Quantitative Analysis Summary Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Sequence TableData File Sample Name Sample Type Position Volume Level Acq Method File

BT06_LC1_PS_FS2g_isd1-

r001.d

is d3 Blank P1-A1 10 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

BT06_LC1_PS_FS2g_isd1-

r002.d

is d3 Blank P1-A1 10 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

BT06_LC1_PS_FS2g_isd1-

r003.d

is d3 Blank P1-A1 10 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

cal p1.d cal l1 Calibration P1-B1 -1 P1 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

cal p2.d cal l2 Calibration P1-B2 -1 P2 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

cal p3.d cal l3 Calibration P1-B3 -1 P3 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

cal p4.d cal l4 Calibration P1-B4 -1 P4 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

cal p5.d cal l5 Calibration P1-B5 -1 P5 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

cal p6.d cal l6 Calibration P1-B6 -1 P6 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

cal p7.d cal l7 Calibration P1-B7 -1 P7 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

QuantReport_ISTD_Complete_B_05_00.xlsx Page 1 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Summary Report

Data File Sample Name Sample Type Position Volume Level Acq Method File

SPe1-r002.d SPE1 Sample P1-C1 -1 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

SPe2-r001.d SPE2 Sample P1-C2 -1 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

SPe2-r002.d SPE2 Sample P1-C2 -1 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

SPe200-r001.d SPE 200ml Sample P1-C3 -1 20120410_LC1_PS_C1

8_pheno_FS4GH3200_

Atrazine_V10min.m

Quantitation ResultsTarget Compound ATRAZINEData File Compound ISTD Sample Type Response ISTD Resp Resp Ratio Final Conc Exp Conc Accuracy

BT06_LC1_PS_FS2g_isd1-

r001.d

ATRAZINE ATRAZINE-D5 Blank 707 2466924 0.0003 0.1017

BT06_LC1_PS_FS2g_isd1-

r003.d

ATRAZINE ATRAZINE-D5 Blank 2673 5360909 0.0005 0.1047

cal p1.d ATRAZINE ATRAZINE-D5 Calibration 19239 5052331 0.0038 0.1525 0.0100 1525.33

cal p2.d ATRAZINE ATRAZINE-D5 Calibration 46714 5462488 0.0086 0.2211 0.1000 221.06

cal p3.d ATRAZINE ATRAZINE-D5 Calibration 215765 5164173 0.0418 0.7011 0.5000 140.22

cal p4.d ATRAZINE ATRAZINE-D5 Calibration 405429 5080153 0.0798 1.2504 1.0000 125.04

cal p5.d ATRAZINE ATRAZINE-D5 Calibration 1629015 5516761 0.2953 4.3633 5.0000 87.27

cal p6.d ATRAZINE ATRAZINE-D5 Calibration 3151160 4669751 0.6748 9.8461 10.0000 98.46

cal p7.d ATRAZINE ATRAZINE-D5 Calibration 6173638 4432671 1.3928 20.2180 20.0000 101.09

SPe1-r001.d ATRAZINE ATRAZINE-D5 Sample 113624 1394644 0.0815 1.2745

SPe2-r001.d ATRAZINE ATRAZINE-D5 Sample 187713 2281187 0.0823 1.2863

SPe2-r002.d ATRAZINE ATRAZINE-D5 Sample 136054 1780318 0.0764 1.2015

SPe200-r001.d ATRAZINE ATRAZINE-D5 Sample 79971 2500942 0.0320 0.5595

QuantReport_ISTD_Complete_B_05_00.xlsx Page 2 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Calibration Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Calibration InfoISTD Compound ATRAZINE-D5

Calibration STD Cal Type Level Enabled Response Exp Conc RF

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p1.d Calibration P1 5052331 200.0000 25261.6564

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p2.d Calibration P2 5462488 200.0000 27312.4379

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p3.d Calibration P3 5164173 200.0000 25820.8650

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p4.d Calibration P4 5080153 200.0000 25400.7666

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p5.d Calibration P5 5516761 200.0000 27583.8029

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p6.d Calibration P6 4669751 200.0000 23348.7526

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p7.d Calibration P7 4432671 200.0000 22163.3557

Target Compound ATRAZINE

Calibration STD Cal Type Level Enabled Response Exp Conc RF

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p1.d Calibration P1 19239 0.0100 76.1606

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p2.d Calibration P2 46714 0.1000 17.1036

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p3.d Calibration P3 215765 0.5000 16.7125

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p4.d Calibration P4 405429 1.0000 15.9613

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p5.d Calibration P5 1629015 5.0000 11.8114

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p6.d Calibration P6 3151160 10.0000 13.4961

QuantReport_ISTD_Complete_B_05_00.xlsx Page 3 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Calibration Report

Calibration STD Cal Type Level Enabled Response Exp Conc RF

D:\MassHunter\Data\Franck\BT

06\120518_vendredi\cal p7.d Calibration P7 6173638 20.0000 13.9276

QuantReport_ISTD_Complete_B_05_00.xlsx Page 4 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 08:57 Data File BT06_LC1_PS_FS2g_isd1-r001.d

Position P1-A1 Sample Name is d3

Dilution 1 Sample Info

Inj Vol 10 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Blank Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.290 707 2466924 0.0003 0.1017

QuantReport_ISTD_Complete_B_05_00.xlsx Page 5 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 6 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 09:06 Data File BT06_LC1_PS_FS2g_isd1-r002.d

Position P1-A1 Sample Name is d3

Dilution 1 Sample Info

Inj Vol 10 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Blank Comment

Sample Chromatogram

QuantReport_ISTD_Complete_B_05_00.xlsx Page 7 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 8 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 09:29 Data File BT06_LC1_PS_FS2g_isd1-r003.d

Position P1-A1 Sample Name is d3

Dilution 1 Sample Info

Inj Vol 10 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Blank Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.127 2673 5360909 0.0005 0.1047

QuantReport_ISTD_Complete_B_05_00.xlsx Page 9 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 10 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 09:38 Data File cal p1.d

Position P1-B1 Sample Name cal l1

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Calibration Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.117 19239 5052331 0.0038 0.1525 1525.33

QuantReport_ISTD_Complete_B_05_00.xlsx Page 11 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 12 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 09:47 Data File cal p2.d

Position P1-B2 Sample Name cal l2

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Calibration Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.143 46714 5462488 0.0086 0.2211 221.06

QuantReport_ISTD_Complete_B_05_00.xlsx Page 13 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 14 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 09:56 Data File cal p3.d

Position P1-B3 Sample Name cal l3

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Calibration Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.130 215765 5164173 0.0418 0.7011 140.22

QuantReport_ISTD_Complete_B_05_00.xlsx Page 15 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 16 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 10:05 Data File cal p4.d

Position P1-B4 Sample Name cal l4

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Calibration Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.126 405429 5080153 0.0798 1.2504 125.04

QuantReport_ISTD_Complete_B_05_00.xlsx Page 17 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 18 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 10:14 Data File cal p5.d

Position P1-B5 Sample Name cal l5

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Calibration Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.120 1629015 5516761 0.2953 4.3633 87.27

QuantReport_ISTD_Complete_B_05_00.xlsx Page 19 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 20 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 10:23 Data File cal p6.d

Position P1-B6 Sample Name cal l6

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Calibration Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.121 3151160 4669751 0.6748 9.8461 98.46

QuantReport_ISTD_Complete_B_05_00.xlsx Page 21 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 22 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 10:31 Data File cal p7.d

Position P1-B7 Sample Name cal l7

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Calibration Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.127 6173638 4432671 1.3928 20.2180 101.09

QuantReport_ISTD_Complete_B_05_00.xlsx Page 23 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 24 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 10:40 Data File SPe1-r001.d

Position P1-C1 Sample Name SPE1

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Sample Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.120 113624 1394644 0.0815 1.2745

QuantReport_ISTD_Complete_B_05_00.xlsx Page 25 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 26 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 10:49 Data File SPe1-r002.d

Position P1-C1 Sample Name SPE1

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Sample Comment

Sample Chromatogram

QuantReport_ISTD_Complete_B_05_00.xlsx Page 27 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 28 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 11:02 Data File SPe2-r001.d

Position P1-C2 Sample Name SPE2

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Sample Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.174 187713 2281187 0.0823 1.2863

QuantReport_ISTD_Complete_B_05_00.xlsx Page 29 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 30 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 11:11 Data File SPe2-r002.d

Position P1-C2 Sample Name SPE2

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Sample Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.173 136054 1780318 0.0764 1.2015

QuantReport_ISTD_Complete_B_05_00.xlsx Page 31 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 32 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Batch Data Path D:\MassHunter\Data\Franck\BT06\120518_vendredi\QuantResults\18mai.batch.bin

Analysis Time 5/18/2012 11:32 AM Analyst Name merlier-PC\admin

Report Time 5/18/2012 11:34 AM Reporter Name merlier-PC\admin

Last Calib Update 5/18/2012 11:32 AM Batch State Processed2012-05-18T11:32:43.270858+02:00 2012-05-18T11:34:31.3122553+02:00 2012-05-18T11:32:43.2240579+02:00

Analysis Info

Acq Time 2012-05-18 11:20 Data File SPe200-r001.d

Position P1-C3 Sample Name SPE 200ml

Dilution 1 Sample Info

Inj Vol -1 Acq Method File 20120410_LC1_PS_C18_pheno_FS4GH3200_Atrazine_V10min.m

Sample Type Sample Comment

Sample Chromatogram

Quantitation Results

Compound ISTD RT Response ISTD Resp RR Conc Accuracy

ATRAZINE ATRAZINE-D5 5.177 79971 2500942 0.0320 0.5595

QuantReport_ISTD_Complete_B_05_00.xlsx Page 33 of 34 Printed at: 11:34 AM on: 12/05/18

Quantitative Analysis Sample Report

Compound Graphics

ISTD Compound ATRAZINE-D5

Target Compound ATRAZINE

QuantReport_ISTD_Complete_B_05_00.xlsx Page 34 of 34 Printed at: 11:34 AM on: 12/05/18