Powder creation using spraydryers - Delft Solids Solutions Beekman... · Powder creation using...
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Powder creation using spray dryers
Cris Beekman
Technology manager
CBE/2016-10-25
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Who we are
About Tetra Pak
CBE/2016-10-25
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Packaging
Tetra Pak – a single source supplier
Processing
ServiceCBE/2016-10-25 / 3
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Line solution for the following area’s
► Dairy, Beverage & Prepared Food
► Cheese and Whey
► Ice cream, Filtration and Cosmetics
► Automation Solutions
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Processing solutions and know-how
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Our strength
► Strong company, able to handle major turn key projects
► Scope from raw milk silo to powder bag
► Local presence and local service
► Taylor made solutions
► Top quality powders
► Test centre semi industrial scale
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Tetra Pak is global and works locally
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Fluid Dynamics Services within Tetra Pak CPS
► Modern software tools for CFD
analysis
− Star-CCM+
− ANSYS-Fluent
− ANSYS-CFX
► Largest computer cluster of
Northern Europe, with more than
>5000 cpu’s
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State of the art Technologies – CFD
Spray dryer air flows in a nutshell
CPU demand: 500 cpu’s for 1 month
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The machine
Spray dryer components
CBE/2016-10-25
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Principle of spray drying
► To transform a solution into many small droplets
(by means of atomisation) which are then
exposed to a fast current of hot air
► Smaller droplets means
− larger droplet surface
− more rapid water evaporation
► Atomisation determines shape, size and density
of the final particles
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Spray Dryers components
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Spray dryer main components
► Hot air system and air distribution
► Drying chamber
► Concentrate feed system
► Atomising systems
► Powder separation system
► Fluid bed after-drying/cooling
► Pneumatic conveying and cooling system
► CIP and safety system
► Instrumentation and automation
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Spray dryers components
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Hart of the spray dryer
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Spray dryers components
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The hart of the dryer
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Spray dryers components
Sunflower air distributor
STAD
Aim: low pressure drop & uniform
temperature and flow profile
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And the body
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Spray dryers components
Our concepts
Tall Wide Body
− Co-current airflows
− Reduced fouling compared to TFD
− Better cleanable
Tall Wide Body
− Wide body concept
− For more difficult drying products
Tall Form Bustle
− Better powder separation in cone
than wide body
− Less recirculation of fines
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Other Chambers
► U-tube dryer
− Single stage dryer
− Powder separated by cyclones or baghouse
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Spray dryers components
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Other Chambers
► Multi-stage dryer
− Two or three stage drying
− 10-30% of air is supplied by
internal bed
− Larger beds can only handle
agglomerated products
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Spray dryers components
► Rewetter
− Used when straight through
agglomeration is not possible
− Produces stronger and
coarser agglomerates
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Fluid Beds
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Spray dryers components
alternatives for second stage drying:- Static well mix bed
- Shaking bed
- Vibrating bed
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Fluid Beds
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Spray dryers components
► Static Bed
− Secondary drying or cooling
− Ensures homogeneous moisture and
temperature profile
− Removes stickiness for sticky products
− Air exhausts into the chamber
− Diameter 1.4 – 2.5 m
− Temperature: 40 – 120°C
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► Shaking or vibrating beds
− Shaking or vibrating movement
− Improve fluidization
− minimum to powder particles damage
− Well-mix and plug flow sections possible
− homogeneous moisture and temperature
profile
− Secondary drying
− Removes stickiness
− Cooling
− Bed width: 0.6 – 2.0m
− Bed length: 4 – 14m
Fluid Beds
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Spray dryers components
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Fitration and Heating
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Spray dryers components
► To clean and heat inlet air
► Types of heating:
− Steam heating
− Indirect gas heating
− Direct gas heating
− Electrical heating
− Thermal oil heating
► Choice depends demands
and available utility
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Improving air supply to a direct fired gas burner
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Use of CFD in optimization dryers
High velocity of cold air
Non-uniform velocity distribution
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Exhaust
air dryer
Fines
Air
Two choises for powder separation system
► Cyclones
− Higher losses
− Higher pressure drops
− Lower investment
Spray dryers components
► Bag filters
− Lower losses
− Lower pressure drops
− Higher investment
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Powder creation
In a spray dryer
CBE/2016-10-25
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Agglomeration
► Getting smaller particles to adhere to each other to form a powder
consisting of bigger conglomerates/agglomerates, which are
essential for an easy reconstitution in water.
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Agglomeration
Bridging particles
Non-agglomerated Agglomerated
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FIB-SEM micrographs of powders
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Agglomeration
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High pressure nozzle
► In a nozzle atomizer pressure is
used to atomise the concentrate
− concentrate is pumped at high pressure
through a swirl chamber and orifice,
inducing rotating motion
− concentrate leaves the orifice as a thin
film at about 200 m/s which breaks
down into small droplets.
− nozzle pressures 150 to 300 bar
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Atomization
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Differences between nozzles
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Atomization
SD SF SG
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Agglomeration principles
CBE/2016-10-25
Agglomeration
► Agglomerates will form as a result of:
− Collision between droplets
− Collision between droplets and dry particles
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Individual spray Inter spray mixing Lance on swivel
No agglomeration Agglomeration Swivel adjustment
Adjustable swivel system
► Adjustable swivel system will manipulate the distance the of the
nozzle tip to each other
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Atomization
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Viscosity will have an impact on collision outcomes
• Above example = water
• Viscosity changes regime bounds
Agglomeration principles
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Agglomeration
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Particle history during drying
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Agglomeration
Stickiness
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Importance of glass transition
► Glass transition is a phenomenon, of powders that at specific
combinations of moisture and temperature, at the surface of the
particles allows viscous flows during particle contact.
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Agglomeration
EquilibrationMoisture Sorption or Heating
Dry
SurfaceWet
SurfaceAttraction
Fusion
Free
Flowing
Cohesive
(Sticky)
Caked
(Sticky)
Caked
(Hard)
Drying orCoolingCaked
(Sticky)
Continued
Sorption
or Melting
ContinuedRe-wetting
Drying orCooling
Drying or
Cooling
Liquid Bridge Formation (Peleg and Bagley, 1993)
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Particle phases in a spray dryer
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Agglomeration
Liquid surface
Plastic surface
Plastic sticky surface
Low sticky surface
Atomisation
Non-sticky powder
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► Example, Drying of Malto
Dextrin 20
► TS = 40%
► A: Tin / Tout = 110/74ºC
► B: Tin / Tout = 170/145ºC
► C: Tin / Tout = 200/173ºC
Temperature Effects during Spray Drying
Agglomeration
L. Alamilla-Beltran, Journal of Food Engineering 67 (2005) 179–184 CBE/2016-10-25 / 32
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Relation between dryer, feed and powder properties
Processing parameters
Physical configuration of drier- Configuration
(e.g. co-current, 2-stage)
- Secondary feeds (e.g. fines return)
- Air pattern and mixing
- Atomizer type
Feed characteristics- Chemical Composition
- Solids content
- Temperature
- Degree of homogenization
- Viscosity
- Foam-ability
- Pre-treatment
- pH
Operation conditions-Feed rate
-Gas flow rate
-Gas composition
-Drying temperature
Primary powder
properties
- Moisture content
- Particle Size distribution
- Particle density
- Particle morphology
- Color
- Component distribution
- Surface composition
Secondary powder
properties
- Reconstitution properties
- Protein Stability
- Oxidative Stability
- Hygroscopicity
- Stickiness
- Flowability
- Dustiness
- Volatile retention
- (Surface) Free Fat
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Q&A
CBE/2016-10-25