PROGRMSREPORT USEDFORRULLCONSTRUCTION · PDF filerapid rate, it also increasesthe weldcrack...

89
PROGRMS REPORT on F(( METALLURGICALQUALITYOFSTEEIJS USEDFOR RULLCONSTRUCTION by, C. E. SIMS,H. M. BANTAAND A. L. WALTERS BATTELLEMlldORIAL INSTITUTE UnderNavy Contract NObs-31.219 COMMITTEEQi SHIPCONSTRUCTION DIVISIONOF,ENG@JEEMNGANDINDUSTRIAL~EARCH NATIONALRI?aSEARCH COUNCIL Advisoryto BUREAUOF SHIPS,NAVYDEPARTMf!NT UnderContract” NObs-31t231 SerialNo. SSC-13 CopyNo. ~; L Date: Noveniber 17, 1%7 -.

Transcript of PROGRMSREPORT USEDFORRULLCONSTRUCTION · PDF filerapid rate, it also increasesthe weldcrack...

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PROGRMS REPORT

on

F((

METALLURGICALQUALITYOF STEEIJSUSEDFOR RULL CONSTRUCTION

by,

C. E. SIMS,H. M. BANTAAND A. L. WALTERSBATTELLEMlldORIALINSTITUTE

UnderNavy ContractNObs-31.219

COMMITTEEQi SHIPCONSTRUCTIONDIVISIONOF,ENG@JEEMNG AND INDUSTRIAL~EARCH

NATIONALRI?aSEARCHCOUNCIL

Advisoryto

BUREAUOF SHIPS,NAVYDEPARTMf!NTUnderContract”NObs-31t231

SerialNo. SSC-13

Copy No. ~; L

Date: Noveniber17, 1%7

-.

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NATIONALRJ&MRCH COUNCIL2101 ConstitutionAvenue

Washington,D. C.

November17, 191+7

Chief,Bureauof ShipsNavyDepartment:Jashington,D. C.

Dear Sir:

Attachedis ReportSerialNo. SSC-13entitledWetall.urdcslQualit:rof Steelsusedfor Hull Construction”.Thisrepo;thas been&bmitted by the contractoras a progressreportof the work done on Research?rojectSR-87underContractNObs-31219betweenthe Bureauof Ships,NavyDepartmentand Battel.leMemorialInstitute.

The reporthas beenreviewedand acceptancerecom-mendedby representativesof the Committeeon Ship Con-struction}Divisionof Engineeringand IndustrialResearch,NRC, in accordancewith the termsof the contractbetweenthe Bureauof Ships,NavyDepartmentand the NationalAcademyof Sciencesg

Very trulyyours,....,,: .....-, ,.,--,

,., ..- \ l(bk.3,.,,.,L\ ,(,Q $:(l-p..=-.,Enclosure

FrederickM. FeM~er,L%airmanDivisionof EngineeringandIndustrialResearch

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Preface—.,.

The Navy”Department~throughthe.Bureau..of 5~psto thoseagenciesand individualsthatwere activelysearchm’oaram.Thisre~ortrepresentsa ~ertof the

,- .,is distributingthisreportassociatedwith this re-researchwork contracted

for und& ;he sectiono> the I&vy1sdirec~ive‘Jtoinvestigatethe designandconstructionof weldedsteelmerchantvessels.’1

.,

,..,,,The distributionof this report.is .asfollows:

. . ,.. “copyNo. 1 - Chief,Bureauof Ships,’NavyDepar&entCopyNo.:2.- Dr. D. W. Bronk,‘hairrnan$National Research‘ouncil

Committeeon Ship Construction

CopyNo. 3,- V. H. bchnee,Chairrrian ,COPYNo. 4.:-J..L. Batescopy No. 5 - H. C. BoardmanCOPY No,, 6 - PaulFfield.Copy No. 7 - M~ A. GrossmancopyNo. 8 - C. H. Herty,Jr.CopyNo. 9- A. B. finzel. . .,copyNo.’10- J. M. Leesells . , .~~CopyNo. 11 - G, S. kikhalapouCopy No. 12,- J. OrmondroydCopy No. 13 - H. ~~.PierceCOpyNo. 14 - E. C. Smith ,:copyNoti15 - ‘r.T. WatsonCopyNo. 16 - Finn @nassen, Researchcoordinator

. .

F&mbe~sOf ProjectAdvisory.CorrrmitteeeSR-8?,SR-89,SR-92and.SR-1OO ,, :

CopyNo. 16 - Finn Jonassen, ChairmanCopyNo,,17 - R. H. !ibornCopy No. 18 - L. C. bibberCopyNo. 5 - H. J, Boar@nancopy No“ 6 - PaulFfieldCopyNo. 7 - M. A. GrossmanCOPYNO,, 8 - C. H. Herty,Jr.CopyiiO.19 - C. H. Jennings ~.:Copy No. 10- J. M. LesseZls ,.,CopyNo. 11 - G. S. MikhalajywCopy No. 12 - J, Ormondroyd :CopyNo. 13 - H. /. Pierce .. ~.:.CopyNo. 14 - E. C. bmithcopyNo. 15 - T. T,,Watson ...Copyi~o.20 - W. MO Wileon ,,

,,?,...

,:

..

,.

.s-,

CopyNo. 21 - A. G. Bissell,dureauof Ships,Liaisori:.’copyNo, 22 - E. M, h,acCutcheos,Jr., U. b. Coast,Guard,LiaisonCOpyNO, 23 - E. Rassman,.:Bureauof Ships,Liiieori:Copy No, 24 . Comdr.i, DO Schmidtmm, U. S. CoastGuard,LiaisonCC:pYNO. 25 - T, L. Soo-Hoo~Bureauof &hips,iiaisonCopyNo, 26 - JohnVasta,U. S. kritime Commission,Liaison

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...,,,..

copy~No, 27 -CopjNo, 28 -

COpY NO; 29 -CopyNo. 30 -copy No. 31 -CopyNo, 4 -COPYNo. 32 -Copy No. % -

CopyNo.33 -CopyNo. 3)+-Copy No.35 -eOpYNO. 24-COPY NO,36 -Copy No.37 -CopyNo. 3$ -Copy No, 22 -Copy No. 39 -COPY No, 26 -Copy No,,40 -COPYNo. 27 -CopyNo,.28 -COpy 1{0.16 -Copy No,,Al -CopyNo. 42 -Copy No, 43 -Copy No. 44-

Copj,No. 45 -copy No, 21 -CopyNo. /+6-CopyNo. 47 -Copy No. 4E -copy No. 49 -Copy No. 50 -Copy No. 51 -COpY NO. 52 -Copy No. 53 -Copies54 andCopy No. 56 -CopyNo. 57 -Copies58 andCopies60 and

R.i. Wiley,Bureauof Ships,“LiaisonJ, L, Wilson,Asi&ricanLi@au bf tihipping,Liai,son

Ship,$tructureC“timnittee,., :, ,., .

HearAdmiralEllisReed-Hill,USCG,LhairmanRearAdmiral!ha.rlesD. Vheelock,USN, Bureauof bhipsBrigadierGeneralPaulF. Yodnt,Jar DepartmentJ. L. Bates,,U,,.p. N,aritueCommissionD. P, Brown,,+ierican%reau of bhippingV. H, uchnee,Committeeon @@”Construction, Liaison”

Ship btructureSub-Committee”

CaptainL. V, Honsinfler,USN@ureau of.$Qips~G,hairmanCaptainR. A. Hi.nners,USN$ DavidTaylorModel,~as+,nComdr.R. H. Lambert,USN,Bureauof SiiipsComdr.R. D. Schnidtman,USCG,U. S. Coast,GuRTd‘FleadquirtersCol. ‘/ernerJ. ltoore,USA, OfficeChiefof ‘1’ran5pOrtati0n,‘!~ar’Dept.HubertKempel,,OfficeChiefof Transportation,jar..DepartmentMathewLetich,Americandureauof Shipping,, ,,,,,E. hi.hacCutcheon,Jr., U. b. CoastGtirdHeadquartersR. M. ‘~obertson,Officeof Navalltesearofi,USN ;JohnVasta,U. ~. haritirneComni.ssion ,,1. J. ‘danless,U. b. haritimeCommission~~~R. d. Hiley,$ureauof Ships,USN ,,.,,:, ,,:J. L, /ilson,&nericanBureauof &hippingFinn Jonassen,LiaisonRepresentativej NRCd..H. .DavidsonJ IiaisonRepreseut,ative,AISIPaul Gerhart,LiaisonRepresentative,AISI!tin,Spraragen,LiaisonRepresentative,l“i?CWm. ~. ‘!ilson,TechnicalSecretary

NavyDepartment.

Comdr.it.S, MndeLkorn, USN,NavaLAdministrativeUnitA. G, Bissel.1,Bureauof Ships ~~~J. u. Jenkins,Bureauof Ships .-,.NoahKahnjNew York NavalShipyard .,~~.~1‘ ~ ;I. E. Kramer,Officeof NavalHeee$xch . .,;OB.,OsgoodjDavidTaylorliodeldaki.n ~ . ~,,N. d. Promisel,Bureauof AeronauticsK. D. !illiams,Bureauof bhips ~~NavalAcademy,PostGraduatebchool :,NavalResearchLaboratory55- U. S. NavalEngineeringExperiment.StationNew YorkNaval$h}pyard,MaterialDivisidnPhiladelphiaNavalShipyard” .’59 - Wol.ications,Board,NavyDept,via Bureag..of Ships,Code33Oc61 .-.TechnicalLibrary,Bureauof ~hips,Code337-L

. ...——

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U, S,,CoastGuard

Copy No. 62 - Capta,ind. ~3,LankjJr., USCGCopy No. 63 - CaptainG.,A.Tyler,USCGcopy NO. 64 - Testitig&nrlDevelopmentDivis,ion. . .

U. 5. MaritimeCotission

Copy No. 65 - E. 6. Martirisky

Representativesof AmericanIronand SteelInstituteCommitteeon ManufacturingProblems

Copy No. 66 - C. Ivi.Parker,Secretary,GeneralTechnicalUorumittee,AmericanIronand bteelInstitute

CopyNo. 18 - L, C. aibber~ Carnegie-IllinoisSteelcorporationCopyNo. 8 - C, H, Herty,Jr.,BebhlehemSteelCompanyCopyNo. 14 - E. C. Smith$RepublicSteelCorporation

WeldingResearchCountil

CopyNo, 67 - C. A. Adams CopyNo. 69 -LaMotteGroverCopyNo. 68 - EverettCiiapman copyNoo 43 - ‘dn.hpraragen

— .

Ccp~,NO.,70 - F. h. Feiker,ChairmenjDivisionof Engineering& IndustrialResearch,NRC

COPYNo. 71 - Clyde~Jilliams,Chairman,Commi.ttee on EngineeringMaterialsCopyNo. 3 - V. R. rxhnee,dhairman,(kromi.tteeon Ship ConstructionCopyNo. 16 - Finn Jonassen,ResearchCoordinator,Committeeon Ship Constructm~CopyNO. 44 - “,~m.G, ,(ilson,TechnicalAide,Committeeon Ship constructionCopyNo.,72 - C, E. Sims,Investigator,i{esearchProjectW-87CopyNo, 73 - H, M, Banta,Investigator,ResearchProjectSR-8’7CopyNo, 74 - A. L. “alters,Ii’westigator,ResearchprojectSR-~CopyNo. 10 - J, b!,Lessens, Investigator,ResearchProjectSR-101COpyNo. 75 - ScottB. Lilly,Investigator,ResearchProjectSR-98CopyNo,,76 - C. H..Lorig,Investigator,ResearchProjectSR-97CopyNo, 77 - J. R.,Low, Jr,, Investigator,ResearchProject SR-96Copj-1[0.78 - AlbertWller, Investigateor, ResearchProject SR-25CopyNo. 79 - E,,R. Parker,Investigator,ResearchProjectSR-.92CopyNo, 80- GeorgeSachs,Investigator,ResearthProjectSR-99Copy No. 81 - C. J. Voldrich,Investigator,ResearchProjectSW1OOCopyNo,.82 - ClarenceAltenburger,GreatLakesSteelCompanyCopyNo, 83 - A. d. Bagsar,Sun Oil CompanyCopyNo, 84 - E. L, Cochrane,MassachusettssInstituteof TechnologyCopj,NO, 85 - GeorgeEllinger,Nationaldureauof StandardscopyNO, %6 - kaxwell(kmsamer,Carnegie-IllinOisSteelCOrpOrationCcpyNo. 87 - S. L. Hop.,BattelleivranorialInstituteCopyNo, 88 - BruceJohnston~ LehighUniversitycopyNO,,89 . N,.M. Newmark [k:..:ersity of Illii)oiSCopyNo. 90 - L. J. Ftohl,Carncg:!e-IllinoisSteelCorp.

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copy NO. 91 - “:’1,P. noopjDivisionof Engineering,SwarthmOreCOllegeCopies92 thru116 - 1. G. Slater,britishAdmiraltyDelegation ,copy No. 117 - ‘frarmportationCorpsBoard,Brooklyn,N. y.Copies118 thru 122 - Libraryof Congressvia Bureauof bhips,Code330cCopy NO. 123 - File Copy,Committeeon bhip constructionCopyNo. 12/+- NACA,Committeeon MaterialsResearchCoordination,USN

COPY NO, 125 -COPYNO. 126 -COPYNo, 127 -Copy No. 128 -CopyiiO,129 -CopyNo. 130 - ‘Copy No. 131 - “COpyNo. 132 -copyNo, 133 -copy No. 134 -copy No. 135 -CopyNo. 136 -CopyNo. 137 - -COpyNo. 138 -CopyNo. 139 -copyNo. ll+o-copyNo. 141 -COpyNo. lk2 -copyNo. 143 -copyNo. 1!+/+-CopyNo. 1!45-copy No. 146 -copy No. 14’7-copy No. 148 -copyNo. 149 -CopyNo. 150 -

,,

Copies125 thru 150 - rhu-eai“of

(TotalNo, of copies- 150)

.,

,..

Ships

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011

NAVY RESEARCHPROJECTNObs 31219

)ME’I’AJ.LuRGICALQUALITY OF STEELSUSED FOR

HULL CONSTRUCTION

by

C. E. Sims,H. M. Banta,and A. L. [Walters

BATTELLE MEMORIAL INSTITUTE

May 31, 1947

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TABLECF CONTENTS

NW! AR Y..,....

INTRODIJCTIOii. . . .

EKPERIMENTAL WORK . .

. .

. . . . . . . . .

. . . . . . . . .

. . . . . . . . .

. . . . . . . . . . . . .

. . . . . . . . . ...>

,. ..,. . . . . . . .

A Studyof the Influence of Chemical Composition . . . . . .

Preparationof LaboratoryHeats .

TensileProperties . . . . . . .

Effectof

Effectof

‘SffeOtof

Effectof

Effectof

Effectof

UnderbeadWeld

Effectof

Effectof

Effectof

Effect.of

Effectof

Effectof

Carbon Content . .

Manganese Content

Silicon Content .

Molybdenum Content

Vanadium Content .

Aluminum Content .

Crack Sensitivity

Carbon Content .

Manganese Content

Silioon Content .

Molybdenum Content

VanadiumContent

AluminumContent

[email protected] Properties .

Effect of Carbon Content .

Effsctof ManganeseContent

Effectof SiliconContent .

Effect of 1.5olybdenumContent

., ..>... .>.

.. ”.., . . . . .

. . . . . . . ..’.

. . . ...” . . . .

. . . . . . . . . . .

. . . . . . . . . . .

. . . . . . . . . . .

. ...=.. . . . .

,, . . . . . . . . .

Page

1

4

5

5

5

6

8

8

12

12

12

16

16

. . . . . . . . . . . . 16

. . . . . . . . . . .

. . . . . . . . . . .

. . . . . . . . . . .

. . . . . . . . . . .

. . . . . . . . . . .

. . . . . . . . . . .

. . . . . . . . . . .

,!, . . . . . . . .

. . . . . . . . . . .

. . . . . . . . . . .

16

20

20

20

20

24

24

29

29

29

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TABLE OF CONTENTS (Continued)—.

. .

Effectof VanadiumContent. , . . . . , . .. . .

Effect.of AluminumContent. . . , . , . . ,. . .,. .,

Wandard-(;onpositionIieats. , . . . . . , .

A Discussion cf the Siguifiw.nce of the Test Data

The Influence of .41ummum Content Upon the. . ~je~har,i.ca.iproperties Norma].to the ?late surface

Tensile Properties Normal to Plate Surface .

. .

. . .

.,.

. . .

.,<

,,.

Notched-Bar Impact Strength Normal to the PlateSurface ..:...... . . . . . . . . . . .

FUTURE WORK ..,.,... . . . . . .. . . . . . . . . . ,,,. .

APPENDIX A . , . . .

. .

.,,.

. .

,,.

,..

.,,

. .

,.

,,.

.

. .

,.

.,,

. . .

,,

. .

. ..

Page

36

3$ ,‘“I

36

50

51

55

55

60

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TABJ.I!CF COITLWNTS(Continued).——. —..

,

Figures——

Figure 1.

Figure2.

Figure3.

Figure4.

FiCure5,

F’igure6.

Figure7’.

Figure8.

Figure9.

Figure10.

Figure11.

Figure12.

Figure13.

Figure14.,.

Figure15.

Figure16.

Figurei7.

Relationship betweenyield strength . . .

Relationship betweenand yield strength .

Relationship betweenyield strength . , .

Relationship betweenand yield strength .

Relationship betweenand yield strength .

The effect of carboncrack sensitivity .

The effectweld crack

The effectweld crack

The effectweld crack

The effect

carbon content and tensile and. . . . . . . . . . . . .*. ,

manganese content and tensile. . . . . . . . . . . . . . . .

silicon content and tensile and. . . . . . . . . . . ..s. .,

molybdenum content and tensile. . . . . . . . . . . . . . . .

vanadium content snd tensile. . . . . . . . . . . . . . . .

content upon the underbee,dweld. . . . . . . . . . . . . . .“

of manganese content upon the underbeadsensitivity . . . . . . . . . . . . . . .

of silicon content upon.the underbeadsensitivity . . . . . . . . . . . . . . .

of molybdenum content upon the underbeadsensitivity <..... . . . . . . . . . .

of vanadium content upon the underbead weld

Page

e 10

. 11

. 13

. 14

. 15

. 18

. 19

. 21

. 22

crack sensitivity . . . . . . . . . . . . . . . . . .

The effect of aluminum content upon the underbead weldcrack sensitivity .,. . . . . . . . . . . . . . . .

Notch-bsr impact properties . . . , . .. . . ,,. . . .

Notch-bar impact properties . . , . . . . , . . . . .

!Jotah-barimps.ct properties . . . ,,, . . . . . . . ,,

Notch-bar impact properties. . .. . . . . . . . . . . .

\totch-barimpact ‘proper’ties’. . . . . . . . , . . . .

\Totch-bar’impact properties . . . . . . . . . . . . .

. . .

23

25

26

27

28

30

31

32

.—

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TABLE OF CONTEY’TS(Continued)--- — ..—.— —.

Page—.—

Figure.18. Notch-barimpactproperties.. . . .,. ... ... . .,. . 33. .

Fi#ure19. Notch-bar impact properties . t . . .“. , . . . . . . 34

Figure 20. ltotch~’oe.r,impo.ct properties . . < , . . , ‘. , , . , . 35—..

‘Figure’21, .Nobch-.barimpact properties . . . . . . . . . . . ,.. 3?,., ,., .

Figure 22, Notch-bar impact properties . . . . . . . . , . i . . 38;.. ,

Figure 23. Notch-bar. imrpe.ct propert~es ~ . , . . . . . ; . . , . 39

Figure fi4.’”Hotck-.barimpactprope?.ties ~ . . . . . . ~ . . . . . 40. . .

Figure 25.

Figure26..

Figure2?..,.

Figure28.,..

Figure 29.,,, .

‘Figure 30.

Figure 31.

Figure32.

Figure 33.. .

,,.

Figure 34..

‘ “ ‘Figu~-e35.

Figure36.

Notch-bar imps.c-kproperties . . . . . . * . . . . . . 41

Notch-bar impact properties . . . . , ., . . . , . ,

The effect of carbon content LWCm the n.etched-htirimpact strength at 75”F, . . . . . . .’. . . . ~ .

The effect of!manganese content upon the nctch~d-barianpaotstrength at 75”F. . .. 0 . . .’. . . . . .

The effect of silicod content ,uponthe notched-barimpact strength at 75°F. . ~ . . . . . . . . . . .

The effect of ?nol?~bdemunconteut upon fhe notched-barimpact,streagth ?.t75°”F. . . . . . .“, . . ~~. . ,

The effect of,vz+.nadiumconteni upon the notched-barimpact strength at 75”F. . . , . . , . . . . . . .

The effect of:atuminum content upon the notched-barimpo.ctstrength at -40”F. . . . . . . .“. . . . . .

,. .,, .,

An illustration of the procedure used for nmking thespecimens t~ determine the tensile properties normaltothe plate surface... . . . . . . . . . . . .. 52

Notched-barsurface , .

Notched-barsurface . .

Notched-barsurface . .

imp~.ct strength normal to the plate. . . . . . ., .,., . . . ... ... . . 56

impact strength normal to the plate.s, ... . . . . . . .. ’..> .?. 57

impact strength normal to the piate. . . . . . . . . . . . . . . . . . . . 58

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TABLE OF CONTENTS (Continued).— ,— —.—.

Tables

Page

Table 1.

Table 2.

Table 3.

Table 4.

Table 5.

Table 6.

APPENDIX A

Table Al.

Table A 2.

Table A.3.

Table A4.

Outlineof laboratorybeetsmade to study the influenceof chemical composition . . . . . . . . . . . . . . . . 6

Chemical analysis of laboratory heats . . . . . . . . . 7

Tensile properties of hot-rolled plate from laboratoryheats . . . . . . . . . . . . . . . . . . . . . . . . . 9

lJnderbeadweld cracking indexes for Heats X.-1to X-28,X-45 and x-46 in the hot-rolled condition . , . . . . . 17

Chemical analysis of laboratory heats made to study theinfluence of aluminum content . . . . . . . . . . . . . 51

Tensile propertied normal to the pl?te surface . . . . . 54

Tensile propertiesHeats .X-1to x-28,

Underbead Orur,king

of hot-rolled plate from laboratoryinclusive, X-45 and x-46 . . . . . . 6(3

values of individual specimens fromlaboratory Heats X.-1to X-28, inclusive, X-45 and X-46inthehot-rol led state . . . . . . . . . . . ,,, ...61

Longitudinal notched-bar impact properties of laboratoryIieatsx-1 to x-28, inclusive,X-45 snd x-46 in the hot-rolled state. All specimens notched parallel to theplate surface.,.... . . . . . . . . . . . . . ..62

Notched-bar impact properties ndrmal to the plate surfaceof Heats X-23 to x-26 in the hot-rolled state , . . . . 63

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PRCGRESS RiiP;RT

on

F,rom:

Report

NAVY RESHARCH PROJECT NObs 31219

METALLURGICAL QUALITY OF STEELSIJSEDFOR

HULL CONSTRUCTION

May 31, 1947

BattelleMemorialInstitute

PreparedBy:H. N. BantaA. L. Walters

C. E. Sims,Supervisor

s~\~r~y.! —.—

In orderto obtaindefiniteinformationconcerningthe relation-

shipsamongchemicalcomposition,underbeadweld cracking,and the

mechanicalproperties,,especiallythe tensileand.notched-barimpact

characteristics,a seriesof 30 laboratoryheats ~~a~made and studied

in,the hot-rolledstateto determinethe individualinfluenceof each

of the following constituents when varied.over a range sufficientlY

broad to definitely establish the trend of the,effect; carbon, manganese,

silicon, molybdenum, vanadium, and alminw.

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-2-

For a standardchemical composition, a typical HTS analysis was

selected,and the elements studied were then varied one at a time in this

standard composition.

This investigation revealed that the oarbon content should mast

probably be limited to 0.15-0,20 per cent as above this value the crack

sensitivity increases with marked rapidity which is entirely out of line

with the increase in tensile and yield strength. Increased carbon

content was also accompanied by a reduction in the notched-bar impact

strength.

While manganese increases the tensile and yield strengths at a. ...,,,

rapid rate, it also increases the weld crack sensit.iyityit A rapid rate.

One advantage of manganese is that it is @ appreciable,,detrimentalto

the notched-bar impact strength in the temperature range of -70°F. to

21O’F.

I:fiilesilicon contents above that normally used in H’fSsteel did

aPPear tO Offer sOme advantages Over plain carbon-manganese steels for

obtaining slightly higher yield strengths tindlow underbead cracking,

silicon is not comparable with either molybdenum or vanadium for this

purpose.

‘The’use of either m~lybderiumor vanadium appeared to be the most,,. ,’promising jeans ‘ofincreasirigthe tensile aridyield strengths without

., ..,.. ,,marked detrimental effects upon the

,,, ,~i

However, both of these alloys ioweri,; . .

an ‘appreciabledegree,especially at., ’., :,,~

degree OF underbead cracking..,;

the notched-bar impact strength

room temperature and lower.

Data from s.single 6cries of heats in which the’aluminum

qddition was varied from c to & pounds per ton indicated that the

to

aluminum content is an important factor in establishing the underbead

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-3-

weld crack sensitivity. The steels made with low and medium amounts of

aluminum were quite craclcsensitive as compared with the steels contain-

ing no aluminum or a very large aluminum content, such as that obtained

by an addition of 5 pounds per ton. Since this wide sluminum range has

not been previously investigated, it will be necessary to confirm these

resuits with additional data.

An aluminum addition of about 2 pounds per ton, .064 per cent

acid-soluble aluminum content in the steel, was found to have the most

beneficial influence upon the notched-bar impact strength. This effect,.

was especially noticeable at low temperatures.

NO relationship was found between the tensile

plate normal to the surface and the aluminum content.

made on commercial plate revealed a good

content and the properties normal to the

in behavior of the laboratory steels and

propertiesof the

A previousstudy

correlationbetweenaluminum

plate surface. This difference

the commercial heats may be

caused by the large difference in the amount of reduction between ingot

and plate, the directional properties being amplified.by the increased

reduction of the commercial product.

The notched-bar impact properties normal to the surface were all

found to be quite low as comparedwith the longitudinal properties. As

in the case of the longitudinal tests, the steel made with an aluminum

addition of 2 pounds per ton displayed the highest notched-bar impact

strength when tested normal to the surface.

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IWIRODtiC?ION.,; , —

The previous work ofithis project has been confined to an

investigation of the mechanical properties, metallurgical characteristics,

and the underbead cracking tendencies of HTS steels that have been used

in welded naval construction. Briefly, the range “ofchemistry covered

was,from 0.14 to 0.23 per cent carbon and 0.S1 to 1.53 per cent manganese,

together with small additions of titanium or mnadiu?? or both. This

range represents about the extreme limits found in commercial steels Of,:

this grade.

In the past,the summation of the carbon, menganese, and other

alloys has been defin.itelylimited because of underbead cracking..

Recent work on this project has revealed that the total alloy content..

of the steel may be relatively high without being detrimental to the

‘tve,ldingcharacteristics, especially underbead cracking, provided the

steel has been homogenized to reduce or eliminate alloy segregation.

This provides a means for using a higher alloy steel with resultant

higher strength which is not susceptibleto underbeadcrackingunder

normal welding conditions.

The purpose of this phase of the investigation is to determine

the influence of chemical compositi~i covering a muoh widerrangethan

foundin the commercialHTS steels. The ultimate object is to find the

composition which will

euffioiently low level

ship construction.

give the highest yield strength and still have a

of crack sensitivity to be satisfactory for welded

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-5-

,,

EXPERIML’NTJLWORK—— .— -—

A Studyof the Influarnceof ChemioalComposition.—

Preparation of Laboratory Heats—.—

Previous work on laboratory heats has shown that in the case of

small induction furnace heats, it was.necessary, to increase slightly the

carbon and manganese oontents in order to obtain the average level of

underbead cro.ekingnormslly found in commercial HTS steels. It wS.S

found that laboratory heats containing 0.21 per cent carbon and 1.32 per

cent manganese were quite suitable for investigationalpurposes as these

steels cracked well within the limits of the weld crack-sensitivitytest

conditions used for conraercialsteels. Using this approximate analysis

as a standard for comparison, a series Of”30 induction furnace heats

were made to study the influence of carbon, mangs.nese,silicon,

molybdenum, vanadium, and aluminum ooritentsupon the welding oharacter-

istios and mechanical properties. These heats consisted of 450-pound

melts deoxidized with an addition of 0“”.4pound of aluminum per ton of

st’eel,with the exception of .!”ixheats made to study the effect of

aluminum additions ranging from O to 5 pounds.

The steel was cast into two ‘6-5/8-inch-squareingots and sub-

sequently’processed by forging from a temperature of 2200”F. to 2300°F.

to 2 by 5-inch slabs. ~oilowing ~eheatin.gto 2200°F., the slabs were

hot rolled to l-inch plate in six passes. The finishing temperature

after rolling was approximately 1750”F. The plates were stood on edge

and allowed to air cool as in normalizing. By processing each ingot in

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-6-

this manner, a uniform hot-rolled conditionwas produced throughout the

seven lots of steel.

‘8-inch

plate,

The heats made with various aluminum contentswere cast in 8 by

ingots and reduced by hot rolling on a oomneroial mill to l-inch,..

the reasons for which will be discussed later.

A brief outline of the heats under consideration is shown in

Table 1 which lists the group and heat numbers, the elements bein~ —

investigated,and the range through which

The complete chemical analysis of

Table 2.

TABLE 1. OUTLINi OF LABORATORYINFLUENCE OF CWWCAL

the elements were varied.

all thirty heats is shown in

HEATS MADE TO S’flJDYTIDICOMPOSITION

,———.- — —

Group , Element Being Range CoversdNo. Heat No. in Group Investigated

.—— ___in Per Cent

..—.— ———

1 X-1 to X-5, incl.’ ““,. Carbon 0.17 to 0.32

2 X-6 to X-9, incl. Manganese 0.93 to 1.51

3 X-10 to X-13, incl. Silicon 0.41 to 0.92

4 X-14 to X-18; incl. Molybdenum 0.10 to 0.43

5 X-19 to X-22,“incl. Vanadium 0.04 to 0.29

6 X-23 to x-28, incl. A.luminurn O to 0.18

7 X-45 to X-46, incl.(S%aniiardcompositionfor comparison —purposes)

— —.—- .— — -

‘.

Tensile Properties

Standard O.505-inch threrided-endtensile specimens were machined

from the center of the plate, duplicate specimeng being prepared in both

the longitudinal and transverse directions with respect to rolling. The

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-’7-

TABLE 2. CHEIIICM +INA+,ysIsOF L.4BG~AToRYHWTS

——._.— ..-— —.—. —

Heat,No. C ],m P.. s Si. Ti MO v Al*,— —.-.. —.

(Group 1)

x-1 0.17x-2 0.20x-3 0.25x-4 0.28x-5 0.32

(Group2)X-6 0.21X-7 0.19X-8 0,.22x-9 “0.21

(.Group3)x-lo 0.21X-n 0.21X-12 0.19X-13 0.20

(Group4)X-14 .0.22X-15 0.21X-16 0.23X-17 0.23x-18 0.24

(Group5)X-19 0.21x-20 0.20X-21 0.20x-22 0.21

‘(Group6)X-23, 0.20X-24 0.23X-25, 0.22X-26 0.22x-27 0.20X-28 0.22

,,.“(Group7) ‘:’ ‘,.:X-45 .0.21

X-46 0.22

1.361..3.01.361.421.26

0.931.221.371.51

1,301.371.391.31

1.451.491.291,321.37

1.271.301.291.28

1.251.361.241.311.291.26

.,

1.351.35

.023

.021

.022

.022

.022

.021

.023

.023

.023

.025

.024

.023

.024

.023

.020

.023

.020,023

,020.021.020,020

.021

.019

.020

.021

.018

.019

.021

.023

.024

.023

.023

.020

.020

.022

.016

.018

.018

.018

.019

.018

.019

.019

.@20

.022

.020,020

.019

.020

.019

.020

.02;

.02’1

.020

:021,020.020

.030

.032

0.310.250.290.220.22

0.270.280.290.29

0.410.550.790.92

0.300.350.280.300.29

0.3200300.+300.29

0.270.290.270.270.310.27

0.270.28

.014

.001

.014

.014

.013

.010

.011

.012

.011

.012

.012

.011

.010

.025

.012

.012

.012>014

.013”

.016

.014,018

.007,006.013.016.015.015

.015

.015

.

-.

0.100.120,240.320,43

,-

.

.

.

.,

0.04 -0.08 -0.19 ..0.29 -

Nil<.005<.005.029.064

-. ;C 0.180

-- .003.- .003

* Acid-soluble aluminum contentHeats X-1 to X-22, inclusive,madewith an additionof 0.4 lbs. aluminum per ton.

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,

.,

yield strengthwas determined

loadat 0.2 “per””cent offset.

-8-

frOm the

The data

in Table 3 “iwhi”ohlists the average of the duplicate tests. The complete

str,osk-straindiagram using the

from these tests are .smmnarized

data are listed in Table 1 of App~ndix A.

,,

Uffect of Carbon Content.‘ The influence of carbon content in the

range of 0.17 to 0.32 per cent upon the‘tensileand yield strength is

shown graphically in Figure 1. This figure reveals that as the carbon

is raised ,from0.1.7to 0.32 per.cent, the longitudinal yield and tensile.

strength increased progre~sively from approximately 45;000 p.s.i. to

55,000p.s.i. and the tensilestrengthfrom 71,000p.s.i. to 90,000p.s.i.

This increase in strength was accolT,panied,by the usual decrease in

ductility as indicated ‘bythe elongation and reduction in area.

A comparison of the transverse and longitudinal properties

revealed the expected lower ductility in the transverse direction. There

yas alsd a tendenc~-for slightly lower yield and tensile strength in the

transverse direction, but in most cases, the”difference can not be con-

sidered significant. J,similar,difference in directional.properties was

noted throughout all thirty heats.

The Effect of Manganese Content. Figure 2 illustrates the—“—. —

influezioeof manganese in the range of 0.93 to 1.51 per cent upon the

tensile and yield strength. .Asthe manganese is increased from 0.93 to

1.51 per cent ,’the longitudinal yield strength increased progressively

from approximately 39,000 p.s.i. tG 48,000 p.s.i., and the longitudinal

tensile strength from 70,(?00p.s.i. to

strengths were found in the transverse

77,000 p.s.i. A similar trend and

direction. ,,.

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-%

TA.BLE 3. TENSILE PROPERTIES CF HCT-ROL,LiDPLiWIEFROMLABORATORY HEATS

-—. -————————.—————— . ——_.._._

Elong.in Red. in Yield TensileRest Test 2 Inches, fires, Strength,No. Direction “$

Strength,?; p.s.i. p.s.i.

—-.—..——. .—. c

(Group 1)x-1

f!

x-2!!

:x-3!!

,x-4!1

x.5II

(Group,2)&6

f!

X.-7It

X-8t%

2$-9t,

(GrouP.,3)x-loIt

x-n!1

i-12t,

X-131!

I,on~.Trans.

Long,Trans.

Long.Trans.

Long.Trans.

Long.Trans.

Long+Trans.

J,ong.Trans.

Long.‘Trams.

Long.Trans.

Long .Trans.

. Long.Trans.

Long.

Trans.

Long.Trans.

37.331.5

36.032.8

31.829.5

30.927.8

28.526.5

35.532.0

34.829.9

35.630.0

34.831.6

34.932,3

33.229.7

33.028.8

33.030.5

74,562.1

68.963.0

67.061,1

67.556.4

64.852,4

66.556.2

8s.658,3

70.559.2

‘.72.159.6

69.760,2

68.660.7

68.556.9

66.059.6

45,63044,750

44,25041,630

47,36046,250

51,00048,750

55,00049,360

39,13039,630

44,63043,130

46,75044,500

48,38046,380

47,63044,130

50:88046,630

52,50051,000

49”/75049,250

71,38072,400

74,60073,680

81,55060,200

66,85086,450

69,80087,280

70,15069,500

73,45071,900

77,35075,950

77,18077,650

78,45076,300

80,00079,600

65,45083,630

83,95083,200

—.—

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-9a-

TABLE..3. (Corrtinued)

Elong. in Red,,.,in Yiel,d TensileHeat Test 2 Inches, Area? Strength,No,

Strength,Direction $~.-.— — -— ._____ $ —p.s.i. p.s.i,

(Gro’up’4)x-14If

,,

31.8 66.928.8 58.6

Long,Trans.

50,63046,000

51,38048,880

56,00056,750

68,63066,250

78,250‘75,880

80,00079,050

81,40080,950

82,25082,650

98,63093,610

99,49097,280

79,60078,100

84,20082,450

93,53092,550

1o5,130100,400

74,90073,800

82,23081,850

77,38076,380

79,65079,980

~-15,,

31.8 64,128.8 58.3

Long.Trsns.

‘X-16U

Long.Transo

29.0 63.224.1 55.2

X-17H

Long.Trans.

24.0 63.020.9 49.7

X-18II

Long.Trans.

22.0 62.620.8 53.5

(Group 5)X-19,1

Long.Trans.

32.4 65.829.5 59.0

,49,13047,750

56,68054,000

66,68064,630

78,50073,880

X-20ff

I,ong.Trans.

32.6 67.827.3 59.5

27.0 61.123.0 52.4

X-21II

Long.Trans.

“ x-22If

,,

Long.Trans.

25.3 59.420.3 48.8

(Group G)X-23,1

Long.Trans.

34.5 66.429.3 52.2

47,50045,750

ko,88049,360

47,75046,380

49,63049,380

.A.-_L_”__

X-24II

31.3 64.527.8 50.7

Long.Trans.

‘X-25M

Long.Trans.

33.0 ““68.227.6 54.1

X-26,1

Long.Trans,

33.0 68.126.8 53.3

...,..,

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-91J-

TAFII,E3. (Continued)

—.— “——. —___ .

Elong. in Red. in Yield Tensile]~e~t Test 2 Inches, Area, Strength, Strength,,No. Direction % % p.s.i. p.s.?>

—.——. — ., .—..—

x.-27 Long. 33.5 69.6 48,250 76>6001! Trs.ns, 26.3 56.9 45,750 75,980

x-28 Long. 33..5 68.7 48,380 77,750It Trans. 28.5 55.9 46,880 75,800

(Group 7)X-45 Long. 33.8 67.2 52,100 79:100II ‘lrans. 23,8 35.7 48,880 75,950

X-46 Long. 35.0 70.1 50$750 80,30011 Trans. 28,0 51.2 52,000 79,~3(J

— ——.—==_—--—. ,—===—-—--- :===— -.— —.—

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-10-

-1

● ~ollp I HEATS

100 — D STANDARD COMPOSITION HEATS

90 —

80 —

70 —

60 —

50- ●Y”●

40.15 .20 .25 ,30 .35

GARBON CONTENT -IER CENT

FIGURE i . RELATIONSHIP BETWEEN CARBON CONTENT

AND TENSILE AND YIELD STRENGTH

0-6412

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-11-

90

80

,

: 60zwat-tn

50

40

30

● GROUP 2 HEATS

o STANDARO COMPOSITION HEATS

o0

.s0 1.10 I .30 1.50

MANGANESE CONTENT-PER CENT

FIGURE 2. RELATIONSHIP BETWEEN MANGANESE

CONTENT AND TENSILE AND YIELD STRENGTH

0-5413

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-1,2-

The increased manganese content did not decrease the ductility

as indicated by the reduction of area snd elongation in both the longi-

tudinal amd transverse directions. ihile there was a slight increase in

the reduction of area in the longitudinal direction with increased

manganese conteut, this change was not enmgh to ‘beconsidered signifi-

Carlt.

The Effect of Silicon Content. The long itudinal tensile data..—. ————

from the four heats made to study the influence of silicon content are

shown in Figure 3. From this figure it will be noted that the silicon

content in the

upon the yield.

slight.

In the

influence upon

range of about 0.30 to 0.90 per cent he.s little influence

strength and the effect upon the tensile strength is only

range investigated, the silicon content had no perceptible

the elongation or reduction in area.

Effect of Molybdenum Contex,t. The marked influence of molybdenum—, ——.. —.— .— —,.-.

content upon the longitudinal yield and tensile strengths is show in

Figure 4. By increasing the molybdenum content from 0.10 to 0.43 per

cent, the yield strength was raised from approximately 51,000 p,s,i. tO

78,000psi. and the tensile strength from 57,000 psi to 99,000 psi.

This incrw.sein strengthwas ficcompcniedwith the usual

decreasein elongationand reductionin &.rea.

The Mfect of Vanadiumcontent. Figure5 revealsthatthe

increasein longitudinalyieldand tensilestrengthproducedby the

additionof vanadiumwas evenmoremarkedthan thatof molybdenum. By

increasing the vanadium content from O.04 to O.29 per cent, the yield

strength was raised from 49,000 p,s.i. to 78,000 p.’s.i:j,and the-tensile

strength from 60,000 p.s.i. to 104,000 p.s.i. With this

.—

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-13-

100

0

9C

o00

6(

5(

● GROUP 3 HEATS

o STANOARD COWQSITION HUTS

-,!TENSILE STRENGTH

�✚✍●

YIELD STRENGTH

,?0

SILICON CONTENT- FER CENT

FIGURE 3 . RELATIONS 1P BETWEEN SILICON CONTENT

AND TENSILE AND YIELD STRENGTH

0-s414

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-14-

100

90

:

~ 80

0

~

: 70

z

z1-(n

60

5C

4(

● GROUP 4 HEATS

e STANDARD COMIWSITKXI HEATS●

o 0.10 0.20 0.30 040

MOLYBDENUM coNTENT - PER CENT

FIGURE 4 . RELATIONSHIP BETWEEN MOLYBDENUM CONTENT

AND TENSILE AND YIELD STRENGTH

0-s415

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-15-

Ilc

I0(

x

Jvi

c 8C

:

,

Ela: 7Ca1-ul

60

5C

40

~o

/

,,t.

●● GROUP 5

.

HEATS

o STANDARD COMPOSITION HEATS

.05 .10 ,15 . Zo .25 .30

FIGuRE 5.

VANADIUM CONTENT-PER CENT

RELATIONSHIP BETWEEN VANADIUM CONTENT

AND TENSILE AND YIELD STRENGTH

0-s416

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-16-

increase in strength, the elon~ation dropped from 32.4 to 25.3 per cent

and the reduction of .are&from 65.8 to 59.4 pe”rcent.

The Effect of Aluminum”Content. AS would be expected, the— ——-,,.

aluminum content had no per~ep%ible effect upon the tensile properties

of either the longitudinal or transverse tests. The influehce of-.

aluminum upon the properties normal to the surface will be di6cussed

later in this report.

Vnderbead ‘TeldCrack Sensitivity—.

The underbes.dweld crack sensitivity of all thirty heats in the

hot-rolled condition was determiriedby the single-bead weld test as

previously described in the reports on this project. Five weld specimens

were made on each heat and a summary of the results is listed in

Table 4. The complete data are listed in Table 2 of the Appendix.

The Effect of Carbon Content. The pronounced influence— — .—

content upon the extent of underbead cracking is illustrated in

of carbon

Figure 6.

This figure shows that the crack sensitivity increases quite rapidly as

the carbon content is raised. The heats with 0.20 per cent or less

carbon had a cracking index of 27 or less as compared with 85 and higher.

for heats with 0.25 per cent or more carbon.

The Effect of Wanganese Content. The effeet of ms.nganese content————

in the range of O.93 per cent to 1.51 per cent upon the degree of under-

bead cracking is shwn in Figure 7. While the data in this figure do not

form a smooth curve because of other factors such as the variation in

carbon content, the results do indicate that the underbead cracking

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-17-,.

TABLE 4, UNDERBtiADW3LD CRACKING INDEcwS WIR MATS XL1 iO X-28,x-45 AND x-46 IN THE HOT-ROLLED CONDITION

- -—~ — —.—.

Heat ConSt!.tuerit—.—

No.~feId Crack..

Varied—. SenSi+iviity Index

‘v ,. -1x-2X-3X-4X-5

X-6x-7x-8x-9

x-loX-IIX-12X-13

X-14X-15X-16X-17x-18

X-19X-20X-21x-22

X-23X-24,X-25X-26X-27X-28

x-45X-46

0.17 ) 210“20 ) ;: 27;0.25 ) Carbon 850.28 ) content 970.32 ) 104

0.93 ) % 281.22 ) Nanganese 191.37 ) content ,. 751.51 ) 59

0.41 ) % 500.55 ) Silicon 840.79 ) content 840.92 ) 64

0,10 ) 690.12 ) * 860.24 ) l(oly~denum 660.32 ) content 710,43 ) 66

0?04 ) -’/= 510.06 ) Vanadium 640.19 ) content 780.29 ) 74

nil ) 6.< .005) “ 95C .005) Y Aluminum ~ 74

.029) content 81

.064) (acid soluble) 67

.180) 17

Standard composition heat 57II “ t, It 60

,’

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-18-

✎ ● GROUP I HEATSo STANDARO COMPOSITION HEATS

.15 .20 .25 .30 .35

CARBON CONTENT-PER CENT

FIGURE 6 . THE EFFECT OF CARBON CONTENT UPON THEUNDERBEACJ WELD CRACK SENSITIVITY

0-5417

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-19-

100

80

60

40

20

● GROUP 2 HEATS—

o STANOARO COMPOSITION HEATS

— o

—,

.90 1.10 1.30 1.50 1.60

MANGANESE CONTENT—PER CENT

FIGURE 7. THE EFFECT OF MANGANESE CONTENT UPON THE

UNDERBEAD WELD CRACK SENSITIVITY

o 5418

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j.ncreaseclrapidly

obtained on these

-20-

ctsthe manganese content increased, Yor& dcta will be

steels in order to obtain more points for plotting the

manganese content-crack sensitivity-cu.rvo.

The Effectof Silicon Content. The addition of silicon above.——— —..— —..—.

that normally used in HTS steel wns found to increase the extent of

underbead crncking. The data show, however, that an increase from 0.79

per cent to 0.92 per cent silicon resulted in a decrease in the crack

sensitivity. (See Figure 8.) 11’bileit is well established that large

additions of silicon, about 1.00 per cent, decrease the tensile and yield

strengths as illustrated in Figure 3, additional data m-e needed to

confirm the effect of silicon content in this range upon the weld crack

sensitivity. The high-silicon end of the crack-sensitivity

Figure 8, therefore, should be considered as incomplete.

Elffcct of MOlybdenum Content. MO1ybdenum——.—. —.—...

thut additions ranging from 0.10 to 0.43 per cent

bead cracking to any appreciable extent, although

strength~ wore incroe.sed to a marked extent. The

proved to

curve in

be unique in

did not increase under-

the yield and tensile

curve comparing under-

bead cracking with the molybdenum content is shown in Figure 9.

The Effect of Vanadium Centent. The relationship of underbead—..————,—.

cracking to the vanadiwm content is illustrated in Figure 10. This

figure indicates that additions of vanadium increases the undorbead

crackingto a very small extent.

The Effect of Aluminum Content. The study of the effect of_—. —— .——

aluminum content in the range of O to 0.18 per cent (acid soluble)

yielded reeults which wore quite unexpected and will require additional

data for confirmation.

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-21-

./o

● GROUP 3 HEATS

0 S TANOARD COMWWION HEATS

‘“t

0.20 0.40 0s0 0.s0 I .00

SILICON CONTENT - PER CENT

FIGURE 8 . THE EFFECT OF SILICON CONTENT

UNDERBEAD WELD CRACK SENSITIVITY

UKIN THE

0-5419

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100

●●

● GROUP 4 HEATSo STANDARD COMPOSITION HEATS—

o .10 .20 .30 .40

MOLYBDENUM CONTENT-PER CENT

FIGURE 9 . THE EFFECT OF MOLYBDENUM CONTENT UPON

THE UNDERBEAD WELD CRACK SENSITIVITY

0-S420

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-23-

● GROUP 5 HEATS

O STANDARO COMPOSITION HEATS

o .05 .10 .15 .20 .25

V#NADIUM CONTENT-PER CENT

FIGURE 10. THE EFFECT OF

uNDERBEAD WELD

VANADIUM CONTENT UPON THE

CRACK SENSITIVITY

0-5421

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The

sensitivity

Figure 11.

-z4-

data shawingthe influe!uceof

of the six heatsmade in this

nluminum content upon the crack

investigationare shown in

These data indio~te that the extent of underbead cracking is

extremely low in the steel made with no aluminum addition and inoressed

very rapidly as the aluminum was added, the.maximum cracking occurring in

tho neighborhood of .01 per cent aluminum and progressively decreasing

with additional aluminum.

Since the reasons for the apparent marked influence of alu!rinum

content are not obvious at this time, and as the above results were un-

expected and based on rolativcly few data, it will be necessary to ‘obtain

additional dsta to confirm or refute these results.

~Totched-BarImpact Properties.. —.—.-—

In order to determine the effect of chemical composition upon the

notchad-bar

each of the

from -754F.

impact properties, four duplicate specimens were broken from

30 experimental h~ats at five different tem.paraturesrvnging

to 210°F. The stondard !7ho.rpytsst specimcm was used with

the V-type Izoclnotch out pm’r.llel with the plate surface. l:nlylongi-

tudinal tests were msd.c,the length of the test specimen being the

direction of rolling.

The refiultsof

32, inclusive, and the

these tests are shown graphically in Figures 12 to

datt~from which those figures were constructed are

listed in Table 3 of Appendix A.

The Effeot of Carbon Content..

inclusi~e, reveals that &s the carbon

A,comparison of Figures 12 to 14,

cent.ontis raised, the notched-bar

imp::ctstrength drops rapidly> ‘Thisis well illustrated in Figure 27

which shows the impact strength at +75”F. for a carbon range of 0.17per

cent to 0.32 per cent.

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-25-

● GROUP 6 HEATSo STANDARD COMPOSITION HEAT’S

o .02 .04 .0s OS .10 12 .14 .16 .18 .20

ALUMINUM CWTENT - PER CENT

FIGURE I I . THE EFFECT (J= AIJJMINuM WNTENT uPoN THE

UNDERBEAD WELD CRACK SENSITIVITY

O-5422

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180

140

100

60

-26-

HEAT NO. X. I

HOT ROLLED

C-.17

0

-80 -40 0 40 80 120 160 200

TEMPERATIJRE — DEG. F.

ko0Il.40

100

60

20

0

L

HEAT NO. X-2

HOT ROLLED

C-.2O

lu--80 -40 0 40 eo I 20 160 200

TEMPERATURE — DEG. F.

FIGURE 12, NOTCH -BAR IMPACT PROPERTIES

O-S4Z3

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-2?-

180 —

140 .

I 00 .

HEAT NO. X-3

HOT ROLLED

C-.25

60 —<

20 —

o-80 -40 0 40 80 I20 160 200

TEMPERATURE — DEG. F.

00z~180a.

;o0

’14C

I Oc

60

HEAT NO. X-4

HOT ROLLED

C-.28

20 –

o

-80

FIGURE

-40 0 40

TEMPERATURE

3. NOTCH - 8AR IMPACT

80 I 20 180 200

— DEG. F.

PROPERTIES

@5424

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I80

140

100

60

HEAT NO. X-5

HOT ROLLED

C- .32

Imaz=1800a

I 00

60

-80 -40 0 40 80 I 20 160 200

TEMPERATURE — OEG. E

HEAT NO. X-6

HoT ROLLED

MO-.93

20

0- 80 -40 0 40 so 120 160 200

TEMPERATURE — DEG. F.

FIGURE 14 . NOTCH- BAR MPACT PROPERTIES

0-542!5

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to 1.51

.2:;-

Effect of Uang?nese Content. In the range investigated, 0.93

per cent, it wes found that the manganese content had little if

any influeuce upon the notched-bar impact strength. (See Figures 14 to

IL, inclusive.)

Figure 2! shows the impact strength at room temperature plotted

agaifistthe .?nangnncsecontent. “Whilethese data ,mightbe interpreted as

indicating that an intermediatemanganese content was advantageous, it

appears &flatthis indication is only incidental as similar conditions

are not noted at lower or higher temperatures.

Effect oi’Silicon Content. At room temperature end lower, the—. —..—....— —.— _

notched-bar impact strength falls off rapidly as the

increqsed. (See Figure. 16 to 16, inclusive. ) Thj.s

content at room temperature is illustrated ir.Figure

silicon content is

effect of silicon

2.9.

At a tempernturo of 10”F’., the silicon content hos no

appreci.ablee:efectupon the impact strength.

Effect of ?!’olyhdenumContent. “,hilethe addition of O.iO per

cent molybdenum lowered to some extent the notched-bar im~!aotstrength

when tested at 75’F.,

further effects. ‘The

content was raised.to

to a marked extent.

!l!heinfluence

increased contents up to 0.32 per cent had no

irrdj.cationswere, however, tnritas the molybdenum

about 0.40 per cent, the impact strength dropped

of molybdenum content upon the impact strength at

75”F. is shown in FiKure 30. The data for the entire ranEe of temper-

atures and compositic,ns stu.dic;d are shown in Fi~ures 18 to 20, inclusive.

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10

14

la

HEAT NO. X-7

HOT ROLLEOMn -1.22

0

-80 -40 0 40 80 120 160 200

TEMPERATURE — DEG. F.

IHEAT NO. X-8

HOT ROLLEO

Mn -1.37

I 00

60

0

20 –

o-eo -40 0 40 60 I 20 I 60 200

TEMPERATURE - DEG. F.

FIGURE 4S. NOTCH-BAR IMPACT PROPERTIES0-s426

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-sl-

180—

HEAT NO. x-9

HOT ROLLEOMn - 1.51

140 —

I 00 —

60 —

>

: 20—

x

~o I

I -80 -40 0 40 80 I 20In

160 200TEMPERATURE — DEG. F.Q

z

HEAT NO. X-IO

HOT ROLLEDsi-.4l

140 —

I 00 —

60 —

20—

0

- so -40 0 40 so 120 160 200TEMPERATURE — DEG. F.

FIGURE 16. NOTCH- BAR IMPACT PROPERTIES

0-5427.

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-s2-

13

14

Ic

6

IVIaz30n:180

140

Ioc

6C

2C

0

HEAT NO. X-11HOT ROLLED

SI- .55

-80 -40 0 40 80 120 160 200

TEMPERATURE- DEG. F.

HEAT NO. X-12

HOT ROLLED

61-.7S

----80 -40 0 40 60 120 160 200

TEMPERATURE — DEG. F.

FIGURE 17, NOTCH-BAR IMPACT PROPERTIESO-5426

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180

I 40

I 00

60

I

-33-

HEAT NO. X-13HOT ROLLED

Si -.92

0

80

140

I 00

60

20

0

-so -40 0 46 so 120 160 2Q0

TEMPERATURE — DEG. F.

HEAT NO. X-14

HOT ROLLED

Me-. IO

-80 -40 0 40 60 120 160 200

FIGURE

TEMPERATURE - DEG. I!

8 NOTCH - BAR IMPACT PROPERTIES

O-5429

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-34-

18

14

10

6

2

c

8

14

10

6

2

c

HEAT NO. X- 15

HOT ROLLED

Mo-.12

-eo -40 0 40 80 I 20 160 200

TEMPERATURE — oEG. F.

HEAT NO. X-16

HOT RU.LED

Mo- .24

0

.. .- .- _--Ou -%u u 40 80 I 20 160 200

TEMPERATURE — DEG. F.

FIGURE 19 , NO TCH-SAR IMPACT PROPERTIES0-543(

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-s15-

1,80—HEAT NO. X-17

HOT ROLLED

MO-.32

140 —

I 00 —

60 —

>a.

: 20 .x

00I -80 -40 0 40 80 120 160 200

Wa

TEMPERATURE — DEG. F.za:

g 1s0 -0L

HEAT NO. X-18

HOT ROLLED

Mo-.43

I40 —

100 —

60 —

2 o—

0-80 -40 0 40 60 120 160 200

TEMPERATURE — DEG. F.

FIGURE 20 . NOTCH. BAR IMPACT PROPERTIES0-5431

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-36-

ii’ffectof Vanadium Content. Th9 effect of vanadium—.—. ———

the notched-bar impact strength at 75”F. is shown in Figure

this figureit will be seenthatthe

vcmadi,.uncontentis increased. This

marked increase in yield strength.

impact strength decreases

would be expected in view

content upon

31. From

as the

of the

The effect of tempero.tureupon the impact strength of the four

vanadium-bearing steels is shown in Figures 21 and 22.

Effect of Aluminum Content. The aluminum con-tentwas found to_._,_ —.—

influence the notched-bar impact strength in the expected manner, that

is, the impact strength especially at low temperatures increased as the

aluminum content (acid soluble) was increased until a maximum was reached,

after which the impsct strength declined with further addition of aluminum.

The aluminm content is known to affect other properties such as grain-

coarsenin~ temperature and hardenability ixln similar manner,

The influence of aluminum contentupon the notched-bhrimpaot

strength at -40’F. is illustrated in Ipigure32. The complete data

covering the entire temperature range studied are chown in Figures 23 to

25, inclusive.

Standard-compositionHeats. The notched-bar.— .—

of the two standard chemical composition heats, X-45

in Figure 26. The curves for these two heats tirein

impact properties

and x-46, are shovm

good agreement b~t do

rot duplics.t~th(src,sulto for hects of similcr composition, X-8 for

exmple, as well as might be expected.

A Discussion of the Signif’ioance.of the Test Data-—.. -

A study of thfitensile properties, weld crack flensi.tivity,and

the notc?led-barimpact properties of the thirty experimental hetits

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-37-

180

I 40

I00

60

HEAT NO. X-19

HOT ROLLED

v- .04

-80 -40 0 40 80 I 20 160 200

TEMPERATURE — DEG. F.

HEAT NO. X-20

HOT ROLLED

v- .08

I 40 —

100 —8

60 —

,20 —

o-80 -40 0 40 80 I20 160 200

TEMPERATURE —DEG. F.

FIGURE 21 NOTCH . BAR IMPACT PROPERTIES0-5432

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180

100

60

IIn

230n

~ 180

0L

140

100

60

20

-38-

HEAT NO. X-21

HOT ROLLED

v- .19

-80 .40 0 40 80 I 20 160 200

TEMPERATURE — DEG. F.

HEAT NO. X-22

HOT ROLLED

V-.29

0

1 I Io 1 L

-80 -40 0 40 w I 20 160 200

TEMPERATURE— DEG. F.

.>FIGURE 22 . NOTCH . 8AR IMPACT PROPERTIES

o-5433

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-40-

1160r HEAT NO. X-25

● HOT ROLLED

Al- <.005

0

100 —

60 —

*aK

: 20 —

v

,01-

UI -80 -40 0 40 80 120 160 200

0 TEMPERATURE— OEG. F.z30n I

HEAT NO. X-26

HOT ROLLED

Al - .029

140

r

too

60

1

20

0-80 -40 0 40 so I 20 160 200

TEMPERATURE— DEG. F.

FIGURE 24 . NOTCH-BAR IMPACT PROPERTIES

o-54ti

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-39-

180 —HEAT No. )(-23

HOT ROLLED

Al-O

140 .

I00 — B

60 —

:=20 .u

~o I I I II -60 -40 0 40 80 I20 160 20C

(na

30a

: 180

;

140

I00

60

20

TEMPERATURE — OEG. F.

HEAT NO. X-24

HOT ROLLEO

Al -<005

/

-80 -40 0 40 60 I 20 160 200

TEMPERATURE- DEG. F.

FIGURE 23. NOTCH-BAR IMPACT PROPERTIES0-5434

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-41

18(

1°UIn

5:glaou.

14

10

6

2

c

.

HEAT NO. X-27

HOT ROLLED

Al -.064

1

1 I I I I . I-60 -40 0 40 80 120 160 200

TEMPERATURE - DEG. F.

HEAT NO.X-28

HOT ROLLED

Al -.100

-60

FIGURE

#

I I-40 0 40 60 I 20 160 200

TEMPERATURE - DEG. F.

25 . NOTCH- eAR IMPACT PROPERTIES

0-5436

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-42--

.

/

HEAT NO. X-45

0 AS ROLLEO

STANDARD COMPOSITION

i

I I-60 -40 0 40 80 I20 160 200

TEMPERATURE –OEG. F.

e

e0

.

HEAT NO. X-46

AS ROLLEO

sTANOARO COMPOSITION

-60 -40 0 40 80 I20 160 200

TEMPERATuRE —DEG. F.

FIGURE 26. NOTCH-BAR IMPACT PROPERTIES

0-5437

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-43-

● ()— m

o }I TESTED AT 756 F,( o AS ROLLEO

t ●

● GROUP I HEATs

o STANOARD COMPOSITION HEATS

II

.15 .20 .25 .30 .3sCARBON CONTENT— -R CENT

FIGURE 27. THE EFFECT OF

NOTCHED - BAR IMPACTCARSON CONTENT uPON THE

STRENGTH AT 750 F.

0-5438

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-44-

120

20

0

0

— C8●

0000

●●

●● ●

— ●

● ●

● ●

—●

TESTED AT 75” F.— AS ROLLED

● GROUP 2 HEATSo STANOARD COMPOSITION HEATS

.90 1.10 1.30 1.50

MANGANEsE CONTENT — PER CENT

FIGURE 2S . THE EFFECT OF MANGANESE CONTENT UFUN THE

NOTCHED- BAR IMPACT STRENGTH AT 75° F.

o-5439

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-45-

12(

Ioc

20

0

_mO TESTED AT 750 E

~AS ROLLEO

●—

● GROUP 3 HEATS

o STANOARO COMPOSITION HEATS

.40 .60 .80 I.00SILICON CONTENT–PER CENT

FIGuRE 29. THE EFFECT OF SILICON CONTENT UPON THE

NOTCHED - BAR IMPACT STRENGTH AT 750 F.

0-5440

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-46-

)—1

TESTEO AT 750EAS ROLLEO

b

o

● ●

GROUP 4 HEATsSTANDARO COMPOSITION HEATS\

I I.10 .20 .30 .40

MOLY80ENUM CONTENT-PER CENT

FIGURE 30. THE EFFECT OF MOLYBDENUM CONTENT UPONTHE NOTCHED - BAR IMPACT STRENGTH AT 75° F.

o-544 I

———_

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-47-

120

100

20

0

\

GROUP 5 HEATS - ●

STANOARO COMPOSITION HEATS - 0—

\

TESTEO AT T5” F.AS ROLLED

— :

—●

● \

I.05 .10 .15 .20 .25 .30

VAN AOIUM CONTENT— PER cENT

FIGURE 3 I. THE EFFECT OF vANADluM ~TENT upoN ‘HENOTCHED - BAR IMPACT STRENGTH AT 75° F.

0-5442

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-48-

—TESTEO AT -40” F.

AS ROLLED

GROUP 6 HEATS

.04 .08 .12 .16 .20

ALUMINUM CONTENT— P2R CENT

FIGURE 32. THE EFFECT OF ALUMINUM GONTENT UPON THE

NOTCHED-BAR IMPACT STRENGTH AT -40*F.

0-5443

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-49-

tested in the hot-rolled state reveals the limitations and possible

advantages Wmt might be obtained by varying the carbon, manganese,

silicon, molybdenum, vanadium, and aluminum contents.

Frcm this investigation, it is quite o’oviousthat the carbon ‘

content is very definitely limited. J,bovethis limitinE value of

about 0.15 to 0.20 per cent carbon, the crack sensitivity increases with

marked rapidity which is entirely out of line with the increase in yield

strength. The increase in carbon is also accompaniedwith a reduction in

the notched-bar impact strength.

While manganese increases the yield strength to a marked extent,

it also raises the crack sensitivity quite rapidly and is, therefore,

limited in the case of hot-rolled steel to some place between about

1.1(Ito 1.30 per cent, depending upon other factors. One apparent

advantage of manganese is that it is not detrimental to the notched..bar

impact strength in the range investigated,

while the use of silicon as arlalloy in this grade of steel

appears to offer an advtmtage over plain carbon-manganese steels for

obtaining yield strengths up to about 52,000 p.s.i., silicon is not

comparablewith either molybdenum or vanadium for producing higher yield

strength steels that exhibit a low degree of underbead cracking,

It appears quite possible that the use of molybdenum and ‘ranadiwm

as alloying agents may prove to be advantageous. Additions of either of

these alloys produces a substantial increase in the yield and tensile

strength. which in the case of molybdenum is accompanied by little or

no increase in weld crack sensiti.vit.y,and only a moderate increase in

the case of vanadium. The addition of these alleys does, however, lower

the notched-bar imps.otstrength especially at room temperature and b$low.

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.-50-

The data fromthe sixheatsmade to studythe influenceof

aluminpmcontentindicate that aluminumis an extremelytiportant

faotorin establishingthe weld cracksensitivity,the 10~.and.medi~m

alumiri!nnsteels being quite craok sensitive as compared with steels

containing no aluminum or very large additions of aluminum.,.

Since this pronounced effect of aluminum had not been noted in

the previotiiwork, which may be because the proper range was not,.

investigated, it will be necessary to obtain more data to confirm or

refute these results.

The study of aluminum content again confirmed the beneficial

effects of relatively large aluminum additions, two uounds per ton,

upon the notched-bar impact strength. This effect is especially

noticeable at low temperatures.

The Influence of Aluminum,Content TJponthe ~—. —.,— +_.n!eohani~alpr~pertles }]Orwl t~e~a~surface——.—— —.-. .—v .,_..

In order to obtain more iqforme.tionabout the influence of

altqninwnand especially its effent upon the physical properties normal

to the plate surface, JIeatsX-23 to x-28, inclusive, were made with

al~inum additions ranging from O to 5 pounds per ton. (See Tables 1

and 2.)

These ~eats were made from 350-pound induction furnace melts

which were poured into a single 8 by 8-inch ingot, the maximum size ths,t

can be eonyiently handled in the laboratory. This large size was

selected in order to obtain the maximum reduction during hot-rolling to

a l-inch plate. TO prevent the structtue from being broken up by

forging, these ingots were rolled directly to l-inch plate on a small

oominercie.1mill.

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-51.-

The analysis

aluminum content and

.,

of’these six heats, including the acid-soluble

the amount of aluminum added, are shown in Table 5.

TABLE 5. CHIY,fICJiLANALYSIS OF LABORATORY HEATS MA.DETOSTUDY THE INFLUENCE GF ALUMINUM CONTENT

-— — —_— _,, —

HeatNo” c

Aluminum Added:?n P s Si Ti Al in $&s. Per Ton

-— ..—— —— .—.

X-23 0.20 1.25 .021 .022 0.27 .007 Nil o

X.-24 0.23 1.36 .019 .021 0.29 .006 <.005 1/4

X-25 0.22 1.24 ,020 ..020 0.27 .013 <.005 1/2

.X-26 0.22 1,31, .021 .021 027 .016 .029 1

X-27 ,0.20 1.29 >018 .020 0.31 .015 .064 2

X-28 0.22 1.26 .019 ,020 0.27 .015 ,160 5

. .——— .._._.——. ——.., ——

Tensile properties I$ormal“to“PlateSurfa:cei In order to.—-—--=—_. _——

determine ‘thetensile strength of these steels in the direction normal

to the plate surface, tensile specimens ‘wereprepared from the hot-rolled,,

plate by welding and machining as indicated in Figure 33. Three by six-

inch specimens were cut from each of the six heats,”Heats x-23 to x-28,

inclusives 3eveled plateswere then welded to these specimens a< show

in the above figure. The ‘weldswere made with four passes using

J.incolnSh.ield-fire100(4‘7S-EICIOIO)electrodes. The first pass was made

‘witha 3/32-inch electrode and reverse polarity direct “currentusing

1.30to 140 amperes and an arc voltage of 27 to ‘3h’.,,

Following rough turning of the tensi~~ specimens, they “were

etched li~htly in order to es+abl.ish definitely ihe location of the test

plate. After determining the position of the test plate, a 3/4-inch

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-52-

_rI

.505 “ TENSILE SPECIMENS

---f- )

III

~

I-Nal

/!- 4 PASS WELDS

FIGURE 33. AN ILLUSTRATION OF THE PROCEDURE USEO FOR MAKING THE

SPECIMENS TO OETERMINE THE TENSILE PROPERTIES

NORMAL TO THE PLATE SURFACE’

0-902

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-53-

section midway between the extremes of the test plate we.s ground to

0.505-inch diameter, leaving the renminder of the bar 0.550 inch. This

precaution was taken to insure that the fracture would occur in the

deiir~d Section. ““ ‘. ,.,.

,Theresults of the tensile tests are shown in Table 6. A study!, .,,,

of these data do not show a marked relationship”between the uluminum

content and ‘thetensile properties, It will be noted, however, that both

the yield and tensile strength of the heat made with no aluminum

additi”on,Heat X-23, are 10-wcompared with the other heats in the series.

The lcm strength, however, is not caused entirely by the absence of

aluminum since both the carbon and ms.nganese contents are 1ow. While the

data my be interpretedin such a manner as to indicate a slight incrense

in ductility with increased aluminum, this increase is’so small that it,,

cannot be considered significant.

A previous study mode on commercial HTS steels’and reported on

pages 87 to 69 of the August 24, 1945, report showed a distinct

relationship between the aluminumcontent and the reduction in area, the,,

steels with little or no acid-soluble aluminum content displaying a much

higher reduction in aretithat those containing an appreciable amount of

aluminum. A siriilw’but less marked relationship wcs noted between the

aluminum comtent and the per cent elon~r.tion. The tensile strength in

the higher aluminum commercial steels W(.Sfound to be erratic end

sometimes quite low.

This difference between the behavior of the laboratory steels and

the commercio.1heats can probably be attributed to the difference in the

amount of reductior!between ingot md plate, the directional properties

obviously being amplified by inoreased reduction.

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.-F:4-

TABLE 6. TEiWILE PROPERTIES NCRMAL TO THE PLATE SURFACE

——. — ,-— ..—- ~—.—.==~ — —.i,luminum Zlong. in Red. in Yield TensileContent, 3/4 Inch, Area, Strength, Strength,

<’Heat YO. ,. z T p.s.i. p.s.i.-

74,60073:25073>750

x-23,,!!

~Jil 14.79.314.7

18.414.518.1

54,00053,00058,750

82,88080,63084,500

x-24!1!t

‘“:.005 10.76.79.3

12.6,11.514.1

63,75062,50062,500

61,50060,’75062,000

60,75079,00079,380

x-25,,,,

<:.005 17.316.013.3

22.720.618.1

61,00060,00061,500

78,38077,8807’7,750

T-261!t,

,.029 13.3‘13.313.3

18.818.821.3

23.727,827.8

63,00061,50061,500

78,00078,25078,630

x-271!It

.064 14.717’317.3

79,00074,50077,880

. lP.O 1:.: 24.1-*

18.4

62,00063,00063,000

x-28,,If 16.0

—. .——

*Speoimen”broke in gauge mark.

See Fi<ure 19 for details concerning the preparationof the tens,ile specimens.

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-55-

l,]&c,hed-Bnr Impact Strength Normal to the Pie.te Surface. ~Totched-—— ,— .....—.. --. -—.. --.. ——

bar impact specimens, Chsrpy specimens with V-Izod notches, were prepared

from sections similar to those used for the tensile specimens. (See

Figure 33.)

Four duplicate specimens ‘werebroken at five different temperatures

between the limits of -40”F. and +21O”T. The data from these tests are

shown in Figures 34 to 36, inclusive. The test values are recorded in

Table 4 of Appendix A. The above figures reveal that the notched-bar

impact strength normal to

the aluminum content, the

pounds.

the plate

values at

surface is qdite low regardless of

+75°F. falling between 7 and 20-foot-

A.comparison of the six different steels reveals that Heat x-27

made with an addition of two pounds of aluminum per ton had definitely

better impact strength as compared with the other heats. Similar

results were noted when

direction, that is, the

inclusive.)

the steels were tested

direction of rolling,

in the longitudinal

(See Figures23 to 25,

In order to check the effect of aluminum content upon underbead

cracking, a second series of heats will be made with aluminum additions

ranging from O to 5 pounds per ton.

Since increased additions of molybdenum apparently did not

i.ncresse

strength

of he<.ts

previous

the cre.cksensitivity but did raise the tensile and yield

to a mnrked extent, it appears desirable to make

but at a slightly lower car”~onlevel in order to

results.

s,second series

confirm the

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HEAT NO. X-23

30 — HOT ROLLEO

NO Al ADDED

20 —m

10 — 0 ●

o-80 -40 0 40 so I 20 160 200

TEMPER ATURE— OEG. F.

1- HEAT NO. X-2430 HOT ROLLED

10 —

o-Go -40 0 40 So I 20 160 200

TEMPERATURE — DEG. F.

FIGURE 34. NOTCH EO-BAR IMPACT STRENGTH NORMAL TO THE PLATE

SURFACE

o-5444

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-5?-

“40 .

HEAT NO. X-25

30 — HOT ROLLED

+ L& Al ADDED P2R TON

20 —

10 —● ●

.:0

ur~o

I-80 -40 0 40 so 120 160 m

TEMPERATURE — DEG. F.

HEAT NQ X-26

HOT ROLLED

1 LB. Al ADDED PER TON

-00 -40 0 40 so 120 160 200

TEMPERATURE — 0E6. F.

FIGURE 36. NOTCHED- BAR IMPAGT STREN6TH NORMAL ~ ~tZ

PLATE SURFACC0-8445

—.

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1HEAT NO. X-27

HOT ROLLED

30 2 LES. Al ADOED PER TON

0

020 —

010 —

*na 0a

o

;0I -80 -40 0 40 80 1200

1s0 200TEMPERATURE -DEG.F,

2a

2 40!

bo HEAT NO. x.28o ,L HOT ROLLEO

30 — 5L6S. AI AOOED PER TON

20 —

10 .

0-so -40 0 40 60 I20 1s0 200

TEMPERATuRE -DEG. F.

FIGURE 36. NOTCHEO-BAR IMPACT STRENGTH NORMAL TO

THE PLATE SURFAGE ,

0-6446

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-Lj~-

The influence of homogenization upon the crack sensitivity and

physical properties of the 30 heats discussed in this report will be

studied. This phase of the work should aid in establishing the maximum

chemical composition ~hst may be used without excessive underbead cracking.

Since it appears that the most practical place to carry out a

homogenization treatment in cormnercialproduction is while the slab is

being heated for rolling to plc.te,it will be necessary to determine the

time and temperature required for this treatment. Sections of commercial

sls.bsof HTS steel have been obtained and a.study is being made to

determine the time-temperature cyole necessary to homogenize the slab

and also the effect of this temperature upon the crack sensitivity of

the plate rolled from the treated slab.

Data used in this report can be found in Laboratory Notebook

No. 2581, pages 6 to 51, inclusive.

CES:K D QLW/abJune 18, 1947RevisedOctober9, 1947

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APPENDIX A

TABJ.ESOF COWLETE TEST DATA

by

H. M. Banta and A. L. Walters

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-63-

TABLE AI.. TENSILE PROPBR’llIES OF HOT-ROLL3D PI,M’EI’RI.MLA.8CR~,TCRYRdATS.X-1TC K-28, INCLUSIVE>X-45 AND X-46

—. .—.—_— —-——-Elong.”in Red. ifi Yield Tensile

Heat, Test 2 Inches, Area, Strength, Strength,NO; DirectiOn. %. % p.s.i. p.s.i.

———.—.

x-1f,,! .,, “

X-2IIIt1,

x-3!1!1tt

x-4II1,!1

x-5 ,It1! .!1

X-61!1,u

x.?,%It ~II

x-8!1!1!,

Long. ‘11 .

Trans~II

Long.tt

Trans.!1

Long.!1

Trans.?!

Long,It

Trans.!1 ‘

Long.,?

Trans$’1!

Long.1!

Trans.II

Long.’II

Trani.,1

Long.It

Trap;.r!

—.—.

37.037.5 “’31.5’31,5’

37.0’35.033.532,0’

31.032.5”29.5’29,5 ““

31.730.028.027.5)

29.527.526.0’27.0

36.035.0 “’33.031.0 ‘

34.535<0 ,’,,30.0 ‘29.7

35.535.730.030.0

73s974.962.162.1

67.969.963;362,8 “

65.466.661.161.1

66.266)856’.056.6

65.963.353.351.4

67:065.958.6 ,,57.8

691969.358.161.8

71.’4,,69.760.6 ‘(57.5

44,250,,47>00045,50044,000

45,50043,00041,000,42,250

46,750,”48,000,48,250,44,250

52,75049,250,49,00048,500

55,50054,50049,00049,750

39,75036>50~36,50d40,750

45,25044,00043,50042,750

46,50047,00044>50044,500

70,750722000

72,30072,500

75,10074,10073$90073,850

61,00062,10080,00060,400

67,60085,90066,70086,200

69,90089,70067,40067,150

70,20070,10069,50069,500

74,1007Z>8007~,9i3(3

71,900

77,60077;10075,60076,100

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-60a-

T,ABLEAl. (Continued)

—“”=gni7——— Red. in—-.

,, ... ,., Yield Tensile -Heat Test 2 Inches, Area, Strength, Strength,

No. Direction . ~~—.. ——— ~,, p.s.i. p.s.i.—.———

x-9!!,,,!

x-lot!,!!!

X-12!!!!!1

X-13’11 ,,,!1,,

.

X-14’u!l:..’f,

X-151,11,,

X-16It!7,,

X-17!!M,,

Long.t!

Trans..II

Long.II

Trans.II

Long.11

Traqs.11

Long’.,,

Tre.ns.!,

Long’.!1

Trans.,1

.,Long.,,

Trans.,,

Long.,1

Trans..,1

Long.,1

Trans.t,

Long.!1

Tis.ns,tl

35.034.531.531.6

35?534.233.531.0

32.034.330.229..2

..33.033..029.028..5

33.033*O30.5”30.5

31.032.528.029.5

31.532.029.028.5

29.029.0.24.5.23.7.

23.025.02i.320.5

73.570,659.160.3

70.469.061.658.6

67.969,3.57.559.6

68?868.259.458.3

66.165.959,659.6

65.967.958.658..6“’

62.865.457.5 ‘59.1

62.663.655.554.9 ~

61.364.749.849.5

49,25047,50046,76046,000

47,75047,50044,00044,250

52,50049,25047,00046,250

53,00052,00052,00050,000

49,75049,75049,50049,000

60,00051,25046,50045,500

51,00051,750”49,00046,750

55,00057,00057,00056,500

66,75070,50065,25067,250

77,60076,75077,70077,600

78,30076,60076,50076,100

79,40080,60079,60079,400

65,40085,50083,75083,900

63,80084,10083,30083,100

80,00080;80079,00079,100

81,00081,70080,80081,000

81,000.83,50082,70082,600

97,750.99,50093,50094,125

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-60b-,..,.-

‘TABLEAl. (Continued)

———.——.—. .—. —..—. —— —--___,__Elong. in Red. in

HeatYield Tensile

Test 2 Inches, Area, Strength, Strength,No. Di’’’ti”” A: $ ~.soi. p,sOi._.— +...— ,-----

x-18:,,It,1

X-19II11It

X-20!,,!n

x.-z111Ii,,

x-22,,,,,!

X-23,,It,1

X-24It,,II

X-25Itt!!8

x-26II1?11

Long.It

Trans.!?

Long.,,

Trans,.1! ‘

Long.”!!

Trans.’,!1

Long.11

‘1’rans.II

Long.,.11

Trans.!!

Long.!t

Trans.II

Long.!1

Trans.,1

Long.n

‘Mans,1!

Long.It

Trans.!1

21.522,520.5.21.0.

32.032.?29.0,30.0,

32,7”32.5,27.027.5

27.027.0 .,24.022.0

25.525.020.020.6

35.034.029.029,5

32>030.528,027.5

33.033.028.027.5

33.033.027.026.5

62.8”62.353.3 “53.6 “

65,665.960.6 “5’7.3 “

67.767.95B.360.6

60.661.652.552.2

59.459.449.248.4

6’7.385.452.551.9

68.660.353.647.6

68.268.255.2530

68.467.753-852.8

77,00079,50076,50075,250

48,75049,50047,500’48,000

57,25056,50053,750.54,250

67,75066,00063,25066,000

77,50079,50074,00073,750

47:00048,00046,00Q45,509

50,50051,25049,00049,750

47,50048,00046,75046,000

49,00050,25049,25049,500

98,100100,87597275096,800

79,20080,00078,00078,200

84,40084,00082,50062,400

92,70094,35092,60092,500

104,500105,750100,400100,400

74,40C75,40073,80073,800

81,70082,75081,80081,900

76,75076,00076,35076,400

78,90080,40060,15079,800

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,. -60c-

TABLE Al.“ (Continued)

— —. -,-

Elong. in Red. in Yield l!ensileHeat ‘Test 2 Inches, Area, Strength, S$rength,.‘‘?:0. Dire.etion “o . p.s.?. ~~~ p.s.i.——

x-z? Long, 33.0, 69.0,. 49,000 77,200!! ,1 34’.0 ‘70.1 47,500!?

76,000Trans. 29.0 57.”8’ 46,760 75,850

,! ,1 27.5 56.0 44,750 76,100

X-28 Long. 33.5 6%,8. 48,500 78,000t! !1 33.5, 68.6 48,250 77,500,,. ‘lrans. 29,5 57.3 47,250 75,800t! II 27.5 54.5 . 46,500 75,800

X-4’5 Long. 34:5, 69.0 51,750,!

78,900It 3s.0 65.4

If52,500

TraiM.79;250

24’.5 37.9 48,250 77,500,1 ,! 23.0 33.4 49,500 77,400

x-46 Long. 35’.0’ 70.1 49,75011

79,9001! 35.0 70.1 51,750 80,750

!,:” Trahs. 28”.0 52.8 52,500 79,900,, II, 28.0 49.5 51,500 79,750

.,

,.

.,,,

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-61-..’

TABLE .42. UNDERBEAD CRACKING VALUES OF INDIVIDUAL SPECIMENS.FRONiLABORATORY HBATS X-1 TO X-28, INCLIJSIVE,X-45 AND X-46 IN ‘THEHOT-ROLLEI)STAT!!;

. –—..-PTInderbead

Heat Speci~en L .Cracking,~NO. ?!0. Per Cent

x-1 1234567e910

x-2 12345678910

x-3 12345678910

123Q5678910

X-4

1134162919333251324 Avg, 212

3521183016262133

4821 Avg. 277;

94807091898895788480 Avg. 85%

10410589819310810668113105. Avg. 9T;<

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,.. .-61a-

TABLE A.?. (Continued)

.— —. —Underbead

Heat ~pec.imen,.: Cracking,No. “’ hTO. Per Cent

x-5 1.2345678910

X.-6 1234567E910

x-7 12345678910

X-8 12

. 3.,.:456?8910

120115104889610310110410999 Avg. 104~

48362318242519302531 Avg. 285

818839113544059 Avg. 197%

74768671887069795089 Avg. 75?:.

— —

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.,, . -61b-

~ .,TfiBLMAd. (Continued)

.— ,.———.-Underbead

Tieat Specimen Cracking,No. ,. ~~~. Per Cent

.-———.. -—

x-9 1 712 743 764 685 606 347 588 70

x-lo

910

123456789

10

671 Avg. 597;

53806573462344704520 Avg. 60~;

X-n 1 842 793 764 935 816 897 788 899 9510 80 A,vg, 84?

X-12 12345678910

91758675787891689085 Avg. 84$

—,, .——. —..-—

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. .-61c-

‘J?AB~E‘A2.“:(continued)

.—— ------- - ‘“‘“’

Underbead~~eat Specimen ,,,

FO ,Cracking, .

NO.-4. Per Cent

X-13 12345676910

X-14

X-15

X-16

12345678910

12345678910

123456769

,10

64605680836368596643 Avg, 64$

59808658756676508953 Avg. 697

95788486819386698093 Avg, B6%

73686958807056694874 Avg. 66%

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-61d.-

TA~,LEA2, (Continued)

.—..—— .,—_______ . —.. __._,._Underbea.d

lleat Specimen Cracking,110,. NO. Per Cent.—. _._e —. —.. ,____

,,

X-17 12345676910

X-18 12345678910

12345678910

x-20 12345679910

X-19

’71745474717163818464 Avg. 7l%

64706368607073696660 Avg. 667;

58345650554860615043 A.vg, 51%

73497955616168630348 A~g. 64$

.—

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..,.

-61e-

TABLEiA2. (Continued)

—!

.——

Heat ~.Underbead

Specimen . Cracking, .NO, “ iio. Per Cent

——_

x-22

X-21 1234567%9

10

1

234567a910

X-23 12345678910

X-24 12345678910

80906074756481817975 Avg. 78%

74807870716595797054 Avg. 74$

055

1301851440

9598899099869495104101

Avg. 6’7%

Avg. 95;4

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-61f-

..?

TABLI A2. (Co&inued)

:; 1.

..— — — ________ ,,_,.._._____ .—.— .———,—,.. [Jnderbead

Heat .,~, “ipec.imen Cracking,yiJ. ‘. . NO. per cent

.— ___. __, _.. ____. _,,,,._,_”_,___

1-25 12345678910

X-26 1234567’8910

X-27 12345676910

x-28 12345670910

83 “’708368806670856569 Avg, 74J

868683858ti8568797878 Avg. 8~Z

467446 , ,,40713550646568 Avg. 5‘?;(

30-15 “’194162318112315 Avg. l?~

Page 86: PROGRMSREPORT USEDFORRULLCONSTRUCTION · PDF filerapid rate, it also increasesthe weldcrack sensit.iyityit A rapid rate. One advantageofmanganese is that it is @ appreciable,,detrimentalto

.’, .-Glg~

TAk3LEA2, (Continued)

.— ________ ——Underbead

iieat Specimen Cracking,p~~. BTo. Per Cent’

——

X-45 1 142 403 994 705 646 257 918 469 3610 83 Avg. 57%

X-46 1 642 753 904 665 296 537 686 759 910 53 Avgs 60%

Steel 37 1 10(Control) 2 !3

3 244 85 66 197 58 309 5

10 5 Avg. 1l?

Page 87: PROGRMSREPORT USEDFORRULLCONSTRUCTION · PDF filerapid rate, it also increasesthe weldcrack sensit.iyityit A rapid rate. One advantageofmanganese is that it is @ appreciable,,detrimentalto

-—.———.. .—

Heat.—

v~,Testing Temperature, Degrees F._—— —.-——. ——. —.———”.._—.. ______ .—___

-75” -40° -5° +75” +210”————.— ————

K-1

X-2

X-3

X-4

X-5

X-6

~...7

x-8

X-9

X:lo

X-n

X-12

X-13

X-14

X-15

3s5

824

432

234

424

342

434

555

463

545

332

,3.3- 5

.4 4 2

222

632

2

3

2

4

2

3

4

3

2

3

3

4

2

2

3

68

4

7

5

7

6

8

8

22

5

7

9

13.

3

~

25

7

3

3

8

6

8

10

5

7

5

‘6

14

4

9

21

4

8

4

7

7

8

24

16

6

6

8

3

5

3

32

3

7

4

6.

4

9

14

6

32

7

4

4

6

11

L06

24

13

8.

13

9

48

42

48

20

2?2

20

12

13

20

119

22

21

18

18

19

20

46

46

19

21

~2

18

12

.11

31

16

17

10

12

18

33

48

41

37

14

12

9

9

11

30

14

8

8

19

30

21

14

24

16

34

14

12”

13

19.

107

107

34

26

36

35

101

105

98

63

03

37

25

78

53

124 111 112

95 66 67

40 41 44

47 51 37

31 25 35

73 103 92

95 92 108

95 119 110

47 104 78

108 93 112

54 55 91

.58 33 44.

18 19 31

50 34 43

43 38 44

120 124 1.19 129

123 llL 125 112

56 85 84 ii

74 9@ 83 81

67 68 76 71

96 119 98 108&

Ice loQ 134 118 ~

95 112 108 115

106 97 109 105

100 110 106 105

86 85 98 96

89 .90 97 110

85 ’85 93 91

% 96 90 92

95 50 93 97

Page 88: PROGRMSREPORT USEDFORRULLCONSTRUCTION · PDF filerapid rate, it also increasesthe weldcrack sensit.iyityit A rapid rate. One advantageofmanganese is that it is @ appreciable,,detrimentalto

TABLE A3. (Continued)

Heat Testing Temperature, Degrees F.No. -75° -40° -5. +75” =210”

x-i6

“X-17

X-18

.X-19

I X-20

I X-21

x-22

X-23

X-24

X-25

‘X-26

X-27

X-28

X-45

X-46

6223

3342

3333

5232

3233

2222

2233

4542

3325

4422

4353

i0544.

‘654&

46622

6899

54

79

43

67

37

3 13

32

46

7?

9 14

15 10

34 26

11 21

8

8

3

5

8

3

2

3

10

17

18

18

f!

14 19 46

20 30 41

7 35

3 9

13 5

5 ,12

“5 8

3 “8

2 ‘“3

21 13

8 18

7 “17

10 26

22 45

12 29

105 27

75 30

21

21

4

40

11

6

3

33

17

22

35

’45

e5

102

1.00

12 26

15 12

44

25 28

13 23

94

.4,2

14 11

18 13

19 44

26 58

66 “34

57 55

111 125

115 121

69 64

33 59

13 10

48 32

113 101

27 10

45

94 89

55 99

96 98

99 111

104 108

80 89

113 116

115 116

96 .81

41 36

10 10

33 65

79 100

13 20

65

90 96

45 63

98 98

93 95

109 105

105 90

121 12:

123 129

77

78

84

89

94

87

37

108

106

.105

99

73 92 ,86

65 81 81

82 87 95

51 94 85

89 35 103

86 85 84

44 27 21A

107 104 105 ;

1(25 98 103

103 113 118

L09 ,109 ,106

106 .1G5- 104 :.’38

105 104 108 106

104 111 116 116

100 110 110 133

.——.—Note: The above impact values are given in foot-pounds. The s?ecimens used were the standard Y-not.ch Charpy

bars which were broken on a Riehle impact machine having an initial energy of 220 foot-pounds.

Page 89: PROGRMSREPORT USEDFORRULLCONSTRUCTION · PDF filerapid rate, it also increasesthe weldcrack sensit.iyityit A rapid rate. One advantageofmanganese is that it is @ appreciable,,detrimentalto

TABLE A4. NO TWi3D-BAR 1?!?ACT ?ROFMTIES NCRN4ATC THE PLATEWRF’AC12G3 lIEATSX-23TO X-28 IN lWE HCT-ROLLEDSTATE

Heat Testing Temperature, Degrees F.—— ———Xo. -40° 5° +400 +?i” +210”.,

—-—. —.-

x-23 2222 2222 9454 6 9118 21 21 25 17

X-24 2322 3232 5643 6778 17 18 18 i+

X-25 2322 4434 7645 10899 18 19 18 19

X-26 2222 5543 7887 10 11 13 12 18 18 20 19

X-27 6273 13 12 11 7 12 14 12’ 17 16 19 17 13 27 28 24 22

x-28 2222 4555 810108 15 14 12 13 23 22 22 21

.—— —. — ——— ———..

Fete: The aboveimpactvaluesare givenin foot-pounds.The specimensused were the standard V-notchCharp:r‘oarswhich were broken on a Riehle impact machine having an initial energy of 220foot-pounds.

I