>2ü

Soil or

Sediment

N/A Samples not received in Methanol

Samples received in Methanol: covering soil/sediment

not covering soil/sediment

ü ü

ml Methanol/g soil

1:1 +/-25%ü

Other

Samples received in air-tight container

Temperature Received on iceü Received at 4 ± 2 ºCü

Were all QA/QC procedures followed as required by the VPH method? Yes

Were any significant modifications made to the VPH method as specified in section 11.3? No

Were all performance/acceptance standards for required QA/QC procedures achieved? Yes

The following outlines the condition of all EPH samples contained within this report upon laboratory receipt.

Matrices Soil

Containers ü Satisfactory

Aqueous Preservative N/A pH<2 pH>2 pH adjusted to <2 in labü

Temperature Received on ice Received at 4 ± 2 ºCü ü

Were all QA/QC procedures followed as required by the EPH method? Yes

Were any significant modifications made to the EPH method as specified in Section 11.3? No


I attest that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained

in this report is, to the best of my knowledge and belief, accurate and complete.

Authorized by:

Dawn E. Wojcik

Laboratory Director


Page 3 of 3017-Oct-17 17:45

MassDEP Analytical Protocol Certification Form

Laboratory Name: Eurofins Spectrum Analytical, Inc. Project #: 60478638.5.01

Project Location: LMC-Wilmington- 40 Fordham Rd. - MA RTN:

This form provides certifications for the following data set: SC40242-01 through SC40242-02

Matrices: Methanol/Deionized Water

Soil

CAM Protocol

8260 VOC

CAM II A

7470/7471 Hg

CAM III B

MassDEP VPH

CAM IV A

8081 Pesticides

CAM V B

7196 Hex Cr

CAM VI B

MassDEP APH

CAM IX A

8270 SVOC

CAM II B

7010 Metals

CAM III C

MassDEP EPH

CAM IV B

8151 Herbicides

CAM V C

8330 Explosives

CAM VIII A

TO-15 VOC

CAM IX B

6010 Metals

CAM III A

6020 Metals

CAM III D

8082 PCB

CAM V A

9014 Total

Cyanide/PAC

CAM VI A

6860 Perchlorate

CAM VIII B

ü

ü

ü

ü

Affirmative responses to questions A through F are required for "Presumptive Certainty" status

Were all samples received in a condition consistent with those described on the Chain of Custody, properly

preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding

times?

Were the analytical method(s) and all associated QC requirements specified in the selected CAM

protocol(s) followed?

Were all required corrective actions and analytical response actions specified in the selected CAM

protocol(s) implemented for all identified performance standard non-conformances?

Does the laboratory report comply with all the reporting requirements specified in CAM VII A, "Quality

Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?

a. VPH, EPH, and APH Methods only: Was each method conducted without significant modification(s)?

b. APH and TO-15 Methods only: Was the complete analyte list reported for each method?

Were all applicable CAM protocol QC and performance standard non-conformances identified and

evaluated in a laboratory narrative (including all "No" responses to questions A through E)?

Responses to questions G, H and I below are required for "Presumptive Certainty" status

Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocol(s)?

Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability and representativeness

requirements described in 310 CMR 40. 1056 (2)(k) and WSC-07-350.

Were all QC performance standards specified in the CAM protocol(s) achieved?

Were results reported for the complete analyte list specified in the selected CAM protocol(s)?

All negative responses are addressed in a case narrative on the cover page of this report.

I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the

information, the material contained in this analytical report is, to the best of my knowledge and belief, accurate and complete.

Dawn E. Wojcik

Laboratory Director

Date: 10/17/2017

A

B

C

D

E

F

G

H

I

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

ü

ü

ü

ü

ü

ü

ü

ü

ü

Yes No

ü

9012 Total

Cyanide/PAC

CAM VI A


Page 4 of 3017-Oct-17 17:45

CASE NARRATIVE:

Data has been reported to the RDL. This report excludes estimated concentrations detected below the RDL and above the MDL

(J-Flag).

All non-detects and all results below the reporting limit are reported as �<� (less than) the reporting limit in this report.

The samples were received 3.7 degrees Celsius, please refer to the Chain of Custody for details specific to temperature upon receipt.

An infrared thermometer with a tolerance of +/- 1.0 degrees Celsius was used immediately upon receipt of the samples.

If a Matrix Spike (MS), Matrix Spike Duplicate (MSD) or Duplicate (DUP) was not requested on the Chain of Custody, method

criteria may have been fulfilled with a source sample not of this Sample Delivery Group. If method or program required

MS/MSD/Dup were not performed, sufficient sample was not provided to the laboratory.

MADEP has published a list of analytical methods (CAM) which provides a series of recommended protocols for the acquisition,

analysis and reporting of analytical data in support of MCP decisions. "Presumptive Certainty" can be established only for those

methods published by the MADEP in the MCP CAM. The compounds and/or elements reported were specifically requested by the

client on the Chain of Custody and in some cases may not include the full analyte list as defined in the method. Regulatory limits may

not be achieved if specific method and/or technique was not requested on the Chain of Custody.

According to WSC-CAM 5/2009 Rev.1, Table 11 A-1, recovery for some VOC analytes have been deemed potentially difficult.

Although they may still be within the recommended recovery range, a range has been set based on historical control limits.

Some target analytes which are not listed as exceptions in the Summary of CAM Reporting Limits may exceed the recommended RL

based on sample initial volume or weight provided, % moisture content, or responsiveness of a particular analyte to purge and trap

instrumentation.

All VOC soils samples submitted and analyzed in methanol will have a minimum dilution factor of 50. This is the minimum amount of

solvent allowed on the instrumentation without causing interference. Soils are run on a manual load instrument. 100ug of sample

(MEOH) is spiked into 5ml DI water along with the surrogate and added directly onto the instrument. Additional dilution factors may

be required to keep analyte concentration within instrument calibration range.

Method SW846 5035A is designed to use on samples containing low levels of VOCs, ranging from 0.5 to 200 ug/Kg. Target analytes

that are less responsive to purge and trap may be present at concentrations over 200ug/Kg but may not be reportable in the methanol

preserved vial (SW846 5030). This is the result of the inherent dilution factor required for the methanol preservation.

See below for any non-conformances and issues relating to quality control samples and/or sample analysis/matrix.

MADEP EPH 5/2004 R

Calibration:

S707773-ICV1

Analyte percent recovery is outside individual acceptance criteria.

2-Methylnaphthalene (aliphatic fraction) (0%)

Naphthalene (aliphatic fraction) (0%)

This affected the following samples:

1717419-BLK1

1717419-BS1

1717419-BS2

1717419-BSD1

S709112-CCV1

S709112-CCV2

S709112-CCV3

SW846 8260C

Calibration:


Page 5 of 3017-Oct-17 17:45

SW846 8260C

Calibration:

1710009

Analyte quantified by quadratic equation type calibration.

1,1,1,2-Tetrachloroethane

1,1,2,2-Tetrachloroethane

1,2,3-Trichlorobenzene

1,2,4-Trichlorobenzene

1,2-Dibromo-3-chloropropane

1,2-Dibromoethane (EDB)

2-Hexanone (MBK)

4-Methyl-2-pentanone (MIBK)

Bromochloromethane

Bromodichloromethane

Bromoform

Carbon disulfide

Carbon tetrachloride

cis-1,3-Dichloropropene

Dibromochloromethane

Naphthalene

Styrene

trans-1,3-Dichloropropene

Vinyl chloride


S708827-ICV1

Laboratory Control Samples:

1717436 BS/BSD

1,1,2-Trichlorotrifluoroethane (Freon 113) percent recoveries (67/61) are outside individual acceptance criteria, but within overall

method allowances. All reported results of the following samples are considered to have a potentially low bias:

TB_101117-1

Bromomethane percent recoveries (158/158) are outside individual acceptance criteria, but within overall method allowances. All

reported results of the following samples are considered to have a potentially high bias:

TB_101117-1

1717540 BS/BSD

2,2-Dichloropropane percent recoveries (149/140) are outside individual acceptance criteria, but within overall method

allowances. All reported results of the following samples are considered to have a potentially high bias:

SP11_101117-1

Bromomethane percent recoveries (174/164) are outside individual acceptance criteria, but within overall method allowances. All


SP11_101117-1

Samples:

S709049-CCV1

Analyte percent difference is outside individual acceptance criteria (20), but within overall method allowances.

1,1,2-Trichlorotrifluoroethane (Freon 113) (-38.9%)

Dichlorodifluoromethane (Freon12) (-29.9%)

Hexachlorobutadiene (-22.4%)

Tetrachloroethene (-23.8%)


Page 6 of 3017-Oct-17 17:45

SW846 8260C

Samples:

S709049-CCV1

Analyte percent drift is outside individual acceptance criteria (20), but within overall method allowances.

Bromomethane (58.0%)

Carbon tetrachloride (-24.9%)


1717436-BLK1

1717436-BS1

1717436-BSD1

TB_101117-1

S709100-CCV1


2,2-Dichloropropane (40.6%)




1717540-BLK1

1717540-BS1

1717540-BSD1

SP11_101117-1

SC40242-01 SP11_101117-1

Reporting limits reflect SW846 5035A High Level extraction technique due to interference and/or QC issues using SW846 5035A

Low Level extraction technique.


Page 7 of 3017-Oct-17 17:45

Sample Acceptance Check Form

Client:

Work Order:

Project:

Sample(s) received on:

AECOM Environment - Chelmsford, MA

LMC-Wilmington- 40 Fordham Rd. - MA / 60478638.5.01

SC40242

10/11/2017

Yes No N/A

Were samples received at a temperature of 6°C?

Were custody seals present?

Were custody seals intact?

ü

ü

ü

The following outlines the condition of samples for the attached Chain of Custody upon receipt.

Were samples cooled on ice upon transfer to laboratory representative? ü

Were samples properly labeled (labels affixed to sample containers and include sample ID, site

location, and/or project number and the collection date)?

ü

Were sample containers received intact?

Were samples accompanied by a Chain of Custody document?

Did sample container labels agree with Chain of Custody document?

Were samples received within method-specific holding times?

ü

ü

ü

ü

Does Chain of Custody document include proper, full, and complete documentation, which shall

include sample ID, site location, and/or project number, date and time of collection, collector's name,

preservation type, sample matrix and any special remarks concerning the sample?

ü


Page 8 of 3017-Oct-17 17:45

Summary of Hits

Client ID: SP11_101117-1Lab ID: SC40242-01

ResultParameter Units Analytical MethodReporting LimitFlag

Arsenic SW846 6010C1.5910.4 mg/kg

Chromium SW846 6010C1.0611.5 mg/kg

Copper SW846 6010C1.068.37 mg/kg

Lead SW846 6010C1.598.35 mg/kg

Zinc SW846 6010C1.0616.5 mg/kg

Please note that because there are no reporting limits associated with hazardous waste characterizations or micro analyses , this

summary does not include hits from these analyses if included in this work order.


Page 9 of 3017-Oct-17 17:45

SP11_101117-1

Sample IdentificationMatrix

11-Oct-17 10:30

Collection Date/Time Received

11-Oct-17

Client Project #

60478638.5.01 SoilSC40242-01

Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL

Volatile Organic Compounds

Prepared by method Volatiles

VOC Soil

Extraction

N/AField

extracted

VOC Extraction 1 1717410MBR

Volatile Organic Compounds by SW846 8260 VOC8

Initial weight: 18.22 gPrepared by method SW846 5035A Soil (high level)

SW846 8260C 16-Oct-1716-Oct-17µg/kg dry 48.4< 48.476-13-1 1,1,2-Trichlorotrifluoroetha

ne (Freon 113)

50 1717540MP24.5D

" ""µg/kg dry 484< 48467-64-1 Acetone 50 ""194D

" ""µg/kg dry 48.4< 48.471-43-2 Benzene 50 ""12.8D

" ""µg/kg dry 48.4< 48.4108-86-1 Bromobenzene 50 ""12.9D

" ""µg/kg dry 48.4< 48.474-97-5 Bromochloromethane 50 ""24.4D

" ""µg/kg dry 48.4< 48.475-27-4 Bromodichloromethane 50 ""32.3D

" ""µg/kg dry 48.4< 48.475-25-2 Bromoform 50 ""46.2D

" ""µg/kg dry 96.8< 96.874-83-9 Bromomethane 50 ""43.7D

" ""µg/kg dry 96.8< 96.878-93-3 2-Butanone (MEK) 50 ""86.6D

" ""µg/kg dry 48.4< 48.4104-51-8 n-Butylbenzene 50 ""13.8D

" ""µg/kg dry 48.4< 48.4135-98-8 sec-Butylbenzene 50 ""8.81D

" ""µg/kg dry 48.4< 48.498-06-6 tert-Butylbenzene 50 ""10.8D

" ""µg/kg dry 96.8< 96.875-15-0 Carbon disulfide 50 ""31.0D

" ""µg/kg dry 48.4< 48.456-23-5 Carbon tetrachloride 50 ""39.6D

" ""µg/kg dry 48.4< 48.4108-90-7 Chlorobenzene 50 ""15.2D

" ""µg/kg dry 96.8< 96.875-00-3 Chloroethane 50 ""26.9D

" ""µg/kg dry 48.4< 48.467-66-3 Chloroform 50 ""26.0D

" ""µg/kg dry 96.8< 96.874-87-3 Chloromethane 50 ""20.0D

" ""µg/kg dry 48.4< 48.495-49-8 2-Chlorotoluene 50 ""12.1D

" ""µg/kg dry 48.4< 48.4106-43-4 4-Chlorotoluene 50 ""11.4D

" ""µg/kg dry 96.8< 96.896-12-8 1,2-Dibromo-3-chloroprop

ane

50 ""70.0D

" ""µg/kg dry 48.4< 48.4124-48-1 Dibromochloromethane 50 ""32.8D

" ""µg/kg dry 48.4< 48.4106-93-4 1,2-Dibromoethane (EDB) 50 ""32.5D

" ""µg/kg dry 48.4< 48.474-95-3 Dibromomethane 50 ""25.2D

" ""µg/kg dry 48.4< 48.495-50-1 1,2-Dichlorobenzene 50 ""12.6D



" ""µg/kg dry 96.8< 96.875-71-8 Dichlorodifluoromethane

(Freon12)

50 ""18.3D

" ""µg/kg dry 48.4< 48.475-34-3 1,1-Dichloroethane 50 ""12.7D

" ""µg/kg dry 48.4< 48.4107-06-2 1,2-Dichloroethane 50 ""17.3D

" ""µg/kg dry 48.4< 48.475-35-4 1,1-Dichloroethene 50 ""25.3D

" ""µg/kg dry 48.4< 48.4156-59-2 cis-1,2-Dichloroethene 50 ""18.0D

" ""µg/kg dry 48.4< 48.4156-60-5 trans-1,2-Dichloroethene 50 ""25.7D

" ""µg/kg dry 48.4< 48.478-87-5 1,2-Dichloropropane 50 ""25.4D



" ""µg/kg dry 48.4< 48.4563-58-6 1,1-Dichloropropene 50 ""15.6D

" ""µg/kg dry 48.4< 48.410061-01-5 cis-1,3-Dichloropropene 50 ""29.2D

" ""µg/kg dry 48.4< 48.410061-02-6 trans-1,3-Dichloropropene 50 ""25.4D

" ""µg/kg dry 48.4< 48.4100-41-4 Ethylbenzene 50 ""6.97D


Page 10 of 3017-Oct-17 17:45

SP11_101117-1


11-Oct-17 10:30


11-Oct-17

Client Project #

60478638.5.01 SoilSC40242-01



Volatile Organic Compounds by SW846 8260 VOC8

Initial weight: 18.22 g

SW846 8260C 16-Oct-1716-Oct-17µg/kg dry 48.4< 48.487-68-3 Hexachlorobutadiene 50 1717540MP24.3D

" ""µg/kg dry 96.8< 96.8591-78-6 2-Hexanone (MBK) 50 ""59.4D

" ""µg/kg dry 48.4< 48.498-82-8 Isopropylbenzene 50 ""9.54D

" ""µg/kg dry 48.4< 48.499-87-6 4-Isopropyltoluene 50 ""10.4D

" ""µg/kg dry 48.4< 48.41634-04-4 Methyl tert-butyl ether 50 ""17.8D

" ""µg/kg dry 96.8< 96.8108-10-1 4-Methyl-2-pentanone

(MIBK)

50 ""24.9D

" ""µg/kg dry 96.8< 96.875-09-2 Methylene chloride 50 ""19.2D

" ""µg/kg dry 48.4< 48.491-20-3 Naphthalene 50 ""28.8D

" ""µg/kg dry 48.4< 48.4103-65-1 n-Propylbenzene 50 ""7.84D

" ""µg/kg dry 48.4< 48.4100-42-5 Styrene 50 ""9.73D

" ""µg/kg dry 48.4< 48.4630-20-6 1,1,1,2-Tetrachloroethane 50 ""41.1D

" ""µg/kg dry 48.4< 48.479-34-5 1,1,2,2-Tetrachloroethane 50 ""41.0D

" ""µg/kg dry 48.4< 48.4127-18-4 Tetrachloroethene 50 ""16.6D

" ""µg/kg dry 48.4< 48.4108-88-3 Toluene 50 ""15.7D

" ""µg/kg dry 48.4< 48.487-61-6 1,2,3-Trichlorobenzene 50 ""17.0D

" ""µg/kg dry 48.4< 48.4120-82-1 1,2,4-Trichlorobenzene 50 ""35.7D

" ""µg/kg dry 48.4< 48.471-55-6 1,1,1-Trichloroethane 50 ""16.1D

" ""µg/kg dry 48.4< 48.479-00-5 1,1,2-Trichloroethane 50 ""35.1D

" ""µg/kg dry 48.4< 48.479-01-6 Trichloroethene 50 ""13.2D

" ""µg/kg dry 48.4< 48.475-69-4 Trichlorofluoromethane

(Freon 11)

50 ""26.1D

" ""µg/kg dry 48.4< 48.496-18-4 1,2,3-Trichloropropane 50 ""36.3D

" ""µg/kg dry 48.4< 48.495-63-6 1,2,4-Trimethylbenzene 50 ""11.8D

" ""µg/kg dry 48.4< 48.4108-67-8 1,3,5-Trimethylbenzene 50 ""8.33D

" ""µg/kg dry 48.4< 48.475-01-4 Vinyl chloride 50 ""16.4D

" ""µg/kg dry 96.8< 96.8179601-23-1 m,p-Xylene 50 ""8.71D

" ""µg/kg dry 48.4< 48.495-47-6 o-Xylene 50 ""13.6D

" ""µg/kg dry 96.8< 96.8109-99-9 Tetrahydrofuran 50 ""76.3D

" ""µg/kg dry 48.4< 48.460-29-7 Ethyl ether 50 ""43.9D

" ""µg/kg dry 48.4< 48.4994-05-8 Tert-amyl methyl ether 50 ""16.2D

" ""µg/kg dry 48.4< 48.4637-92-3 Ethyl tert-butyl ether 50 ""26.1D

" ""µg/kg dry 48.4< 48.4108-20-3 Di-isopropyl ether 50 ""9.00D

" ""µg/kg dry 968< 968123-91-1 1,4-Dioxane 50 ""841D

Surrogate recoveries:

70-130 % " " ""4-Bromofluorobenzene 98 "460-00-4

70-130 % " " ""Toluene-d8 102 "2037-26-5

70-130 % " " ""1,2-Dichloroethane-d4 105 "17060-07-0

70-130 % " " ""Dibromofluoromethane 97 "1868-53-7

MADEP VPH Carbon Ranges

Initial weight: 16.93 gPrepared by method VPH - EPA 5035A Soil

MADEP VPH

5/2004 Rev. 1.1

12-Oct-1712-Oct-17mg/kg dry 1.29< 1.29C5-C8 Aliphatic

Hydrocarbons

50 1717194SD0.150D

" ""mg/kg dry 0.311< 0.311C9-C12 Aliphatic

Hydrocarbons

50 ""0.108D


Page 11 of 3017-Oct-17 17:45

SP11_101117-1


11-Oct-17 10:30


11-Oct-17

Client Project #

60478638.5.01 SoilSC40242-01





MADEP VPH

5/2004 Rev. 1.1

12-Oct-1712-Oct-17mg/kg dry 0.311< 0.311C9-C10 Aromatic

Hydrocarbons

50 1717194SD0.0314D

" ""mg/kg dry 1.29< 1.29Unadjusted C5-C8

Aliphatic Hydrocarbons

50 ""0.121D



50 ""0.137D


70-130 % " " ""2,5-Dibromotoluene (FID) 117 "615-59-8

70-130 % " " ""2,5-Dibromotoluene (PID) 125 "615-59-8

Extractable Petroleum Hydrocarbons

MADEP EPH Carbon Ranges

Prepared by method SW846 3546

MADEP EPH

5/2004 R

14-Oct-1713-Oct-17mg/kg dry 10.5< 10.5C9-C18 Aliphatic

Hydrocarbons

1 1717419EDT2.14


Hydrocarbons

1 ""2.83

" ""mg/kg dry 10.5< 10.5C11-C22 Aromatic

Hydrocarbons

1 ""4.41


Aromatic Hydrocarbons

1 ""4.41


40-140 % " " ""1-Chlorooctadecane 58 "3386-33-2

40-140 % " " ""Ortho-Terphenyl 97 "84-15-1

40-140 % " " ""2-Fluorobiphenyl 72 "321-60-8

Total Metals by EPA 6000/7000 Series Methods

Prepared by method SW846 3051A

SW846 6010C 13-Oct-1713-Oct-17mg/kg dry 1.5910.47440-38-2 Arsenic 1 1717347CAW0.202

" 16-Oct-17"mg/kg dry 1.0611.57440-47-3 Chromium 1 ""0.141

" 13-Oct-17"mg/kg dry 1.068.377440-50-8 Copper 1 ""0.255

" ""mg/kg dry 1.598.357439-92-1 Lead 1 ""0.225

" ""mg/kg dry 1.0616.57440-66-6 Zinc 1 ""0.822

General Chemistry Parameters

SM2540 G (11)

Mod.

12-Oct-1712-Oct-17%92.6% Solids 1 1717352MBR

Prepared by method SW846 9010B

SW846 9012B 14-Oct-1713-Oct-17mg/kg dry 0.281< 0.28157-12-5 Cyanide (total) 1 1717429RLT0.237


Page 12 of 3017-Oct-17 17:45

TB_101117-1


11-Oct-17 10:25


11-Oct-17

Client Project #

60478638.5.01 Methanol/Deionized

WaterSC40242-02



Volatile Organic Compounds by SW846 8260

Prepared by method SW846 5035A Soil (high level)

SW846 8260C 14-Oct-1713-Oct-17µg/kg wet 50.0< 50.076-13-1 1,1,2-Trichlorotrifluoroetha

ne (Freon 113)

50 1717436MP25.4D

" ""µg/kg wet 500< 50067-64-1 Acetone 50 ""200D

" ""µg/kg wet 50.0< 50.071-43-2 Benzene 50 ""13.2D

" ""µg/kg wet 50.0< 50.0108-86-1 Bromobenzene 50 ""13.4D

" ""µg/kg wet 50.0< 50.074-97-5 Bromochloromethane 50 ""25.2D

" ""µg/kg wet 50.0< 50.075-27-4 Bromodichloromethane 50 ""33.4D

" ""µg/kg wet 50.0< 50.075-25-2 Bromoform 50 ""47.7D

" ""µg/kg wet 100< 10074-83-9 Bromomethane 50 ""45.2D

" ""µg/kg wet 100< 10078-93-3 2-Butanone (MEK) 50 ""89.4D

" ""µg/kg wet 50.0< 50.0104-51-8 n-Butylbenzene 50 ""14.3D

" ""µg/kg wet 50.0< 50.0135-98-8 sec-Butylbenzene 50 ""9.10D

" ""µg/kg wet 50.0< 50.098-06-6 tert-Butylbenzene 50 ""11.2D

" ""µg/kg wet 100< 10075-15-0 Carbon disulfide 50 ""32.0D

" ""µg/kg wet 50.0< 50.056-23-5 Carbon tetrachloride 50 ""40.9D

" ""µg/kg wet 50.0< 50.0108-90-7 Chlorobenzene 50 ""15.6D

" ""µg/kg wet 100< 10075-00-3 Chloroethane 50 ""27.8D

" ""µg/kg wet 50.0< 50.067-66-3 Chloroform 50 ""26.8D

" ""µg/kg wet 100< 10074-87-3 Chloromethane 50 ""20.6D

" ""µg/kg wet 50.0< 50.095-49-8 2-Chlorotoluene 50 ""12.4D

" ""µg/kg wet 50.0< 50.0106-43-4 4-Chlorotoluene 50 ""11.8D

" ""µg/kg wet 100< 10096-12-8 1,2-Dibromo-3-chloroprop

ane

50 ""72.2D

" ""µg/kg wet 50.0< 50.0124-48-1 Dibromochloromethane 50 ""33.9D

" ""µg/kg wet 50.0< 50.0106-93-4 1,2-Dibromoethane (EDB) 50 ""33.6D

" ""µg/kg wet 50.0< 50.074-95-3 Dibromomethane 50 ""26.0D

" ""µg/kg wet 50.0< 50.095-50-1 1,2-Dichlorobenzene 50 ""13.0D



" ""µg/kg wet 100< 10075-71-8 Dichlorodifluoromethane

(Freon12)

50 ""19.0D

" ""µg/kg wet 50.0< 50.075-34-3 1,1-Dichloroethane 50 ""13.1D

" ""µg/kg wet 50.0< 50.0107-06-2 1,2-Dichloroethane 50 ""17.9D

" ""µg/kg wet 50.0< 50.075-35-4 1,1-Dichloroethene 50 ""26.2D

" ""µg/kg wet 50.0< 50.0156-59-2 cis-1,2-Dichloroethene 50 ""18.6D

" ""µg/kg wet 50.0< 50.0156-60-5 trans-1,2-Dichloroethene 50 ""26.5D

" ""µg/kg wet 50.0< 50.078-87-5 1,2-Dichloropropane 50 ""26.2D



" ""µg/kg wet 50.0< 50.0563-58-6 1,1-Dichloropropene 50 ""16.1D

" ""µg/kg wet 50.0< 50.010061-01-5 cis-1,3-Dichloropropene 50 ""30.2D

" ""µg/kg wet 50.0< 50.010061-02-6 trans-1,3-Dichloropropene 50 ""26.2D

" ""µg/kg wet 50.0< 50.0100-41-4 Ethylbenzene 50 ""7.20D

" ""µg/kg wet 50.0< 50.087-68-3 Hexachlorobutadiene 50 ""25.1D

" ""µg/kg wet 100< 100591-78-6 2-Hexanone (MBK) 50 ""61.4D

" ""µg/kg wet 50.0< 50.098-82-8 Isopropylbenzene 50 ""9.85D


Page 13 of 3017-Oct-17 17:45

TB_101117-1


11-Oct-17 10:25


11-Oct-17

Client Project #


WaterSC40242-02




SW846 8260C 14-Oct-1713-Oct-17µg/kg wet 50.0< 50.099-87-6 4-Isopropyltoluene 50 1717436MP10.8D

" ""µg/kg wet 50.0< 50.01634-04-4 Methyl tert-butyl ether 50 ""18.4D

" ""µg/kg wet 100< 100108-10-1 4-Methyl-2-pentanone

(MIBK)

50 ""25.7D

" ""µg/kg wet 100< 10075-09-2 Methylene chloride 50 ""19.8D

" ""µg/kg wet 50.0< 50.091-20-3 Naphthalene 50 ""29.8D

" ""µg/kg wet 50.0< 50.0103-65-1 n-Propylbenzene 50 ""8.10D

" ""µg/kg wet 50.0< 50.0100-42-5 Styrene 50 ""10.0D

" ""µg/kg wet 50.0< 50.0630-20-6 1,1,1,2-Tetrachloroethane 50 ""42.5D

" ""µg/kg wet 50.0< 50.079-34-5 1,1,2,2-Tetrachloroethane 50 ""42.3D

" ""µg/kg wet 50.0< 50.0127-18-4 Tetrachloroethene 50 ""17.1D

" ""µg/kg wet 50.0< 50.0108-88-3 Toluene 50 ""16.2D

" ""µg/kg wet 50.0< 50.087-61-6 1,2,3-Trichlorobenzene 50 ""17.6D

" ""µg/kg wet 50.0< 50.0120-82-1 1,2,4-Trichlorobenzene 50 ""36.8D

" ""µg/kg wet 50.0< 50.071-55-6 1,1,1-Trichloroethane 50 ""16.6D

" ""µg/kg wet 50.0< 50.079-00-5 1,1,2-Trichloroethane 50 ""36.2D

" ""µg/kg wet 50.0< 50.079-01-6 Trichloroethene 50 ""13.6D

" ""µg/kg wet 50.0< 50.075-69-4 Trichlorofluoromethane

(Freon 11)

50 ""27.0D

" ""µg/kg wet 50.0< 50.096-18-4 1,2,3-Trichloropropane 50 ""37.5D

" ""µg/kg wet 50.0< 50.095-63-6 1,2,4-Trimethylbenzene 50 ""12.2D

" ""µg/kg wet 50.0< 50.0108-67-8 1,3,5-Trimethylbenzene 50 ""8.60D

" ""µg/kg wet 50.0< 50.075-01-4 Vinyl chloride 50 ""16.9D

" ""µg/kg wet 100< 100179601-23-1 m,p-Xylene 50 ""9.00D

" ""µg/kg wet 50.0< 50.095-47-6 o-Xylene 50 ""14.0D

" ""µg/kg wet 100< 100109-99-9 Tetrahydrofuran 50 ""78.8D

" ""µg/kg wet 50.0< 50.060-29-7 Ethyl ether 50 ""45.3D

" ""µg/kg wet 50.0< 50.0994-05-8 Tert-amyl methyl ether 50 ""16.7D

" ""µg/kg wet 50.0< 50.0637-92-3 Ethyl tert-butyl ether 50 ""27.0D

" ""µg/kg wet 50.0< 50.0108-20-3 Di-isopropyl ether 50 ""9.30D

" ""µg/kg wet 1000< 1000123-91-1 1,4-Dioxane 50 ""868D



70-130 % " " ""Toluene-d8 100 "2037-26-5




Page 14 of 3017-Oct-17 17:45

Volatile Organic Compounds - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitFlagAnalyte(s) *RDL

MADEP VPH 5/2004 Rev. 1.1

Batch 1717194 - VPH - EPA 5035A Soil

Blank (1717194-BLK1) Prepared: 11-Oct-17 Analyzed: 12-Oct-17

mg/kg wetD< 1.25C5-C8 Aliphatic Hydrocarbons 1.25


mg/kg wetD< 0.300C9-C10 Aromatic Hydrocarbons 0.300

mg/kg wetD< 1.25Unadjusted C5-C8 Aliphatic Hydrocarbons 1.25

mg/kg wetD< 0.300Unadjusted C9-C12 Aliphatic

Hydrocarbons

0.300

50.0 70-130Surrogate: 2,5-Dibromotoluene (FID) 56.5 µg/kg 113

50.0 70-130Surrogate: 2,5-Dibromotoluene (PID) 60.2 µg/kg 120

LCS (1717194-BS1) Prepared: 11-Oct-17 Analyzed: 12-Oct-17

60.0 70-130µg/kgD41.7 70C5-C8 Aliphatic Hydrocarbons


20.0 70-130µg/kgD21.7 108C9-C10 Aromatic Hydrocarbons

200 70-130µg/kgD187 94Unadjusted C5-C8 Aliphatic Hydrocarbons

80.0 70-130µg/kgD70.2 88Unadjusted C9-C12 Aliphatic

Hydrocarbons



LCS Dup (1717194-BSD1) Prepared: 11-Oct-17 Analyzed: 12-Oct-17

60.0 2570-130 2µg/kgD42.7 71C5-C8 Aliphatic Hydrocarbons

60.0 2570-130 6µg/kgD51.5 86C9-C12 Aliphatic Hydrocarbons

20.0 2570-130 2µg/kgD22.0 110C9-C10 Aromatic Hydrocarbons

200 2570-130 4µg/kgD181 90Unadjusted C5-C8 Aliphatic Hydrocarbons

80.0 2570-130 5µg/kgD73.6 92Unadjusted C9-C12 Aliphatic

Hydrocarbons



SW846 8260C

Batch 1717436 - SW846 5035A Soil (high level)

Blank (1717436-BLK1) Prepared & Analyzed: 13-Oct-17

µg/kg wetD< 50.01,1,2-Trichlorotrifluoroethane (Freon 113) 50.0

µg/kg wetD< 500Acetone 500

µg/kg wetD< 50.0Benzene 50.0

µg/kg wetD< 50.0Bromobenzene 50.0

µg/kg wetD< 50.0Bromochloromethane 50.0

µg/kg wetD< 50.0Bromodichloromethane 50.0

µg/kg wetD< 50.0Bromoform 50.0

µg/kg wetD< 100Bromomethane 100

µg/kg wetD< 1002-Butanone (MEK) 100

µg/kg wetD< 50.0n-Butylbenzene 50.0

µg/kg wetD< 50.0sec-Butylbenzene 50.0

µg/kg wetD< 50.0tert-Butylbenzene 50.0

µg/kg wetD< 100Carbon disulfide 100

µg/kg wetD< 50.0Carbon tetrachloride 50.0

µg/kg wetD< 50.0Chlorobenzene 50.0

µg/kg wetD< 100Chloroethane 100

µg/kg wetD< 50.0Chloroform 50.0

µg/kg wetD< 100Chloromethane 100

µg/kg wetD< 50.02-Chlorotoluene 50.0


µg/kg wetD< 1001,2-Dibromo-3-chloropropane 100


Page 15 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



µg/kg wetD< 50.0Dibromochloromethane 50.0

µg/kg wetD< 50.01,2-Dibromoethane (EDB) 50.0

µg/kg wetD< 50.0Dibromomethane 50.0

µg/kg wetD< 50.01,2-Dichlorobenzene 50.0



µg/kg wetD< 100Dichlorodifluoromethane (Freon12) 100

µg/kg wetD< 50.01,1-Dichloroethane 50.0


µg/kg wetD< 50.01,1-Dichloroethene 50.0

µg/kg wetD< 50.0cis-1,2-Dichloroethene 50.0

µg/kg wetD< 50.0trans-1,2-Dichloroethene 50.0

µg/kg wetD< 50.01,2-Dichloropropane 50.0



µg/kg wetD< 50.01,1-Dichloropropene 50.0

µg/kg wetD< 50.0cis-1,3-Dichloropropene 50.0

µg/kg wetD< 50.0trans-1,3-Dichloropropene 50.0

µg/kg wetD< 50.0Ethylbenzene 50.0

µg/kg wetD< 50.0Hexachlorobutadiene 50.0

µg/kg wetD< 1002-Hexanone (MBK) 100

µg/kg wetD< 50.0Isopropylbenzene 50.0

µg/kg wetD< 50.04-Isopropyltoluene 50.0

µg/kg wetD< 50.0Methyl tert-butyl ether 50.0

µg/kg wetD< 1004-Methyl-2-pentanone (MIBK) 100

µg/kg wetD< 100Methylene chloride 100

µg/kg wetD< 50.0Naphthalene 50.0

µg/kg wetD< 50.0n-Propylbenzene 50.0

µg/kg wetD< 50.0Styrene 50.0

µg/kg wetD< 50.01,1,1,2-Tetrachloroethane 50.0


µg/kg wetD< 50.0Tetrachloroethene 50.0

µg/kg wetD< 50.0Toluene 50.0

µg/kg wetD< 50.01,2,3-Trichlorobenzene 50.0


µg/kg wetD< 50.01,1,1-Trichloroethane 50.0


µg/kg wetD< 50.0Trichloroethene 50.0

µg/kg wetD< 50.0Trichlorofluoromethane (Freon 11) 50.0

µg/kg wetD< 50.01,2,3-Trichloropropane 50.0

µg/kg wetD< 50.01,2,4-Trimethylbenzene 50.0


µg/kg wetD< 50.0Vinyl chloride 50.0

µg/kg wetD< 100m,p-Xylene 100

µg/kg wetD< 50.0o-Xylene 50.0

µg/kg wetD< 100Tetrahydrofuran 100

µg/kg wetD< 50.0Ethyl ether 50.0

µg/kg wetD< 50.0Tert-amyl methyl ether 50.0

µg/kg wetD< 50.0Ethyl tert-butyl ether 50.0

µg/kg wetD< 50.0Di-isopropyl ether 50.0


Page 16 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



µg/kg wetD< 10001,4-Dioxane 1000

50.0 70-130Surrogate: 4-Bromofluorobenzene 47.7 µg/kg 95

50.0 70-130Surrogate: Toluene-d8 50.5 µg/kg 101

50.0 70-130Surrogate: 1,2-Dichloroethane-d4 53.8 µg/kg 108

50.0 70-130Surrogate: Dibromofluoromethane 52.1 µg/kg 104

LCS (1717436-BS1) Prepared & Analyzed: 13-Oct-17

20.0 70-130µg/kgQC2, D13.3 671,1,2-Trichlorotrifluoroethane (Freon 113)

20.0 70-130µg/kgD25.6 128Acetone

20.0 70-130µg/kgD21.4 107Benzene

20.0 70-130µg/kgD21.8 109Bromobenzene

20.0 70-130µg/kgD21.6 108Bromochloromethane

20.0 70-130µg/kgD21.6 108Bromodichloromethane

20.0 70-130µg/kgD21.9 110Bromoform

20.0 70-130µg/kgD31.5 158Bromomethane

20.0 70-130µg/kgD19.5 982-Butanone (MEK)

20.0 70-130µg/kgD17.1 86n-Butylbenzene

20.0 70-130µg/kgD18.0 90sec-Butylbenzene

20.0 70-130µg/kgD18.6 93tert-Butylbenzene

20.0 70-130µg/kgD17.8 89Carbon disulfide

20.0 70-130µg/kgD15.9 79Carbon tetrachloride

20.0 70-130µg/kgD21.5 107Chlorobenzene

20.0 70-130µg/kgD23.5 118Chloroethane

20.0 70-130µg/kgD22.2 111Chloroform

20.0 70-130µg/kgD18.3 92Chloromethane

20.0 70-130µg/kgD21.6 1082-Chlorotoluene


20.0 70-130µg/kgD20.8 1041,2-Dibromo-3-chloropropane

20.0 70-130µg/kgD21.6 108Dibromochloromethane

20.0 70-130µg/kgD21.2 1061,2-Dibromoethane (EDB)

20.0 70-130µg/kgD23.1 115Dibromomethane

20.0 70-130µg/kgD21.6 1081,2-Dichlorobenzene



20.0 70-130µg/kgD14.7 73Dichlorodifluoromethane (Freon12)

20.0 70-130µg/kgD21.8 1091,1-Dichloroethane


20.0 70-130µg/kgD17.7 891,1-Dichloroethene

20.0 70-130µg/kgD22.2 111cis-1,2-Dichloroethene

20.0 70-130µg/kgD19.3 97trans-1,2-Dichloroethene

20.0 70-130µg/kgD22.3 1121,2-Dichloropropane



20.0 70-130µg/kgD16.5 821,1-Dichloropropene

20.0 70-130µg/kgD19.7 98cis-1,3-Dichloropropene

20.0 70-130µg/kgD20.0 100trans-1,3-Dichloropropene

20.0 70-130µg/kgD20.4 102Ethylbenzene

20.0 70-130µg/kgD16.6 83Hexachlorobutadiene

20.0 70-130µg/kgD19.7 982-Hexanone (MBK)

20.0 70-130µg/kgD19.2 96Isopropylbenzene

20.0 70-130µg/kgD18.4 924-Isopropyltoluene


Page 17 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 70-130µg/kgD21.6 108Methyl tert-butyl ether

20.0 70-130µg/kgD20.5 1034-Methyl-2-pentanone (MIBK)

20.0 70-130µg/kgD21.5 108Methylene chloride

20.0 70-130µg/kgD19.7 98Naphthalene

20.0 70-130µg/kgD18.9 95n-Propylbenzene

20.0 70-130µg/kgD20.2 101Styrene

20.0 70-130µg/kgD21.4 1071,1,1,2-Tetrachloroethane


20.0 70-130µg/kgD16.5 83Tetrachloroethene

20.0 70-130µg/kgD20.5 103Toluene

20.0 70-130µg/kgD20.3 1011,2,3-Trichlorobenzene


20.0 70-130µg/kgD18.3 921,1,1-Trichloroethane


20.0 70-130µg/kgD19.6 98Trichloroethene

20.0 70-130µg/kgD17.0 85Trichlorofluoromethane (Freon 11)

20.0 70-130µg/kgD23.6 1181,2,3-Trichloropropane

20.0 70-130µg/kgD21.1 1051,2,4-Trimethylbenzene


20.0 70-130µg/kgD22.1 111Vinyl chloride

20.0 70-130µg/kgD20.8 104m,p-Xylene

20.0 70-130µg/kgD22.4 112o-Xylene

20.0 70-130µg/kgD21.2 106Tetrahydrofuran

20.0 70-130µg/kgD25.5 128Ethyl ether

20.0 70-130µg/kgD24.3 121Tert-amyl methyl ether

20.0 70-130µg/kgD22.1 111Ethyl tert-butyl ether

20.0 70-130µg/kgD21.7 109Di-isopropyl ether

200 70-130µg/kgD179 891,4-Dioxane





LCS Dup (1717436-BSD1) Prepared & Analyzed: 13-Oct-17

20.0 3070-130 9µg/kgQC2, D12.2 611,1,2-Trichlorotrifluoroethane (Freon 113)

20.0 3070-130 11µg/kgD22.9 115Acetone

20.0 3070-130 4µg/kgD20.5 102Benzene

20.0 3070-130 6µg/kgD20.6 103Bromobenzene

20.0 3070-130 3µg/kgD20.8 104Bromochloromethane

20.0 3070-130 3µg/kgD21.0 105Bromodichloromethane

20.0 3070-130 2µg/kgD21.4 107Bromoform

20.0 3070-130 0.3µg/kgD31.6 158Bromomethane

20.0 3070-130 2µg/kgD20.0 1002-Butanone (MEK)

20.0 3070-130 3µg/kgD16.7 83n-Butylbenzene

20.0 3070-130 7µg/kgD16.8 84sec-Butylbenzene

20.0 3070-130 7µg/kgD17.3 87tert-Butylbenzene

20.0 3070-130 11µg/kgD16.0 80Carbon disulfide

20.0 3070-130 6µg/kgD15.0 75Carbon tetrachloride

20.0 3070-130 5µg/kgD20.4 102Chlorobenzene

20.0 3070-130 7µg/kgD22.0 110Chloroethane

20.0 3070-130 3µg/kgD21.5 108Chloroform


Page 18 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 3070-130 8µg/kgD17.0 85Chloromethane

20.0 3070-130 7µg/kgD20.2 1012-Chlorotoluene


20.0 3070-130 2µg/kgD21.3 1061,2-Dibromo-3-chloropropane

20.0 3070-130 2µg/kgD21.1 105Dibromochloromethane

20.0 3070-130 2µg/kgD20.8 1041,2-Dibromoethane (EDB)

20.0 3070-130 0.04µg/kgD23.1 115Dibromomethane

20.0 3070-130 3µg/kgD21.1 1051,2-Dichlorobenzene



20.0 3070-130 5µg/kgD14.0 70Dichlorodifluoromethane (Freon12)

20.0 3070-130 4µg/kgD20.9 1051,1-Dichloroethane


20.0 3070-130 5µg/kgD16.9 841,1-Dichloroethene

20.0 3070-130 6µg/kgD21.0 105cis-1,2-Dichloroethene

20.0 3070-130 5µg/kgD18.5 92trans-1,2-Dichloroethene

20.0 3070-130 3µg/kgD21.6 1081,2-Dichloropropane



20.0 3070-130 2µg/kgD16.1 811,1-Dichloropropene

20.0 3070-130 1µg/kgD19.4 97cis-1,3-Dichloropropene

20.0 3070-130 0.1µg/kgD20.0 100trans-1,3-Dichloropropene

20.0 3070-130 5µg/kgD19.3 97Ethylbenzene

20.0 3070-130 7µg/kgD15.5 78Hexachlorobutadiene

20.0 3070-130 2µg/kgD20.0 1002-Hexanone (MBK)

20.0 3070-130 7µg/kgD18.0 90Isopropylbenzene

20.0 3070-130 3µg/kgD17.8 894-Isopropyltoluene

20.0 3070-130 0µg/kgD21.6 108Methyl tert-butyl ether

20.0 3070-130 0.2µg/kgD20.6 1034-Methyl-2-pentanone (MIBK)

20.0 3070-130 14µg/kgD18.6 93Methylene chloride

20.0 3070-130 2µg/kgD19.3 96Naphthalene

20.0 3070-130 7µg/kgD17.6 88n-Propylbenzene

20.0 3070-130 5µg/kgD19.1 96Styrene

20.0 3070-130 5µg/kgD20.4 1021,1,1,2-Tetrachloroethane


20.0 3070-130 8µg/kgD15.2 76Tetrachloroethene

20.0 3070-130 6µg/kgD19.3 97Toluene

20.0 3070-130 4µg/kgD19.4 971,2,3-Trichlorobenzene


20.0 3070-130 6µg/kgD17.3 871,1,1-Trichloroethane


20.0 3070-130 5µg/kgD18.6 93Trichloroethene

20.0 3070-130 5µg/kgD16.1 81Trichlorofluoromethane (Freon 11)

20.0 3070-130 2µg/kgD23.0 1151,2,3-Trichloropropane

20.0 3070-130 7µg/kgD19.7 991,2,4-Trimethylbenzene


20.0 3070-130 12µg/kgD19.6 98Vinyl chloride

20.0 3070-130 7µg/kgD19.3 96m,p-Xylene

20.0 3070-130 7µg/kgD21.0 105o-Xylene

20.0 3070-130 0.7µg/kgD21.4 107Tetrahydrofuran


Page 19 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 3070-130 7µg/kgD23.7 118Ethyl ether

20.0 3070-130 3µg/kgD23.5 117Tert-amyl methyl ether

20.0 3070-130 0.2µg/kgD22.1 110Ethyl tert-butyl ether

20.0 3070-130 2µg/kgD21.3 107Di-isopropyl ether

200 3070-130 1µg/kgD177 881,4-Dioxane







µg/kg wetD< 50.01,1,2-Trichlorotrifluoroethane (Freon 113) 50.0

µg/kg wetD< 500Acetone 500

µg/kg wetD< 50.0Benzene 50.0

µg/kg wetD< 50.0Bromobenzene 50.0

µg/kg wetD< 50.0Bromochloromethane 50.0

µg/kg wetD< 50.0Bromodichloromethane 50.0

µg/kg wetD< 50.0Bromoform 50.0

µg/kg wetD< 100Bromomethane 100

µg/kg wetD< 1002-Butanone (MEK) 100

µg/kg wetD< 50.0n-Butylbenzene 50.0

µg/kg wetD< 50.0sec-Butylbenzene 50.0

µg/kg wetD< 50.0tert-Butylbenzene 50.0

µg/kg wetD< 100Carbon disulfide 100

µg/kg wetD< 50.0Carbon tetrachloride 50.0

µg/kg wetD< 50.0Chlorobenzene 50.0

µg/kg wetD< 100Chloroethane 100

µg/kg wetD< 50.0Chloroform 50.0

µg/kg wetD< 100Chloromethane 100



µg/kg wetD< 1001,2-Dibromo-3-chloropropane 100

µg/kg wetD< 50.0Dibromochloromethane 50.0

µg/kg wetD< 50.01,2-Dibromoethane (EDB) 50.0

µg/kg wetD< 50.0Dibromomethane 50.0




µg/kg wetD< 100Dichlorodifluoromethane (Freon12) 100



µg/kg wetD< 50.01,1-Dichloroethene 50.0

µg/kg wetD< 50.0cis-1,2-Dichloroethene 50.0

µg/kg wetD< 50.0trans-1,2-Dichloroethene 50.0




µg/kg wetD< 50.01,1-Dichloropropene 50.0

µg/kg wetD< 50.0cis-1,3-Dichloropropene 50.0

µg/kg wetD< 50.0trans-1,3-Dichloropropene 50.0


Page 20 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



µg/kg wetD< 50.0Ethylbenzene 50.0

µg/kg wetD< 50.0Hexachlorobutadiene 50.0

µg/kg wetD< 1002-Hexanone (MBK) 100

µg/kg wetD< 50.0Isopropylbenzene 50.0

µg/kg wetD< 50.04-Isopropyltoluene 50.0

µg/kg wetD< 50.0Methyl tert-butyl ether 50.0

µg/kg wetD< 1004-Methyl-2-pentanone (MIBK) 100

µg/kg wetD< 100Methylene chloride 100

µg/kg wetD< 50.0Naphthalene 50.0

µg/kg wetD< 50.0n-Propylbenzene 50.0

µg/kg wetD< 50.0Styrene 50.0



µg/kg wetD< 50.0Tetrachloroethene 50.0

µg/kg wetD< 50.0Toluene 50.0





µg/kg wetD< 50.0Trichloroethene 50.0

µg/kg wetD< 50.0Trichlorofluoromethane (Freon 11) 50.0

µg/kg wetD< 50.01,2,3-Trichloropropane 50.0



µg/kg wetD< 50.0Vinyl chloride 50.0

µg/kg wetD< 100m,p-Xylene 100

µg/kg wetD< 50.0o-Xylene 50.0

µg/kg wetD< 100Tetrahydrofuran 100

µg/kg wetD< 50.0Ethyl ether 50.0

µg/kg wetD< 50.0Tert-amyl methyl ether 50.0

µg/kg wetD< 50.0Ethyl tert-butyl ether 50.0

µg/kg wetD< 50.0Di-isopropyl ether 50.0

µg/kg wetD< 10001,4-Dioxane 1000






20.0 70-130µg/kgD22.9 1141,1,2-Trichlorotrifluoroethane (Freon 113)

20.0 70-130µg/kgD21.8 109Acetone

20.0 70-130µg/kgD23.3 117Benzene

20.0 70-130µg/kgD23.1 115Bromobenzene

20.0 70-130µg/kgD22.6 113Bromochloromethane

20.0 70-130µg/kgD22.6 113Bromodichloromethane

20.0 70-130µg/kgD23.3 116Bromoform

20.0 70-130µg/kgQC2, D34.8 174Bromomethane

20.0 70-130µg/kgD21.4 1072-Butanone (MEK)

20.0 70-130µg/kgD23.3 116n-Butylbenzene

20.0 70-130µg/kgD23.5 117sec-Butylbenzene

20.0 70-130µg/kgD23.4 117tert-Butylbenzene


Page 21 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 70-130µg/kgD23.3 116Carbon disulfide

20.0 70-130µg/kgD22.7 113Carbon tetrachloride

20.0 70-130µg/kgD22.9 114Chlorobenzene

20.0 70-130µg/kgD24.5 122Chloroethane

20.0 70-130µg/kgD23.4 117Chloroform

20.0 70-130µg/kgD17.9 89Chloromethane



20.0 70-130µg/kgD22.5 1131,2-Dibromo-3-chloropropane

20.0 70-130µg/kgD22.6 113Dibromochloromethane

20.0 70-130µg/kgD21.9 1101,2-Dibromoethane (EDB)

20.0 70-130µg/kgD23.8 119Dibromomethane




20.0 70-130µg/kgD21.4 107Dichlorodifluoromethane (Freon12)



20.0 70-130µg/kgD22.6 1131,1-Dichloroethene

20.0 70-130µg/kgD23.8 119cis-1,2-Dichloroethene

20.0 70-130µg/kgD23.2 116trans-1,2-Dichloroethene



20.0 70-130µg/kgQC2, D29.8 1492,2-Dichloropropane

20.0 70-130µg/kgD23.6 1181,1-Dichloropropene

20.0 70-130µg/kgD22.3 112cis-1,3-Dichloropropene

20.0 70-130µg/kgD22.5 113trans-1,3-Dichloropropene

20.0 70-130µg/kgD23.7 119Ethylbenzene

20.0 70-130µg/kgD22.8 114Hexachlorobutadiene

20.0 70-130µg/kgD21.0 1052-Hexanone (MBK)

20.0 70-130µg/kgD23.2 116Isopropylbenzene

20.0 70-130µg/kgD24.2 1214-Isopropyltoluene

20.0 70-130µg/kgD23.2 116Methyl tert-butyl ether

20.0 70-130µg/kgD21.3 1064-Methyl-2-pentanone (MIBK)

20.0 70-130µg/kgD21.6 108Methylene chloride

20.0 70-130µg/kgD21.7 108Naphthalene

20.0 70-130µg/kgD23.4 117n-Propylbenzene

20.0 70-130µg/kgD21.8 109Styrene



20.0 70-130µg/kgD22.1 111Tetrachloroethene

20.0 70-130µg/kgD22.8 114Toluene





20.0 70-130µg/kgD23.4 117Trichloroethene

20.0 70-130µg/kgD24.5 122Trichlorofluoromethane (Freon 11)

20.0 70-130µg/kgD23.4 1171,2,3-Trichloropropane



Page 22 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C




20.0 70-130µg/kgD24.7 124Vinyl chloride

20.0 70-130µg/kgD23.8 119m,p-Xylene

20.0 70-130µg/kgD23.9 120o-Xylene

20.0 70-130µg/kgD22.8 114Tetrahydrofuran

20.0 70-130µg/kgD24.3 122Ethyl ether

20.0 70-130µg/kgD22.6 113Tert-amyl methyl ether

20.0 70-130µg/kgD23.8 119Ethyl tert-butyl ether

20.0 70-130µg/kgD22.8 114Di-isopropyl ether

200 70-130µg/kgD179 891,4-Dioxane






20.0 3070-130 15µg/kgD19.6 981,1,2-Trichlorotrifluoroethane (Freon 113)

20.0 3070-130 6µg/kgD20.6 103Acetone

20.0 3070-130 4µg/kgD22.5 112Benzene

20.0 3070-130 7µg/kgD21.6 108Bromobenzene

20.0 3070-130 4µg/kgD21.7 108Bromochloromethane

20.0 3070-130 4µg/kgD21.8 109Bromodichloromethane

20.0 3070-130 2µg/kgD22.9 114Bromoform

20.0 3070-130 5µg/kgQC2, D32.9 164Bromomethane

20.0 3070-130 2µg/kgD20.9 1042-Butanone (MEK)

20.0 3070-130 5µg/kgD22.2 111n-Butylbenzene

20.0 3070-130 7µg/kgD22.0 110sec-Butylbenzene

20.0 3070-130 6µg/kgD22.1 111tert-Butylbenzene

20.0 3070-130 25µg/kgD18.1 91Carbon disulfide

20.0 3070-130 5µg/kgD21.5 107Carbon tetrachloride

20.0 3070-130 5µg/kgD21.8 109Chlorobenzene

20.0 3070-130 7µg/kgD22.9 114Chloroethane

20.0 3070-130 3µg/kgD22.8 114Chloroform

20.0 3070-130 6µg/kgD16.8 84Chloromethane



20.0 3070-130 3µg/kgD21.8 1091,2-Dibromo-3-chloropropane

20.0 3070-130 3µg/kgD21.8 109Dibromochloromethane

20.0 3070-130 1µg/kgD21.7 1091,2-Dibromoethane (EDB)

20.0 3070-130 3µg/kgD23.1 115Dibromomethane




20.0 3070-130 4µg/kgD20.5 102Dichlorodifluoromethane (Freon12)



20.0 3070-130 7µg/kgD21.1 1051,1-Dichloroethene

20.0 3070-130 4µg/kgD22.8 114cis-1,2-Dichloroethene

20.0 3070-130 4µg/kgD22.4 112trans-1,2-Dichloroethene




Page 23 of 3017-Oct-17 17:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 3070-130 6µg/kgQC2, D28.1 1402,2-Dichloropropane

20.0 3070-130 5µg/kgD22.4 1121,1-Dichloropropene

20.0 3070-130 2µg/kgD21.9 109cis-1,3-Dichloropropene

20.0 3070-130 1µg/kgD22.2 111trans-1,3-Dichloropropene

20.0 3070-130 5µg/kgD22.6 113Ethylbenzene

20.0 3070-130 5µg/kgD21.7 109Hexachlorobutadiene

20.0 3070-130 3µg/kgD20.4 1022-Hexanone (MBK)

20.0 3070-130 5µg/kgD22.1 110Isopropylbenzene

20.0 3070-130 6µg/kgD22.7 1144-Isopropyltoluene

20.0 3070-130 0.2µg/kgD23.2 116Methyl tert-butyl ether

20.0 3070-130 2µg/kgD20.9 1044-Methyl-2-pentanone (MIBK)

20.0 3070-130 20µg/kgD17.6 88Methylene chloride

20.0 3070-130 10µg/kgD19.7 98Naphthalene

20.0 3070-130 6µg/kgD22.1 110n-Propylbenzene

20.0 3070-130 5µg/kgD20.7 103Styrene



20.0 3070-130 7µg/kgD20.7 104Tetrachloroethene

20.0 3070-130 5µg/kgD21.6 108Toluene





20.0 3070-130 5µg/kgD22.3 112Trichloroethene

20.0 3070-130 5µg/kgD23.3 116Trichlorofluoromethane (Freon 11)

20.0 3070-130 1µg/kgD23.1 1161,2,3-Trichloropropane



20.0 3070-130 2µg/kgD25.1 126Vinyl chloride

20.0 3070-130 5µg/kgD22.8 114m,p-Xylene

20.0 3070-130 4µg/kgD22.9 115o-Xylene

20.0 3070-130 3µg/kgD22.1 110Tetrahydrofuran

20.0 3070-130 2µg/kgD23.9 120Ethyl ether

20.0 3070-130 1µg/kgD22.4 112Tert-amyl methyl ether

20.0 3070-130 0.08µg/kgD23.8 119Ethyl tert-butyl ether

20.0 3070-130 3µg/kgD22.2 111Di-isopropyl ether

200 3070-130 0.5µg/kgD178 891,4-Dioxane






Page 24 of 3017-Oct-17 17:45

Extractable Petroleum Hydrocarbons - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


MADEP EPH 5/2004 R

Batch 1717419 - SW846 3546


mg/kg wet< 9.98C9-C18 Aliphatic Hydrocarbons 9.98


mg/kg wet< 9.98C11-C22 Aromatic Hydrocarbons 9.98

mg/kg wet< 9.98Unadjusted C11-C22 Aromatic

Hydrocarbons

9.98

mg/kg wet< 29.9Total Petroleum Hydrocarbons 29.9

mg/kg wet< 29.9Unadjusted Total Petroleum Hydrocarbons 29.9

mg/kg wet0.00Naphthalene (aliphatic fraction)

mg/kg wet0.002-Methylnaphthalene (aliphatic fraction)

3.33 40-140Surrogate: 1-Chlorooctadecane 2.21 mg/kg wet 67

3.33 40-140Surrogate: Ortho-Terphenyl 1.84 mg/kg wet 55

2.66 40-140Surrogate: 2-Fluorobiphenyl 1.36 mg/kg wet 51


19.9 40-140mg/kg wet19.9 100C9-C18 Aliphatic Hydrocarbons 9.93


45.0 40-140mg/kg wet32.8 73Unadjusted C11-C22 Aromatic

Hydrocarbons

9.93

2.65 0-200mg/kg wet0.00Naphthalene (aliphatic fraction)

2.65 0-200mg/kg wet0.002-Methylnaphthalene (aliphatic fraction)








Hydrocarbons

10.0






LCS Dup (1717419-BSD1) Prepared: 13-Oct-17 Analyzed: 14-Oct-17

19.8 2540-140 22mg/kg wet15.9 81C9-C18 Aliphatic Hydrocarbons 9.88


44.8 2540-140 16mg/kg wet38.4 86Unadjusted C11-C22 Aromatic

Hydrocarbons

9.88







Page 25 of 3017-Oct-17 17:45

Total Metals by EPA 6000/7000 Series Methods - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 6010C

Batch 1717347 - SW846 3051A


mg/kg wet< 0.987Chromium 0.987

mg/kg wet< 1.48Arsenic 1.48

mg/kg wet< 0.987Copper 0.987

mg/kg wet< 0.987Zinc 0.987

mg/kg wet< 1.48Lead 1.48

Reference (1717347-SRM1) Prepared & Analyzed: 13-Oct-17

15.0 70.3-130.

1

mg/kg wet14.5 97Arsenic 1.50

77.6 81.7-117.

6

mg/kg wet78.0 100Copper 1.00

70.5 82-117.3mg/kg wet65.8 93Lead 1.50

113 83-117mg/kg wet105 93Zinc 1.00

51.7 80.1-119.

6

mg/kg wet49.7 96Chromium 1.00

Reference (1717347-SRM2) Prepared & Analyzed: 13-Oct-17

14.9 70.3-130.

1

mg/kg wet13.5 91Arsenic 1.50

77.0 81.7-117.

6


69.9 82-117.3mg/kg wet63.0 90Lead 1.50

51.3 80.1-119.

6


112 83-117mg/kg wet104 93Zinc 1.00


Page 26 of 3017-Oct-17 17:45

General Chemistry Parameters - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 9012B

Batch 1717429 - General Preparation


mg/kg wet< 0.500Cyanide (total) 0.500


25.0 90-110mg/kg wet24.8 99Cyanide (total) 0.500

Duplicate (1717429-DUP1) Prepared: 13-Oct-17 Analyzed: 14-Oct-17Source: SC40242-01

35mg/kg dry BRL< 0.317Cyanide (total) 0.317

Matrix Spike (1717429-MS1) Prepared: 13-Oct-17 Analyzed: 14-Oct-17Source: SC40242-01

15.1 90-110mg/kg dry BRL14.3 95Cyanide (total) 0.301

Matrix Spike Dup (1717429-MSD1) Prepared: 13-Oct-17 Analyzed: 14-Oct-17Source: SC40242-01

16.3 3590-110 11mg/kg dry BRL16.0 98Cyanide (total) 0.326

Reference (1717429-SRM1) Prepared: 13-Oct-17 Analyzed: 14-Oct-17

65.2 39.4-183mg/kg wet76.8 118Cyanide (total) 1.13


Page 27 of 3017-Oct-17 17:45

Extractable Petroleum Hydrocarbons - CCV Evaluation Report

CCRF % D Limit

Average

RFAnalyte(s)

Batch S709112

Calibration Check (S709112-CCV1)

C9-C18 Aliphatic Hydrocarbons 301660.5 191658.6 25-13.2


Naphthalene (aliphatic fraction) 271837.9

2-Methylnaphthalene (aliphatic fraction) 271519.6




Unadjusted C11-C22 Aromatic Hydrocarbons 218532.8 194608.1 255.0

Naphthalene (aliphatic fraction) 271837.9 233315.4 -14.2

2-Methylnaphthalene (aliphatic fraction) 271519.6 17758.84 -93.5


C9-C18 Aliphatic Hydrocarbons 301660.5 262964.3 2520.8





Page 28 of 3017-Oct-17 17:45

The following list indicates the date and time low-level VOC soil/sediment samples were placed in the freezer at the lab:

SC40242-01 SP11_101117-1 10/11/2017 6:31 PM


Page 29 of 3017-Oct-17 17:45

Notes and Definitions

Data reported from a dilutionD

Analyte out of acceptance range in QC spike but no reportable concentration present in sample.QC2

Reporting limits reflect SW846 5035A High Level extraction technique due to interference and/or QC issues using SW846

5035A Low Level extraction technique.

VOC8

RPD Relative Percent Difference

dry Sample results reported on a dry weight basis

Not ReportedNR

Laboratory Control Sample (LCS): A known matrix spiked with compound(s) representative of the target analytes, which is used to

document laboratory performance.

Matrix Duplicate: An intra-laboratory split sample which is used to document the precision of a method in a given sample matrix.

Matrix Spike: An aliquot of a sample spiked with a known concentration of target analyte(s). The spiking occurs prior to sample

preparation and analysis. A matrix spike is used to document the bias of a method in a given sample matrix.

Method Blank: An analyte-free matrix to which all reagents are added in the same volumes or proportions as used in sample

processing. The method blank should be carried through the complete sample preparation and analytical procedure. The method blank

is used to document contamination resulting from the analytical process.

Method Detection Limit (MDL): The minimum concentration of a substance that can be measured and reported with 99% confidence

that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the

analyte.

Reportable Detection Limit (RDL): The lowest concentration that can be reliably achieved within specified limits of precision and

accuracy during routine laboratory operating conditions. For many analytes the RDL analyte concentration is selected as the lowest

non-zero standard in the calibration curve. While the RDL is approximately 5 to 10 times the MDL, the RDL for each sample takes

into account the sample volume/weight, extract/digestate volume, cleanup procedures and, if applicable, dry weight correction. Sample

RDLs are highly matrix-dependent.

Surrogate: An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical

process, but which is not normally found in environmental samples. These compounds are spiked into all blanks, standards, and

samples prior to analysis. Percent recoveries are calculated for each surrogate.

Continuing Calibration Verification: The calibration relationship established during the initial calibration must be verified at periodic

intervals. Concentrations, intervals, and criteria are method specific.


Page 30 of 3017-Oct-17 17:45

Batch Summary

1717194


1717194-BLK1

1717194-BS1

1717194-BSD1

SC40242-01 (SP11_101117-1)

1717347


1717347-BLK1

1717347-SRM1

1717347-SRM2

SC40242-01 (SP11_101117-1)

1717352


SC40242-01 (SP11_101117-1)

1717419


1717419-BLK1

1717419-BS1

1717419-BS2

1717419-BSD1

SC40242-01 (SP11_101117-1)

1717429


1717429-BLK1

1717429-BS1

1717429-DUP1

1717429-MS1

1717429-MSD1

1717429-SRM1

SC40242-01 (SP11_101117-1)

1717436


1717436-BLK1

1717436-BS1

1717436-BSD1

SC40242-02 (TB_101117-1)

1717540


1717540-BLK1

1717540-BS1

1717540-BSD1

SC40242-01 (SP11_101117-1)

S707773


S707773-CAL1

S707773-CAL2

S707773-CAL3

S707773-CAL4

S707773-CAL5

S707773-CAL6

S707773-CAL7

S707773-CAL8

S707773-CAL9

S707773-CALA

S707773-CALB

S707773-CALC

S707773-ICV1

S707773-LCV1

S708827


S708827-CAL1

S708827-CAL2

S708827-CAL3

S708827-CAL4

S708827-CAL5

S708827-CAL6

S708827-CAL7

S708827-CAL8

S708827-CAL9

S708827-ICV1

S708827-LCV1

S708827-LCV2

S708827-TUN1

S708847


S708847-CAL1

S708847-CAL2

S708847-CAL3

S708847-CAL4

S708847-CAL5

S708847-CAL6

S708847-CAL7

S708847-ICV1

S708847-LCV1

S708990


S708990-CCV1

S708990-CCV2

S709049


S709049-CCV1

S709049-TUN1

S709100


S709100-CCV1

S709100-TUN1

S709112


S709112-CCV1

S709112-CCV2

S709112-CCV3

Report Date:

06-Nov-17 11:47

Final Report

Revised Reportü

Laboratory Report

SC40987

AECOM Environment

250 Apollo Drive


Attn: Art Taddeo

Project:

Project #:


60478638.5.01

I attest that the information contained within the report has been reviewed for accuracy and checked against the quality control

requirements for each method. These results relate only to the sample(s) as received.

All applicable NELAC requirements have been met.

Massachusetts # M-MA138/MA1110

Connecticut # PH-0777

Florida # E87936

Maine # MA138

New Hampshire # 2972/2538

New Jersey # MA011

New York # 11393

Pennsylvania # 68-04426/68-02924

Rhode Island # LAO00348

USDA # P330-15-00375

Vermont # VT-11393

Eurofins Spectrum Analytical holds primary certification in the State of Massachusetts for the analytes as indicated with an X in the

"Cert." column within this report. Please note that the State of Massachusetts does not offer certification for all analytes. Please refer to

our website for specific certification holdings in each state.

Please note that this report contains 26 pages of analytical data plus Chain of Custody document(s). When the Laboratory Report is

indicated as revised, this report supersedes any previously dated reports for the laboratory ID(s) referenced above. Where this report

identifies subcontracted analyses, copies of the subcontractor's test report are available upon request. This report may not be

reproduced, except in full, without written approval from Eurofins Spectrum Analytical, Inc.

Eurofins Spectrum Analytical, Inc. is a NELAC accredited laboratory organization and meets NELAC testing standards. Use of the NELAC logo

however does not insure that Eurofins Spectrum Analytical, Inc. is currently accredited for the specific method or analyte indicated. Please refer to

our "Quality" web page at www.spectrum-analytical.com for a full listing of our current certifications and fields of accreditation. States in which

Eurofins Spectrum Analytical, Inc. holds NELAC certification are New York, New Hampshire, New Jersey, Pennsylvania and Florida. All analytical

work for Volatile Organic and Air analysis are transferred to and conducted at our 830 Silver Street location (PA-68-04426).

Please contact the Laboratory or Technical Director at 800-789-9115 with any questions regarding the data contained in this laboratory report.

Eurofins Spectrum Analytical, Inc. 830 Silver Street T | 413-789-9018

Agawam, MA 01001 F | 413-789-4076

www.EurofinsUS.com/Spectrum Page 1 of 26

Authorized by:

Dawn WojcikLaboratory Director

Sample Summary

Work Order:

Project:

Project Number:

SC40987


60478638.5.01

Laboratory ID Client Sample ID Matrix Date Sampled Date Received

SC40987-01 TB-110117 Methanol/Deionized Water 01-Nov-17 10:00 01-Nov-17 15:56

SC40987-02 SP12_110117-1 Soil 01-Nov-17 10:15 01-Nov-17 15:56


Page 2 of 2606-Nov-17 11:47

The following outlines the condition of all VPH samples contained within this report upon laboratory receipt .

Matrices Soil

Containers Satisfactoryü

Sample

Preservative

Aqueous

(acid preserved)

N/A pH<2 pH>2ü

Soil or

Sediment

N/A Samples not received in Methanol

Samples received in Methanol: covering soil/sediment

not covering soil/sediment

ü ü

ml Methanol/g soil

1:1 +/-25%ü

Other

Samples received in air-tight container

Temperature Received on ice Received at 4 ± 2 ºCü

Were all QA/QC procedures followed as required by the VPH method? Yes

Were any significant modifications made to the VPH method as specified in section 11.3? No


The following outlines the condition of all EPH samples contained within this report upon laboratory receipt.

Matrices Soil

Containers ü Satisfactory

Aqueous Preservative N/A pH<2 pH>2 pH adjusted to <2 in labü

Temperature Received on ice Received at 4 ± 2 ºCü

Were all QA/QC procedures followed as required by the EPH method? Yes

Were any significant modifications made to the EPH method as specified in Section 11.3? No


I attest that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained

in this report is, to the best of my knowledge and belief, accurate and complete.

Authorized by:

Dawn E. Wojcik

Laboratory Director


Page 3 of 2606-Nov-17 11:47

MassDEP Analytical Protocol Certification Form

Laboratory Name: Eurofins Spectrum Analytical, Inc. Project #: 60478638.5.01

Project Location: LMC-Wilmington- 40 Fordham Rd. - MA RTN:

This form provides certifications for the following data set: SC40987-01 through SC40987-02

Matrices: Methanol/Deionized Water

Soil

CAM Protocol

8260 VOC

CAM II A

7470/7471 Hg

CAM III B

MassDEP VPH

CAM IV A

8081 Pesticides

CAM V B

7196 Hex Cr

CAM VI B

MassDEP APH

CAM IX A

8270 SVOC

CAM II B

7010 Metals

CAM III C

MassDEP EPH

CAM IV B

8151 Herbicides

CAM V C

8330 Explosives

CAM VIII A

TO-15 VOC

CAM IX B

6010 Metals

CAM III A

6020 Metals

CAM III D

8082 PCB

CAM V A

9014 Total

Cyanide/PAC

CAM VI A

6860 Perchlorate

CAM VIII B

ü

ü

ü

ü

Affirmative responses to questions A through F are required for "Presumptive Certainty" status

Were all samples received in a condition consistent with those described on the Chain of Custody, properly

preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding

times?

Were the analytical method(s) and all associated QC requirements specified in the selected CAM

protocol(s) followed?

Were all required corrective actions and analytical response actions specified in the selected CAM

protocol(s) implemented for all identified performance standard non-conformances?

Does the laboratory report comply with all the reporting requirements specified in CAM VII A, "Quality

Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?

a. VPH, EPH, and APH Methods only: Was each method conducted without significant modification(s)?

b. APH and TO-15 Methods only: Was the complete analyte list reported for each method?

Were all applicable CAM protocol QC and performance standard non-conformances identified and

evaluated in a laboratory narrative (including all "No" responses to questions A through E)?

Responses to questions G, H and I below are required for "Presumptive Certainty" status

Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocol(s)?

Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability and representativeness

requirements described in 310 CMR 40. 1056 (2)(k) and WSC-07-350.

Were all QC performance standards specified in the CAM protocol(s) achieved?

Were results reported for the complete analyte list specified in the selected CAM protocol(s)?

All negative responses are addressed in a case narrative on the cover page of this report.

I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the

information, the material contained in this analytical report is, to the best of my knowledge and belief, accurate and complete.

Dawn E. Wojcik

Laboratory Director

Date: 11/6/2017

A

B

C

D

E

F

G

H

I

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

ü

ü

ü

ü

ü

ü

ü

ü

ü

Yes No

ü

9012 Total

Cyanide/PAC

CAM VI A


Page 4 of 2606-Nov-17 11:47

CASE NARRATIVE:

Data has been reported to the RDL. This report excludes estimated concentrations detected below the RDL and above the MDL

(J-Flag).

All non-detects and all results below the reporting limit are reported as �<� (less than) the reporting limit in this report.

The samples were received 3.5 degrees Celsius, please refer to the Chain of Custody for details specific to temperature upon receipt.

An infrared thermometer with a tolerance of +/- 1.0 degrees Celsius was used immediately upon receipt of the samples.

If a Matrix Spike (MS), Matrix Spike Duplicate (MSD) or Duplicate (DUP) was not requested on the Chain of Custody, method

criteria may have been fulfilled with a source sample not of this Sample Delivery Group. If method or program required

MS/MSD/Dup were not performed, sufficient sample was not provided to the laboratory.

MADEP has published a list of analytical methods (CAM) which provides a series of recommended protocols for the acquisition,

analysis and reporting of analytical data in support of MCP decisions. "Presumptive Certainty" can be established only for those

methods published by the MADEP in the MCP CAM. The compounds and/or elements reported were specifically requested by the

client on the Chain of Custody and in some cases may not include the full analyte list as defined in the method. Regulatory limits may

not be achieved if specific method and/or technique was not requested on the Chain of Custody.

According to WSC-CAM 5/2009 Rev.1, Table 11 A-1, recovery for some VOC analytes have been deemed potentially difficult.

Although they may still be within the recommended recovery range, a range has been set based on historical control limits.

Some target analytes which are not listed as exceptions in the Summary of CAM Reporting Limits may exceed the recommended RL

based on sample initial volume or weight provided, % moisture content, or responsiveness of a particular analyte to purge and trap

instrumentation.

All VOC soils samples submitted and analyzed in methanol will have a minimum dilution factor of 50. This is the minimum amount of

solvent allowed on the instrumentation without causing interference. Soils are run on a manual load instrument. 100ug of sample

(MEOH) is spiked into 5ml DI water along with the surrogate and added directly onto the instrument. Additional dilution factors may

be required to keep analyte concentration within instrument calibration range.

Method SW846 5035A is designed to use on samples containing low levels of VOCs, ranging from 0.5 to 200 ug/Kg. Target analytes

that are less responsive to purge and trap may be present at concentrations over 200ug/Kg but may not be reportable in the methanol

preserved vial (SW846 5030). This is the result of the inherent dilution factor required for the methanol preservation.

See below for any non-conformances and issues relating to quality control samples and/or sample analysis/matrix.

SW846 6010C

Duplicates:

1718549-DUP1 Source: SC40987-02

Analyses are not controlled on RPD values from sample concentrations that are less than 5 times the reporting level. The batch is

accepted based upon the difference between the sample and duplicate is less than or equal to the reporting limit.

Copper

SW846 8260C

Calibration:

1710003

Analyte quantified by quadratic equation type calibration.

1,4-Dioxane

2-Hexanone (MBK)

Naphthalene


Page 5 of 2606-Nov-17 11:47

SW846 8260C

Calibration:

1710003


1718543-BLK1

1718543-BS1

1718543-BSD1

S708708-ICV1

S709711-CCV1

SP12_110117-1

TB-110117

Laboratory Control Samples:

1718543 BS/BSD

1,4-Dioxane percent recoveries (65/68) are outside individual acceptance criteria, but within overall method allowances. All

reported results of the following samples are considered to have a potentially low bias:

SP12_110117-1

TB-110117

Acetone percent recoveries (172/126) are outside individual acceptance criteria, but within overall method allowances. All


SP12_110117-1

TB-110117

Carbon disulfide percent recoveries (97/52) are outside individual acceptance criteria, but within overall method allowances. All


SP12_110117-1

TB-110117

Naphthalene percent recoveries (91/69) are outside individual acceptance criteria, but within overall method allowances. All


SP12_110117-1

TB-110117

n-Butylbenzene percent recoveries (134/118) are outside individual acceptance criteria, but within overall method allowances. All


SP12_110117-1

TB-110117

Trichlorofluoromethane (Freon 11) percent recoveries (139/119) are outside individual acceptance criteria, but within overall

method allowances. All reported results of the following samples are considered to have a potentially high bias:

SP12_110117-1

TB-110117

1718543 BSD

Acetone RPD 31% (30%) is outside individual acceptance criteria.

Bromomethane RPD 33% (30%) is outside individual acceptance criteria.

Carbon disulfide RPD 60% (30%) is outside individual acceptance criteria.

Samples:

S709711-CCV1


Page 6 of 2606-Nov-17 11:47

SW846 8260C

Samples:

S709711-CCV1


1,2,3-Trichlorobenzene (21.3%)

1,2-Dibromo-3-chloropropane (-20.2%)

4-Isopropyltoluene (25.2%)

Bromoform (-25.4%)


Chloroethane (23.1%)

n-Butylbenzene (34.4%)

Tert-amyl methyl ether (29.8%)

Trichlorofluoromethane (Freon 11) (39.1%)


1,4-Dioxane (-35.2%)

Acetone (72.2%)


1718543-BLK1

1718543-BS1

1718543-BSD1

SP12_110117-1

TB-110117


Page 7 of 2606-Nov-17 11:47

Sample Acceptance Check Form

Client:

Work Order:

Project:

Sample(s) received on:

AECOM Environment - Chelmsford, MA

LMC-Wilmington- 40 Fordham Rd. - MA / 60478638.5.01

SC40987

11/1/2017

Yes No N/A

Were samples received at a temperature of 6°C?

Were custody seals present?

Were custody seals intact?

ü

ü

ü

The following outlines the condition of samples for the attached Chain of Custody upon receipt.

Were samples refrigerated upon transfer to laboratory representative? ü

Were samples properly labeled (labels affixed to sample containers and include sample ID, site

location, and/or project number and the collection date)?

ü

Were sample containers received intact?

Were samples accompanied by a Chain of Custody document?

Did sample container labels agree with Chain of Custody document?

Were samples received within method-specific holding times?

ü

ü

ü

ü

Does Chain of Custody document include proper, full, and complete documentation, which shall

include sample ID, site location, and/or project number, date and time of collection, collector's name,

preservation type, sample matrix and any special remarks concerning the sample?

ü


Page 8 of 2606-Nov-17 11:47

Summary of Hits

Client ID: SP12_110117-1Lab ID: SC40987-02

ResultParameter Units Analytical MethodReporting LimitFlag

C11-C22 Aromatic Hydrocarbons MADEP EPH 5/2004 R10.520.8 mg/kg

C19-C36 Aliphatic Hydrocarbons MADEP EPH 5/2004 R10.598.2 mg/kg

Unadjusted C11-C22 Aromatic

Hydrocarbons

MADEP EPH 5/2004 R10.522.0 mg/kg

Arsenic SW846 6010C1.5812.8 mg/kg

Chromium SW846 6010C1.0513.2 mg/kg

Lead SW846 6010C1.588.59 mg/kg

Zinc SW846 6010C1.0522.9 mg/kg

Please note that because there are no reporting limits associated with hazardous waste characterizations or micro analyses , this

summary does not include hits from these analyses if included in this work order.


Page 9 of 2606-Nov-17 11:47

TB-110117


01-Nov-17 10:00


01-Nov-17

Client Project #


WaterSC40987-01




Prepared by method SW846 5035A Soil (low level)

SW846 8260C 02-Nov-1702-Nov-17µg/kg wet 5.00< 5.0076-13-1 1,1,2-Trichlorotrifluoroetha

ne (Freon 113)

1 1718543MP2.54

" ""µg/kg wet 50.0< 50.067-64-1 Acetone 1 ""20.0

" ""µg/kg wet 5.00< 5.0071-43-2 Benzene 1 ""1.32

" ""µg/kg wet 5.00< 5.00108-86-1 Bromobenzene 1 ""1.34

" ""µg/kg wet 5.00< 5.0074-97-5 Bromochloromethane 1 ""2.52

" ""µg/kg wet 5.00< 5.0075-27-4 Bromodichloromethane 1 ""3.34

" ""µg/kg wet 5.00< 5.0075-25-2 Bromoform 1 ""4.77

" ""µg/kg wet 10.0< 10.074-83-9 Bromomethane 1 ""4.52

" ""µg/kg wet 10.0< 10.078-93-3 2-Butanone (MEK) 1 ""8.94

" ""µg/kg wet 5.00< 5.00104-51-8 n-Butylbenzene 1 ""1.43

" ""µg/kg wet 5.00< 5.00135-98-8 sec-Butylbenzene 1 ""0.91

" ""µg/kg wet 5.00< 5.0098-06-6 tert-Butylbenzene 1 ""1.12

" ""µg/kg wet 10.0< 10.075-15-0 Carbon disulfide 1 ""3.20

" ""µg/kg wet 5.00< 5.0056-23-5 Carbon tetrachloride 1 ""4.09

" ""µg/kg wet 5.00< 5.00108-90-7 Chlorobenzene 1 ""1.56

" ""µg/kg wet 10.0< 10.075-00-3 Chloroethane 1 ""2.78

" ""µg/kg wet 5.00< 5.0067-66-3 Chloroform 1 ""2.68

" ""µg/kg wet 10.0< 10.074-87-3 Chloromethane 1 ""2.06

" ""µg/kg wet 5.00< 5.0095-49-8 2-Chlorotoluene 1 ""1.24

" ""µg/kg wet 5.00< 5.00106-43-4 4-Chlorotoluene 1 ""1.18

" ""µg/kg wet 10.0< 10.096-12-8 1,2-Dibromo-3-chloroprop

ane

1 ""7.22

" ""µg/kg wet 5.00< 5.00124-48-1 Dibromochloromethane 1 ""3.39

" ""µg/kg wet 5.00< 5.00106-93-4 1,2-Dibromoethane (EDB) 1 ""3.36

" ""µg/kg wet 5.00< 5.0074-95-3 Dibromomethane 1 ""2.60

" ""µg/kg wet 5.00< 5.0095-50-1 1,2-Dichlorobenzene 1 ""1.30



" ""µg/kg wet 10.0< 10.075-71-8 Dichlorodifluoromethane

(Freon12)

1 ""1.90

" ""µg/kg wet 5.00< 5.0075-34-3 1,1-Dichloroethane 1 ""1.31

" ""µg/kg wet 5.00< 5.00107-06-2 1,2-Dichloroethane 1 ""1.79

" ""µg/kg wet 5.00< 5.0075-35-4 1,1-Dichloroethene 1 ""2.62

" ""µg/kg wet 5.00< 5.00156-59-2 cis-1,2-Dichloroethene 1 ""1.86

" ""µg/kg wet 5.00< 5.00156-60-5 trans-1,2-Dichloroethene 1 ""2.65

" ""µg/kg wet 5.00< 5.0078-87-5 1,2-Dichloropropane 1 ""2.62



" ""µg/kg wet 5.00< 5.00563-58-6 1,1-Dichloropropene 1 ""1.61

" ""µg/kg wet 5.00< 5.0010061-01-5 cis-1,3-Dichloropropene 1 ""3.02

" ""µg/kg wet 5.00< 5.0010061-02-6 trans-1,3-Dichloropropene 1 ""2.62

" ""µg/kg wet 5.00< 5.00100-41-4 Ethylbenzene 1 ""0.72

" ""µg/kg wet 5.00< 5.0087-68-3 Hexachlorobutadiene 1 ""2.51

" ""µg/kg wet 10.0< 10.0591-78-6 2-Hexanone (MBK) 1 ""6.14

" ""µg/kg wet 5.00< 5.0098-82-8 Isopropylbenzene 1 ""0.98


Page 10 of 2606-Nov-17 11:47

TB-110117


01-Nov-17 10:00


01-Nov-17

Client Project #


WaterSC40987-01




SW846 8260C 02-Nov-1702-Nov-17µg/kg wet 5.00< 5.0099-87-6 4-Isopropyltoluene 1 1718543MP1.08

" ""µg/kg wet 5.00< 5.001634-04-4 Methyl tert-butyl ether 1 ""1.84

" ""µg/kg wet 10.0< 10.0108-10-1 4-Methyl-2-pentanone

(MIBK)

1 ""2.57

" ""µg/kg wet 10.0< 10.075-09-2 Methylene chloride 1 ""1.98

" ""µg/kg wet 5.00< 5.0091-20-3 Naphthalene 1 ""2.98

" ""µg/kg wet 5.00< 5.00103-65-1 n-Propylbenzene 1 ""0.81

" ""µg/kg wet 5.00< 5.00100-42-5 Styrene 1 ""1.00

" ""µg/kg wet 5.00< 5.00630-20-6 1,1,1,2-Tetrachloroethane 1 ""4.25

" ""µg/kg wet 5.00< 5.0079-34-5 1,1,2,2-Tetrachloroethane 1 ""4.23

" ""µg/kg wet 5.00< 5.00127-18-4 Tetrachloroethene 1 ""1.71

" ""µg/kg wet 5.00< 5.00108-88-3 Toluene 1 ""1.62

" ""µg/kg wet 5.00< 5.0087-61-6 1,2,3-Trichlorobenzene 1 ""1.76

" ""µg/kg wet 5.00< 5.00120-82-1 1,2,4-Trichlorobenzene 1 ""3.68

" ""µg/kg wet 5.00< 5.0071-55-6 1,1,1-Trichloroethane 1 ""1.66

" ""µg/kg wet 5.00< 5.0079-00-5 1,1,2-Trichloroethane 1 ""3.62

" ""µg/kg wet 5.00< 5.0079-01-6 Trichloroethene 1 ""1.36

" ""µg/kg wet 5.00< 5.0075-69-4 Trichlorofluoromethane

(Freon 11)

1 ""2.70

" ""µg/kg wet 5.00< 5.0096-18-4 1,2,3-Trichloropropane 1 ""3.75

" ""µg/kg wet 5.00< 5.0095-63-6 1,2,4-Trimethylbenzene 1 ""1.22

" ""µg/kg wet 5.00< 5.00108-67-8 1,3,5-Trimethylbenzene 1 ""0.86

" ""µg/kg wet 5.00< 5.0075-01-4 Vinyl chloride 1 ""1.69

" ""µg/kg wet 10.0< 10.0179601-23-1 m,p-Xylene 1 ""0.90

" ""µg/kg wet 5.00< 5.0095-47-6 o-Xylene 1 ""1.40

" ""µg/kg wet 10.0< 10.0109-99-9 Tetrahydrofuran 1 ""7.88

" ""µg/kg wet 5.00< 5.0060-29-7 Ethyl ether 1 ""4.53

" ""µg/kg wet 5.00< 5.00994-05-8 Tert-amyl methyl ether 1 ""1.67

" ""µg/kg wet 5.00< 5.00637-92-3 Ethyl tert-butyl ether 1 ""2.70

" ""µg/kg wet 5.00< 5.00108-20-3 Di-isopropyl ether 1 ""0.93

" ""µg/kg wet 100< 100123-91-1 1,4-Dioxane 1 ""86.8



70-130 % " " ""Toluene-d8 101 "2037-26-5




Page 11 of 2606-Nov-17 11:47

SP12_110117-1


01-Nov-17 10:15


01-Nov-17

Client Project #

60478638.5.01 SoilSC40987-02



Prepared by method Volatiles

VOC Soil

Extraction

N/AField

extracted

VOC Extraction 1 1718522MBR


Initial weight: 6.13 gPrepared by method SW846 5035A Soil (low level)

SW846 8260C 02-Nov-1702-Nov-17µg/kg dry 4.61< 4.6176-13-1 1,1,2-Trichlorotrifluoroetha

ne (Freon 113)

1 1718543MP2.34

" ""µg/kg dry 46.1< 46.167-64-1 Acetone 1 ""18.4

" ""µg/kg dry 4.61< 4.6171-43-2 Benzene 1 ""1.22

" ""µg/kg dry 4.61< 4.61108-86-1 Bromobenzene 1 ""1.23

" ""µg/kg dry 4.61< 4.6174-97-5 Bromochloromethane 1 ""2.33

" ""µg/kg dry 4.61< 4.6175-27-4 Bromodichloromethane 1 ""3.07

" ""µg/kg dry 4.61< 4.6175-25-2 Bromoform 1 ""4.39

" ""µg/kg dry 9.21< 9.2174-83-9 Bromomethane 1 ""4.16

" ""µg/kg dry 9.21< 9.2178-93-3 2-Butanone (MEK) 1 ""8.24

" ""µg/kg dry 4.61< 4.61104-51-8 n-Butylbenzene 1 ""1.32

" ""µg/kg dry 4.61< 4.61135-98-8 sec-Butylbenzene 1 ""0.84

" ""µg/kg dry 4.61< 4.6198-06-6 tert-Butylbenzene 1 ""1.03

" ""µg/kg dry 9.21< 9.2175-15-0 Carbon disulfide 1 ""2.95

" ""µg/kg dry 4.61< 4.6156-23-5 Carbon tetrachloride 1 ""3.77

" ""µg/kg dry 4.61< 4.61108-90-7 Chlorobenzene 1 ""1.44

" ""µg/kg dry 9.21< 9.2175-00-3 Chloroethane 1 ""2.56

" ""µg/kg dry 4.61< 4.6167-66-3 Chloroform 1 ""2.47

" ""µg/kg dry 9.21< 9.2174-87-3 Chloromethane 1 ""1.90

" ""µg/kg dry 4.61< 4.6195-49-8 2-Chlorotoluene 1 ""1.15

" ""µg/kg dry 4.61< 4.61106-43-4 4-Chlorotoluene 1 ""1.08

" ""µg/kg dry 9.21< 9.2196-12-8 1,2-Dibromo-3-chloroprop

ane

1 ""6.66

" ""µg/kg dry 4.61< 4.61124-48-1 Dibromochloromethane 1 ""3.12

" ""µg/kg dry 4.61< 4.61106-93-4 1,2-Dibromoethane (EDB) 1 ""3.09

" ""µg/kg dry 4.61< 4.6174-95-3 Dibromomethane 1 ""2.40

" ""µg/kg dry 4.61< 4.6195-50-1 1,2-Dichlorobenzene 1 ""1.20



" ""µg/kg dry 9.21< 9.2175-71-8 Dichlorodifluoromethane

(Freon12)

1 ""1.75

" ""µg/kg dry 4.61< 4.6175-34-3 1,1-Dichloroethane 1 ""1.21

" ""µg/kg dry 4.61< 4.61107-06-2 1,2-Dichloroethane 1 ""1.65

" ""µg/kg dry 4.61< 4.6175-35-4 1,1-Dichloroethene 1 ""2.41

" ""µg/kg dry 4.61< 4.61156-59-2 cis-1,2-Dichloroethene 1 ""1.71

" ""µg/kg dry 4.61< 4.61156-60-5 trans-1,2-Dichloroethene 1 ""2.44

" ""µg/kg dry 4.61< 4.6178-87-5 1,2-Dichloropropane 1 ""2.41



" ""µg/kg dry 4.61< 4.61563-58-6 1,1-Dichloropropene 1 ""1.48

" ""µg/kg dry 4.61< 4.6110061-01-5 cis-1,3-Dichloropropene 1 ""2.78

" ""µg/kg dry 4.61< 4.6110061-02-6 trans-1,3-Dichloropropene 1 ""2.42

" ""µg/kg dry 4.61< 4.61100-41-4 Ethylbenzene 1 ""0.66


Page 12 of 2606-Nov-17 11:47

SP12_110117-1


01-Nov-17 10:15


01-Nov-17

Client Project #

60478638.5.01 SoilSC40987-02





SW846 8260C 02-Nov-1702-Nov-17µg/kg dry 4.61< 4.6187-68-3 Hexachlorobutadiene 1 1718543MP2.31

" ""µg/kg dry 9.21< 9.21591-78-6 2-Hexanone (MBK) 1 ""5.65

" ""µg/kg dry 4.61< 4.6198-82-8 Isopropylbenzene 1 ""0.91

" ""µg/kg dry 4.61< 4.6199-87-6 4-Isopropyltoluene 1 ""0.99

" ""µg/kg dry 4.61< 4.611634-04-4 Methyl tert-butyl ether 1 ""1.70

" ""µg/kg dry 9.21< 9.21108-10-1 4-Methyl-2-pentanone

(MIBK)

1 ""2.37

" ""µg/kg dry 9.21< 9.2175-09-2 Methylene chloride 1 ""1.83

" ""µg/kg dry 4.61< 4.6191-20-3 Naphthalene 1 ""2.74

" ""µg/kg dry 4.61< 4.61103-65-1 n-Propylbenzene 1 ""0.75

" ""µg/kg dry 4.61< 4.61100-42-5 Styrene 1 ""0.93

" ""µg/kg dry 4.61< 4.61630-20-6 1,1,1,2-Tetrachloroethane 1 ""3.92

" ""µg/kg dry 4.61< 4.6179-34-5 1,1,2,2-Tetrachloroethane 1 ""3.90

" ""µg/kg dry 4.61< 4.61127-18-4 Tetrachloroethene 1 ""1.58

" ""µg/kg dry 4.61< 4.61108-88-3 Toluene 1 ""1.49

" ""µg/kg dry 4.61< 4.6187-61-6 1,2,3-Trichlorobenzene 1 ""1.62

" ""µg/kg dry 4.61< 4.61120-82-1 1,2,4-Trichlorobenzene 1 ""3.39

" ""µg/kg dry 4.61< 4.6171-55-6 1,1,1-Trichloroethane 1 ""1.53

" ""µg/kg dry 4.61< 4.6179-00-5 1,1,2-Trichloroethane 1 ""3.34

" ""µg/kg dry 4.61< 4.6179-01-6 Trichloroethene 1 ""1.26

" ""µg/kg dry 4.61< 4.6175-69-4 Trichlorofluoromethane

(Freon 11)

1 ""2.48

" ""µg/kg dry 4.61< 4.6196-18-4 1,2,3-Trichloropropane 1 ""3.45

" ""µg/kg dry 4.61< 4.6195-63-6 1,2,4-Trimethylbenzene 1 ""1.12

" ""µg/kg dry 4.61< 4.61108-67-8 1,3,5-Trimethylbenzene 1 ""0.79

" ""µg/kg dry 4.61< 4.6175-01-4 Vinyl chloride 1 ""1.56

" ""µg/kg dry 9.21< 9.21179601-23-1 m,p-Xylene 1 ""0.83

" ""µg/kg dry 4.61< 4.6195-47-6 o-Xylene 1 ""1.29

" ""µg/kg dry 9.21< 9.21109-99-9 Tetrahydrofuran 1 ""7.26

" ""µg/kg dry 4.61< 4.6160-29-7 Ethyl ether 1 ""4.17

" ""µg/kg dry 4.61< 4.61994-05-8 Tert-amyl methyl ether 1 ""1.54

" ""µg/kg dry 4.61< 4.61637-92-3 Ethyl tert-butyl ether 1 ""2.48

" ""µg/kg dry 4.61< 4.61108-20-3 Di-isopropyl ether 1 ""0.86

" ""µg/kg dry 92.1< 92.1123-91-1 1,4-Dioxane 1 ""80.0



70-130 % " " ""Toluene-d8 102 "2037-26-5




Initial weight: 17.52 gPrepared by method VPH - EPA 5035A Soil

MADEP VPH

5/2004 Rev. 1.1

02-Nov-1702-Nov-17mg/kg dry 0.723< 0.723C5-C8 Aliphatic

Hydrocarbons

50 1718546SD0.140D


Hydrocarbons

50 ""0.100D


Page 13 of 2606-Nov-17 11:47

SP12_110117-1


01-Nov-17 10:15


01-Nov-17

Client Project #

60478638.5.01 SoilSC40987-02





MADEP VPH

5/2004 Rev. 1.1

02-Nov-1702-Nov-17mg/kg dry 0.386< 0.386C9-C10 Aromatic

Hydrocarbons

50 1718546SD0.0293D



50 ""0.112D



50 ""0.128D


70-130 % " " ""2,5-Dibromotoluene (FID) 91 "615-59-8

70-130 % " " ""2,5-Dibromotoluene (PID) 89 "615-59-8


MADEP EPH Carbon Ranges

Prepared by method SW846 3546

MADEP EPH

5/2004 R

04-Nov-1702-Nov-17mg/kg dry 10.5< 10.5C9-C18 Aliphatic

Hydrocarbons

1 1718533EDT2.15

" ""mg/kg dry 10.598.2C19-C36 Aliphatic

Hydrocarbons

1 ""2.85

" ""mg/kg dry 10.520.8C11-C22 Aromatic

Hydrocarbons

1 ""4.43

" ""mg/kg dry 10.522.0Unadjusted C11-C22

Aromatic Hydrocarbons

1 ""4.43


40-140 % " " ""1-Chlorooctadecane 52 "3386-33-2

40-140 % " " ""Ortho-Terphenyl 47 "84-15-1

40-140 % " " ""2-Fluorobiphenyl 50 "321-60-8


Prepared by method SW846 3051A

SW846 6010C 02-Nov-1702-Nov-17mg/kg dry 1.5812.87440-38-2 Arsenic 1 1718549TBC0.200

" ""mg/kg dry 1.0513.27440-47-3 Chromium 1 ""0.140

" ""mg/kg dry 13.7< 13.77440-50-8 Copper 1 ""0.253

" ""mg/kg dry 1.588.597439-92-1 Lead 1 ""0.223

" 03-Nov-17"mg/kg dry 1.0522.97440-66-6 Zinc 1 ""0.816


SM2540 G (11)

Mod.

02-Nov-1702-Nov-17%94.5% Solids 1 1718557MBR

Prepared by method SW846 9010B

SW846 9012B 03-Nov-1703-Nov-17mg/kg dry 0.281< 0.28157-12-5 Cyanide (total) 1 1718456RLT0.237


Page 14 of 2606-Nov-17 11:47


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


MADEP VPH 5/2004 Rev. 1.1

Batch 1718546 - VPH - EPA 5035A Soil

Blank (1718546-BLK1) Prepared & Analyzed: 02-Nov-17



mg/kg wetD< 0.400C9-C10 Aromatic Hydrocarbons 0.400

mg/kg wetD< 0.750Unadjusted C5-C8 Aliphatic Hydrocarbons 0.750

mg/kg wetD< 0.400Unadjusted C9-C12 Aliphatic

Hydrocarbons

0.400



LCS (1718546-BS1) Prepared & Analyzed: 02-Nov-17



20.0 70-130µg/kgD19.0 95C9-C10 Aromatic Hydrocarbons

200 70-130µg/kgD197 98Unadjusted C5-C8 Aliphatic Hydrocarbons

80.0 70-130µg/kgD71.0 89Unadjusted C9-C12 Aliphatic

Hydrocarbons



LCS Dup (1718546-BSD1) Prepared & Analyzed: 02-Nov-17

60.0 2570-130 0.7µg/kgD52.0 87C5-C8 Aliphatic Hydrocarbons

60.0 2570-130 0.4µg/kgD52.3 87C9-C12 Aliphatic Hydrocarbons

20.0 2570-130 6µg/kgD20.2 101C9-C10 Aromatic Hydrocarbons

200 2570-130 1µg/kgD199 100Unadjusted C5-C8 Aliphatic Hydrocarbons

80.0 2570-130 2µg/kgD72.4 91Unadjusted C9-C12 Aliphatic

Hydrocarbons



SW846 8260C

Batch 1718543 - SW846 5035A Soil (low level)


µg/kg wet< 5.001,1,2-Trichlorotrifluoroethane (Freon 113) 5.00

µg/kg wet< 50.0Acetone 50.0

µg/kg wet< 5.00Benzene 5.00

µg/kg wet< 5.00Bromobenzene 5.00

µg/kg wet< 5.00Bromochloromethane 5.00

µg/kg wet< 5.00Bromodichloromethane 5.00

µg/kg wet< 5.00Bromoform 5.00

µg/kg wet< 10.0Bromomethane 10.0

µg/kg wet< 10.02-Butanone (MEK) 10.0

µg/kg wet< 5.00n-Butylbenzene 5.00

µg/kg wet< 5.00sec-Butylbenzene 5.00

µg/kg wet< 5.00tert-Butylbenzene 5.00

µg/kg wet< 10.0Carbon disulfide 10.0

µg/kg wet< 5.00Carbon tetrachloride 5.00

µg/kg wet< 5.00Chlorobenzene 5.00

µg/kg wet< 10.0Chloroethane 10.0

µg/kg wet< 5.00Chloroform 5.00

µg/kg wet< 10.0Chloromethane 10.0

µg/kg wet< 5.002-Chlorotoluene 5.00

µg/kg wet< 5.004-Chlorotoluene 5.00

µg/kg wet< 10.01,2-Dibromo-3-chloropropane 10.0


Page 15 of 2606-Nov-17 11:47


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



µg/kg wet< 5.00Dibromochloromethane 5.00

µg/kg wet< 5.001,2-Dibromoethane (EDB) 5.00

µg/kg wet< 5.00Dibromomethane 5.00

µg/kg wet< 5.001,2-Dichlorobenzene 5.00



µg/kg wet< 10.0Dichlorodifluoromethane (Freon12) 10.0

µg/kg wet< 5.001,1-Dichloroethane 5.00

µg/kg wet< 5.001,2-Dichloroethane 5.00

µg/kg wet< 5.001,1-Dichloroethene 5.00

µg/kg wet< 5.00cis-1,2-Dichloroethene 5.00

µg/kg wet< 5.00trans-1,2-Dichloroethene 5.00

µg/kg wet< 5.001,2-Dichloropropane 5.00



µg/kg wet< 5.001,1-Dichloropropene 5.00

µg/kg wet< 5.00cis-1,3-Dichloropropene 5.00

µg/kg wet< 5.00trans-1,3-Dichloropropene 5.00

µg/kg wet< 5.00Ethylbenzene 5.00

µg/kg wet< 5.00Hexachlorobutadiene 5.00

µg/kg wet< 10.02-Hexanone (MBK) 10.0

µg/kg wet< 5.00Isopropylbenzene 5.00

µg/kg wet< 5.004-Isopropyltoluene 5.00

µg/kg wet< 5.00Methyl tert-butyl ether 5.00

µg/kg wet< 10.04-Methyl-2-pentanone (MIBK) 10.0

µg/kg wet< 10.0Methylene chloride 10.0

µg/kg wet< 5.00Naphthalene 5.00

µg/kg wet< 5.00n-Propylbenzene 5.00

µg/kg wet< 5.00Styrene 5.00

µg/kg wet< 5.001,1,1,2-Tetrachloroethane 5.00

µg/kg wet< 5.001,1,2,2-Tetrachloroethane 5.00

µg/kg wet< 5.00Tetrachloroethene 5.00

µg/kg wet< 5.00Toluene 5.00

µg/kg wet< 5.001,2,3-Trichlorobenzene 5.00

µg/kg wet< 5.001,2,4-Trichlorobenzene 5.00

µg/kg wet< 5.001,1,1-Trichloroethane 5.00

µg/kg wet< 5.001,1,2-Trichloroethane 5.00

µg/kg wet< 5.00Trichloroethene 5.00

µg/kg wet< 5.00Trichlorofluoromethane (Freon 11) 5.00

µg/kg wet< 5.001,2,3-Trichloropropane 5.00

µg/kg wet< 5.001,2,4-Trimethylbenzene 5.00

µg/kg wet< 5.001,3,5-Trimethylbenzene 5.00

µg/kg wet< 5.00Vinyl chloride 5.00

µg/kg wet< 10.0m,p-Xylene 10.0

µg/kg wet< 5.00o-Xylene 5.00

µg/kg wet< 10.0Tetrahydrofuran 10.0

µg/kg wet< 5.00Ethyl ether 5.00

µg/kg wet< 5.00Tert-amyl methyl ether 5.00

µg/kg wet< 5.00Ethyl tert-butyl ether 5.00

µg/kg wet< 5.00Di-isopropyl ether 5.00


Page 16 of 2606-Nov-17 11:47


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



µg/kg wet< 1001,4-Dioxane 100






20.0 70-130µg/kg23.3 1161,1,2-Trichlorotrifluoroethane (Freon 113)

20.0 70-130µg/kgQM934.4 172Acetone

20.0 70-130µg/kg21.2 106Benzene

20.0 70-130µg/kg19.4 97Bromobenzene

20.0 70-130µg/kg20.1 101Bromochloromethane

20.0 70-130µg/kg20.8 104Bromodichloromethane

20.0 70-130µg/kg14.9 75Bromoform

20.0 70-130µg/kg24.6 123Bromomethane

20.0 70-130µg/kg20.4 1022-Butanone (MEK)

20.0 70-130µg/kgQM926.9 134n-Butylbenzene

20.0 70-130µg/kg23.0 115sec-Butylbenzene

20.0 70-130µg/kg21.8 109tert-Butylbenzene

20.0 70-130µg/kg19.4 97Carbon disulfide

20.0 70-130µg/kg21.9 110Carbon tetrachloride

20.0 70-130µg/kg20.1 101Chlorobenzene

20.0 70-130µg/kg24.6 123Chloroethane

20.0 70-130µg/kg21.7 109Chloroform

20.0 70-130µg/kg19.7 99Chloromethane

20.0 70-130µg/kg22.3 1112-Chlorotoluene

20.0 70-130µg/kg23.0 1154-Chlorotoluene

20.0 70-130µg/kg16.0 801,2-Dibromo-3-chloropropane

20.0 70-130µg/kg18.5 92Dibromochloromethane

20.0 70-130µg/kg19.2 961,2-Dibromoethane (EDB)

20.0 70-130µg/kg21.0 105Dibromomethane

20.0 70-130µg/kg21.7 1091,2-Dichlorobenzene



20.0 70-130µg/kg18.7 94Dichlorodifluoromethane (Freon12)

20.0 70-130µg/kg21.5 1081,1-Dichloroethane

20.0 70-130µg/kg22.9 1151,2-Dichloroethane

20.0 70-130µg/kg22.2 1111,1-Dichloroethene

20.0 70-130µg/kg20.9 104cis-1,2-Dichloroethene

20.0 70-130µg/kg20.3 101trans-1,2-Dichloroethene

20.0 70-130µg/kg20.4 1021,2-Dichloropropane



20.0 70-130µg/kg21.8 1091,1-Dichloropropene

20.0 70-130µg/kg18.2 91cis-1,3-Dichloropropene

20.0 70-130µg/kg17.2 86trans-1,3-Dichloropropene

20.0 70-130µg/kg21.5 108Ethylbenzene

20.0 70-130µg/kg23.6 118Hexachlorobutadiene

20.0 70-130µg/kg18.8 942-Hexanone (MBK)

20.0 70-130µg/kg22.3 112Isopropylbenzene

20.0 70-130µg/kg25.0 1254-Isopropyltoluene


Page 17 of 2606-Nov-17 11:47


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 70-130µg/kg16.1 80Methyl tert-butyl ether

20.0 70-130µg/kg16.1 804-Methyl-2-pentanone (MIBK)

20.0 70-130µg/kg20.0 100Methylene chloride

20.0 70-130µg/kg18.3 91Naphthalene

20.0 70-130µg/kg23.2 116n-Propylbenzene

20.0 70-130µg/kg18.9 95Styrene

20.0 70-130µg/kg19.3 971,1,1,2-Tetrachloroethane

20.0 70-130µg/kg18.7 931,1,2,2-Tetrachloroethane

20.0 70-130µg/kg22.2 111Tetrachloroethene

20.0 70-130µg/kg21.3 107Toluene

20.0 70-130µg/kg24.2 1211,2,3-Trichlorobenzene

20.0 70-130µg/kg23.3 1171,2,4-Trichlorobenzene

20.0 70-130µg/kg21.0 1051,1,1-Trichloroethane

20.0 70-130µg/kg19.5 971,1,2-Trichloroethane

20.0 70-130µg/kg22.0 110Trichloroethene

20.0 70-130µg/kgQM927.8 139Trichlorofluoromethane (Freon 11)

20.0 70-130µg/kg19.0 951,2,3-Trichloropropane

20.0 70-130µg/kg22.7 1141,2,4-Trimethylbenzene

20.0 70-130µg/kg22.3 1121,3,5-Trimethylbenzene

20.0 70-130µg/kg24.0 120Vinyl chloride

20.0 70-130µg/kg20.0 100m,p-Xylene

20.0 70-130µg/kg20.3 102o-Xylene

20.0 70-130µg/kg17.7 88Tetrahydrofuran

20.0 70-130µg/kg21.4 107Ethyl ether

20.0 70-130µg/kg26.0 130Tert-amyl methyl ether

20.0 70-130µg/kg17.5 88Ethyl tert-butyl ether

20.0 70-130µg/kg20.7 103Di-isopropyl ether

200 70-130µg/kg130 651,4-Dioxane






20.0 3070-130 10µg/kg21.1 1051,1,2-Trichlorotrifluoroethane (Freon 113)

20.0 3070-130 31µg/kgQR525.1 126Acetone

20.0 3070-130 9µg/kg19.5 97Benzene

20.0 3070-130 6µg/kg18.3 91Bromobenzene

20.0 3070-130 11µg/kg18.1 90Bromochloromethane

20.0 3070-130 0.9µg/kg20.6 103Bromodichloromethane

20.0 3070-130 5µg/kg14.2 71Bromoform

20.0 3070-130 33µg/kgQR217.5 88Bromomethane

20.0 3070-130 10µg/kg22.6 1132-Butanone (MEK)

20.0 3070-130 13µg/kg23.5 118n-Butylbenzene

20.0 3070-130 10µg/kg20.7 104sec-Butylbenzene

20.0 3070-130 11µg/kg19.5 98tert-Butylbenzene

20.0 3070-130 60µg/kgQM9,

QR510.5 52Carbon disulfide

20.0 3070-130 7µg/kg20.4 102Carbon tetrachloride

20.0 3070-130 3µg/kg19.4 97Chlorobenzene

20.0 3070-130 24µg/kg19.4 97Chloroethane


Page 18 of 2606-Nov-17 11:47


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 3070-130 3µg/kg21.1 105Chloroform

20.0 3070-130 8µg/kg21.4 107Chloromethane

20.0 3070-130 9µg/kg20.4 1022-Chlorotoluene

20.0 3070-130 11µg/kg20.6 1034-Chlorotoluene

20.0 3070-130 4µg/kg15.4 771,2-Dibromo-3-chloropropane

20.0 3070-130 1µg/kg18.3 91Dibromochloromethane

20.0 3070-130 3µg/kg18.6 931,2-Dibromoethane (EDB)

20.0 3070-130 5µg/kg20.0 100Dibromomethane

20.0 3070-130 11µg/kg19.5 971,2-Dichlorobenzene



20.0 3070-130 5µg/kg19.6 98Dichlorodifluoromethane (Freon12)

20.0 3070-130 6µg/kg20.3 1021,1-Dichloroethane

20.0 3070-130 5µg/kg21.8 1091,2-Dichloroethane

20.0 3070-130 21µg/kg17.9 891,1-Dichloroethene

20.0 3070-130 7µg/kg19.4 97cis-1,2-Dichloroethene

20.0 3070-130 16µg/kg17.2 86trans-1,2-Dichloroethene

20.0 3070-130 2µg/kg20.1 1001,2-Dichloropropane



20.0 3070-130 12µg/kg19.4 971,1-Dichloropropene

20.0 3070-130 5µg/kg17.3 87cis-1,3-Dichloropropene

20.0 3070-130 5µg/kg16.2 81trans-1,3-Dichloropropene

20.0 3070-130 8µg/kg19.8 99Ethylbenzene

20.0 3070-130 3µg/kg22.9 115Hexachlorobutadiene

20.0 3070-130 28µg/kg14.2 712-Hexanone (MBK)

20.0 3070-130 10µg/kg20.1 101Isopropylbenzene

20.0 3070-130 12µg/kg22.2 1114-Isopropyltoluene

20.0 3070-130 5µg/kg15.3 76Methyl tert-butyl ether

20.0 3070-130 3µg/kg15.6 784-Methyl-2-pentanone (MIBK)

20.0 3070-130 7µg/kg18.6 93Methylene chloride

20.0 3070-130 28µg/kgQM913.7 69Naphthalene

20.0 3070-130 12µg/kg20.6 103n-Propylbenzene

20.0 3070-130 13µg/kg16.6 83Styrene

20.0 3070-130 3µg/kg18.7 931,1,1,2-Tetrachloroethane

20.0 3070-130 1µg/kg18.5 921,1,2,2-Tetrachloroethane

20.0 3070-130 10µg/kg20.1 100Tetrachloroethene

20.0 3070-130 4µg/kg20.5 103Toluene

20.0 3070-130 17µg/kg20.4 1021,2,3-Trichlorobenzene

20.0 3070-130 13µg/kg20.4 1021,2,4-Trichlorobenzene

20.0 3070-130 5µg/kg20.0 1001,1,1-Trichloroethane

20.0 3070-130 2µg/kg19.9 991,1,2-Trichloroethane

20.0 3070-130 7µg/kg20.4 102Trichloroethene

20.0 3070-130 15µg/kg23.9 119Trichlorofluoromethane (Freon 11)

20.0 3070-130 1µg/kg18.8 941,2,3-Trichloropropane

20.0 3070-130 14µg/kg19.7 991,2,4-Trimethylbenzene

20.0 3070-130 12µg/kg19.8 991,3,5-Trimethylbenzene

20.0 3070-130 21µg/kg19.5 97Vinyl chloride

20.0 3070-130 9µg/kg18.3 91m,p-Xylene

20.0 3070-130 6µg/kg19.1 95o-Xylene


Page 19 of 2606-Nov-17 11:47


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 8260C



20.0 3070-130 8µg/kg16.3 82Tetrahydrofuran

20.0 3070-130 12µg/kg19.0 95Ethyl ether

20.0 3070-130 0.8µg/kg25.8 129Tert-amyl methyl ether

20.0 3070-130 5µg/kg16.6 83Ethyl tert-butyl ether

20.0 3070-130 3µg/kg20.0 100Di-isopropyl ether

200 3070-130 4µg/kg135 681,4-Dioxane






Page 20 of 2606-Nov-17 11:47

Extractable Petroleum Hydrocarbons - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


MADEP EPH 5/2004 R

Batch 1718533 - SW846 3546

Blank (1718533-BLK1) Prepared: 02-Nov-17 Analyzed: 03-Nov-17



mg/kg wet< 9.94C11-C22 Aromatic Hydrocarbons 9.94

mg/kg wet< 9.94Unadjusted C11-C22 Aromatic

Hydrocarbons

9.94

mg/kg wet< 29.8Total Petroleum Hydrocarbons 29.8

mg/kg wet< 29.8Unadjusted Total Petroleum Hydrocarbons 29.8

mg/kg wet0.00Naphthalene (aliphatic fraction)

mg/kg wet0.002-Methylnaphthalene (aliphatic fraction)




LCS (1718533-BS1) Prepared: 02-Nov-17 Analyzed: 03-Nov-17




Hydrocarbons

9.92






LCS (1718533-BS2) Prepared: 02-Nov-17 Analyzed: 03-Nov-17




Hydrocarbons

10.0






LCS Dup (1718533-BSD1) Prepared: 02-Nov-17 Analyzed: 03-Nov-17



45.2 2540-140 2mg/kg wet34.0 75Unadjusted C11-C22 Aromatic

Hydrocarbons

9.98







Page 21 of 2606-Nov-17 11:47

Total Metals by EPA 6000/7000 Series Methods - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 6010C

Batch 1718549 - SW846 3051A


mg/kg wet< 0.984Chromium 0.984

mg/kg wet< 12.8Copper 12.8

mg/kg wet< 1.48Lead 1.48

mg/kg wet< 0.984Zinc 0.984

mg/kg wet< 1.48Arsenic 1.48

Duplicate (1718549-DUP1) Prepared: 02-Nov-17 Analyzed: 03-Nov-17Source: SC40987-02

2016mg/kg dry 22.919.5Zinc 1.06

2012mg/kg dry 12.814.3Arsenic 1.59

2019mg/kg dry 13.216.0Chromium 1.06

2045mg/kg dryJ,QR8 13.58.60Copper 13.8

202mg/kg dry 8.598.72Lead 1.59

Matrix Spike (1718549-MS1) Prepared & Analyzed: 02-Nov-17Source: SC40987-02

131 75-125mg/kg dry 13.5151 105Copper 13.6

131 75-125mg/kg dry 8.59143 103Lead 1.57

131 75-125mg/kg dry 22.9155 101Zinc 1.05

131 75-125mg/kg dry 13.2155 108Chromium 1.05

131 75-125mg/kg dry 12.8152 106Arsenic 1.57

Matrix Spike Dup (1718549-MSD1) Prepared & Analyzed: 02-Nov-17Source: SC40987-02

130 2075-125 2mg/kg dry 12.8155 110Arsenic 1.56

130 2075-125 2mg/kg dry 13.2159 112Chromium 1.04

130 2075-125 3mg/kg dry 13.5155 109Copper 13.5

130 2075-125 0.01mg/kg dry 8.59143 103Lead 1.56

130 2075-125 2mg/kg dry 22.9158 104Zinc 1.04

Post Spike (1718549-PS1) Prepared & Analyzed: 02-Nov-17Source: SC40987-02

132 80-120mg/kg dry 12.8143 99Arsenic 1.58

132 80-120mg/kg dry 22.9155 100Zinc 1.05

132 80-120mg/kg dry 8.59131 93Lead 1.58

132 80-120mg/kg dry 13.2149 103Chromium 1.05

132 80-120mg/kg dry 13.5130 89Copper 13.7

Reference (1718549-SRM1) Prepared & Analyzed: 02-Nov-17

50.4 80.9-120mg/kg wet55.2 110Arsenic 1.50

53.9 77.5-121.

5


83.6 80.7-118.

7


44.5 81.2-118.

8

mg/kg wet47.5 107Lead 1.50

73.0 82.1-117.

9

mg/kg wet80.9 111Zinc 1.00


44.3 81.2-118.

8

mg/kg wet47.5 107Lead 1.50

50.1 80.9-120mg/kg wet54.4 109Arsenic 1.50

83.1 80.7-118.

7


72.6 82.1-117.

9

mg/kg wet76.4 105Zinc 1.00

53.6 77.5-121.

5



Page 22 of 2606-Nov-17 11:47

General Chemistry Parameters - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846 9012B

Batch 1718456 - General Preparation


mg/kg wet< 0.500Cyanide (total) 0.500


25.0 90-110mg/kg wet26.0 104Cyanide (total) 0.500

Duplicate (1718456-DUP1) Prepared & Analyzed: 03-Nov-17Source: SC40987-02

35mg/kg dry BRL< 0.301Cyanide (total) 0.301

Matrix Spike (1718456-MS1) Prepared & Analyzed: 03-Nov-17Source: SC40987-02

14.6 90-110mg/kg dry BRL15.4 106Cyanide (total) 0.291

Matrix Spike Dup (1718456-MSD1) Prepared & Analyzed: 03-Nov-17Source: SC40987-02

14.0 3590-110 7mg/kg dry BRL14.4 102Cyanide (total) 0.281


65.2 39.4-183mg/kg wet67.1 103Cyanide (total) 1.36


Page 23 of 2606-Nov-17 11:47

Extractable Petroleum Hydrocarbons - CCV Evaluation Report

CCRF % D Limit

Average

RFAnalyte(s)

Batch S709765




Unadjusted C11-C22 Aromatic Hydrocarbons 284390.2 208417.6 25-7.8






Unadjusted C11-C22 Aromatic Hydrocarbons 284390.2 209781.3 25-7.1




Page 24 of 2606-Nov-17 11:47

The following list indicates the date and time low-level VOC soil/sediment samples were placed in the freezer at the lab:

SC40987-02 SP12_110117-1 11/1/2017 3:56 PM


Page 25 of 2606-Nov-17 11:47

Notes and Definitions

Data reported from a dilutionD

The spike recovery for this QC sample is outside the established control limits. The sample results for the QC batch were

accepted based on LCS/LCSD or SRM recoveries within the control limits.

QM9

The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the

QC batch were accepted based on percent recoveries and completeness of QC data.

QR2

RPD out of acceptance range.QR5

Analyses are not controlled on RPD values from sample concentrations that are less than 5 times the reporting level. The

batch is accepted based upon the difference between the sample and duplicate is less than or equal to the reporting limit.

QR8

RPD Relative Percent Difference

dry Sample results reported on a dry weight basis

Not ReportedNR

J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).

Laboratory Control Sample (LCS): A known matrix spiked with compound(s) representative of the target analytes, which is used to

document laboratory performance.

Matrix Duplicate: An intra-laboratory split sample which is used to document the precision of a method in a given sample matrix.

Matrix Spike: An aliquot of a sample spiked with a known concentration of target analyte(s). The spiking occurs prior to sample

preparation and analysis. A matrix spike is used to document the bias of a method in a given sample matrix.

Method Blank: An analyte-free matrix to which all reagents are added in the same volumes or proportions as used in sample

processing. The method blank should be carried through the complete sample preparation and analytical procedure. The method blank

is used to document contamination resulting from the analytical process.

Method Detection Limit (MDL): The minimum concentration of a substance that can be measured and reported with 99% confidence

that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the

analyte.

Reportable Detection Limit (RDL): The lowest concentration that can be reliably achieved within specified limits of precision and

accuracy during routine laboratory operating conditions. For many analytes the RDL analyte concentration is selected as the lowest

non-zero standard in the calibration curve. While the RDL is approximately 5 to 10 times the MDL, the RDL for each sample takes

into account the sample volume/weight, extract/digestate volume, cleanup procedures and, if applicable, dry weight correction. Sample

RDLs are highly matrix-dependent.

Surrogate: An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical

process, but which is not normally found in environmental samples. These compounds are spiked into all blanks, standards, and

samples prior to analysis. Percent recoveries are calculated for each surrogate.

Continuing Calibration Verification: The calibration relationship established during the initial calibration must be verified at periodic

intervals. Concentrations, intervals, and criteria are method specific.


Page 26 of 2606-Nov-17 11:47

Batch Summary

1718456


1718456-BLK1

1718456-BS1

1718456-DUP1

1718456-MS1

1718456-MSD1

1718456-SRM1

SC40987-02 (SP12_110117-1)

1718533


1718533-BLK1

1718533-BS1

1718533-BS2

1718533-BSD1

SC40987-02 (SP12_110117-1)

1718543


1718543-BLK1

1718543-BS1

1718543-BSD1

SC40987-01 (TB-110117)

SC40987-02 (SP12_110117-1)

1718546


1718546-BLK1

1718546-BS1

1718546-BSD1

SC40987-02 (SP12_110117-1)

1718549


1718549-BLK1

1718549-DUP1

1718549-MS1

1718549-MSD1

1718549-PS1

1718549-SRM1

1718549-SRM2

SC40987-02 (SP12_110117-1)

1718557


SC40987-02 (SP12_110117-1)

S708708


S708708-CAL1

S708708-CAL2

S708708-CAL3

S708708-CAL4

S708708-CAL5

S708708-CAL6

S708708-CAL7

S708708-CAL8

S708708-CAL9

S708708-ICV1

S708708-LCV1

S708708-TUN1

S709111


S709111-CAL1

S709111-CAL2

S709111-CAL3

S709111-CAL4

S709111-CAL5

S709111-CAL6

S709111-CAL7

S709111-ICV1

S709111-LCV1

S709454


S709454-CAL1

S709454-CAL2

S709454-CAL3

S709454-CAL4

S709454-CAL5

S709454-CAL6

S709454-CAL7

S709454-CAL8

S709454-CAL9

S709454-CALA

S709454-CALB

S709454-CALC

S709454-ICV1

S709454-LCV1

S709685


S709685-CCV1

S709685-CCV2

S709711


S709711-CCV1

S709711-TUN1

S709765


S709765-CCV1

S709765-CCV2


APPENDIX B – WASTE DISPOSAL DOCUMENTATION

Release Abatement Measure Status Report No. 2 Site ... · disposal site, identified as 50 Fordham...

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Transcript of Release Abatement Measure Status Report No. 2 Site ... · disposal site, identified as 50 Fordham...