Questionnaire for Phosgenation Plants - JAAS（ … · Web viewPhosgenation section APR 6 100...

CONFIDENTIAL

Questionnaire for Phosgenation Plants CL-475135-1Seite 1 von 11

Please append supplementary information to any section where you consider it may be of use and send it back to [email protected] or Fax: +41 61 8256 737,

1. GENERAL INFORMATION

Customer:

Address:

Contact person:

Phone:

Telefax:

E-mail:

End-user:

Address:

Plant location:

What kind of product(s) shall be manufactured with phosgene?

Formula/Name/Molecular weight Purity wt-%

ISOCYANATES CHLOROFOMATES ACID CHLORIDES POLYCARBONATES

NOTE: Pre filled data refer to BCT Standard, please correct/delete if not applicable.

© BUSS ChemTech AG, 2006Made by: Daniel Hariri

Issue Date: 19.10.2006 Filed by: QM

mailto:[email protected]

CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1

Seite 2 von 11

2. PROCESS & TECHNICAL DATA

2.1 Plant capacity

PRODUCT: Annual production MT/year

MT/day

Annual production time hours/year hours/day

800024

Type of operation --- Batch ContinuousProduction rate kg/h Reaction time / Residence time min. Design Pressure // Temperature --- -1 /+6 barg // -0 / +100°CRemarks:

2.2 Reaction conditionsPhysical state - Gas/Liquid Slurry Rated flow rate kg/h Reaction Pressure Min. / Average / Max. barg / / Reaction Temperature Min. / Average / Max. °C / / Reaction Density Min. / Average / Max. kg/m3 / / Reaction Specific Heat capacity Min. / Average / Max. kJ/kgK / / Reaction Therm. Conductivity Min. / Average / Max. W/mK / / Reaction Viscosity Min. / Average / Max. mPas / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. balanceRemarks:

2.3 Reaction data

REACTIONS Heat of reaction Reac.P

Reac.T

MAIN REACTION kJ/kmol BASIS barg °C + + + + + + + +

SIDE REACTION kJ/kmol BASIS barg °C + + + + + + + +


Seite 3 von 11

2.4 Product & Raw material specification

Product: Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. balanceOthersColour (Hazen, APHA, …) Appearance (e.g.Turbidity max.) Remarks:

Raw material: Phosgene, COCl2Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure at consumer Min. / Average / Max. barg 0.1 / 0.2 / 0.3Supply Temperature at consumer Min. / Average / Max. °C 50 / 55 / 60Density Min. / Average / Max. kg/m3 4.1 / 4.3 / 4.6Specific Heat capacity Min. / Average / Max. kJ/kgK 0.60 / 0.60 / 0.60Therm. Conductivity Min. / Average / Max. W/mK 0.01 / 0.01 / 0.01Viscosity Min. / Average / Max. mPas 0.01 / 0.01 / 0.01CompositionCOCl2 wt.-% min. 98.0000 Ar wt.-% max. 0.0013CO wt.-% max. 1.1893 wt.-% max. CO2 wt.-% max. 0.0374 wt.-% max. HCl wt.-% max. 0.4135 wt.-% max. CCl4 wt.-% max. 0.0197 wt.-% max. Cl2 wt.-% max. 0.0027 N2 wt.-% max. BalanceSupply: Liquid from an existing plant Tank farm

Not available on site Remarks:


Seite 4 von 11

Raw material: Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. balanceOthersColour (Hazen, APHA, …) Appearance (e.g.Turbidity max.) Remarks:

Raw material: Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. BalanceSupply: Liquid from an existing plant Tank farm

Not available on site OthersColour (Hazen, APHA, …) Appearance Remarks:


Seite 5 von 11

2.5 Solvent & Catalyst specificationSolvent: Physical state - Gas Liquid SlurryRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. BalanceSupply: Liquid from an existing plant Tank farm

Not available on site Others Remarks:

Catalyst: Type - Heterogeneous

HomogeneousPhysical state - Gas Liquid SlurryRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point °C Particle size distribution Min. / Average / Max. m / / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. BalanceSupply: Drum Tank farm As slurry Not available on site

Dissolved in as solution

Remarks:


Seite 6 von 11

3. UTILITIES (conditions defined at BCT battery limit inlet/outlet flange)

Cooling Water Process Water Chilled Water Hot Water Demin. WaterAbbreviation WC WP WCH WH WDMTemperature Min. 12 °C °C 5 °C °C 12 °C

Max. 25 °C °C 10 °C °C 20 °CT Max. 10 °C °C 3 °C °C °CPressure Min. 4.0 barg barg 4.0 barg barg 2.0 barg

Max. 5.0 barg barg 5.0 barg barg 3.0 bargP Max. 1.0 bar bar 1.0 bar bar barFouling factor 0.00052 m2K/W m2K/W 0.00020 m2K/W m2K/W 0.00035 m2K/WAvailable capacity m3/h m3/h m3/h m3/h m3/h

Quality Filtered Treated

Filtered Treated

Filtered Treated

Filtered Treated

Filtered Treated

Remark:

Brine Sat. Steam Abbreviation MBR S Temperature Min. °C 162 °C °C °C °C

Max. °C 165 °C °C °C °CT Max. °C °C °C °C °CPressure Min. barg 5.5 barg barg barg barg

Max. barg 6.0 barg barg barg bargP Max. bar 2.0 bar bar bar barFouling factor m2K/W 0.00026 m2K/W m2K/W m2K/W m2K/WAvailable capacity m3/h kg/h /h /h /h

Quality Filtered Treated

Filtered Treated

Remark:

Instrument Air Purge Air Nitrogen VacuumAbbreviation AI AP N2 VACTemp. Min. 5 °C 20 °C 5 °C °C 10 °C

Max. 30 °C 40 °C 40 °C °C 50 °CDew point (atm. cond.) -50 °C -50 °C -50 °C °C °CPressure Min. 5.0 barg 0.2 barg 6.0 barg barg 10 mbara

Max. 6.5 barg 6.0 barg 8.0 barg barg 50 mbaraAvailable capacity Nm3/h Nm3/h Nm3/h /h kg/h

Quality Filtered Free of oil/dust

Filtered Free of oil/dust

Filtered Free of oil/dust

Available: YES

NO

Remark:

Electric power supplyPower voltage :

Voltage Tolerance:Neutral available:

Frequency ± Tolerance:Available Power:

± %NHzkW

3x400V 1x230V ± 10% ± %

Yes No 50Hz ± 5% 60Hz ± 5% Hz ± %

Control voltage: 24VDC Emergency power available:

YES NO

UPS: Power: kW Diesel generator: Power: kW : Power: kW

Remarks


Seite 7 von 11


Seite 8 von 11

4. scope of BCT supply

SCOPE OF BCT

SUPPLY

Abb

revi

atio

n

Bas

ic E

ng.

Exte

nded

Bas

ic E

ng.

Det

ail E

ng.

Softw

are

Eng.

Eq

uipm

ent

Valv

ing

Pipi

ng

Inst

rum

enta

tion

Fiel

d C

ablin

gC

ontr

ol c

abin

etD

CS

Har

dwar

ePH

A S

tudy

( i.e

. Haz

op )

Ex Z

one,

1,

2 or

non

eSt

eel S

truc

ture

Phosgenation section APR -- 2Process Absorption section PA -- 2Caustic Soda dilution section CSD Product treatment section PT Solvent recovery section SR HCL recovery section HCl

PLANT LOCATION: Indoor Outdoor TYPE: Modular built Stick built

Motor Control Centre MCC Distributed Control System DCS YOKOGAWA

Emergency Shutdown System ESD YOKOGAWA PROSAFE HIMA

Remarks

5. DEFINITION OF EXPLOSION ZONE & PROTECTIONHazard Classification

Hazard Zone: Group:Temp. Class: 1-6

Zone 2 IIA IIB IIC T4

Hazard Zone (USA) Class- Division- Group-

EEx-Protection (Multiple options for valves & instrumentation, based on availability of corresponding Ex. Protection)

Drives & Motors e d de Solenoid valves e d i Instrumentation e d i p Remarks


Seite 9 von 11

6. STANDARDS & CODESApplicable Standard:

DIN ANSI Applicable Code & Regulation (Mechanical Engineering):

Druckgeräterichtlinie 97/23/EG AD 2000 Regelwerk ASME

Applicable Code & Regulation (Electrical Engineering): IEC NEC / NEMA

Applicable Code & Regulation (Explosion Protection): ATEX

Inspection Authority: SVTI TUEV Lloyds Stoomwezen

Remarks:

7. GENERAL DATA REFERENCE

PRICE:Offer Accuracy± 30 % Fixed Price SHIPPING INSTRUCTIONS:

Ex-Works Pratteln FOB CIF

ENGINEERING DOCUMENTATION:English German

Standard number of copies: Additional number of copies:For Approval: 2x Final: 3x

Remarks:

8. construction site & SITE CONDITIONSAvailable space: A & Measures: L x W x H & Max. admissible floor load: FLA = m2 L = m W = m H = m FL= kg/m2

SITE CONDITIONS:Amb. Temperature Min. / Average / Max. °C / / Relative humidity Min. / Average / Max. % / / Barom. Pressure Min. / Average / Max. mbara / / Annual rain fall Min. / Average / Max. mm / / Rain fall Max. during 10-15 min. mm Snow load Design kg/m2 Seismic intensity Max.

Max.Richter scaleAccelerationRated zoneStandard

Wind Max. Max. at 10 m height

m/s // km/hm/s // km/h

// //

N W S E NE NW SW SE

Remarks

9. Material of construction & design conditions


Seite 10 von 11

SCOPE OF BCT

SUPPLY

Abb

revi

atio

n

Material of construction for all parts in contact with the raw

material or the product

Des

ign

Pres

. ba

rg

Des

ign

Tem

p. °

C

Phosgenation section APR 6 100Process Absorption section PA 0 50Caustic Soda dilution section CSD Product treatment section PT


Seite 11 von 11

Solvent recovery section SR HCL recovery section HCl

Remarks

Questionnaire for Phosgenation Plants - JAAS（ … · Web viewPhosgenation section APR 6 100...

Documents

Transcript of Questionnaire for Phosgenation Plants - JAAS（ … · Web viewPhosgenation section APR 6 100...