PHASE II

ENVIRONMENTAL

SITE ASSESSMENT

November 16, 2020

GBTS File: 20-0683.02

Prepared By:

Gallagher Bassett Technical Services 22 IBM Road – Suite 101 Poughkeepsie, New York 12601

Prepared For:

STEL, Inc. 715 Central Avenue Dunkirk, New York 14048

Environmental investigation services were performed by Gallagher Bassett Technical Services (GBTS). The undersigned have reviewed this Phase II Environmental Site Assessment and certify to STEL, Inc. that the information provided in this document is accurate as of the date of issuance by this office.

Victoria Panico Gallagher Bassett Technical Services

Assistant Project Manager

___________________________

Scott Spitzer Gallagher Bassett Technical Services

Technical Director – Environmental Consulting

TABLE OF CONTENTS

1.0 INTRODUCTION ............................................................................................... 1

1.1 Purpose ..................................................................................................... 1

1.2 Limitations ................................................................................................ 1

1.3 Site Location and Description ................................................................... 1

1.4 Previous Environmental Reports .............................................................. 2

2.0 SUBSURFACE INVESTIGATION .......................................................................... 2

2.1 Summary of Services ................................................................................. 2

2.2 Fieldwork Activities ................................................................................... 2

2.2.1 Site Preparation Services

2.2.2 Fieldwork Methodology

2.3 Laboratory Analysis .................................................................................. 4

2.3.1 Standards, Criteria and/or Guidance

2.3.2 Sample Submission

2.3.3 Laboratory Results

3.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................... 6

APPENDICES

A Fieldwork Map

B Data Summary Tables

C Laboratory Reports

PHASE II ENVIRONMENTAL SITE ASSESSMENT NOVEMBER 16, 2020

GBTS FILE: 20-0683.02 PAGE 1 OF 6

1.0 INTRODUCTION

1.1 Purpose

This Phase II Environmental Site Assessment (Report) documents environmental fieldwork performed by Gallagher Bassett Technical Services (GBTS) at the property located at 1416 Franklin Avenue, Borough of Bronx, New York City, New York (Site). Investigative and analytical work were performed to address potential environmental liabilities on specified portions of the subject property, which were identified during a previous Phase I investigation (see Section 1.4). The specific purpose of this Report is to summarize the work performed by GBTS and GBTS’s subcontractors, and to identify any on-site conditions that may require further investigation and/or remedial actions.

This Report describes all fieldwork methodologies for the work conducted by GBTS, includes discussions of the resulting analytical data from collected samples and provides conclusions and recommendations drawn from the fieldwork and analytical data.

1.2 Limitations

This written analysis summarizes the site characterization activities conducted on a specified portion of the above-referenced property and is not relevant to other portions of this property or any other property. It is a representation of those portions of the property analyzed as of the respective dates of fieldwork. This Report cannot account for activities or events resulting in contamination after the dates of fieldwork.

Services summarized in this Report were performed in accordance with generally accepted practices and established New York State Department of Environmental Conservation (NYSDEC) protocols. Unless specifically noted, GBTS’s findings and conclusions must be considered not as scientific certainties, but as probabilities based on professional judgement.

1.3 Site Location and Description

The property is an irregular, generally “L”-shaped 0.24-acre parcel located on the eastern side of Franklin Avenue and the northern side of East 170th Street. The property is vacant overgrown land with limited areas of pavement at the western portion. The property was historically used as an automotive repair facility from 1956 to 2004. Spill number 0508859 was reported for the Site due to contamination in an exterior stormwater basin (apparently identified during an earlier investigation). Laboratory analysis documented elevated volatile organic compounds (VOCs; gasoline compounds and a chlorinated solvent) in the water, supporting the conclusion that surface releases at the property may have impacted on-site soils.

A Fieldwork Map indicating specific Site characteristics is provided in Appendix A.



1.4 Previous Environmental Reports

A Phase I Environmental Site Assessment performed on the property by GBTS in August 2020 identified the following:

• Potential impacts from former on-site automotive repair activities (including an on-site closed spill event); and,

• Potential impacts from a former off-site dry cleaning activities.

2.0 SUBSURFACE INVESTIGATION

2.1 Summary of Services

GBTS conducted the following services at the Site on September 17, 2020:

• Advanced twelve (12) test pits (TP-01 through TP-12) throughout the Site to a maximum depth of 5 feet below surface grade (bsg);

• Installed six (6) temporary soil vapor probes (SV-01 through SV-06); and,

• Documented the presence or absence of contamination through sampling and laboratory analysis of subsurface soil and soil vapor samples.

This Report is divided into sections that document fieldwork methodology (Section 2.2) and laboratory results (Section 2.3), and present GBTS’s conclusions and recommendations (Section 3.0). A map indicating fieldwork locations and selected Site features is provided in Appendix A.

2.2 Fieldwork Activities

2.2.1 Site Preparation Services

GBTS requested a complete utility markout (as required by New York State Department of Labor regulations) and on-site personnel reviewed the markout and underground utility locations prior to the initiation of fieldwork.

2.2.2 Fieldwork Methodology

General Protocols

Encountered material was screened (as appropriate) with a properly calibrated MiniRAE 3000 (Model PGM 7320) photo-ionization detector (PID) for volatile organic vapors. GBTS documented field observations in log books, including specific characteristics, the presence of foreign materials, and any indications of contamination).

GBTS collected samples in general conformance with NYSDEC and NYSDOH fieldwork protocols. All field personnel wore dedicated, disposable gloves during relevant fieldwork activities, and any non-dedicated sampling instruments were decontaminated prior to media collection.



All samples were collected into appropriately-sized containers provided by the laboratory (with preservatives as required for the specific analysis), and were maintained at proper temperatures (using ice-packs and coolers as needed) while in GBTS’s custody. Samples were transported via courier on September 17, 2020 to York Analytical Laboratories, a NYSDOH-certified laboratory (ELAP Certification Number 10854) for chemical analyses under chain-of-custody procedures.

Extension of Test Pits

GBTS advanced twelve (12) test pits (TP-01 through TP-12) throughout the Site on September 17, 2020 (see Fieldwork Map). Test pits were located as follows:

• In the area of former on-site buildings (TP-01, TP-03, TP-04, TP-06 and TP-07);

• Near areas previously observed to have stained soils and/or used for storage of containers surrounding former on-site buildings to the south (TP-02), center (TP-05), north (TP-08) and northwest (TP-09); and,

• Former vehicle storage area at the western portion (TP-10, TP-11 and TP-12).

All test pits were advanced by personnel from Core Down Drilling LLC (CDD) using an excavator (Kubota KX057-4). Soil samples were collected directly from exposed areas in the test pits, utilizing clean, disposable equipment. Soil collection for VOC analysis was conducted according to USEPA Method 5035 fieldwork protocols, utilizing laboratory sampling kits.

Each test pit was advanced until bedrock was encountered (generally between 2.5 and 1.5 bsg, with depths between 4 and 5 feet bsg at the southern and western-central portions of the Site [TP-01 through TP-04]). Subsurface soils consisted of fill materials (unsorted medium to coarse sand and debris [e.g., brick, concrete and ash]) with trace roots to depths ranging from 0 to 4.5 feet bsg overlying brown medium to coarse sandy silt and trace clay. No field evidence of contamination was observed at any test pit location. Groundwater was not encountered during the extension of the test pits.

Collection of Soil Vapor

Six temporary soil vapor sampling points were installed at the following locations:

• In the area of former on-site buildings (SV-01 through SV-03);

• At the central portion (SV-04); and,

• Former vehicle storage area at the western portion (SV-05 and SV-06).

CDD constructed each temporary soil vapor probe by drilling a ½-inch hole in the soil to a depth of 4 feet (SV-01 through SV-03 and SV-06), 3 feet (SV-05) and 2 feet (SV-04) bsg. A ¼” Teflon tube attached to an air-stone was inserted to the invert of each hole, which was covered with clean #1 silica sand and backfilled with hydrated bentonite to prevent infiltration of surface air.



Each soil vapor boring was purged prior to sampling for at least a period of five minutes, using a GilAir air-sampling pump, at a rate of approximately 0.2 liters/minute. Samples were collected into 6-liter Summa Canisters equipped with two-hour flow controllers. No PID readings were recorded at soil vapor locations after purging.

2.3 Laboratory Analysis

2.3.1 Standards, Criteria and/or Guidance

Soil

Laboratory results for all compounds detected in soils are compared to NYSDEC Remedial Program Soil Cleanup Objectives (SCOs) for Unrestricted Use (UU) and Restricted-Residential Use (RRU) as provided in 6 NYCRR Subpart 375, Tables 375-6.8(a) and 375-6.8(b), and (as needed) Soil Cleanup Levels (for gasoline and fuel oil contaminated Soils) presented in NYSDEC CP-51 (Soil Cleanup Guidance, October 2010) Tables 2 through 3.

Vapor

The State of New York does not have any standards, criteria or guidance values for volatile chemicals in subsurface vapors (either soil vapor or sub-slab vapor). In the absence of SCG, soil vapor results were reviewed as a whole and compared to the results of all other environmental sampling.

2.3.2 Sample Submission

The scope of work included media sampling locations intended to provide a general screening of the Site. Submission of soil samples was biased (as warranted) based on field observations, including the presence or absence of elevated PID readings, unusual odors, discoloration, or, any other unusual patterns.

Soil samples were analyzed for the following: volatile organic compounds (VOCs) using USEPA Method 8260; semi-volatile organic compounds (SVOCs) using USEPA Method 8270; Target Analyte List (TAL) metals using USEPA Method 6010/7043; and, pesticides and PCBs using USEPA Methods 8081/8082. Soil vapor samples were analyzed for VOCs using USEPA Method TO-15 (SV-04 could not be analyzed due to a canister malfunction).

2.3.3 Laboratory Results

A summary of the results of the laboratory analyses is presented below. Results are referenced as parts per million (ppm, equivalent to milligrams per kilogram) for soil and micrograms per cubic meter (µg/m3) for soil vapor. Data summary tables and laboratory reports are provided as Appendices B and C, respectively.

SOIL

Soil data is summarized in Tables 1 through 4.



VOCs

No VOCs were detected in any soil sample.

SVOCs

Multiple polycyclic aromatic hydrocarbons (PAHs) were detected above RRU SCOs or UU SCOs at TP-10 and TP-12, including peak concentrations (reported at TP-10) of: benzo(a)anthracene (2.35 ppm, RRU SCO 1 ppm); benzo(a)pyrene (2.18 ppm, RRU SCO 1 ppm); benzo(b)fluoranthene (1.78 ppm, RRU SCO 1 ppm); benzo(k)fluoranthene (1.65 ppm, UU SCO 0.8 ppm), chrysene (2.35 ppm, RRU SCO 3.9 ppm); and, indeno(1,2,3-cd)pyrene (1.49 ppm, RRU SCO 0.5 ppm; also found at TP-04 at 0.578 ppm). Trace to low-levels of SVOCs were detected in all soil samples with the exception of TP-01.

Pesticides/PCBs

No pesticides were detected above RRU SCOs. DDT (0.032 ppm) and DDE (0.004 ppm) were detected above UU SCOs (0.0033 ppm) at TP-10; no pesticides were reported in any other sample. No PCBs were detected above SCOs. Trace levels of one PCB (Aroclor 1260) were detected at TP-04, TP-09 and TP-10, only.

TAL Metals

Elevated lead (637 ppm, RRU SCO 400 ppm) was reported at TP-03, and was detected above the UU SCO (63 ppm) in all other samples. Elevated mercury (1.24 ppm and 0.977 ppm, respectively, RRU SCO 0.81 ppm) was reported at TP-06 and TP-09, and was detected above the UU SCO (0.18 ppm) in multiple other samples, as were copper and zinc (peak concentrations of copper and zinc at TP-11 and TP-03, respectively).

SOIL VAPOR

Multiple VOCs were reported in all samples, generally at trace to low levels typical of commercial and/or urban settings.

A relatively elevated concentration of the chlorinated solvent tetrachloroethene (PCE; 160 µg/m3) was reported at SV-03. Relatively elevated concentrations of petroleum compounds were reported at SV-03 to SV-06 (location of peak impacts), including: 1,2,4-trimethylbenzene (73 µg/m3), cyclohexane (110 µg/m3), total xylene (168 µg/m3) and toluene (81 µg/m3).



3.0 CONCLUSIONS AND RECOMMENDATIONS

GBTS has completed the services summarized in Section 2.0 on specified portions of the property located at 1416 Franklin Avenue, Borough of Bronx, New York City, New York. Fieldwork (conducted to document the presence or absence of subsurface contamination resulting from historical use of the property) included: extension of twelve (12) test pits; installation of six (6) soil vapor implants; and, collection of soil and soil vapor samples.

Conclusions and recommendations (in bold), based on the fieldwork services and laboratory data, are as follows:

Shallow fill soils throughout the Site are impacted by elevated levels of polycyclic aromatic hydrocarbons (PAHs) and metals, with some analytes present at concentrations exceeding the NYSDEC Soil Cleanup Objectives for Restricted-Residential Use. Limited contamination by pesticides was identified at on sampling location. Other than PAHs, no significant concentrations of organic compounds were found in test pit samples. Soil and soil vapor data are consistent with low-grade impacts from historical commercial uses and are not likely indicative of any significant source areas (such as residual contamination from spill events). Based on the intended use, future Site development may require removal or capping of poor-quality soils and/or installation of a mitigation system to prevent soil vapor intrusion into new structures.

No further investigation is recommended at this time. Additional investigative and remedial work may be needed in coordination with Site development and/or regulatory requirements.

APPENDIX A

Fieldwork Map

SV-02SV-01

SV-04*

SV-03

SV-05TP-12

TP-11

TP-10

TP-08

TP-09

TP-07

TP-06

TP-05

TP-04

TP-03 TP-02 TP-01

residential

residential

Mott Hall111 Public

School

N

residential

mixed-use(deli & residential)

damaged paved areas

vacantovergrown

land

0 5025

SCALE IN FEET(APPROXIMATELY)

SV-06

Fieldwork Map File: 20-0683.02

Appendix A

Scale as shown

November 2020

All feature locations are approximate. This map is intended as a schematic to be used in conjunction with the associated report, and it should not be relied upon as a survey for planning or other activities.

Legend:subject property border

FRA

NKL

IN A

VEN

UE

EAST 170TH STREET

1416 Franklin AvenueBorough of the Bronx, New York

residential

residential

former on-site building locationslocation of 55-gallon drums (partially �lled with water)soil vapor location(* SV-04 could not be analyzed due to canister malfunction)test pit location

APPENDIX B

Data Summary Tables

Table 1: VOCs in SoilsGBTS File: 20-0683.02

Notes: SCOs based on NYSDEC Part 375-6.8 and CP-51 NA = not available Result Qualifiers: J = approximate E = estimated B = detected in blank D = diluted Table Page 1 of 12

All data in mg/Kg (ppm) Sample IDU= Not Detected ≥ value Sample DateData above SCOs shown in Bold Dilution Factor 1 1 1 1

VOCs, 8260 UU SCO RRU SCO Result Qualifier Result Qualifier Result Qualifier Result Qualifier1,1,1,2-Tetrachloroethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,1,1-Trichloroethane 0.68 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,1,2,2-Tetrachloroethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,1,2-Trichloro-1,2,2-trifluoroethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,1,2-Trichloroethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,1-Dichloroethane 0.27 26 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,1-Dichloroethylene (1,1-DCE) 0.33 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,2,3-Trichlorobenzene NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,2,3-Trichloropropane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,2,4-Trichlorobenzene NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,2,4-Trimethylbenzene 3.6 52 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,2-Dibromo-3-chloropropane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,2-Dibromoethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,2-Dichlorobenzene 1.1 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,2-Dichloroethane 0.02 3.1 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,2-Dichloropropane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,3,5-Trimethylbenzene 8.4 52 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,3-Dichlorobenzene 2.4 49 0.0037 U 0.0036 U 0.0026 U 0.0034 U1,4-Dichlorobenzene 1.8 13 0.0037 U 0.0036 U 0.0026 U 0.0034 U

1,4-Dioxane 0.1 13 0.074 U 0.071 U 0.052 U 0.067 U2-Butanone (MEK) 0.12 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U

2-Hexanone NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U4-Methyl-2-pentanone NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Acetone 0.05 100 0.0074 U 0.0071 U 0.0052 U 0.0067 UAcrolein NA NA 0.0074 U 0.0071 U 0.0052 U 0.0067 U

Acrylonitrile NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UBenzene 0.06 4.8 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Bromochloromethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UBromodichloromethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Bromoform NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UBromomethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UCarbon disulfide NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Carbon tetrachloride 0.76 2.4 0.0037 U 0.0036 U 0.0026 U 0.0034 UChlorobenzene 1.1 100 0.0037 U 0.0036 U 0.0026 U 0.0034 UChloroethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UChloroform 0.37 49 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Chloromethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 Ucis-1,2-Dichloroethylene (cis-DCE) 0.25 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U

cis-1,3-Dichloropropylene NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UCyclohexane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Dibromochloromethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UDibromomethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Dichlorodifluoromethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UEthyl Benzene 1 41 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Hexachlorobutadiene NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UIsopropylbenzene 2.3 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Methyl acetate NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UMethyl tert-butyl ether (MTBE) 0.93 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Methylcyclohexane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UMethylene chloride 0.05 100 0.0074 U 0.0071 U 0.0052 U 0.0067 U

n-Butylbenzene 12 100 0.0037 U 0.0036 U 0.0026 U 0.0034 Un-Propylbenzene 3.9 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U

o-Xylene 0.26 100 0.0037 U 0.0036 U 0.0026 U 0.0034 Up- & m- Xylenes 0.26 100 0.0074 U 0.0071 U 0.0052 U 0.0067 U

p-Isopropyltoluene 10 NA 0.0037 U 0.0036 U 0.0026 U 0.0034 Usec-Butylbenzene 11 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Styrene NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 Utert-Butyl alcohol (TBA) NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

tert-Butylbenzene 5.9 100 0.0037 U 0.0036 U 0.0026 U 0.0034 UTetrachloroethylene (PCE) 1.3 19 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Toluene 0.7 100 0.0037 U 0.0036 U 0.0026 U 0.0034 Utrans-1,2-Dichloroethylene (trans-DCE) 0.19 100 0.0037 U 0.0036 U 0.0026 U 0.0034 U

trans-1,3-Dichloropropylene NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 UTrichloroethylene (TCE) 0.47 21 0.0037 U 0.0036 U 0.0026 U 0.0034 UTrichlorofluoromethane NA NA 0.0037 U 0.0036 U 0.0026 U 0.0034 U

Vinyl chloride (VC) 0.02 0.9 0.0037 U 0.0036 U 0.0026 U 0.0034 UXylenes, Total 0.26 100 0.011 U 0.011 U 0.0078 U 0.01 U

(2020-09-17)TP-04 2TP-01 2 TP-02 2 TP-03 3

(2020-09-17) (2020-09-17) (2020-09-17)



All data in mg/Kg (ppm) Sample IDU= Not Detected ≥ value Sample DateData above SCOs shown in Bold Dilution Factor

VOCs, 8260 UU SCO RRU SCO1,1,1,2-Tetrachloroethane NA NA

1,1,1-Trichloroethane 0.68 1001,1,2,2-Tetrachloroethane NA NA

1,1,2-Trichloro-1,2,2-trifluoroethane NA NA1,1,2-Trichloroethane NA NA1,1-Dichloroethane 0.27 26

1,1-Dichloroethylene (1,1-DCE) 0.33 1001,2,3-Trichlorobenzene NA NA1,2,3-Trichloropropane NA NA1,2,4-Trichlorobenzene NA NA1,2,4-Trimethylbenzene 3.6 52

1,2-Dibromo-3-chloropropane NA NA1,2-Dibromoethane NA NA

1,2-Dichlorobenzene 1.1 1001,2-Dichloroethane 0.02 3.1

1,2-Dichloropropane NA NA1,3,5-Trimethylbenzene 8.4 52

1,3-Dichlorobenzene 2.4 491,4-Dichlorobenzene 1.8 13

1,4-Dioxane 0.1 132-Butanone (MEK) 0.12 100

2-Hexanone NA NA4-Methyl-2-pentanone NA NA

Acetone 0.05 100Acrolein NA NA

Acrylonitrile NA NABenzene 0.06 4.8

Bromochloromethane NA NABromodichloromethane NA NA

Bromoform NA NABromomethane NA NACarbon disulfide NA NA

Carbon tetrachloride 0.76 2.4Chlorobenzene 1.1 100Chloroethane NA NAChloroform 0.37 49

Chloromethane NA NAcis-1,2-Dichloroethylene (cis-DCE) 0.25 100

cis-1,3-Dichloropropylene NA NACyclohexane NA NA

Dibromochloromethane NA NADibromomethane NA NA

Dichlorodifluoromethane NA NAEthyl Benzene 1 41

Hexachlorobutadiene NA NAIsopropylbenzene 2.3 100

Methyl acetate NA NAMethyl tert-butyl ether (MTBE) 0.93 100

Methylcyclohexane NA NAMethylene chloride 0.05 100

n-Butylbenzene 12 100n-Propylbenzene 3.9 100

o-Xylene 0.26 100p- & m- Xylenes 0.26 100

p-Isopropyltoluene 10 NAsec-Butylbenzene 11 100

Styrene NA NAtert-Butyl alcohol (TBA) NA NA

tert-Butylbenzene 5.9 100Tetrachloroethylene (PCE) 1.3 19

Toluene 0.7 100trans-1,2-Dichloroethylene (trans-DCE) 0.19 100

trans-1,3-Dichloropropylene NA NATrichloroethylene (TCE) 0.47 21Trichlorofluoromethane NA NA

Vinyl chloride (VC) 0.02 0.9Xylenes, Total 0.26 100

1 1 1 1Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.08 U 0.057 U 0.077 U 0.082 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.008 U 0.0057 U 0.0077 U 0.0082 U0.008 U 0.0057 U 0.0077 U 0.0082 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.008 U 0.0057 U 0.0077 U 0.0082 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.008 U 0.0057 U 0.0077 U 0.0082 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.004 U 0.0028 U 0.0039 U 0.0041 U0.012 U 0.0085 U 0.012 U 0.012 U

TP-06 1.5(2020-09-17) (2020-09-17) (2020-09-17)(2020-09-17)

TP-05 1 TP-07 1 TP-08 2




VOCs, 8260 UU SCO RRU SCO1,1,1,2-Tetrachloroethane NA NA

1,1,1-Trichloroethane 0.68 1001,1,2,2-Tetrachloroethane NA NA

1,1,2-Trichloro-1,2,2-trifluoroethane NA NA1,1,2-Trichloroethane NA NA1,1-Dichloroethane 0.27 26

1,1-Dichloroethylene (1,1-DCE) 0.33 1001,2,3-Trichlorobenzene NA NA1,2,3-Trichloropropane NA NA1,2,4-Trichlorobenzene NA NA1,2,4-Trimethylbenzene 3.6 52

1,2-Dibromo-3-chloropropane NA NA1,2-Dibromoethane NA NA

1,2-Dichlorobenzene 1.1 1001,2-Dichloroethane 0.02 3.1

1,2-Dichloropropane NA NA1,3,5-Trimethylbenzene 8.4 52

1,3-Dichlorobenzene 2.4 491,4-Dichlorobenzene 1.8 13

1,4-Dioxane 0.1 132-Butanone (MEK) 0.12 100

2-Hexanone NA NA4-Methyl-2-pentanone NA NA

Acetone 0.05 100Acrolein NA NA

Acrylonitrile NA NABenzene 0.06 4.8

Bromochloromethane NA NABromodichloromethane NA NA

Bromoform NA NABromomethane NA NACarbon disulfide NA NA

Carbon tetrachloride 0.76 2.4Chlorobenzene 1.1 100Chloroethane NA NAChloroform 0.37 49

Chloromethane NA NAcis-1,2-Dichloroethylene (cis-DCE) 0.25 100

cis-1,3-Dichloropropylene NA NACyclohexane NA NA

Dibromochloromethane NA NADibromomethane NA NA

Dichlorodifluoromethane NA NAEthyl Benzene 1 41

Hexachlorobutadiene NA NAIsopropylbenzene 2.3 100

Methyl acetate NA NAMethyl tert-butyl ether (MTBE) 0.93 100

Methylcyclohexane NA NAMethylene chloride 0.05 100

n-Butylbenzene 12 100n-Propylbenzene 3.9 100

o-Xylene 0.26 100p- & m- Xylenes 0.26 100

p-Isopropyltoluene 10 NAsec-Butylbenzene 11 100

Styrene NA NAtert-Butyl alcohol (TBA) NA NA

tert-Butylbenzene 5.9 100Tetrachloroethylene (PCE) 1.3 19

Toluene 0.7 100trans-1,2-Dichloroethylene (trans-DCE) 0.19 100

trans-1,3-Dichloropropylene NA NATrichloroethylene (TCE) 0.47 21Trichlorofluoromethane NA NA

Vinyl chloride (VC) 0.02 0.9Xylenes, Total 0.26 100

1 1 1 1Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.065 U 0.072 U 0.052 U 0.065 U

0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0065 U 0.0072 U 0.0052 U 0.0065 U0.0065 U 0.0072 U 0.0052 U 0.0065 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0065 U 0.0072 U 0.0052 U 0.0065 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0065 U 0.0072 U 0.0052 U 0.0065 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0033 U 0.0036 U 0.0026 U 0.0032 U0.0098 U 0.011 U 0.0078 U 0.0097 U

TP-10 1 TP-11 2 TP-12 1(2020-09-17) (2020-09-17) (2020-09-17) (2020-09-17)

TP-09 3

Table 2: SVOCs in SoilsGBTS File: 20-0683.02



SVOCs, 8270 UU SCO RRU SCO Result Qualifier Result Qualifier Result Qualifier Result Qualifier1,1'-Biphenyl NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

1,2,4,5-Tetrachlorobenzene NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 U1,2,4-Trichlorobenzene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U1,2-Dichlorobenzene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

1,2-Diphenylhydrazine (Azobenzene) NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U1,3-Dichlorobenzene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U1,4-Dichlorobenzene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

2,3,4,6-Tetrachlorophenol NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 U2,4,5-Trichlorophenol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U2,4,6-Trichlorophenol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U2,4-Dichlorophenol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U2,4-Dimethylphenol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U2,4-Dinitrophenol NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 U2,4-Dinitrotoluene NA NA 0.0454 U 0.0452 U 0.951 D 0.0459 U2,6-Dinitrotoluene NA NA 0.0454 U 0.0452 U 1.38 D 0.0459 U

2-Chloronaphthalene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U2-Chlorophenol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

2-Methylnaphthalene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U2-Methylphenol 0.33 100 0.0454 U 0.0452 U 0.0494 U 0.0459 U2-Nitroaniline NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 U2-Nitrophenol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

3- & 4-Methylphenols 0.33 100 0.0454 U 0.0452 U 0.0494 U 0.0459 U3,3'-Dichlorobenzidine NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

3-Nitroaniline NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 U4,6-Dinitro-2-methylphenol NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 U

4-Bromophenyl phenyl ether NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U4-Chloro-3-methylphenol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

4-Chloroaniline NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U4-Chlorophenyl phenyl ether NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

4-Nitroaniline NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 U4-Nitrophenol NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 UAcenaphthene 20 100 0.0454 U 0.0452 U 0.0494 U 0.0564 JD

Acenaphthylene 100 100 0.0454 U 0.0512 JD 0.0494 U 0.104 DAcetophenone NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Aniline NA NA 0.182 U 0.181 U 0.197 U 0.183 UAnthracene 100 100 0.0454 U 0.0452 U 0.438 D 0.203 D

Atrazine NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UBenzaldehyde NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Benzidine NA NA 0.182 U 0.181 U 0.197 U 0.183 UBenzo(a)anthracene 1 1 0.0454 U 0.129 D 0.344 D 0.739 D

Benzo(a)pyrene 1 1 0.0454 U 0.156 D 0.299 D 0.737 DBenzo(b)fluoranthene 1 1 0.0454 U 0.16 D 0.248 D 0.691 DBenzo(g,h,i)perylene 100 100 0.0454 U 0.154 D 0.201 D 0.566 DBenzo(k)fluoranthene 0.8 3.9 0.0454 U 0.141 D 0.24 D 0.648 D

Benzoic acid NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UBenzyl alcohol NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Benzyl butyl phthalate NA NA 0.0454 U 0.617 D 0.0741 JD 0.673 DBis(2-chloroethoxy)methane NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Bis(2-chloroethyl)ether NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UBis(2-chloroisopropyl)ether NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UBis(2-ethylhexyl)phthalate NA NA 0.0454 U 0.0902 D 0.0494 U 0.129 D

Caprolactam NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 UCarbazole NA NA 0.0454 U 0.0452 U 0.0494 U 0.113 DChrysene 1 3.9 0.0454 U 0.152 D 0.366 D 0.839 D

Dibenzo(a,h)anthracene 0.33 0.33 0.0454 U 0.0452 U 0.0494 U 0.0459 UDibenzofuran 7 59 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Diethyl phthalate NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UDimethyl phthalate NA NA 0.0454 U 0.0452 U 0.459 D 0.0459 UDi-n-butyl phthalate NA NA 0.0454 U 0.062 JD 0.0494 U 0.0681 JDDi-n-octyl phthalate NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Diphenylamine NA NA 0.0907 U 0.0902 U 0.0986 U 0.0916 UFluoranthene 100 100 0.0454 U 0.229 D 0.589 D 1.47 D

Fluorene 30 100 0.0454 U 0.0452 U 0.0494 U 0.0637 JDHexachlorobenzene 0.33 1.2 0.0454 U 0.0452 U 0.0494 U 0.0459 UHexachlorobutadiene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Hexachlorocyclopentadiene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UHexachloroethane NA NA 0.0454 U 0.0452 U 0.927 D 0.0459 U

Indeno(1,2,3-cd)pyrene 0.5 0.5 0.0454 U 0.149 D 0.221 D 0.578 DIsophorone NA NA 0.0454 U 0.0452 U 0.439 D 0.0459 U

Naphthalene 12 100 0.0454 U 0.0452 U 0.0494 U 0.0459 UNitrobenzene NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 U

N-Nitrosodimethylamine NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UN-nitroso-di-n-propylamine NA NA 0.0454 U 0.0452 U 0.102 D 0.0459 U

N-Nitrosodiphenylamine NA NA 0.0454 U 0.0452 U 0.0494 U 0.0459 UPentachlorophenol 0.8 6.7 0.0454 U 0.0452 U 0.0494 U 0.0459 U

Phenanthrene 100 100 0.0454 U 0.123 D 0.463 D 0.957 DPhenol 0.33 100 0.0454 U 0.0452 U 0.0494 U 0.0459 UPyrene 100 100 0.0454 U 0.214 D 0.627 D 1.48 D

Analyte DetectedAnalyte Above UU SCOAnalyte Above RRU SCO

(2020-09-17) (2020-09-17) (2020-09-17) (2020-09-17)TP-01 0-2 TP-02 0-2 TP-03 2-4 TP-04 0-2




SVOCs, 8270 UU SCO RRU SCO1,1'-Biphenyl NA NA

1,2,4,5-Tetrachlorobenzene NA NA1,2,4-Trichlorobenzene NA NA1,2-Dichlorobenzene NA NA

1,2-Diphenylhydrazine (Azobenzene) NA NA1,3-Dichlorobenzene NA NA1,4-Dichlorobenzene NA NA

2,3,4,6-Tetrachlorophenol NA NA2,4,5-Trichlorophenol NA NA2,4,6-Trichlorophenol NA NA2,4-Dichlorophenol NA NA2,4-Dimethylphenol NA NA2,4-Dinitrophenol NA NA2,4-Dinitrotoluene NA NA2,6-Dinitrotoluene NA NA

2-Chloronaphthalene NA NA2-Chlorophenol NA NA

2-Methylnaphthalene NA NA2-Methylphenol 0.33 1002-Nitroaniline NA NA2-Nitrophenol NA NA

3- & 4-Methylphenols 0.33 1003,3'-Dichlorobenzidine NA NA

3-Nitroaniline NA NA4,6-Dinitro-2-methylphenol NA NA

4-Bromophenyl phenyl ether NA NA4-Chloro-3-methylphenol NA NA

4-Chloroaniline NA NA4-Chlorophenyl phenyl ether NA NA

4-Nitroaniline NA NA4-Nitrophenol NA NAAcenaphthene 20 100

Acenaphthylene 100 100Acetophenone NA NA

Aniline NA NAAnthracene 100 100

Atrazine NA NABenzaldehyde NA NA

Benzidine NA NABenzo(a)anthracene 1 1

Benzo(a)pyrene 1 1Benzo(b)fluoranthene 1 1Benzo(g,h,i)perylene 100 100Benzo(k)fluoranthene 0.8 3.9

Benzoic acid NA NABenzyl alcohol NA NA

Benzyl butyl phthalate NA NABis(2-chloroethoxy)methane NA NA

Bis(2-chloroethyl)ether NA NABis(2-chloroisopropyl)ether NA NABis(2-ethylhexyl)phthalate NA NA

Caprolactam NA NACarbazole NA NAChrysene 1 3.9

Dibenzo(a,h)anthracene 0.33 0.33Dibenzofuran 7 59

Diethyl phthalate NA NADimethyl phthalate NA NADi-n-butyl phthalate NA NADi-n-octyl phthalate NA NA

Diphenylamine NA NAFluoranthene 100 100

Fluorene 30 100Hexachlorobenzene 0.33 1.2Hexachlorobutadiene NA NA

Hexachlorocyclopentadiene NA NAHexachloroethane NA NA

Indeno(1,2,3-cd)pyrene 0.5 0.5Isophorone NA NA

Naphthalene 12 100Nitrobenzene NA NA

N-Nitrosodimethylamine NA NAN-nitroso-di-n-propylamine NA NA

N-Nitrosodiphenylamine NA NAPentachlorophenol 0.8 6.7

Phenanthrene 100 100Phenol 0.33 100Pyrene 100 100


2 2 2 2Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.127 D 0.0475 U 0.0468 U 0.0563 JD

0.0462 U 0.0475 U 0.0468 U 0.0484 U0.185 U 0.19 U 0.187 U 0.193 U

0.0766 JD 0.0475 U 0.0508 JD 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.185 U 0.19 U 0.187 U 0.193 U0.251 D 0.154 D 0.136 D 0.148 D0.267 D 0.186 D 0.147 D 0.161 D0.279 D 0.162 D 0.125 D 0.159 D0.237 D 0.122 D 0.111 D 0.143 D0.262 D 0.142 D 0.119 D 0.141 D

0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U

1.15 D 0.268 D 1.31 D 0.802 D0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.105 D 0.123 D0.0922 U 0.0948 U 0.0934 U 0.0965 U0.0486 JD 0.0475 U 0.0468 U 0.0484 U0.292 D 0.164 D 0.154 D 0.161 D

0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0501 JD 0.0475 U 0.121 D 0.0648 JD0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0922 U 0.0948 U 0.0934 U 0.0965 U0.491 D 0.32 D 0.264 D 0.271 D

0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.239 D 0.13 D 0.113 D 0.145 D

0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.0462 U 0.0475 U 0.0468 U 0.0484 U0.267 D 0.114 D 0.117 D 0.134 D

0.0462 U 0.0475 U 0.0468 U 0.0484 U0.477 D 0.309 D 0.247 D 0.271 D

(2020-09-17) (2020-09-17)TP-06 0-1.5

(2020-09-17) (2020-09-17)TP-07 0-2 TP-08 0-2TP-05 0-2




SVOCs, 8270 UU SCO RRU SCO1,1'-Biphenyl NA NA

1,2,4,5-Tetrachlorobenzene NA NA1,2,4-Trichlorobenzene NA NA1,2-Dichlorobenzene NA NA

1,2-Diphenylhydrazine (Azobenzene) NA NA1,3-Dichlorobenzene NA NA1,4-Dichlorobenzene NA NA

2,3,4,6-Tetrachlorophenol NA NA2,4,5-Trichlorophenol NA NA2,4,6-Trichlorophenol NA NA2,4-Dichlorophenol NA NA2,4-Dimethylphenol NA NA2,4-Dinitrophenol NA NA2,4-Dinitrotoluene NA NA2,6-Dinitrotoluene NA NA

2-Chloronaphthalene NA NA2-Chlorophenol NA NA

2-Methylnaphthalene NA NA2-Methylphenol 0.33 1002-Nitroaniline NA NA2-Nitrophenol NA NA

3- & 4-Methylphenols 0.33 1003,3'-Dichlorobenzidine NA NA

3-Nitroaniline NA NA4,6-Dinitro-2-methylphenol NA NA

4-Bromophenyl phenyl ether NA NA4-Chloro-3-methylphenol NA NA

4-Chloroaniline NA NA4-Chlorophenyl phenyl ether NA NA

4-Nitroaniline NA NA4-Nitrophenol NA NAAcenaphthene 20 100

Acenaphthylene 100 100Acetophenone NA NA

Aniline NA NAAnthracene 100 100

Atrazine NA NABenzaldehyde NA NA

Benzidine NA NABenzo(a)anthracene 1 1

Benzo(a)pyrene 1 1Benzo(b)fluoranthene 1 1Benzo(g,h,i)perylene 100 100Benzo(k)fluoranthene 0.8 3.9

Benzoic acid NA NABenzyl alcohol NA NA

Benzyl butyl phthalate NA NABis(2-chloroethoxy)methane NA NA

Bis(2-chloroethyl)ether NA NABis(2-chloroisopropyl)ether NA NABis(2-ethylhexyl)phthalate NA NA

Caprolactam NA NACarbazole NA NAChrysene 1 3.9

Dibenzo(a,h)anthracene 0.33 0.33Dibenzofuran 7 59

Diethyl phthalate NA NADimethyl phthalate NA NADi-n-butyl phthalate NA NADi-n-octyl phthalate NA NA

Diphenylamine NA NAFluoranthene 100 100

Fluorene 30 100Hexachlorobenzene 0.33 1.2Hexachlorobutadiene NA NA

Hexachlorocyclopentadiene NA NAHexachloroethane NA NA

Indeno(1,2,3-cd)pyrene 0.5 0.5Isophorone NA NA

Naphthalene 12 100Nitrobenzene NA NA

N-Nitrosodimethylamine NA NAN-nitroso-di-n-propylamine NA NA

N-Nitrosodiphenylamine NA NAPentachlorophenol 0.8 6.7

Phenanthrene 100 100Phenol 0.33 100Pyrene 100 100


2 10 2 2Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.047 U 0.0584 JD 0.0476 U 0.046 U

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.047 U 0.0452 U 0.0476 U 0.867 D0.047 U 0.0452 U 0.0476 U 1.26 D0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0988 D 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0642 JD 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.0938 U 0.0902 U 0.0951 U 0.0917 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.0938 U 0.0902 U 0.0951 U 0.0917 U0.047 U 0.396 D 0.0476 U 0.099 D0.093 JD 0.392 D 0.0509 JD 0.085 JD0.047 U 0.0452 U 0.0476 U 0.046 U0.188 U 0.181 U 0.19 U 0.184 U0.104 D 1.19 D 0.0783 JD 0.284 D0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.188 U 0.181 U 0.19 U 0.184 U0.422 D 2.35 D 0.264 D 1.03 D0.467 D 2.18 D 0.28 D 1.07 D0.38 D 1.78 D 0.239 D 0.946 D0.341 D 1.48 D 0.198 D 0.861 D0.369 D 1.65 D 0.228 D 0.933 D0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U1.37 D 2.84 D 0.599 D 0.288 D0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.357 D 0.351 D 0.144 D 0.199 D

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.0473 JD 0.345 D 0.0476 U 0.15 D0.482 D 2.35 D 0.289 D 1.09 D0.047 U 0.113 D 0.0737 JD 0.0645 JD0.047 U 0.162 D 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U

0.0975 D 0.321 D 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U

0.0938 U 0.0902 U 0.0951 U 0.0917 U0.803 D 4.79 D 0.45 D 1.89 D0.047 U 0.374 D 0.0476 U 0.0909 JD0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.891 D0.338 D 1.49 D 0.21 D 0.826 D0.047 U 0.0452 U 0.0476 U 0.191 D0.047 U 0.173 D 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.046 U0.047 U 0.0452 U 0.0476 U 0.117 D0.047 U 0.0452 U 0.0476 U 0.046 U0.377 D 4.97 D 0.254 D 1.24 D0.047 U 0.0452 U 0.0476 U 0.046 U

0.8 D 5.34 D 0.48 D 1.98 D

(2020-09-17)TP-12 0-1.5

(2020-09-17) (2020-09-17) (2020-09-17)TP-09 1-3 TP-10 0-2 TP-11 0-2

Table 3: Pesticides and PCBs in SoilsGBTS File: 20-0683.02



Pesticides, 8081 UU SCO RRU SCO Result Qualifier Result Qualifier Result Qualifier Result Qualifier4,4'-DDD 0.0033 13 0.002 U 0.002 U 0.002 U 0.002 U4,4'-DDE 0.0033 8.9 0.002 U 0.002 U 0.002 U 0.002 U4,4'-DDT 0.0033 7.9 0.002 U 0.002 U 0.002 U 0.002 U

Aldrin 0.005 0.097 0.002 U 0.002 U 0.002 U 0.002 Ualpha-BHC 0.02 0.48 0.002 U 0.002 U 0.002 U 0.002 U

alpha-Chlordane 0.094 4.2 0.002 U 0.002 U 0.002 U 0.002 Ubeta-BHC 0.036 0.36 0.002 U 0.002 U 0.002 U 0.002 U

Chlordane (total) NA NA 0.036 U 0.036 U 0.040 U 0.036 Udelta-BHC 0.04 100 0.002 U 0.002 U 0.002 U 0.002 U

Dieldrin 0.005 0.2 0.002 U 0.002 U 0.002 U 0.002 UEndosulfan I 2.4 24 0.002 U 0.002 U 0.002 U 0.002 UEndosulfan II 2.4 24 0.002 U 0.002 U 0.002 U 0.002 U

Endosulfan sulfate 2.4 24 0.002 U 0.002 U 0.002 U 0.002 UEndrin 0.014 11 0.002 U 0.002 U 0.002 U 0.002 U

Endrin aldehyde NA NA 0.002 U 0.002 U 0.002 U 0.002 UEndrin ketone NA NA 0.002 U 0.002 U 0.002 U 0.002 U

gamma-BHC (Lindane) 0.1 1.3 0.002 U 0.002 U 0.002 U 0.002 Ugamma-Chlordane NA NA 0.002 U 0.002 U 0.002 U 0.002 U

Heptachlor 0.042 2.1 0.002 U 0.002 U 0.002 U 0.002 UHeptachlor Epoxide NA NA 0.002 U 0.002 U 0.002 U 0.002 U

Methoxychlor NA NA 0.009 U 0.009 U 0.010 U 0.009 UToxaphene NA NA 0.091 U 0.092 U 0.101 U 0.091 U

Sample IDSample Date

Dilution Factor 1 1 1 1PCBs, 8082 UU SCO RRU SCO Result Qualifier Result Qualifier Result Qualifier Result QualifierAroclor 1016 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor 1221 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor 1232 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor 1242 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor 1248 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor 1254 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor 1260 0.1 1.00 0.018 U 0.018 U 0.020 U 0.022Aroclor 1262 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor 1268 0.1 1.00 0.018 U 0.018 U 0.020 U 0.018 UAroclor, Total 0.1 1.00 0.018 U 0.018 U 0.020 U 0.022

Analyte DetectedAnalyte Above UU SCO

(2020-09-17) (2020-09-17) (2020-09-17)(2020-09-17)TP-03 2-4 TP-04 0-2

(2020-09-17) (2020-09-17)TP-03 2-4 TP-04 0-2

TP-01 0-2

TP-01 0-2(2020-09-17)

TP-02 0-2(2020-09-17)

TP-02 0-2




Pesticides, 8081 UU SCO RRU SCO4,4'-DDD 0.0033 134,4'-DDE 0.0033 8.94,4'-DDT 0.0033 7.9

Aldrin 0.005 0.097alpha-BHC 0.02 0.48

alpha-Chlordane 0.094 4.2beta-BHC 0.036 0.36

Chlordane (total) NA NAdelta-BHC 0.04 100

Dieldrin 0.005 0.2Endosulfan I 2.4 24Endosulfan II 2.4 24

Endosulfan sulfate 2.4 24Endrin 0.014 11

Endrin aldehyde NA NAEndrin ketone NA NA

gamma-BHC (Lindane) 0.1 1.3gamma-Chlordane NA NA

Heptachlor 0.042 2.1Heptachlor Epoxide NA NA

Methoxychlor NA NAToxaphene NA NA


Dilution FactorPCBs, 8082 UU SCO RRU SCOAroclor 1016 0.1 1.00Aroclor 1221 0.1 1.00Aroclor 1232 0.1 1.00Aroclor 1242 0.1 1.00Aroclor 1248 0.1 1.00Aroclor 1254 0.1 1.00Aroclor 1260 0.1 1.00Aroclor 1262 0.1 1.00Aroclor 1268 0.1 1.00Aroclor, Total 0.1 1.00


5 5 5 5Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.036 U 0.038 U 0.037 U 0.038 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.009 U 0.009 U 0.009 U 0.010 U0.092 U 0.095 U 0.095 U 0.097 U

1 1 1 1Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U0.018 U 0.019 U 0.019 U 0.019 U

(2020-09-17)TP-08 0-2TP-05 0-2 TP-06 0-1.5

(2020-09-17)TP-07 0-2

(2020-09-17) (2020-09-17)

(2020-09-17)(2020-09-17) (2020-09-17) (2020-09-17)TP-08 0-2TP-05 0-2 TP-06 0-1.5 TP-07 0-2




Pesticides, 8081 UU SCO RRU SCO4,4'-DDD 0.0033 134,4'-DDE 0.0033 8.94,4'-DDT 0.0033 7.9

Aldrin 0.005 0.097alpha-BHC 0.02 0.48

alpha-Chlordane 0.094 4.2beta-BHC 0.036 0.36

Chlordane (total) NA NAdelta-BHC 0.04 100

Dieldrin 0.005 0.2Endosulfan I 2.4 24Endosulfan II 2.4 24

Endosulfan sulfate 2.4 24Endrin 0.014 11

Endrin aldehyde NA NAEndrin ketone NA NA

gamma-BHC (Lindane) 0.1 1.3gamma-Chlordane NA NA

Heptachlor 0.042 2.1Heptachlor Epoxide NA NA

Methoxychlor NA NAToxaphene NA NA


Dilution FactorPCBs, 8082 UU SCO RRU SCOAroclor 1016 0.1 1.00Aroclor 1221 0.1 1.00Aroclor 1232 0.1 1.00Aroclor 1242 0.1 1.00Aroclor 1248 0.1 1.00Aroclor 1254 0.1 1.00Aroclor 1260 0.1 1.00Aroclor 1262 0.1 1.00Aroclor 1268 0.1 1.00Aroclor, Total 0.1 1.00


5 5 5 5Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.004 D 0.002 U 0.002 U0.002 U 0.032 DP 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.037 U 0.036 U 0.038 U 0.036 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.002 U 0.002 U 0.002 U 0.002 U0.009 U 0.009 U 0.009 U 0.009 U0.094 U 0.090 U 0.095 U 0.092 U

1 1 1 1Result Qualifier Result Qualifier Result Qualifier Result Qualifier0.019 U 0.018 U 0.019 U 0.018 U0.019 U 0.018 U 0.019 U 0.018 U0.019 U 0.018 U 0.019 U 0.018 U0.019 U 0.018 U 0.019 U 0.018 U0.019 U 0.018 U 0.019 U 0.018 U0.019 U 0.018 U 0.019 U 0.018 U0.033 0.019 0.019 U 0.018 U0.019 U 0.018 U 0.019 U 0.018 U0.019 U 0.018 U 0.019 U 0.018 U0.033 0.019 0.019 U 0.018 U

(2020-09-17) (2020-09-17) (2020-09-17)TP-12 0-1.5(2020-09-17)

TP-09 1-3 TP-10 0-2 TP-11 0-2

(2020-09-17) (2020-09-17) (2020-09-17) (2020-09-17)TP-09 1-3 TP-10 0-2 TP-11 0-2 TP-12 0-1.5

Table 4: TAL Metals in SoilsGBTS File: 20-0683.02



Metals, 6010 and 7473 UU SCO RRU SCO Result Qualifier Result Qualifier Result Qualifier Result QualifierAluminum NA NA 1,140 7,600 16,000 3,030Antimony NA NA 2.74 U 2.77 U 3.02 U 2.76 UArsenic 13 16 2.94 5.97 8.56 11.9Barium 350 400 42.3 154 198 87.2

Beryllium 7.2 72 0.055 U 0.055 0.06 U 0.055 UCadmium 2.5 4.3 0.328 U 1.84 U 0.81 0.806Calcium NA NA 882 20,600 2,630 4,960

Chromium 30 180 8.93 14.4 22.6 8.98Chromium (hexavalent) 1 110 NA NA 0.605 U NA

Cobalt NA NA 4.45 4.2 9.85 4.04Copper 50 270 42.6 59.9 37.9 59.1

Iron NA NA 2,450 10,200 16,200 6,250Lead 63 400 72.6 330 637 162

Magnesium NA NA 113 2,730 2,810 665Manganese 1,600 2,000 20.5 163 440 91

Mercury 0.18 0.81 0.0338 0.273 0.501 0.406Nickel 30 310 9.89 16.8 17 16.8

Potassium NA NA 242 B 924 859 B 454 BSelenium 3.9 180 2.74 U 2.77 B 3.02 U 2.76 U

Silver 2 180 0.547 U 0.554 U 0.605 U 0.553 USodium NA NA 68.8 554 U 157 149Thallium NA NA 2.74 U 2.77 3.02 U 2.76 U

Vanadium NA NA 10.4 21.3 U 30.7 13.1Zinc 109 10,000 28.2 424 427 228

Cyanide (total) 27 27 NA NA 0.605 U NAAnalyte DetectedAnalyte Above UU SCOAnalyte Above RRU SCO

(2020-09-17) (2020-09-17) (2020-09-17)(2020-09-17)TP-01 0-2 TP-02 0-2 TP-03 2-4 TP-04 0-2




Metals, 6010 and 7473 UU SCO RRU SCOAluminum NA NAAntimony NA NAArsenic 13 16Barium 350 400

Beryllium 7.2 72Cadmium 2.5 4.3Calcium NA NA

Chromium 30 180Chromium (hexavalent) 1 110

Cobalt NA NACopper 50 270

Iron NA NALead 63 400

Magnesium NA NAManganese 1,600 2,000

Mercury 0.18 0.81Nickel 30 310

Potassium NA NASelenium 3.9 180

Silver 2 180Sodium NA NAThallium NA NA

Vanadium NA NAZinc 109 10,000

Cyanide (total) 27 27


1 1 1 1Result Qualifier Result Qualifier Result Qualifier Result Qualifier9,280 18,100 7,010 8,2402.78 U 2.86 U 10.5 2.9 U6.06 3.89 5.93 9.52153 135 131 173

0.056 U 0.057 U 0.057 U 0.058 U1.5 0.499 0.726 1.68

36,100 11,700 15,500 25,20014.9 24.8 14.4 23.9NA NA 0.569 U NA4.11 9.28 5.57 5.7744.1 26.6 62.6 79.1

14,500 19,000 19,500 29,600193 106 136 208

4,960 4,140 1,520 2,790204 810 237 254

0.435 1.24 0.495 0.23214.9 20.1 16 26.81,210 B 1,570 B 745 B 1,060 B2.78 U 2.86 U 2.85 U 2.9 U0.556 U 0.572 U 0.569 U 0.58 U742 205 223 5952.78 U 2.86 U 2.85 U 2.9 U21.2 36 16.7 20.9355 114 329 341NA NA 0.569 U NA

(2020-09-17) (2020-09-17)(2020-09-17) (2020-09-17)TP-05 0-2 TP-06 0-1.5 TP-07 0-2 TP-08 0-2




Metals, 6010 and 7473 UU SCO RRU SCOAluminum NA NAAntimony NA NAArsenic 13 16Barium 350 400

Beryllium 7.2 72Cadmium 2.5 4.3Calcium NA NA

Chromium 30 180Chromium (hexavalent) 1 110

Cobalt NA NACopper 50 270

Iron NA NALead 63 400

Magnesium NA NAManganese 1,600 2,000

Mercury 0.18 0.81Nickel 30 310

Potassium NA NASelenium 3.9 180

Silver 2 180Sodium NA NAThallium NA NA

Vanadium NA NAZinc 109 10,000

Cyanide (total) 27 27


1 1 1 1Result Qualifier Result Qualifier Result Qualifier Result Qualifier12,700 18,000 11,100 16,1002.83 U 2.71 U 2.86 U 2.76 U4.68 6.86 6.9 5.27161 158 227 98.8

0.057 U 0.054 U 0.057 U 0.055 U0.808 0.683 1.21 0.6744,070 3,560 23,300 14,40022.2 28.1 18 25.4NA NA 0.572 U NA7.9 8.61 4.92 8.8445.5 43.7 80.1 54.7

15,200 19,100 12,900 17,200207 233 250 147

3,020 3,600 9,990 7,210466 415 253 323

0.977 0.597 0.344 0.18523 19.6 18.5 26

1,460 B 832 B 770 B 931 B2.83 U 2.71 U 2.86 U 2.76 U0.566 U 0.543 U 0.572 U 0.552 U129 135 245 5492.83 U 2.71 U 2.86 U 2.76 U25.5 37.1 28.2 41.7379 185 287 115NA NA 0.572 U NA

TP-11 0-2 TP-12 0-1.5(2020-09-17) (2020-09-17)

TP-09 1-3 TP-10 0-2(2020-09-17) (2020-09-17)

Table 5: VOCs in Soil VaporGBTS File: 20-0683.02

Notes: NA = not available Result Qualifiers: J = approximate E = estimated B = detected in blank Table Page 1 of 1

Sample IDAll data in µg/m 3 Sample DateU= Not Detected ≥ value Dilution Factor 1.752 1.88 1.807 1.784 1.599

Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier1.2 U 1.3 U 1.2 U 1.2 U 1.1 U

0.96 U 1 U 0.99 U 0.97 U 0.87 U1.2 U 1.3 U 1.2 U 1.2 U 1.1 U1.3 U 1.4 U 1.4 U 1.4 U 1.2 U

0.96 U 1 U 0.99 U 0.97 U 0.87 U0.71 U 0.76 U 0.73 U 0.72 U 0.65 U0.69 U 0.75 U 0.72 U 0.71 U 0.63 U1.3 U 1.4 U 1.3 U 1.3 U 1.2 U42 D 35 D 41 D 36 D 73 D1.3 U 1.4 U 1.4 U 1.4 U 1.2 U1.1 U 1.1 U 1.1 U 1.1 U 0.96 U

0.71 U 0.76 U 1.2 D 0.72 U 0.65 U0.81 U 0.87 U 0.83 U 0.82 U 0.74 U1.2 U 1.3 U 1.3 U 1.2 U 1.1 U10 D 8.8 D 10 D 8.5 D 17 D1.2 U 1.2 U 1.2 U 1.2 U 1.1 U1.1 U 1.1 U 1.1 U 1.1 U 0.96 U

0.81 U 0.87 U 0.84 U 0.82 U 0.74 U1.1 U 1.1 U 1.1 U 1.1 U 0.96 U1.3 U 1.4 U 1.3 U 1.3 U 1.2 U1.3 D 1.9 D 4.6 D 0.95 D 14 D1.4 U 1.5 U 3.1 D 1.5 U 2.8 D2.7 U 2.9 U 2.8 U 2.8 U 2.5 U

0.72 U 0.77 U 0.89 D 1.8 D 4.1 D22 D 36 D 35 D 9.8 D 150 D

0.38 U 0.41 U 0.39 U 0.39 U 0.35 U0.67 D 0.72 D 1.7 D 0.85 D 4.3 D0.91 U 0.97 U 0.94 U 0.92 U 0.83 U1.2 U 1.3 U 1.2 U 1.2 U 1.1 U1.8 U 1.9 U 1.9 U 1.8 U 1.7 U

0.68 U 0.73 U 0.7 U 0.69 U 0.62 U0.93 D 0.59 D 2.8 D 0.56 U 0.5 U0.28 U 0.3 U 0.28 U 0.28 U 0.25 U0.81 U 0.87 U 0.83 U 0.82 U 0.74 U0.46 U 0.5 U 0.48 U 0.47 U 0.42 U0.86 U 1.1 D 0.88 U 1.5 D 1.2 D0.36 U 0.39 D 0.49 D 0.37 D 0.66 D0.69 U 0.75 U 0.72 U 0.71 U 0.63 U0.8 U 0.85 U 0.82 U 0.81 U 0.73 U27 D 29 D 95 D 110 D 31 D1.5 U 1.6 U 1.5 U 1.5 U 1.4 U

0.87 U 0.93 U 0.89 U 0.88 U 0.79 U1.3 U 1.4 U 1.3 U 1.3 U 1.2 U11 D 11 D 15 D 15 D 37 D1.9 U 2 U 1.9 U 1.9 U 1.7 U18 D 9.8 D 11 D 130 D 49 D

0.79 D 0.85 D 1.1 D 0.73 U 0.79 D0.63 U 0.68 U 0.65 U 0.64 U 0.58 U1.2 U 1.3 U 1.3 U 1.2 U 1.1 U9.2 U 9.9 U 9.5 U 9.4 U 10 D1.9 D 1.8 D 3.3 D 1.8 D 8.7 D

0.99 D 1.4 D 2.2 D 0.82 D 5 D14 D 13 D 15 D 12 D 48 D31 D 30 D 35 D 27 D 120 D35 D 31 D 36 D 30 D 66 D0.3 U 0.32 U 3.3 D 0.64 D 3.6 D

0.75 U 0.8 U 0.77 U 1.8 D 0.68 U7.1 D 4.7 D 160 D 35 D 28 D1 U 1.1 U 1.1 U 1.1 U 0.94 U

12 D 12 D 19 D 12 D 81 D0.69 U 0.75 U 0.72 U 0.71 U 0.63 U0.8 U 0.85 U 0.82 U 0.81 U 0.73 U

0.24 U 0.25 U 0.39 D 0.48 D 0.26 D1.6 D 1.5 D 1.5 D 1.5 D 1.6 D

0.62 U 0.66 U 0.64 U 0.63 U 0.56 U0.77 U 0.82 U 0.79 U 0.78 U 0.7 U0.45 U 0.48 U 0.46 U 0.46 U 0.41 U

Vinyl acetateVinyl bromideVinyl chloride

Styrene

Detected concentrations

Toluenetrans-1,2-Dichloroethene

trans-1,3-DichloropropeneTrichloroethene

Trichlorofluoromethane

Methyl tert butyl etherMethylene chloride

n-Heptane

TetrachloroetheneTetrahydrofuran

n-Hexaneo-Xylene

p/m-Xylenep-Ethyltoluene

Propylene

Naphthalene

Methyl Methacrylate

ChloroformChloromethane

cis-1,2-Dichloroethenecis-1,3-Dichloropropene

CyclohexaneDibromochloromethaneDichlorodifluoromethane

Ethyl AcetateEthylbenzene

HexachlorobutadieneIsopropanol

Chloroethane

4-Methyl-2-pentanoneAcetone

AcrylonitrileBenzene

Benzyl chlorideBromodichloromethane

BromoformBromomethaneCarbon disulfide

Carbon tetrachlorideChlorobenzene

3-Chloropropene

1,2-Dichloroethane1,2-Dichloropropane

1,2-Dichlorotetrafluoroethane1,3,5-Trimethylbenzene

1,3-Butadiene1,3-Dichlorobenzene1,3-Dichloropropane1,4-Dichlorobenzene

1,4-Dioxane2-Butanone2-Hexanone

1,2-Dichlorobenzene

VOCs, TO-151,1,1,2-Tetrachloroethane

1,1,1-Trichloroethane1,1,2,2-Tetrachloroethane

1,1,2-Trichloro-1,2,2-trifluoroethane1,1,2-Trichloroethane1,1-Dichloroethane1,1-Dichloroethene

1,2,4-Trichlorobenzene1,2,4-Trimethylbenzene

1,2-Dibromoethane

SV-01 SV-02 SV-03 SV-05 SV-06(2020-09-17) (2020-09-17) (2020-09-17) (2020-09-17) (2020-09-17)

APPENDIX C

Laboratory Reports

Technical Report

prepared for:

Gallagher Bassett - Poughkeepsie, NY22 IBM Road, Suite 101

Poughkeepsie NY, 12601

Attention: Victoria Panico

Report Date: 09/25/2020

Client Project ID: 20-0683

York Project (SDG) No.: 20I0806

CT Cert. No. PH-0723 New Jersey Cert. No. CT005 and NY037 PA Cert. No. 68-04440

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371

STRATFORD, CT 06615

New York Cert. Nos. 10854 and 12058

132-02 89th AVENUE RICHMOND HILL, NY 11418

www.YORKLAB.com [email protected]

Page 1 of 166

Client Sample IDYork Sample ID Matrix Date Collected Date Received

TP-01 220I0806-01 Soil 09/17/2020 09/17/2020

TP-02 220I0806-02 Soil 09/17/2020 09/17/2020

TP-03 320I0806-03 Soil 09/17/2020 09/17/2020

TP-04 220I0806-04 Soil 09/17/2020 09/17/2020

TP-05 120I0806-05 Soil 09/17/2020 09/17/2020

TP-06 1.520I0806-06 Soil 09/17/2020 09/17/2020

TP-07 120I0806-07 Soil 09/17/2020 09/17/2020

TP-08 220I0806-08 Soil 09/17/2020 09/17/2020

TP-09 320I0806-09 Soil 09/17/2020 09/17/2020

TP-10 120I0806-10 Soil 09/17/2020 09/17/2020

TP-11 220I0806-11 Soil 09/17/2020 09/17/2020

TP-12 120I0806-12 Soil 09/17/2020 09/17/2020

TP-01 0-220I0806-13 Soil 09/17/2020 09/17/2020

TP-02 0-220I0806-14 Soil 09/17/2020 09/17/2020

TP-03 2-420I0806-15 Soil 09/17/2020 09/17/2020

TP-04 0-220I0806-16 Soil 09/17/2020 09/17/2020

TP-05 0-220I0806-17 Soil 09/17/2020 09/17/2020

TP-06 0-1.520I0806-18 Soil 09/17/2020 09/17/2020

TP-07 0-220I0806-19 Soil 09/17/2020 09/17/2020

TP-08 0-220I0806-20 Soil 09/17/2020 09/17/2020

TP-09 1-320I0806-21 Soil 09/17/2020 09/17/2020

TP-10 0-220I0806-22 Soil 09/17/2020 09/17/2020






22 IBM Road, Suite 101

Gallagher Bassett - Poughkeepsie, NY

Purpose and Results

This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory

on September 17, 2020 and listed below. The project was identified as your project: 20-0683.

The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data

summary tables.

All samples were received in proper condition meeting the customary acceptance requirements for environmental samples

except those indicated under the Sample and Analysis Qualifiers section of this report.

All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags,

the meaning of which are explained in the Sample and Data Qualifiers Relating to This Work Order section of this report and

case narrative if applicable.

The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the

following pages.

Please contact Client Services at 203.325.1371 with any questions regarding this report.

[TOC_1] Introduction and Sample Cross Reference [

Page 2 of 166


TP-11 0-220I0806-23 Soil 09/17/2020 09/17/2020

TP-12 0-1.520I0806-24 Soil 09/17/2020 09/17/2020

General Notes for York Project (SDG) No.: 20I0806

1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to

the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest

standard utilized for the calibration where applicable.

2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.

3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .

4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.

5. All analyses conducted met method or Laboratory SOP requirements. See the Sample and Data Qualifiers Section for further information.

6. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.

7. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.

8. Analyses conducted at York Analytical Laboratories, Inc. Stratford, CT are indicated by NY Cert. No. 10854; those conducted at York

Analytical Laboratories, Inc., Richmond Hill, NY are indicated by NY Cert. No. 12058.

Approved By:

Laboratory Director

Date: 09/25/2020

Benjamin Gulizia

OC_2]General Notes Relating to this Report[TOC]

Page 3 of 166

TP-01 2

York Project (SDG) No.

20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

September 17, 2020 12:00 amSoil20-0683

[TOC_2]TP-01 2[TOC]

09/17/2020

20I0806-01

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

Reported to

LOQLOD/MDL

Volatile Organics, 8260 - Comprehensive

ND mg/kg dry 1630-20-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,1,1,2-TetrachloroethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 171-55-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,1,1-TrichloroethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP


ND mg/kg dry 176-13-1 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP


ND mg/kg dry 175-34-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,1-DichloroethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-35-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,1-DichloroethyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 187-61-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,2,3-TrichlorobenzeneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 196-18-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,2,3-TrichloropropaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP


ND mg/kg dry 195-63-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,2,4-TrimethylbenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 196-12-8 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,2-Dibromo-3-chloropropaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1106-93-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,2-DibromoethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 195-50-1 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,2-DichlorobenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP


ND mg/kg dry 178-87-5 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C1,2-DichloropropaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP




ND mg/kg dry 1123-91-1 TMP09/21/2020 06:35 09/22/2020 01:310.150.074 EPA 8260C1,4-DioxaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 178-93-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C2-ButanoneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1591-78-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C2-HexanoneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

[TOC_1]Sample Results[TOC]

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STRATFORD, CT 06615 132-02 89th AVENUE RICHMOND HILL, NY 11418

[email protected] 4 of 166

TP-01 2


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York Sample ID:

Sample Information

Client Project ID

Client Sample ID:


September 17, 2020 12:00 amSoil20-0683 09/17/2020

20I0806-01




Reported to

LOQLOD/MDL


ND mg/kg dry 1108-10-1 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260C4-Methyl-2-pentanoneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 167-64-1 TMP09/21/2020 06:35 09/22/2020 01:310.0150.0074 EPA 8260CAcetoneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1107-02-8 TMP09/21/2020 06:35 09/22/2020 01:310.0150.0074 EPA 8260CAcroleinCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1107-13-1 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CAcrylonitrileCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 171-43-2 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CBenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 174-97-5 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CBromochloromethaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-27-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CBromodichloromethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-25-2 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CBromoformCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 174-83-9 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CBromomethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-15-0 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CCarbon disulfideCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 156-23-5 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CCarbon tetrachlorideCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1108-90-7 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CChlorobenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-00-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CChloroethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 167-66-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CChloroformCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 174-87-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CChloromethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1156-59-2 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Ccis-1,2-DichloroethyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 110061-01-5 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Ccis-1,3-DichloropropyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1110-82-7 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CCyclohexaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1124-48-1 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CDibromochloromethaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 174-95-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CDibromomethaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-71-8 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CDichlorodifluoromethaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1100-41-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CEthyl BenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 187-68-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CHexachlorobutadieneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

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TP-01 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-01




Reported to

LOQLOD/MDL


ND mg/kg dry 198-82-8 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CIsopropylbenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 179-20-9 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CMethyl acetateCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 11634-04-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CMethyl tert-butyl ether (MTBE)Certifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1108-87-2 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CMethylcyclohexaneCertifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-09-2 TMP09/21/2020 06:35 09/22/2020 01:310.0150.0074 EPA 8260CMethylene chlorideCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1104-51-8 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Cn-ButylbenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1103-65-1 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Cn-PropylbenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 195-47-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Co-XyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,PADEP

ND mg/kg dry 1179601-23-1 TMP09/21/2020 06:35 09/22/2020 01:310.0150.0074 EPA 8260Cp- & m- XylenesCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,PADEP

ND mg/kg dry 199-87-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Cp-IsopropyltolueneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1135-98-8 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Csec-ButylbenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1100-42-5 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CStyreneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-65-0 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Ctert-Butyl alcohol (TBA)Certifications: NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 198-06-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Ctert-ButylbenzeneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1127-18-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CTetrachloroethyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1108-88-3 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CTolueneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 1156-60-5 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Ctrans-1,2-DichloroethyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 110061-02-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260Ctrans-1,3-DichloropropyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 179-01-6 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CTrichloroethyleneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-69-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CTrichlorofluoromethaneCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 175-01-4 TMP09/21/2020 06:35 09/22/2020 01:310.00740.0037 EPA 8260CVinyl ChlorideCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP,PADEP

ND mg/kg dry 11330-20-7 TMP09/21/2020 06:35 09/22/2020 01:310.0220.011 EPA 8260CXylenes, TotalCertifications: CTDOH,NELAC-NY10854,NELAC-NY12058,NJDEP

Surrogate Recoveries Result Acceptance Range

77-12592.6 %Surrogate: SURR:

1,2-Dichloroethane-d4

17060-07-0

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TP-01 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-01




Reported to

LOQLOD/MDL


85-120101 %Surrogate: SURR: Toluene-d82037-26-5

76-130106 %Surrogate: SURR:

p-Bromofluorobenzene

460-00-4

[TOC_3]Miscellaneous Physical Parameters[TOC]

Sample Prepared by Method: % Solids Prep



LOQ

Reported to

Total Solids

91.7 % 1solids KHA09/24/2020 16:32 09/24/2020 16:350.100 SM 2540G* % Solids

Certifications: CTDOH

TP-02 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-02 2[TOC]

09/17/2020

20I0806-02





Reported to

LOQLOD/MDL













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TP-02 2


20I0806

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Sample Information

Client Project ID

Client Sample ID:



20I0806-02




Reported to

LOQLOD/MDL

























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TP-02 2


20I0806

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Sample Information

Client Project ID

Client Sample ID:



20I0806-02




Reported to

LOQLOD/MDL
















17060-07-0




460-00-4





LOQ

Reported to

Total Solids



TP-03 3


20I0806

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Sample Information

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Client Sample ID:



[TOC_2]TP-03 3[TOC]

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TP-03 3


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Client Project ID

Client Sample ID:



[TOC_2]TP-03 3[TOC]

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20I0806-03





Reported to

LOQLOD/MDL


























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TP-03 3


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Sample Information

Client Project ID

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20I0806-03




Reported to

LOQLOD/MDL

























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TP-03 3


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Sample Information

Client Project ID

Client Sample ID:



20I0806-03




Reported to

LOQLOD/MDL


























17060-07-0


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TP-03 3


20I0806

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Sample Information

Client Project ID

Client Sample ID:



20I0806-03




Reported to

LOQLOD/MDL




460-00-4





LOQ

Reported to

Total Solids



TP-04 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-04 2[TOC]

09/17/2020

20I0806-04





Reported to

LOQLOD/MDL














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TP-04 2


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Sample Information

Client Project ID

Client Sample ID:



20I0806-04




Reported to

LOQLOD/MDL

























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TP-04 2


20I0806

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Sample Information

Client Project ID

Client Sample ID:



20I0806-04




Reported to

LOQLOD/MDL















17060-07-0




460-00-4





LOQ

Reported to

Total Solids



TP-05 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-05 1[TOC]

09/17/2020

20I0806-05


Sample Notes:Log-in Notes:Volatile Organics, 8260 - Comprehensive

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TP-05 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-05 1[TOC]

09/17/2020

20I0806-05



Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/TimeReported to

LOQLOD/MDL


























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TP-05 1


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Sample Information

Client Project ID

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20I0806-05




Reported to

LOQLOD/MDL

























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TP-05 1


20I0806

York Sample ID:

Sample Information

Client Project ID

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20I0806-05




Reported to

LOQLOD/MDL

























17060-07-0




460-00-4


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TP-05 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-05





LOQ

Reported to

Total Solids



TP-06 1.5


20I0806

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Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-06 1.5[TOC]

09/17/2020

20I0806-06





Reported to

LOQLOD/MDL

















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TP-06 1.5


20I0806

York Sample ID:

Sample Information

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20I0806-06




Reported to

LOQLOD/MDL

























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TP-06 1.5


20I0806

York Sample ID:

Sample Information

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20I0806-06




Reported to

LOQLOD/MDL












17060-07-0




460-00-4





LOQ

Reported to

Total Solids



TP-07 1


20I0806

York Sample ID:

Sample Information

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[TOC_2]TP-07 1[TOC]

09/17/2020

20I0806-07





Reported to

LOQLOD/MDL



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-07




Reported to

LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-07




Reported to

LOQLOD/MDL

























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-07




Reported to

LOQLOD/MDL

























17060-07-0




460-00-4


www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-07





LOQ

Reported to

Total Solids



TP-08 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-08 2[TOC]

09/17/2020

20I0806-08





Reported to

LOQLOD/MDL

















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-08




Reported to

LOQLOD/MDL

























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-08




Reported to

LOQLOD/MDL












17060-07-0




460-00-4





LOQ

Reported to

Total Solids



TP-09 3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-09 3[TOC]

09/17/2020

20I0806-09





Reported to

LOQLOD/MDL



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-09




Reported to

LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-09




Reported to

LOQLOD/MDL

























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-09




Reported to

LOQLOD/MDL

























17060-07-0




460-00-4


www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-09





LOQ

Reported to

Total Solids



TP-10 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-10 1[TOC]

09/17/2020

20I0806-10





Reported to

LOQLOD/MDL

















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-10 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-10




Reported to

LOQLOD/MDL

























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-10 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-10




Reported to

LOQLOD/MDL












17060-07-0




460-00-4





LOQ

Reported to

Total Solids



TP-11 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-11 2[TOC]

09/17/2020

20I0806-11





Reported to

LOQLOD/MDL



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-11 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-11




Reported to

LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-11 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-11




Reported to

LOQLOD/MDL

























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-11 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-11




Reported to

LOQLOD/MDL

























17060-07-0




460-00-4


www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-11 2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-11





LOQ

Reported to

Total Solids



TP-12 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-12 1[TOC]

09/17/2020

20I0806-12





Reported to

LOQLOD/MDL

















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-12 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-12




Reported to

LOQLOD/MDL

























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-12 1


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-12




Reported to

LOQLOD/MDL












17060-07-0




460-00-4





LOQ

Reported to

Total Solids



TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-01 0-2[TOC]

09/17/2020

20I0806-13

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Sample Prepared by Method: EPA 3550C



Reported to

LOQLOD/MDL

Semi-Volatiles, 8270 - Comprehensive

ND ug/kg dry 292-52-4 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D1,1-BiphenylCertifications: NELAC-NY10854,NJDEP,PADEP

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-13




Reported to

LOQLOD/MDL


ND ug/kg dry 295-94-3 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270D1,2,4,5-TetrachlorobenzeneCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-82-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D1,2,4-TrichlorobenzeneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-50-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D1,2-DichlorobenzeneCertifications: NELAC-NY10854,PADEP

ND ug/kg dry 2122-66-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP,PADEP



ND ug/kg dry 258-90-2 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270D2,3,4,6-TetrachlorophenolCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-95-4 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2,4,5-TrichlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-06-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2,4,6-TrichlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-83-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2,4-DichlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-67-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2,4-DimethylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 251-28-5 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270D2,4-DinitrophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2121-14-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2,4-DinitrotolueneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2606-20-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2,6-DinitrotolueneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-58-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2-ChloronaphthaleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-57-8 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2-ChlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-57-6 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2-MethylnaphthaleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-48-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2-MethylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-74-4 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270D2-NitroanilineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-75-5 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D2-NitrophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265794-96-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D3- & 4-MethylphenolsCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-94-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D3,3-DichlorobenzidineCertifications: NELAC-NY10854,NJDEP,PADEP


www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-13




Reported to

LOQLOD/MDL


ND ug/kg dry 2534-52-1 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270D4,6-Dinitro-2-methylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2101-55-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D4-Bromophenyl phenyl etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 259-50-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D4-Chloro-3-methylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2106-47-8 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D4-ChloroanilineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 27005-72-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270D4-Chlorophenyl phenyl etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP


ND ug/kg dry 2100-02-7 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270D4-NitrophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 283-32-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DAcenaphtheneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2208-96-8 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DAcenaphthyleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-86-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DAcetophenoneCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 262-53-3 OW09/23/2020 13:23 09/24/2020 14:17363182 EPA 8270DAnilineCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-12-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DAnthraceneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 21912-24-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DAtrazineCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-52-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzaldehyde CCV-LCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 292-87-5 OW09/23/2020 13:23 09/24/2020 14:17363182 EPA 8270DBenzidine CCV-LCertifications: CTDOH,NELAC-NY10854,PADEP

ND ug/kg dry 256-55-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzo(a)anthraceneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 250-32-8 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzo(a)pyreneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2205-99-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzo(b)fluorantheneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2191-24-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzo(g,h,i)peryleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2207-08-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzo(k)fluorantheneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265-85-0 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzoic acidCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-51-6 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzyl alcoholCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 285-68-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBenzyl butyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-13




Reported to

LOQLOD/MDL


ND ug/kg dry 2111-91-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBis(2-chloroethoxy)methaneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-44-4 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBis(2-chloroethyl)etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-60-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBis(2-chloroisopropyl)etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2117-81-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DBis(2-ethylhexyl)phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-60-2 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270DCaprolactamCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 286-74-8 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DCarbazoleCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2218-01-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DChryseneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 253-70-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DDibenzo(a,h)anthraceneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2132-64-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DDibenzofuranCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 284-66-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DDiethyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2131-11-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DDimethyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 284-74-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DDi-n-butyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2117-84-0 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DDi-n-octyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2122-39-4 OW09/23/2020 13:23 09/24/2020 14:1718190.7 EPA 8270D* DiphenylamineCertifications:

ND ug/kg dry 2206-44-0 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DFluorantheneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 286-73-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DFluoreneCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2118-74-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DHexachlorobenzeneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 287-68-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DHexachlorobutadieneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 277-47-4 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DHexachlorocyclopentadieneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 267-72-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DHexachloroethaneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2193-39-5 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DIndeno(1,2,3-cd)pyreneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 278-59-1 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DIsophoroneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-20-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DNaphthaleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-13




Reported to

LOQLOD/MDL


ND ug/kg dry 298-95-3 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DNitrobenzeneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 262-75-9 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DN-NitrosodimethylamineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2621-64-7 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DN-nitroso-di-n-propylamineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 286-30-6 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DN-NitrosodiphenylamineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 287-86-5 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DPentachlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 285-01-8 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DPhenanthreneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-95-2 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DPhenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2129-00-0 OW09/23/2020 13:23 09/24/2020 14:1790.745.4 EPA 8270DPyreneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP


20-10870.0 %Surrogate: SURR: 2-Fluorophenol367-12-4

23-11467.5 %Surrogate: SURR: Phenol-d54165-62-2

22-10872.1 %Surrogate: SURR: Nitrobenzene-d54165-60-0

21-11366.5 %Surrogate: SURR: 2-Fluorobiphenyl321-60-8


2,4,6-Tribromophenol

118-79-6

24-11675.4 %Surrogate: SURR: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]




LOQ

Reported to

Pesticides, 8081 target list

ND mg/kg dry 572-54-8 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081B4,4'-DDDCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 572-55-9 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081B4,4'-DDECertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 550-29-3 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081B4,4'-DDTCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 5309-00-2 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BAldrinCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 5319-84-6 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081Balpha-BHCCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 55103-71-9 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081Balpha-ChlordaneCertifications: NELAC-NY10854,NJDEP

ND mg/kg dry 5319-85-7 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081Bbeta-BHCCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 557-74-9 CM09/23/2020 13:26 09/24/2020 17:080.0360 EPA 8081BChlordane, totalCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

www.YORKLAB.com

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TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-13




LOQ

Reported to


ND mg/kg dry 5319-86-8 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081Bdelta-BHCCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 560-57-1 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BDieldrinCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 5959-98-8 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BEndosulfan ICertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 533213-65-9 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BEndosulfan IICertifications: CTDOH,NELAC-NY10854

ND mg/kg dry 51031-07-8 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BEndosulfan sulfateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 572-20-8 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BEndrinCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 57421-93-4 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BEndrin aldehydeCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 553494-70-5 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BEndrin ketoneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 558-89-9 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081Bgamma-BHC (Lindane)Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 55566-34-7 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081Bgamma-ChlordaneCertifications: NELAC-NY10854,NJDEP

ND mg/kg dry 576-44-8 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BHeptachlorCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 51024-57-3 CM09/23/2020 13:26 09/24/2020 17:080.00180 EPA 8081BHeptachlor epoxideCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 572-43-5 CM09/23/2020 13:26 09/24/2020 17:080.00900 EPA 8081BMethoxychlorCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 58001-35-2 CM09/23/2020 13:26 09/24/2020 17:080.0911 EPA 8081BToxapheneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP


30-15079.9 %Surrogate: Decachlorobiphenyl2051-24-3

30-15064.7 %Surrogate: Tetrachloro-m-xylene877-09-8

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]




LOQ

Reported to

Polychlorinated Biphenyls (PCB)

ND mg/kg dry 112674-11-2 BJ09/23/2020 13:26 09/24/2020 18:080.0182 EPA 8082AAroclor 1016Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP




www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-13




LOQ

Reported to





ND mg/kg dry 137324-23-5 BJ09/23/2020 13:26 09/24/2020 18:080.0182 EPA 8082AAroclor 1262Certifications: NELAC-NY10854,NJDEP,PADEP


ND mg/kg dry 11336-36-3 BJ09/23/2020 13:26 09/24/2020 18:080.0182 EPA 8082A* Total PCBsCertifications:




[TOC_3]Metals by ICP[TOC]

Sample Prepared by Method: EPA 3050B



LOQ

Reported to

Metals, Target Analyte

1140 mg/kg dry 17429-90-5 KML09/18/2020 07:36 09/22/2020 21:515.47 EPA 6010DAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-36-0 KML09/18/2020 07:36 09/22/2020 21:512.74 EPA 6010DAntimonyCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2.94 mg/kg dry 17440-38-2 KML09/18/2020 07:36 09/22/2020 21:511.64 EPA 6010DArsenic


42.3 mg/kg dry 17440-39-3 KML09/18/2020 07:36 09/22/2020 21:512.74 EPA 6010DBarium


ND mg/kg dry 17440-41-7 KML09/18/2020 07:36 09/22/2020 21:510.055 EPA 6010DBerylliumCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-43-9 KML09/18/2020 07:36 09/22/2020 21:510.328 EPA 6010DCadmiumCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

882 mg/kg dry 17440-70-2 KML09/18/2020 07:36 09/22/2020 21:515.47 EPA 6010DCalcium


8.93 mg/kg dry 17440-47-3 KML09/18/2020 07:36 09/22/2020 21:510.547 EPA 6010DChromium


4.45 mg/kg dry 17440-48-4 KML09/18/2020 07:36 09/22/2020 21:510.438 EPA 6010DCobalt


42.6 mg/kg dry 17440-50-8 KML09/18/2020 07:36 09/22/2020 21:512.19 EPA 6010DCopper


2450 mg/kg dry 17439-89-6 KML09/18/2020 07:36 09/22/2020 21:5127.4 EPA 6010DIron


72.6 mg/kg dry 17439-92-1 KML09/18/2020 07:36 09/22/2020 21:510.547 EPA 6010DLead


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TP-01 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-13




LOQ

Reported to


113 mg/kg dry 17439-95-4 KML09/18/2020 07:36 09/22/2020 21:515.47 EPA 6010DMagnesium


20.5 mg/kg dry 17439-96-5 KML09/18/2020 07:36 09/22/2020 21:510.547 EPA 6010DManganese


9.89 mg/kg dry 17440-02-0 KML09/18/2020 07:36 09/22/2020 21:511.09 EPA 6010DNickel


242 mg/kg dry 17440-09-7 KML09/18/2020 07:36 09/22/2020 21:515.47 EPA 6010DPotassium B


ND mg/kg dry 17782-49-2 KML09/18/2020 07:36 09/22/2020 21:512.74 EPA 6010DSeleniumCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 KML09/18/2020 07:36 09/22/2020 21:510.547 EPA 6010DSilverCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

68.8 mg/kg dry 17440-23-5 KML09/18/2020 07:36 09/22/2020 21:5154.7 EPA 6010DSodium


ND mg/kg dry 17440-28-0 KML09/18/2020 07:36 09/22/2020 21:512.74 EPA 6010DThalliumCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

10.4 mg/kg dry 17440-62-2 KML09/18/2020 07:36 09/22/2020 21:511.09 EPA 6010DVanadium


28.2 mg/kg dry 17440-66-6 KML09/18/2020 07:36 09/22/2020 21:512.74 EPA 6010DZinc


[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Sample Prepared by Method: EPA 7473 soil



LOQ

Reported to

Mercury by 7473

0.0338 mg/kg dry 17439-97-6 SY09/24/2020 09:36 09/24/2020 12:560.0328 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP





LOQ

Reported to

Total Solids

91.4 % 1solids SK09/21/2020 13:03 09/21/2020 16:510.100 SM 2540G* % Solids


TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-02 0-2[TOC]

09/17/2020

20I0806-14

www.YORKLAB.com

120 RESEARCH DRIVE

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TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-02 0-2[TOC]

09/17/2020

20I0806-14





Reported to

LOQLOD/MDL


ND ug/kg dry 292-52-4 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D1,1-BiphenylCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-94-3 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270D1,2,4,5-TetrachlorobenzeneCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-82-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D1,2,4-TrichlorobenzeneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-50-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D1,2-DichlorobenzeneCertifications: NELAC-NY10854,PADEP

ND ug/kg dry 2122-66-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D1,2-Diphenylhydrazine (as




ND ug/kg dry 258-90-2 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270D2,3,4,6-TetrachlorophenolCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-95-4 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2,4,5-TrichlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP


ND ug/kg dry 2120-83-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2,4-DichlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-67-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2,4-DimethylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 251-28-5 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270D2,4-DinitrophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2121-14-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2,4-DinitrotolueneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP


ND ug/kg dry 291-58-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2-ChloronaphthaleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-57-8 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2-ChlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-57-6 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2-MethylnaphthaleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-48-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2-MethylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-74-4 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270D2-NitroanilineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-75-5 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D2-NitrophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265794-96-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D3- & 4-MethylphenolsCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-94-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D3,3-DichlorobenzidineCertifications: NELAC-NY10854,NJDEP,PADEP

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-14




Reported to

LOQLOD/MDL



ND ug/kg dry 2534-52-1 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270D4,6-Dinitro-2-methylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2101-55-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D4-Bromophenyl phenyl etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 259-50-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D4-Chloro-3-methylphenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2106-47-8 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D4-ChloroanilineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 27005-72-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270D4-Chlorophenyl phenyl etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP


ND ug/kg dry 2100-02-7 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270D4-NitrophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 283-32-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DAcenaphtheneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

51.2 ug/kg dry 2208-96-8 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DAcenaphthylene J


ND ug/kg dry 298-86-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DAcetophenoneCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 262-53-3 KH09/23/2020 13:23 09/24/2020 16:16361181 EPA 8270DAnilineCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-12-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DAnthraceneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 21912-24-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DAtrazineCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-52-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzaldehydeCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 292-87-5 KH09/23/2020 13:23 09/24/2020 16:16361181 EPA 8270DBenzidineCertifications: CTDOH,NELAC-NY10854,PADEP

129 ug/kg dry 256-55-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzo(a)anthracene


156 ug/kg dry 250-32-8 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzo(a)pyrene


160 ug/kg dry 2205-99-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzo(b)fluoranthene


154 ug/kg dry 2191-24-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzo(g,h,i)perylene


141 ug/kg dry 2207-08-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzo(k)fluoranthene


ND ug/kg dry 265-85-0 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzoic acidCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-51-6 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzyl alcoholCertifications: NELAC-NY10854,NJDEP,PADEP

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-14




Reported to

LOQLOD/MDL


617 ug/kg dry 285-68-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBenzyl butyl phthalate


ND ug/kg dry 2111-91-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBis(2-chloroethoxy)methaneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-44-4 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBis(2-chloroethyl)etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-60-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBis(2-chloroisopropyl)etherCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

90.2 ug/kg dry 2117-81-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DBis(2-ethylhexyl)phthalate


ND ug/kg dry 2105-60-2 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270DCaprolactamCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 286-74-8 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DCarbazoleCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

152 ug/kg dry 2218-01-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DChrysene


ND ug/kg dry 253-70-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DDibenzo(a,h)anthraceneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2132-64-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DDibenzofuranCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 284-66-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DDiethyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2131-11-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DDimethyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

62.0 ug/kg dry 284-74-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DDi-n-butyl phthalate J


ND ug/kg dry 2117-84-0 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DDi-n-octyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2122-39-4 KH09/23/2020 13:23 09/24/2020 16:1618090.2 EPA 8270D* DiphenylamineCertifications:

229 ug/kg dry 2206-44-0 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DFluoranthene


ND ug/kg dry 286-73-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DFluoreneCertifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2118-74-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DHexachlorobenzeneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 287-68-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DHexachlorobutadieneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 277-47-4 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DHexachlorocyclopentadieneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 267-72-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DHexachloroethaneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

149 ug/kg dry 2193-39-5 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DIndeno(1,2,3-cd)pyrene


ND ug/kg dry 278-59-1 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DIsophoroneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-14




Reported to

LOQLOD/MDL


ND ug/kg dry 291-20-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DNaphthaleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-95-3 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DNitrobenzeneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 262-75-9 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DN-NitrosodimethylamineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2621-64-7 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DN-nitroso-di-n-propylamineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 286-30-6 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DN-NitrosodiphenylamineCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 287-86-5 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DPentachlorophenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

123 ug/kg dry 285-01-8 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DPhenanthrene


ND ug/kg dry 2108-95-2 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DPhenolCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

214 ug/kg dry 2129-00-0 KH09/23/2020 13:23 09/24/2020 16:1690.245.2 EPA 8270DPyrene









118-79-6






LOQ

Reported to









www.YORKLAB.com

120 RESEARCH DRIVE

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TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-14




LOQ

Reported to
























LOQ

Reported to





www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-14




LOQ

Reported to
















LOQ

Reported to







154 mg/kg dry 17440-39-3 KML09/18/2020 07:36 09/22/2020 21:562.77 EPA 6010DBarium



1.84 mg/kg dry 17440-43-9 KML09/18/2020 07:36 09/22/2020 21:560.332 EPA 6010DCadmium












www.YORKLAB.com

120 RESEARCH DRIVE

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TP-02 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-14




LOQ

Reported to


330 mg/kg dry 17439-92-1 KML09/18/2020 07:36 09/22/2020 21:560.554 EPA 6010DLead




163 mg/kg dry 17439-96-5 KML09/18/2020 07:36 09/22/2020 21:560.554 EPA 6010DManganese








554 mg/kg dry 17440-23-5 KML09/18/2020 07:36 09/22/2020 21:5655.4 EPA 6010DSodium





424 mg/kg dry 17440-66-6 KML09/18/2020 07:36 09/22/2020 21:562.77 EPA 6010DZinc






LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-03 2-4[TOC]

09/17/2020

20I0806-15





Reported to

LOQLOD/MDL
















951 ug/kg dry 2121-14-2 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270D2,4-Dinitrotoluene












www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-15




Reported to

LOQLOD/MDL











ND ug/kg dry 2208-96-8 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DAcenaphthyleneCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP



438 ug/kg dry 2120-12-7 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DAnthracene

















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-15




Reported to

LOQLOD/MDL


74.1 ug/kg dry 285-68-7 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DBenzyl butyl phthalate J





ND ug/kg dry 2117-81-7 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DBis(2-ethylhexyl)phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP








459 ug/kg dry 2131-11-3 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DDimethyl phthalate


ND ug/kg dry 284-74-2 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DDi-n-butyl phthalateCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP









927 ug/kg dry 267-72-1 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DHexachloroethane




439 ug/kg dry 278-59-1 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DIsophorone


www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-15




Reported to

LOQLOD/MDL





102 ug/kg dry 2621-64-7 KH09/23/2020 13:23 09/24/2020 16:4598.649.4 EPA 8270DN-nitroso-di-n-propylamine
















118-79-6






LOQ

Reported to








www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-15




LOQ

Reported to

























LOQ

Reported to




www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-15




LOQ

Reported to












30-14029.0 %Surrogate: Decachlorobiphenyl2051-24-3 S-GC

[TOC_3]Chlorinated Herbicides by GC/ECD[TOC]

Sample Prepared by Method: EPA 3550C/8151A



LOQ

Reported to

Herbicides, Target List

ND ug/kg dry 193-76-5 CM09/24/2020 11:47 09/25/2020 14:5423.9 EPA 8151A2,4,5-TCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 193-72-1 CM09/24/2020 11:47 09/25/2020 14:5423.9 EPA 8151A2,4,5-TP (Silvex)Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 194-75-7 CM09/24/2020 11:47 09/25/2020 14:5423.9 EPA 8151A2,4-DCertifications: CTDOH,NELAC-NY10854,NJDEP,PADEP


21-15077.2 %Surrogate: 2,4-Dichlorophenylacetic

acid (DCAA)

19719-28-9





LOQ

Reported to







www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-15




LOQ

Reported to








































LOQ

Reported to

Mercury by 7473

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-03 2-4


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-15





LOQ

Reported to

Mercury by 7473



[TOC_3]Wet Chemistry Parameters[TOC]

Sample Prepared by Method: EPA SW846-3060



LOQ

Reported to

Chromium, Hexavalent

ND mg/kg dry 118540-29-9 SK09/24/2020 09:23 09/24/2020 16:310.605 EPA 7196AChromium, HexavalentCertifications: NJDEP,CTDOH,NELAC-NY10854,PADEP

Sample Prepared by Method: Analysis Preparation



LOQ

Reported to

Chromium, Trivalent

22.6 mg/kg 116065-83-1 PAM09/25/2020 15:45 09/25/2020 15:500.500 Calculation* Chromium, Trivalent

Certifications:

Sample Prepared by Method: Analysis Preparation Soil



LOQ

Reported to

Cyanide, Total

ND mg/kg dry 157-12-5 JAG09/25/2020 08:44 09/25/2020 14:480.605 EPA 9014/9010CCyanide, totalCertifications: NELAC-NY10854,CTDOH,NJDEP,PADEP





LOQ

Reported to

Total Solids



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-04 0-2[TOC]

09/17/2020

20I0806-16


Sample Notes:Log-in Notes:Semi-Volatiles, 8270 - Comprehensive

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-04 0-2[TOC]

09/17/2020

20I0806-16




LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-16




Reported to

LOQLOD/MDL









56.4 ug/kg dry 283-32-9 KH09/23/2020 13:23 09/24/2020 17:1491.645.9 EPA 8270DAcenaphthene J


104 ug/kg dry 2208-96-8 KH09/23/2020 13:23 09/24/2020 17:1491.645.9 EPA 8270DAcenaphthylene























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-16




Reported to

LOQLOD/MDL





129 ug/kg dry 2117-81-7 KH09/23/2020 13:23 09/24/2020 17:1491.645.9 EPA 8270DBis(2-ethylhexyl)phthalate



113 ug/kg dry 286-74-8 KH09/23/2020 13:23 09/24/2020 17:1491.645.9 EPA 8270DCarbazole














63.7 ug/kg dry 286-73-7 KH09/23/2020 13:23 09/24/2020 17:1491.645.9 EPA 8270DFluorene J

Certifications: NELAC-NY10854,NJDEP,PADEP









www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-16




Reported to

LOQLOD/MDL



















118-79-6






LOQ

Reported to










www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-16




LOQ

Reported to























LOQ

Reported to






www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-16




LOQ

Reported to




0.0220 mg/kg dry 111096-82-5 BJ09/23/2020 13:26 09/24/2020 18:490.0182 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP



0.0220 mg/kg dry 11336-36-3 BJ09/23/2020 13:26 09/24/2020 18:490.0182 EPA 8082A* Total PCBs

Certifications:








LOQ

Reported to






















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-04 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-16




LOQ

Reported to






91.0 mg/kg dry 17439-96-5 KML09/18/2020 07:36 09/22/2020 22:110.553 EPA 6010DManganese



















LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-05 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-05 0-2[TOC]

09/17/2020

20I0806-17





Reported to

LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-05 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-17




Reported to

LOQLOD/MDL















76.6 ug/kg dry 2120-12-7 KH09/23/2020 13:23 09/24/2020 17:4392.246.2 EPA 8270DAnthracene J

















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-05 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-17




Reported to

LOQLOD/MDL









48.6 ug/kg dry 286-74-8 KH09/23/2020 13:23 09/24/2020 17:4392.246.2 EPA 8270DCarbazole J






















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-05 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-17




Reported to

LOQLOD/MDL




















118-79-6






LOQ

Reported to









www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-05 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-17




LOQ

Reported to
























LOQ

Reported to





www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-05 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-17




LOQ

Reported to
















LOQ

Reported to






















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-05 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-17




LOQ

Reported to

























LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-06 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-06 0-1.5[TOC]

09/17/2020

20I0806-18





Reported to

LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-06 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-18




Reported to

LOQLOD/MDL






























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-06 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-18




Reported to

LOQLOD/MDL





























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-06 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-18




Reported to

LOQLOD/MDL




















118-79-6






LOQ

Reported to









www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-06 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-18




LOQ

Reported to
























LOQ

Reported to





www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-06 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-18




LOQ

Reported to
















LOQ

Reported to






















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-06 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-18




LOQ

Reported to

























LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-07 0-2[TOC]

09/17/2020

20I0806-19





Reported to

LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-19




Reported to

LOQLOD/MDL































www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-19




Reported to

LOQLOD/MDL

















121 ug/kg dry 284-74-2 KH09/23/2020 13:23 09/24/2020 18:4293.446.8 EPA 8270DDi-n-butyl phthalate














www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-19




Reported to

LOQLOD/MDL




















118-79-6






LOQ

Reported to









www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-19




LOQ

Reported to
























LOQ

Reported to





www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-19




LOQ

Reported to
















LOQ

Reported to







acid (DCAA)

19719-28-9





LOQ

Reported to




10.5 mg/kg dry 17440-36-0 KML09/18/2020 07:36 09/22/2020 22:322.85 EPA 6010DAntimony




www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-19




LOQ

Reported to








































LOQ

Reported to

Mercury by 7473

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-07 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-19





LOQ

Reported to

Mercury by 7473







LOQ

Reported to






LOQ

Reported to

Chromium, Trivalent


Certifications:




LOQ

Reported to

Cyanide, Total






LOQ

Reported to

Total Solids



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-08 0-2[TOC]

09/17/2020

20I0806-20



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-08 0-2[TOC]

09/17/2020

20I0806-20




LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-20




Reported to

LOQLOD/MDL
































www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-20




Reported to

LOQLOD/MDL






























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-20




Reported to

LOQLOD/MDL



















118-79-6






LOQ

Reported to










www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-20




LOQ

Reported to























LOQ

Reported to






www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-20




LOQ

Reported to















LOQ

Reported to
























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-08 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-20




LOQ

Reported to























LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-09 1-3[TOC]

09/17/2020

20I0806-21

www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-09 1-3[TOC]

09/17/2020

20I0806-21





Reported to

LOQLOD/MDL


























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-21




Reported to

LOQLOD/MDL
































www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-21




Reported to

LOQLOD/MDL










47.3 ug/kg dry 286-74-8 KH09/23/2020 08:15 09/23/2020 19:3293.847.0 EPA 8270DCarbazole J








97.5 ug/kg dry 284-74-2 KH09/23/2020 08:15 09/23/2020 19:3293.847.0 EPA 8270DDi-n-butyl phthalate














www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-21




Reported to

LOQLOD/MDL




















118-79-6






LOQ

Reported to









www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-21




LOQ

Reported to



















30-15025.4 %Surrogate: Tetrachloro-m-xylene877-09-8 S-GC





LOQ

Reported to





www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-21




LOQ

Reported to










Certifications:








LOQ

Reported to






















www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-09 1-3


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-21




LOQ

Reported to

























LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-10 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-10 0-2[TOC]

09/17/2020

20I0806-22





Reported to

LOQLOD/MDL


58.4 ug/kg dry 292-52-4 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270D1,1-Biphenyl J



















98.8 ug/kg dry 291-57-6 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270D2-Methylnaphthalene





64.2 ug/kg dry 265794-96-9 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270D3- & 4-Methylphenols J



www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-10 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-22




Reported to

LOQLOD/MDL










396 ug/kg dry 283-32-9 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270DAcenaphthene























www.YORKLAB.com

120 RESEARCH DRIVE

FAX (203) 357-0166(203) 325-1371



TP-10 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-22




Reported to

LOQLOD/MDL














113 ug/kg dry 253-70-3 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270DDibenzo(a,h)anthracene


162 ug/kg dry 2132-64-9 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270DDibenzofuran




321 ug/kg dry 284-74-2 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270DDi-n-butyl phthalate




4790 ug/kg dry 10206-44-0 KH09/23/2020 08:15 09/24/2020 19:11451226 EPA 8270DFluoranthene


374 ug/kg dry 286-73-7 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270DFluorene









www.YORKLAB.com

120 RESEARCH DRIVE

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TP-10 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-22




Reported to

LOQLOD/MDL


173 ug/kg dry 291-20-3 KH09/23/2020 08:15 09/23/2020 20:0290.245.2 EPA 8270DNaphthalene







4970 ug/kg dry 1085-01-8 KH09/23/2020 08:15 09/24/2020 19:11451226 EPA 8270DPhenanthrene



5340 ug/kg dry 10129-00-0 KH09/23/2020 08:15 09/24/2020 19:11451226 EPA 8270DPyrene









118-79-6






LOQ

Reported to



0.00443 mg/kg dry 572-55-9 CM09/23/2020 07:30 09/24/2020 06:480.00179 EPA 8081B4,4'-DDE


0.0316 mg/kg dry 550-29-3 CM09/23/2020 07:30 09/24/2020 06:480.00179 EPA 8081B4,4'-DDT





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TP-10 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-22




LOQ

Reported to

























LOQ

Reported to




www.YORKLAB.com

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TP-10 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-22




LOQ

Reported to











Certifications:








LOQ

Reported to




















www.YORKLAB.com

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TP-10 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-22




LOQ

Reported to



























LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



www.YORKLAB.com

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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-11 0-2[TOC]

09/17/2020

20I0806-23





Reported to

LOQLOD/MDL


























www.YORKLAB.com

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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-23




Reported to

LOQLOD/MDL
































www.YORKLAB.com

120 RESEARCH DRIVE

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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-23




Reported to

LOQLOD/MDL













73.7 ug/kg dry 253-70-3 KH09/23/2020 08:15 09/23/2020 20:3195.147.6 EPA 8270DDibenzo(a,h)anthracene J


















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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-23




Reported to

LOQLOD/MDL




















118-79-6






LOQ

Reported to









www.YORKLAB.com

120 RESEARCH DRIVE

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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-23




LOQ

Reported to


















30-150102 %Surrogate: Decachlorobiphenyl2051-24-3






LOQ

Reported to





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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-23




LOQ

Reported to
















LOQ

Reported to







acid (DCAA)

19719-28-9





LOQ

Reported to







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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-23




LOQ

Reported to








































LOQ

Reported to

Mercury by 7473

www.YORKLAB.com

120 RESEARCH DRIVE

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TP-11 0-2


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-23





LOQ

Reported to

Mercury by 7473







LOQ

Reported to






LOQ

Reported to

Chromium, Trivalent


Certifications:




LOQ

Reported to

Cyanide, Total






LOQ

Reported to

Total Solids



TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-12 0-1.5[TOC]

09/17/2020

20I0806-24



www.YORKLAB.com

120 RESEARCH DRIVE

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TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]TP-12 0-1.5[TOC]

09/17/2020

20I0806-24




LOQLOD/MDL




























www.YORKLAB.com

120 RESEARCH DRIVE

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TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-24




Reported to

LOQLOD/MDL









99.0 ug/kg dry 283-32-9 KH09/23/2020 08:15 09/23/2020 21:0091.746.0 EPA 8270DAcenaphthene

























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TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-24




Reported to

LOQLOD/MDL












64.5 ug/kg dry 253-70-3 KH09/23/2020 08:15 09/23/2020 21:0091.746.0 EPA 8270DDibenzo(a,h)anthracene J










90.9 ug/kg dry 286-73-7 KH09/23/2020 08:15 09/23/2020 21:0091.746.0 EPA 8270DFluorene J





891 ug/kg dry 267-72-1 KH09/23/2020 08:15 09/23/2020 21:0091.746.0 EPA 8270DHexachloroethane




191 ug/kg dry 278-59-1 KH09/23/2020 08:15 09/23/2020 21:0091.746.0 EPA 8270DIsophorone



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TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-24




Reported to

LOQLOD/MDL





117 ug/kg dry 286-30-6 KH09/23/2020 08:15 09/23/2020 21:0091.746.0 EPA 8270DN-Nitrosodiphenylamine















118-79-6






LOQ

Reported to









www.YORKLAB.com

120 RESEARCH DRIVE

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TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-24




LOQ

Reported to
























LOQ

Reported to





www.YORKLAB.com

120 RESEARCH DRIVE

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TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-24




LOQ

Reported to
















LOQ

Reported to






















www.YORKLAB.com

120 RESEARCH DRIVE

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TP-12 0-1.5


20I0806

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0806-24




LOQ

Reported to

























LOQ

Reported to

Mercury by 7473







LOQ

Reported to

Total Solids



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Analytical Batch Summary

[TOC_1]Quality Batch Summary[TOC]

Batch ID: Preparation Method: Prepared By:BI01001 EPA 3050B SY

YORK Sample ID Client Sample ID Preparation Date

20I0806-13 TP-01 0-2 09/18/20

20I0806-14 TP-02 0-2 09/18/20

20I0806-15 TP-03 2-4 09/18/20

20I0806-16 TP-04 0-2 09/18/20

20I0806-17 TP-05 0-2 09/18/20

20I0806-18 TP-06 0-1.5 09/18/20

20I0806-19 TP-07 0-2 09/18/20

20I0806-20 TP-08 0-2 09/18/20

20I0806-21 TP-09 1-3 09/18/20

20I0806-22 TP-10 0-2 09/18/20

20I0806-23 TP-11 0-2 09/18/20

20I0806-24 TP-12 0-1.5 09/18/20

BI01001-BLK1 Blank 09/18/20

BI01001-DUP1 Duplicate 09/18/20

BI01001-MS1 Matrix Spike 09/18/20

BI01001-PS1 Post Spike 09/18/20

BI01001-SRM1 Reference 09/18/20

Batch ID: Preparation Method: Prepared By:BI01142 % Solids Prep SK


20I0806-13 TP-01 0-2 09/21/20

20I0806-14 TP-02 0-2 09/21/20

20I0806-15 TP-03 2-4 09/21/20

20I0806-16 TP-04 0-2 09/21/20

20I0806-17 TP-05 0-2 09/21/20

20I0806-18 TP-06 0-1.5 09/21/20

20I0806-19 TP-07 0-2 09/21/20

20I0806-20 TP-08 0-2 09/21/20

20I0806-21 TP-09 1-3 09/21/20

20I0806-22 TP-10 0-2 09/21/20

20I0806-23 TP-11 0-2 09/21/20

20I0806-24 TP-12 0-1.5 09/21/20

Batch ID: Preparation Method: Prepared By:BI01211 EPA 5035A KHA


20I0806-01 TP-01 2 09/21/20

20I0806-02 TP-02 2 09/21/20

20I0806-03 TP-03 3 09/21/20

20I0806-04 TP-04 2 09/21/20

20I0806-05 TP-05 1 09/21/20

20I0806-06 TP-06 1.5 09/21/20

20I0806-07 TP-07 1 09/21/20

20I0806-08 TP-08 2 09/21/20

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20I0806-09 TP-09 3 09/21/20

20I0806-10 TP-10 1 09/21/20

20I0806-11 TP-11 2 09/21/20

20I0806-12 TP-12 1 09/21/20

BI01211-BLK1 Blank 09/21/20

BI01211-BS1 LCS 09/21/20

BI01211-BSD1 LCS Dup 09/21/20

Batch ID: Preparation Method: Prepared By:BI01264 EPA 3550C TSS


20I0806-20 TP-08 0-2 09/23/20

20I0806-20 TP-08 0-2 09/23/20

20I0806-21 TP-09 1-3 09/23/20

20I0806-21 TP-09 1-3 09/23/20

20I0806-22 TP-10 0-2 09/23/20

20I0806-22 TP-10 0-2 09/23/20

20I0806-23 TP-11 0-2 09/23/20

20I0806-23 TP-11 0-2 09/23/20

20I0806-24 TP-12 0-1.5 09/23/20

20I0806-24 TP-12 0-1.5 09/23/20

BI01264-BLK1 Blank 09/23/20

BI01264-BLK2 Blank 09/23/20

BI01264-BS1 LCS 09/23/20

BI01264-BS2 LCS 09/23/20


BI01264-MSD2 Matrix Spike Dup 09/23/20

Batch ID: Preparation Method: Prepared By:BI01268 EPA 3550C PD


20I0806-20 TP-08 0-2 09/23/20

20I0806-21 TP-09 1-3 09/23/20

20I0806-22 TP-10 0-2 09/23/20

20I0806-22RE1 TP-10 0-2 09/23/20

20I0806-23 TP-11 0-2 09/23/20

20I0806-24 TP-12 0-1.5 09/23/20

BI01268-BLK1 Blank 09/23/20

BI01268-BS1 LCS 09/23/20

Batch ID: Preparation Method: Prepared By:BI01307 EPA 3550C LJ


20I0806-13 TP-01 0-2 09/23/20

20I0806-14 TP-02 0-2 09/23/20

20I0806-15 TP-03 2-4 09/23/20

20I0806-16 TP-04 0-2 09/23/20

20I0806-17 TP-05 0-2 09/23/20

20I0806-18 TP-06 0-1.5 09/23/20

20I0806-19 TP-07 0-2 09/23/20

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BI01307-BLK1 Blank 09/23/20

BI01307-BS1 LCS 09/23/20

Batch ID: Preparation Method: Prepared By:BI01308 EPA 3550C JV


20I0806-13 TP-01 0-2 09/23/20

20I0806-13 TP-01 0-2 09/23/20

20I0806-14 TP-02 0-2 09/23/20

20I0806-14 TP-02 0-2 09/23/20

20I0806-15 TP-03 2-4 09/23/20

20I0806-15 TP-03 2-4 09/23/20

20I0806-16 TP-04 0-2 09/23/20

20I0806-16 TP-04 0-2 09/23/20

20I0806-17 TP-05 0-2 09/23/20

20I0806-17 TP-05 0-2 09/23/20

20I0806-18 TP-06 0-1.5 09/23/20

20I0806-18 TP-06 0-1.5 09/23/20

20I0806-19 TP-07 0-2 09/23/20

20I0806-19 TP-07 0-2 09/23/20

BI01308-BLK1 Blank 09/23/20

BI01308-BLK2 Blank 09/23/20

BI01308-BS1 LCS 09/23/20

BI01308-BS2 LCS 09/23/20

Batch ID: Preparation Method: Prepared By:BI01367 EPA SW846-3060 SK


20I0806-15 TP-03 2-4 09/24/20

20I0806-19 TP-07 0-2 09/24/20

20I0806-23 TP-11 0-2 09/24/20

BI01367-BLK1 Blank 09/24/20


Batch ID: Preparation Method: Prepared By:BI01370 EPA 7473 soil SY


20I0806-13 TP-01 0-2 09/24/20

20I0806-14 TP-02 0-2 09/24/20

20I0806-15 TP-03 2-4 09/24/20

20I0806-16 TP-04 0-2 09/24/20

20I0806-17 TP-05 0-2 09/24/20

20I0806-18 TP-06 0-1.5 09/24/20

20I0806-19 TP-07 0-2 09/24/20

20I0806-20 TP-08 0-2 09/24/20

20I0806-21 TP-09 1-3 09/24/20

20I0806-22 TP-10 0-2 09/24/20

20I0806-23 TP-11 0-2 09/24/20

20I0806-24 TP-12 0-1.5 09/24/20

BI01370-BLK1 Blank 09/24/20

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BI01370-DUP1 Duplicate 09/24/20



Batch ID: Preparation Method: Prepared By:BI01404 EPA 3550C/8151A LJ


20I0806-15 TP-03 2-4 09/24/20

20I0806-19 TP-07 0-2 09/24/20

20I0806-23 TP-11 0-2 09/24/20

BI01404-BLK1 Blank 09/24/20

BI01404-BS1 LCS 09/24/20

Batch ID: Preparation Method: Prepared By:BI01434 % Solids Prep KHA


20I0806-01 TP-01 2 09/24/20

20I0806-02 TP-02 2 09/24/20

20I0806-03 TP-03 3 09/24/20

20I0806-04 TP-04 2 09/24/20

20I0806-05 TP-05 1 09/24/20

20I0806-06 TP-06 1.5 09/24/20

20I0806-07 TP-07 1 09/24/20

20I0806-08 TP-08 2 09/24/20

20I0806-09 TP-09 3 09/24/20

20I0806-10 TP-10 1 09/24/20

20I0806-11 TP-11 2 09/24/20

20I0806-12 TP-12 1 09/24/20

Batch ID: Preparation Method: Prepared By:BI01452 Analysis Preparation Soil SK


20I0806-15 TP-03 2-4 09/25/20

20I0806-19 TP-07 0-2 09/25/20

20I0806-23 TP-11 0-2 09/25/20

BI01452-BLK1 Blank 09/25/20


Batch ID: Preparation Method: Prepared By:BI01500 Analysis Preparation PAM


20I0806-15 TP-03 2-4 09/25/20

20I0806-19 TP-07 0-2 09/25/20

20I0806-23 TP-11 0-2 09/25/20

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[TOC_1]QA/QC Summary Data[TOC]

Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Volatile Organic Compounds by GC/MS - Quality Control Data

York Analytical Laboratories, Inc.

Flag

olatile Organic Compounds by GC/MS EPA 8260C[TOC]

Batch BI01211 - EPA 5035A

Blank (BI01211-BLK1) Prepared: 09/21/2020 Analyzed: 09/22/2020

mg/kg wetND 0.00501,1,1,2-Tetrachloroethane

"ND 0.00501,1,1-Trichloroethane

"ND 0.00501,1,2,2-Tetrachloroethane

"ND 0.00501,1,2-Trichloro-1,2,2-trifluoroethane (Freon

113)


"ND 0.00501,1-Dichloroethane

"ND 0.00501,1-Dichloroethylene

"ND 0.00501,2,3-Trichlorobenzene

"ND 0.00501,2,3-Trichloropropane


"ND 0.00501,2,4-Trimethylbenzene

"ND 0.00501,2-Dibromo-3-chloropropane

"ND 0.00501,2-Dibromoethane

"ND 0.00501,2-Dichlorobenzene


"ND 0.00501,2-Dichloropropane




"ND 0.101,4-Dioxane

"ND 0.00502-Butanone

"ND 0.00502-Hexanone

"ND 0.00504-Methyl-2-pentanone

"ND 0.010Acetone

"ND 0.010Acrolein

"ND 0.0050Acrylonitrile

"ND 0.0050Benzene

"ND 0.0050Bromochloromethane

"ND 0.0050Bromodichloromethane

"ND 0.0050Bromoform

"ND 0.0050Bromomethane

"ND 0.0050Carbon disulfide

"ND 0.0050Carbon tetrachloride

"ND 0.0050Chlorobenzene

"ND 0.0050Chloroethane

"ND 0.0050Chloroform

"ND 0.0050Chloromethane

"ND 0.0050cis-1,2-Dichloroethylene

"ND 0.0050cis-1,3-Dichloropropylene

"ND 0.0050Cyclohexane

"ND 0.0050Dibromochloromethane

"ND 0.0050Dibromomethane

"ND 0.0050Dichlorodifluoromethane

"ND 0.0050Ethyl Benzene

"ND 0.0050Hexachlorobutadiene

"ND 0.0050Isopropylbenzene

"ND 0.0050Methyl acetate

"ND 0.0050Methyl tert-butyl ether (MTBE)

"ND 0.0050Methylcyclohexane

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



mg/kg wetND 0.010Methylene chloride

"ND 0.0050n-Butylbenzene

"ND 0.0050n-Propylbenzene

"ND 0.0050o-Xylene

"ND 0.010p- & m- Xylenes

"ND 0.0050p-Isopropyltoluene

"ND 0.0050sec-Butylbenzene

"ND 0.0050Styrene

"ND 0.0050tert-Butyl alcohol (TBA)

"ND 0.0050tert-Butylbenzene

"ND 0.0050Tetrachloroethylene

"ND 0.0050Toluene

"ND 0.0050trans-1,2-Dichloroethylene

"ND 0.0050trans-1,3-Dichloropropylene

"ND 0.0050Trichloroethylene

"ND 0.0050Trichlorofluoromethane

"ND 0.0050Vinyl Chloride

"ND 0.015Xylenes, Total

ug/L 50.0 77-125Surrogate: SURR: 1,2-Dichloroethane-d4 90.045.0

" 50.0 85-120Surrogate: SURR: Toluene-d8 10150.5

" 50.0 76-130Surrogate: SURR: p-Bromofluorobenzene 10351.5

LCS (BI01211-BS1) Prepared & Analyzed: 09/21/2020

ug/L37 50.0 75-12973.5 Low Bias1,1,1,2-Tetrachloroethane

"46 50.0 71-13792.81,1,1-Trichloroethane

"49 50.0 79-12998.21,1,2,2-Tetrachloroethane

"69 50.0 58-1461381,1,2-Trichloro-1,2,2-trifluoroethane (Freon

113)

"49 50.0 83-12397.11,1,2-Trichloroethane

"47 50.0 75-13094.81,1-Dichloroethane

"57 50.0 64-1371141,1-Dichloroethylene

"47 50.0 81-14093.01,2,3-Trichlorobenzene

"46 50.0 81-12691.91,2,3-Trichloropropane

"44 50.0 80-14188.11,2,4-Trichlorobenzene

"42 50.0 84-12584.41,2,4-Trimethylbenzene

"47 50.0 74-14294.41,2-Dibromo-3-chloropropane

"47 50.0 86-12394.31,2-Dibromoethane

"47 50.0 85-12294.11,2-Dichlorobenzene

"47 50.0 71-13394.01,2-Dichloroethane

"45 50.0 81-12290.21,2-Dichloropropane

"44 50.0 82-12687.21,3,5-Trimethylbenzene



"1400 1050 10-2281301,4-Dioxane

"49 50.0 58-14798.72-Butanone

"50 50.0 70-13999.42-Hexanone

"50 50.0 72-1321014-Methyl-2-pentanone

"37 50.0 36-15574.2Acetone

"31 50.0 10-23861.4Acrolein

"60 50.0 66-141120Acrylonitrile

"53 50.0 77-127106Benzene

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



ug/L49 50.0 74-12997.8Bromochloromethane

"44 50.0 81-12488.2Bromodichloromethane

"35 50.0 80-13669.2 Low BiasBromoform

"70 50.0 32-177139Bromomethane

"56 50.0 10-136113Carbon disulfide

"48 50.0 66-14396.6Carbon tetrachloride

"48 50.0 86-12095.3Chlorobenzene

"59 50.0 51-142118Chloroethane

"47 50.0 76-13194.6Chloroform

"86 50.0 49-132172 High BiasChloromethane

"49 50.0 74-13297.2cis-1,2-Dichloroethylene

"45 50.0 81-12990.9cis-1,3-Dichloropropylene

"52 50.0 70-130103Cyclohexane

"46 50.0 10-20091.7Dibromochloromethane

"47 50.0 83-12493.3Dibromomethane

"88 50.0 28-158175 High BiasDichlorodifluoromethane

"46 50.0 84-12592.5Ethyl Benzene

"42 50.0 83-13383.6Hexachlorobutadiene

"43 50.0 81-12785.9Isopropylbenzene

"47 50.0 41-14393.0Methyl acetate

"51 50.0 74-131102Methyl tert-butyl ether (MTBE)

"48 50.0 70-13095.4Methylcyclohexane

"52 50.0 57-141104Methylene chloride

"44 50.0 80-13088.8n-Butylbenzene

"43 50.0 74-13686.3n-Propylbenzene

"45 50.0 83-12390.1o-Xylene

"93 100 82-12893.4p- & m- Xylenes

"45 50.0 85-12590.5p-Isopropyltoluene

"47 50.0 83-12594.9sec-Butylbenzene

"49 50.0 86-12697.7Styrene

"270 250 70-130108tert-Butyl alcohol (TBA)

"43 50.0 80-12786.1tert-Butylbenzene

"42 50.0 80-12984.7Tetrachloroethylene

"47 50.0 85-12194.8Toluene

"51 50.0 72-132102trans-1,2-Dichloroethylene

"43 50.0 78-13286.2trans-1,3-Dichloropropylene

"47 50.0 84-12393.6Trichloroethylene

"56 50.0 62-140112Trichlorofluoromethane

"83 50.0 52-130167 High BiasVinyl Chloride

" 50.0 77-125Surrogate: SURR: 1,2-Dichloroethane-d4 92.746.4

" 50.0 85-120Surrogate: SURR: Toluene-d8 99.049.5

" 50.0 76-130Surrogate: SURR: p-Bromofluorobenzene 92.146.1

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Limit Flag Analyte



Flag


LCS Dup (BI01211-BSD1) Prepared: 09/21/2020 Analyzed: 09/22/2020

ug/L38 50.0 3075-12975.6 2.871,1,1,2-Tetrachloroethane

"48 50.0 3071-13796.8 4.241,1,1-Trichloroethane

"49 50.0 3079-12998.5 0.3461,1,2,2-Tetrachloroethane

"66 50.0 3058-146132 4.821,1,2-Trichloro-1,2,2-trifluoroethane (Freon

113)

"50 50.0 3083-12399.9 2.821,1,2-Trichloroethane

"49 50.0 3075-13098.3 3.621,1-Dichloroethane

"55 50.0 3064-137109 4.521,1-Dichloroethylene

"48 50.0 3081-14095.7 2.821,2,3-Trichlorobenzene

"46 50.0 3081-12691.0 0.9841,2,3-Trichloropropane

"46 50.0 3080-14191.8 4.091,2,4-Trichlorobenzene

"43 50.0 3084-12586.5 2.391,2,4-Trimethylbenzene

"47 50.0 3074-14293.8 0.6161,2-Dibromo-3-chloropropane

"48 50.0 3086-12395.7 1.431,2-Dibromoethane

"48 50.0 3085-12295.3 1.251,2-Dichlorobenzene

"47 50.0 3071-13393.6 0.4691,2-Dichloroethane

"46 50.0 3081-12291.4 1.321,2-Dichloropropane

"44 50.0 3082-12688.4 1.341,3,5-Trimethylbenzene



"1200 1050 3010-228118 9.201,4-Dioxane

"54 50.0 3058-147107 8.442-Butanone

"50 50.0 3070-13999.6 0.2612-Hexanone

"51 50.0 3072-132102 1.204-Methyl-2-pentanone

"36 50.0 3036-15572.0 2.93Acetone

"30 50.0 3010-23860.9 0.785Acrolein

"59 50.0 3066-141117 1.81Acrylonitrile

"54 50.0 3077-127108 2.32Benzene

"51 50.0 3074-129101 3.47Bromochloromethane

"45 50.0 3081-12491.0 3.06Bromodichloromethane

"36 50.0 3080-13672.8 5.13Low BiasBromoform

"71 50.0 3032-177143 2.54Bromomethane

"58 50.0 3010-136116 2.92Carbon disulfide

"51 50.0 3066-143102 5.30Carbon tetrachloride

"50 50.0 3086-12099.0 3.81Chlorobenzene

"54 50.0 3051-142108 9.05Chloroethane

"49 50.0 3076-13197.9 3.41Chloroform

"88 50.0 3049-132175 1.73High BiasChloromethane

"50 50.0 3074-13299.7 2.62cis-1,2-Dichloroethylene

"47 50.0 3081-12993.1 2.35cis-1,3-Dichloropropylene

"53 50.0 3070-130106 2.74Cyclohexane

"48 50.0 3010-20095.4 3.91Dibromochloromethane

"48 50.0 3083-12495.3 2.04Dibromomethane

"90 50.0 3028-158179 2.38High BiasDichlorodifluoromethane

"48 50.0 3084-12596.4 4.07Ethyl Benzene

"44 50.0 3083-13388.3 5.44Hexachlorobutadiene

"43 50.0 3081-12786.2 0.372Isopropylbenzene

"46 50.0 3041-14392.8 0.194Methyl acetate

"52 50.0 3074-131103 0.799Methyl tert-butyl ether (MTBE)

"49 50.0 3070-13098.6 3.36Methylcyclohexane

"55 50.0 3057-141110 4.84Methylene chloride

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LCS Dup (BI01211-BSD1) Prepared: 09/21/2020 Analyzed: 09/22/2020

ug/L46 50.0 3080-13092.0 3.54n-Butylbenzene

"44 50.0 3074-13688.4 2.43n-Propylbenzene

"47 50.0 3083-12393.3 3.47o-Xylene

"97 100 3082-12896.6 3.34p- & m- Xylenes

"46 50.0 3085-12592.5 2.25p-Isopropyltoluene

"48 50.0 3083-12596.7 1.84sec-Butylbenzene

"50 50.0 3086-126101 3.18Styrene

"280 250 3070-130112 3.12tert-Butyl alcohol (TBA)

"44 50.0 3080-12787.2 1.29tert-Butylbenzene

"44 50.0 3080-12987.6 3.39Tetrachloroethylene

"49 50.0 3085-12197.3 2.54Toluene

"53 50.0 3072-132106 3.82trans-1,2-Dichloroethylene

"45 50.0 3078-13290.0 4.27trans-1,3-Dichloropropylene

"48 50.0 3084-12395.2 1.76Trichloroethylene

"59 50.0 3062-140117 4.32Trichlorofluoromethane

"87 50.0 3052-130173 3.83High BiasVinyl Chloride

" 50.0 77-125Surrogate: SURR: 1,2-Dichloroethane-d4 92.346.1

" 50.0 85-120Surrogate: SURR: Toluene-d8 99.549.7

" 50.0 76-130Surrogate: SURR: p-Bromofluorobenzene 90.345.1

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RPD

Limit Flag Analyte

Semivolatile Organic Compounds by GC/MS - Quality Control Data


Flag

OC_2]Semivolatile Organic Compounds by GC/MS EPA 8270D[TOC]

Batch BI01268 - EPA 3550C

Blank (BI01268-BLK1) Prepared & Analyzed: 09/23/2020

ug/kg wetND 41.61,1-Biphenyl

"ND 83.01,2,4,5-Tetrachlorobenzene



"ND 41.61,2-Diphenylhydrazine (as Azobenzene)



"ND 83.02,3,4,6-Tetrachlorophenol

"ND 41.62,4,5-Trichlorophenol


"ND 41.62,4-Dichlorophenol

"ND 41.62,4-Dimethylphenol

"ND 83.02,4-Dinitrophenol

"ND 41.62,4-Dinitrotoluene


"ND 41.62-Chloronaphthalene

"ND 41.62-Chlorophenol

"ND 41.62-Methylnaphthalene

"ND 41.62-Methylphenol

"ND 83.02-Nitroaniline

"ND 41.62-Nitrophenol

"ND 41.63- & 4-Methylphenols

"ND 41.63,3-Dichlorobenzidine


"ND 83.04,6-Dinitro-2-methylphenol

"ND 41.64-Bromophenyl phenyl ether

"ND 41.64-Chloro-3-methylphenol

"ND 41.64-Chloroaniline

"ND 41.64-Chlorophenyl phenyl ether



"ND 41.6Acenaphthene

"ND 41.6Acenaphthylene

"ND 41.6Acetophenone

"ND 166Aniline

"ND 41.6Anthracene

"ND 41.6Atrazine

"ND 41.6Benzaldehyde

"ND 166Benzidine

"ND 41.6Benzo(a)anthracene

"ND 41.6Benzo(a)pyrene

"ND 41.6Benzo(b)fluoranthene

"ND 41.6Benzo(g,h,i)perylene

"ND 41.6Benzo(k)fluoranthene

"ND 41.6Benzoic acid

"ND 41.6Benzyl alcohol

"ND 41.6Benzyl butyl phthalate

"ND 41.6Bis(2-chloroethoxy)methane

"ND 41.6Bis(2-chloroethyl)ether

"ND 41.6Bis(2-chloroisopropyl)ether

"ND 41.6Bis(2-ethylhexyl)phthalate

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Flag



ug/kg wetND 83.0Caprolactam

"ND 41.6Carbazole

"ND 41.6Chrysene

"ND 41.6Dibenzo(a,h)anthracene

"ND 41.6Dibenzofuran

"ND 41.6Diethyl phthalate

"ND 41.6Dimethyl phthalate

"ND 41.6Di-n-butyl phthalate

"ND 41.6Di-n-octyl phthalate

"ND 83.0Diphenylamine

"ND 41.6Fluoranthene

"ND 41.6Fluorene

"ND 41.6Hexachlorobenzene


"ND 41.6Hexachlorocyclopentadiene

"ND 41.6Hexachloroethane

"ND 41.6Indeno(1,2,3-cd)pyrene

"ND 41.6Isophorone

"ND 41.6Naphthalene

"ND 41.6Nitrobenzene

"ND 41.6N-Nitrosodimethylamine

"ND 41.6N-nitroso-di-n-propylamine

"ND 41.6N-Nitrosodiphenylamine

"ND 41.6Pentachlorophenol

"ND 41.6Phenanthrene

"ND 41.6Phenol

"ND 41.6Pyrene

" 1660 20-108Surrogate: SURR: 2-Fluorophenol 49.4821

" 1660 23-114Surrogate: SURR: Phenol-d5 51.5855

" 831 22-108Surrogate: SURR: Nitrobenzene-d5 52.4435

" 831 21-113Surrogate: SURR: 2-Fluorobiphenyl 52.7438

" 1660 19-110Surrogate: SURR: 2,4,6-Tribromophenol 62.41040

" 831 24-116Surrogate: SURR: Terphenyl-d14 60.9506

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Limit Flag Analyte



Flag



ug/kg wet501 41.6 831 22-10360.31,1-Biphenyl

"634 83.0 831 10-14476.41,2,4,5-Tetrachlorobenzene

"438 41.6 831 23-13052.71,2,4-Trichlorobenzene

"447 41.6 831 26-11353.81,2-Dichlorobenzene

"502 41.6 831 10-14060.51,2-Diphenylhydrazine (as Azobenzene)



"389 83.0 831 30-13046.92,3,4,6-Tetrachlorophenol

"366 41.6 831 14-13844.12,4,5-Trichlorophenol


"467 41.6 831 23-13356.32,4-Dichlorophenol

"521 41.6 831 15-13162.72,4-Dimethylphenol

"456 83.0 831 10-14955.02,4-Dinitrophenol

"483 41.6 831 30-12358.22,4-Dinitrotoluene

"482 41.6 831 30-12558.12,6-Dinitrotoluene

"422 41.6 831 22-11550.82-Chloronaphthalene

"459 41.6 831 25-12155.22-Chlorophenol

"478 41.6 831 16-12757.52-Methylnaphthalene

"390 41.6 831 10-14647.02-Methylphenol

"478 83.0 831 24-12657.62-Nitroaniline

"549 41.6 831 17-12966.12-Nitrophenol

"340 41.6 831 20-10940.93- & 4-Methylphenols

"363 41.6 831 10-14743.83,3-Dichlorobenzidine

"381 83.0 831 23-12345.93-Nitroaniline

"579 83.0 831 10-14969.84,6-Dinitro-2-methylphenol

"454 41.6 831 30-13854.74-Bromophenyl phenyl ether

"417 41.6 831 16-13850.24-Chloro-3-methylphenol

"280 41.6 831 10-11733.74-Chloroaniline

"429 41.6 831 18-13251.64-Chlorophenyl phenyl ether

"452 83.0 831 14-12554.44-Nitroaniline

"349 83.0 831 10-13642.04-Nitrophenol

"456 41.6 831 17-12454.9Acenaphthene

"448 41.6 831 16-12454.0Acenaphthylene

"500 41.6 831 28-10560.2Acetophenone

"430 166 831 10-11151.8Aniline

"462 41.6 831 24-12455.6Anthracene

"491 41.6 831 22-12059.1Atrazine

"513 41.6 831 21-10061.8Benzaldehyde

"437 41.6 831 25-13452.6Benzo(a)anthracene

"412 41.6 831 29-14449.6Benzo(a)pyrene

"451 41.6 831 20-15154.3Benzo(b)fluoranthene

"431 41.6 831 10-15351.8Benzo(g,h,i)perylene

"424 41.6 831 10-14851.0Benzo(k)fluoranthene

"248 41.6 831 10-11629.9Benzoic acid

"515 41.6 831 17-12862.0Benzyl alcohol

"432 41.6 831 10-13252.0Benzyl butyl phthalate

"470 41.6 831 10-12956.6Bis(2-chloroethoxy)methane

"476 41.6 831 14-12557.3Bis(2-chloroethyl)ether

"671 41.6 831 14-12280.8Bis(2-chloroisopropyl)ether

"434 41.6 831 10-14152.3Bis(2-ethylhexyl)phthalate

"490 83.0 831 10-12359.0Caprolactam

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RPD

Limit Flag Analyte



Flag



ug/kg wet445 41.6 831 31-12053.6Carbazole

"452 41.6 831 24-11654.5Chrysene

"444 41.6 831 17-14753.5Dibenzo(a,h)anthracene

"422 41.6 831 23-12350.8Dibenzofuran

"396 41.6 831 23-12247.7Diethyl phthalate

"509 41.6 831 28-12761.2Dimethyl phthalate

"419 41.6 831 19-12350.4Di-n-butyl phthalate

"444 41.6 831 10-13253.4Di-n-octyl phthalate

"618 83.0 831 40-14074.4Diphenylamine

"449 41.6 831 36-12554.1Fluoranthene

"450 41.6 831 16-13054.2Fluorene

"418 41.6 831 10-12950.3Hexachlorobenzene

"437 41.6 831 22-15352.6Hexachlorobutadiene

"231 41.6 831 10-13427.8Hexachlorocyclopentadiene

"415 41.6 831 20-11250.0Hexachloroethane

"538 41.6 831 10-15564.7Indeno(1,2,3-cd)pyrene

"451 41.6 831 14-13154.3Isophorone

"488 41.6 831 20-12158.7Naphthalene

"442 41.6 831 20-12153.2Nitrobenzene

"410 41.6 831 10-12449.4N-Nitrosodimethylamine

"442 41.6 831 21-11953.2N-nitroso-di-n-propylamine

"611 41.6 831 10-16373.6N-Nitrosodiphenylamine

"317 41.6 831 10-14338.2Pentachlorophenol

"474 41.6 831 24-12357.0Phenanthrene

"493 41.6 831 15-12359.3Phenol

"470 41.6 831 24-13256.6Pyrene







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RPD

Limit Flag Analyte



Flag



ug/kg wetND 41.61,1-Biphenyl

"ND 83.01,2,4,5-Tetrachlorobenzene



"ND 41.61,2-Diphenylhydrazine (as Azobenzene)



"ND 83.02,3,4,6-Tetrachlorophenol



"ND 41.62,4-Dichlorophenol

"ND 41.62,4-Dimethylphenol

"ND 83.02,4-Dinitrophenol



"ND 41.62-Chloronaphthalene

"ND 41.62-Chlorophenol

"ND 41.62-Methylnaphthalene

"ND 41.62-Methylphenol



"ND 41.63- & 4-Methylphenols

"ND 41.63,3-Dichlorobenzidine


"ND 83.04,6-Dinitro-2-methylphenol

"ND 41.64-Bromophenyl phenyl ether

"ND 41.64-Chloro-3-methylphenol

"ND 41.64-Chloroaniline

"ND 41.64-Chlorophenyl phenyl ether



"ND 41.6Acenaphthene

"ND 41.6Acenaphthylene

"ND 41.6Acetophenone

"ND 166Aniline

"ND 41.6Anthracene

"ND 41.6Atrazine

"ND 41.6Benzaldehyde

"ND 166Benzidine

"ND 41.6Benzo(a)anthracene

"ND 41.6Benzo(a)pyrene

"ND 41.6Benzo(b)fluoranthene

"ND 41.6Benzo(g,h,i)perylene

"ND 41.6Benzo(k)fluoranthene

"ND 41.6Benzoic acid

"ND 41.6Benzyl alcohol

"ND 41.6Benzyl butyl phthalate

"ND 41.6Bis(2-chloroethoxy)methane

"ND 41.6Bis(2-chloroethyl)ether

"ND 41.6Bis(2-chloroisopropyl)ether

"ND 41.6Bis(2-ethylhexyl)phthalate

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Limit Flag Analyte



Flag



ug/kg wetND 83.0Caprolactam

"ND 41.6Carbazole

"ND 41.6Chrysene

"ND 41.6Dibenzo(a,h)anthracene

"ND 41.6Dibenzofuran

"ND 41.6Diethyl phthalate

"ND 41.6Dimethyl phthalate

"ND 41.6Di-n-butyl phthalate

"ND 41.6Di-n-octyl phthalate

"ND 83.0Diphenylamine

"ND 41.6Fluoranthene

"ND 41.6Fluorene

"ND 41.6Hexachlorobenzene


"ND 41.6Hexachlorocyclopentadiene

"ND 41.6Hexachloroethane

"ND 41.6Indeno(1,2,3-cd)pyrene

"ND 41.6Isophorone

"ND 41.6Naphthalene

"ND 41.6Nitrobenzene

"ND 41.6N-Nitrosodimethylamine

"ND 41.6N-nitroso-di-n-propylamine

"ND 41.6N-Nitrosodiphenylamine

"ND 41.6Pentachlorophenol

"ND 41.6Phenanthrene

"ND 41.6Phenol

"ND 41.6Pyrene







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RPD

Limit Flag Analyte



Flag


LCS (BI01307-BS1) Prepared: 09/23/2020 Analyzed: 09/24/2020

ug/kg wet543 41.6 831 22-10365.41,1-Biphenyl

"705 83.0 831 10-14484.91,2,4,5-Tetrachlorobenzene

"473 41.6 831 23-13057.01,2,4-Trichlorobenzene


"543 41.6 831 10-14065.31,2-Diphenylhydrazine (as Azobenzene)



"402 83.0 831 30-13048.42,3,4,6-Tetrachlorophenol



"499 41.6 831 23-13360.02,4-Dichlorophenol

"529 41.6 831 15-13163.72,4-Dimethylphenol

"461 83.0 831 10-14955.52,4-Dinitrophenol

"483 41.6 831 30-12358.12,4-Dinitrotoluene

"540 41.6 831 30-12565.02,6-Dinitrotoluene

"467 41.6 831 22-11556.22-Chloronaphthalene

"466 41.6 831 25-12156.12-Chlorophenol

"514 41.6 831 16-12761.92-Methylnaphthalene

"399 41.6 831 10-14648.02-Methylphenol

"533 83.0 831 24-12664.22-Nitroaniline

"570 41.6 831 17-12968.62-Nitrophenol

"336 41.6 831 20-10940.43- & 4-Methylphenols

"385 41.6 831 10-14746.43,3-Dichlorobenzidine

"444 83.0 831 23-12353.43-Nitroaniline

"617 83.0 831 10-14974.24,6-Dinitro-2-methylphenol

"492 41.6 831 30-13859.24-Bromophenyl phenyl ether

"455 41.6 831 16-13854.84-Chloro-3-methylphenol

"386 41.6 831 10-11746.44-Chloroaniline

"468 41.6 831 18-13256.44-Chlorophenyl phenyl ether

"476 83.0 831 14-12557.34-Nitroaniline

"368 83.0 831 10-13644.44-Nitrophenol

"497 41.6 831 17-12459.8Acenaphthene

"496 41.6 831 16-12459.7Acenaphthylene

"485 41.6 831 28-10558.4Acetophenone

"457 166 831 10-11155.0Aniline

"506 41.6 831 24-12460.9Anthracene

"519 41.6 831 22-12062.4Atrazine

"500 41.6 831 21-10060.2Benzaldehyde

"485 41.6 831 25-13458.4Benzo(a)anthracene

"459 41.6 831 29-14455.3Benzo(a)pyrene

"507 41.6 831 20-15161.1Benzo(b)fluoranthene

"498 41.6 831 10-15360.0Benzo(g,h,i)perylene

"459 41.6 831 10-14855.3Benzo(k)fluoranthene

"232 41.6 831 10-11627.9Benzoic acid

"514 41.6 831 17-12861.8Benzyl alcohol

"458 41.6 831 10-13255.2Benzyl butyl phthalate

"505 41.6 831 10-12960.8Bis(2-chloroethoxy)methane

"486 41.6 831 14-12558.5Bis(2-chloroethyl)ether

"681 41.6 831 14-12282.0Bis(2-chloroisopropyl)ether

"459 41.6 831 10-14155.3Bis(2-ethylhexyl)phthalate

"467 83.0 831 10-12356.3Caprolactam

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Result

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%REC

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RPD

Limit Flag Analyte



Flag



ug/kg wet488 41.6 831 31-12058.8Carbazole

"502 41.6 831 24-11660.4Chrysene

"500 41.6 831 17-14760.2Dibenzo(a,h)anthracene

"455 41.6 831 23-12354.8Dibenzofuran

"420 41.6 831 23-12250.6Diethyl phthalate

"436 41.6 831 28-12752.5Dimethyl phthalate

"453 41.6 831 19-12354.6Di-n-butyl phthalate

"480 41.6 831 10-13257.8Di-n-octyl phthalate

"695 83.0 831 40-14083.7Diphenylamine

"481 41.6 831 36-12557.9Fluoranthene

"480 41.6 831 16-13057.8Fluorene

"457 41.6 831 10-12955.1Hexachlorobenzene

"477 41.6 831 22-15357.5Hexachlorobutadiene

"229 41.6 831 10-13427.5Hexachlorocyclopentadiene

"421 41.6 831 20-11250.7Hexachloroethane

"529 41.6 831 10-15563.6Indeno(1,2,3-cd)pyrene

"464 41.6 831 14-13155.9Isophorone

"526 41.6 831 20-12163.4Naphthalene

"455 41.6 831 20-12154.8Nitrobenzene

"423 41.6 831 10-12451.0N-Nitrosodimethylamine

"443 41.6 831 21-11953.4N-nitroso-di-n-propylamine

"669 41.6 831 10-16380.6N-Nitrosodiphenylamine

"299 41.6 831 10-14336.0Pentachlorophenol

"519 41.6 831 24-12362.5Phenanthrene

"513 41.6 831 15-12361.7Phenol

"522 41.6 831 24-13262.9Pyrene







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Units Level

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Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Organochlorine Pesticides by GC/ECD - Quality Control Data


Flag

OC_2]Organochlorine Pesticides by GC/ECD EPA 8081B[TOC]



mg/kg wetND 0.001644,4'-DDD

"ND 0.001644,4'-DDE

"ND 0.001644,4'-DDT

"ND 0.00164Aldrin

"ND 0.00164alpha-BHC

"ND 0.00164alpha-Chlordane

"ND 0.00164beta-BHC

"ND 0.0329Chlordane, total

"ND 0.00164delta-BHC

"ND 0.00164Dieldrin

"ND 0.00164Endosulfan I

"ND 0.00164Endosulfan II

"ND 0.00164Endosulfan sulfate

"ND 0.00164Endrin

"ND 0.00164Endrin aldehyde

"ND 0.00164Endrin ketone

"ND 0.00164gamma-BHC (Lindane)

"ND 0.00164gamma-Chlordane

"ND 0.00164Heptachlor

"ND 0.00164Heptachlor epoxide

"ND 0.00822Methoxychlor

"ND 0.0832Toxaphene

" 0.0664 30-150Surrogate: Decachlorobiphenyl 1070.0712

" 0.0664 30-150Surrogate: Tetrachloro-m-xylene 80.20.0533


mg/kg wet0.0244 0.00164 0.0332 40-14073.44,4'-DDD

"0.0205 0.00164 0.0332 40-14061.74,4'-DDE

"0.0208 0.00164 0.0332 40-14062.64,4'-DDT

"0.0254 0.00164 0.0332 40-14076.5Aldrin

"0.0227 0.00164 0.0332 40-14068.3alpha-BHC

"0.0232 0.00164 0.0332 40-14069.8alpha-Chlordane

"0.0218 0.00164 0.0332 40-14065.6beta-BHC

"0.0242 0.00164 0.0332 40-14073.0delta-BHC

"0.0237 0.00164 0.0332 40-14071.2Dieldrin

"0.0262 0.00164 0.0332 40-14078.8Endosulfan I

"0.0246 0.00164 0.0332 40-14074.1Endosulfan II

"0.0254 0.00164 0.0332 40-14076.4Endosulfan sulfate

"0.0234 0.00164 0.0332 40-14070.5Endrin

"0.0250 0.00164 0.0332 40-14075.3Endrin aldehyde

"0.0246 0.00164 0.0332 40-14074.1Endrin ketone

"0.0229 0.00164 0.0332 40-14068.8gamma-BHC (Lindane)

"0.0233 0.00164 0.0332 40-14070.3gamma-Chlordane

"0.0242 0.00164 0.0332 40-14072.8Heptachlor

"0.0230 0.00164 0.0332 40-14069.3Heptachlor epoxide

"0.0250 0.00822 0.0332 40-14075.2Methoxychlor

" 0.0664 30-150Surrogate: Decachlorobiphenyl 99.60.0661


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Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



mg/kg wetND 0.001644,4'-DDD

"ND 0.001644,4'-DDE

"ND 0.001644,4'-DDT

"ND 0.00164Aldrin

"ND 0.00164alpha-BHC

"ND 0.00164alpha-Chlordane

"ND 0.00164beta-BHC

"ND 0.0329Chlordane, total

"ND 0.00164delta-BHC

"ND 0.00164Dieldrin

"ND 0.00164Endosulfan I

"ND 0.00164Endosulfan II

"ND 0.00164Endosulfan sulfate

"ND 0.00164Endrin

"ND 0.00164Endrin aldehyde

"ND 0.00164Endrin ketone

"ND 0.00164gamma-BHC (Lindane)

"ND 0.00164gamma-Chlordane

"ND 0.00164Heptachlor

"ND 0.00164Heptachlor epoxide

"ND 0.00822Methoxychlor

"ND 0.0832Toxaphene




mg/kg wet0.0144 0.00164 0.0332 40-14043.34,4'-DDD

"0.0146 0.00164 0.0332 40-14044.14,4'-DDE

"0.0156 0.00164 0.0332 40-14047.04,4'-DDT

"0.0140 0.00164 0.0332 40-14042.1Aldrin

"0.0136 0.00164 0.0332 40-14041.1alpha-BHC

"0.0141 0.00164 0.0332 40-14042.6alpha-Chlordane

"0.0145 0.00164 0.0332 40-14043.6beta-BHC

"0.0134 0.00164 0.0332 40-14040.3delta-BHC

"0.0142 0.00164 0.0332 40-14042.6Dieldrin

"0.0146 0.00164 0.0332 40-14043.9Endosulfan I

"0.0136 0.00164 0.0332 40-14041.1Endosulfan II

"0.0151 0.00164 0.0332 40-14045.4Endosulfan sulfate

"0.0147 0.00164 0.0332 40-14044.3Endrin

"0.0140 0.00164 0.0332 40-14042.2Endrin aldehyde

"0.0143 0.00164 0.0332 40-14043.0Endrin ketone

"0.0141 0.00164 0.0332 40-14042.4gamma-BHC (Lindane)

"0.0142 0.00164 0.0332 40-14042.8gamma-Chlordane

"0.0147 0.00164 0.0332 40-14044.1Heptachlor

"0.0150 0.00164 0.0332 40-14045.2Heptachlor epoxide

"0.0176 0.00822 0.0332 40-14053.1Methoxychlor



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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag

Batch Y0G1403 - BF00756

Performance Mix (Y0G1403-PEM1) Prepared & Analyzed: 07/13/2020

ng/mL7.08 0.00 0-2004,4'-DDD

"1.79 0.00 0-2004,4'-DDE

"356 200 0-2001784,4'-DDT

"198 100 0-200198Endrin

"6.28 0.00 0-200Endrin aldehyde

"7.46 0.00 0-200Endrin ketone

Batch Y0I1101 - BI00252

Performance Mix (Y0I1101-PEM1) Prepared & Analyzed: 09/10/2020

ng/mL3.52 0.00 0-2004,4'-DDD

"1.19 0.00 0-2004,4'-DDE

"196 200 0-20098.14,4'-DDT

"86.1 100 0-20086.1Endrin



Batch Y0I2504 - BI01182

Performance Mix (Y0I2504-PEM1) Prepared & Analyzed: 09/24/2020

ng/mL2.64 0.00 0-2004,4'-DDD

"1.15 0.00 0-2004,4'-DDE

"135 200 0-20067.34,4'-DDT

"71.4 100 0-20071.4Endrin



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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Polychlorinated Biphenyls by GC/ECD - Quality Control Data


Flag

OC_2]Polychlorinated Biphenyls by GC/ECD EPA 8082A[TOC]



mg/kg wetND 0.0166Aroclor 1016

"ND 0.0166Aroclor 1221








"ND 0.0166Total PCBs




mg/kg wet0.150 0.0166 0.332 40-13045.1Aroclor 1016

"0.141 0.0166 0.332 40-13042.4Aroclor 1260



Matrix Spike (BI01264-MS2) Prepared: 09/23/2020 Analyzed: 09/24/2020*Source sample: 20I0806-22 (TP-10 0-2)

mg/kg dry0.180 0.0180 0.361 ND 40-14049.9Aroclor 1016

"0.209 0.0180 0.361 0.0194 40-14052.5Aroclor 1260



Matrix Spike Dup (BI01264-MSD2) Prepared: 09/23/2020 Analyzed: 09/24/2020*Source sample: 20I0806-22 (TP-10 0-2)

mg/kg dry0.128 0.0180 0.361 ND 5040-14035.4 33.8Low BiasAroclor 1016

"0.168 0.0180 0.361 0.0194 5040-14041.2 21.6Aroclor 1260



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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Polychlorinated Biphenyls by GC/ECD - Quality Control Data


Flag



mg/kg wetND 0.0166Aroclor 1016









"ND 0.0166Total PCBs




mg/kg wet0.192 0.0166 0.332 40-13057.8Aroclor 1016

"0.179 0.0166 0.332 40-13053.7Aroclor 1260



Batch Y0I2347 - BI01306

Aroclor Reference (Y0I2347-ARC1) Prepared & Analyzed: 09/23/2020

ug/mL 0.200Surrogate: Tetrachloro-m-xylene 1070.214

" 0.200Surrogate: Decachlorobiphenyl 98.50.197

Batch Y0I2443 - BI01319

Aroclor Reference (Y0I2443-ARC1) Prepared & Analyzed: 09/24/2020

ug/mL 0.200Surrogate: Tetrachloro-m-xylene 1100.221

" 0.200Surrogate: Decachlorobiphenyl 1140.229

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Chlorinated Herbicides by GC/ECD - Quality Control Data


Flag

OC_2]Chlorinated Herbicides by GC/ECD EPA 8151A[TOC]

Batch BI01404 - EPA 3550C/8151A


ug/kg wetND 19.92,4,5-T

"ND 19.92,4,5-TP (Silvex)

"ND 19.92,4-D

" 498 21-150Surrogate: 2,4-Dichlorophenylacetic acid

(DCAA)

97.4485


ug/kg wet147 19.9 159 10-12092.52,4,5-T

"148 19.9 159 10-12093.12,4,5-TP (Silvex)

"150 19.9 159 10-11894.42,4-D

" 498 21-150Surrogate: 2,4-Dichlorophenylacetic acid

(DCAA)

97.2484

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Metals by ICP - Quality Control Data


Flag

[TOC_2]Metals by ICP EPA 6010D[TOC]

Batch BI01001 - EPA 3050B


mg/kg wetND 5.00Aluminum

"ND 2.50Antimony

"ND 1.50Arsenic

"ND 2.50Barium

"ND 0.050Beryllium

"ND 0.300Cadmium

"ND 5.00Calcium

"ND 0.500Chromium

"ND 0.400Cobalt

"ND 2.00Copper

"ND 25.0Iron

"ND 0.500Lead

"ND 5.00Magnesium

"ND 0.500Manganese

"ND 1.00Nickel

"23.4 5.00Potassium

"ND 2.50Selenium

"ND 0.500Silver

"ND 50.0Sodium

"ND 2.50Thallium

"ND 1.00Vanadium

"ND 2.50Zinc

Duplicate (BI01001-DUP1) Prepared: 09/18/2020 Analyzed: 09/22/2020*Source sample: 20I0806-24 (TP-12 0-1.5)

mg/kg dry14900 5.52 16100 357.39Aluminum

"ND 2.76 ND 35Antimony

"4.62 1.65 5.27 3513.2Arsenic

"94.4 2.76 98.8 354.53Barium

"ND 0.055 ND 35Beryllium

"0.457 0.331 0.674 3538.5 Non-dir.Cadmium

"6610 5.52 14400 3574.2 Non-dir.Calcium

"22.1 0.552 25.4 3513.7Chromium

"8.68 0.441 8.84 351.82Cobalt

"62.3 2.21 54.7 3513.0Copper

"15800 27.6 17200 358.52Iron

"152 0.552 147 353.34Lead

"4240 5.52 7210 3552.0 Non-dir.Magnesium

"265 0.552 323 3519.7Manganese

"25.1 1.10 26.0 353.37Nickel

"816 5.52 931 3513.2Potassium

"ND 2.76 ND 35Selenium

"ND 0.552 ND 35Silver

"815 55.2 549 3539.1 Non-dir.Sodium

"ND 2.76 ND 35Thallium

"39.3 1.10 41.7 355.87Vanadium

"101 2.76 115 3513.2Zinc

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Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag


Matrix Spike (BI01001-MS1) Prepared: 09/18/2020 Analyzed: 09/22/2020*Source sample: 20I0806-24 (TP-12 0-1.5)

mg/kg dry14700 5.52 221 16100 75-125NR Low BiasAluminum

"5.33 2.76 27.6 ND 75-12519.3 Low BiasAntimony

"161 1.65 221 5.27 75-12570.6 Low BiasArsenic

"252 2.76 221 98.8 75-12569.3 Low BiasBarium

"2.33 0.055 5.52 ND 75-12542.2 Low BiasBeryllium

"4.34 0.331 5.52 0.674 75-12566.4 Low BiasCadmium

"6970 5.52 110 14400 75-125NR Low BiasCalcium

"38.5 0.552 22.1 25.4 75-12559.3 Low BiasChromium

"48.8 0.441 55.2 8.84 75-12572.5 Low BiasCobalt

"86.5 2.21 27.6 54.7 75-125115Copper

"14500 27.6 110 17200 75-125NR Low BiasIron

"218 0.552 55.2 147 75-125128 High BiasLead

"3300 5.52 110 7210 75-125NR Low BiasMagnesium

"261 0.552 55.2 323 75-125NR Low BiasManganese

"64.6 1.10 55.2 26.0 75-12570.1 Low BiasNickel

"947 5.52 110 931 75-12514.2 Low BiasPotassium

"149 2.76 221 ND 75-12567.5 Low BiasSelenium

"4.23 0.552 5.52 ND 75-12576.7Silver

"1060 55.2 110 549 75-125468 High BiasSodium

"151 2.76 221 ND 75-12568.5 Low BiasThallium

"84.3 1.10 55.2 41.7 75-12577.3Vanadium

"160 2.76 55.2 115 75-12581.3Zinc

Post Spike (BI01001-PS1) Prepared: 09/18/2020 Analyzed: 09/22/2020*Source sample: 20I0806-24 (TP-12 0-1.5)

ug/mL146 2.00 146 75-12516.3 Low BiasAluminum

"0.199 0.250 0.011 75-12575.4Antimony

"1.57 2.00 0.048 75-12576.2Arsenic

"2.54 2.00 0.896 75-12582.0Barium

"0.018 0.0500 -0.021 75-12536.6 Low BiasBeryllium

"0.042 0.0500 0.006 75-12572.6 Low BiasCadmium

"128 1.00 131 75-125NR Low BiasCalcium

"0.386 0.200 0.230 75-12577.9Chromium

"0.466 0.500 0.080 75-12577.2Cobalt

"0.700 0.250 0.496 75-12581.6Copper

"154 1.00 156 75-125NR Low BiasIron

"1.71 0.500 1.34 75-12575.5Lead

"65.0 1.00 65.4 75-125NR Low BiasMagnesium

"3.33 0.500 2.93 75-12580.1Manganese

"0.622 0.500 0.235 75-12577.3Nickel

"9.28 1.00 8.44 75-12584.4Potassium

"1.46 2.00 -0.030 75-12572.9 Low BiasSelenium

"0.024 0.0500 -0.007 75-12548.0 Low BiasSilver

"5.96 1.00 4.97 75-12599.1Sodium

"1.42 2.00 -0.028 75-12571.0 Low BiasThallium

"0.765 0.500 0.378 75-12577.4Vanadium

"1.40 0.500 1.04 75-12571.7 Low BiasZinc

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Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag


Reference (BI01001-SRM1) Prepared: 09/18/2020 Analyzed: 09/22/2020

mg/kg wet7310 5.00 8460 50.5-150.186.4Aluminum

"39.9 2.50 120 19-251.733.2Antimony

"71.4 1.50 95.5 70.1-129.874.7Arsenic

"242 2.50 300 75-12580.5Barium

"77.1 0.050 103 75-125.274.9 Low BiasBeryllium

"100 0.300 135 74.8-125.274.4 Low BiasCadmium

"2890 5.00 4720 72.7-127.561.2 Low BiasCalcium

"106 0.500 147 70.1-129.972.3Chromium

"33.9 0.400 43.2 75-12578.4Cobalt

"118 2.00 150 75.3-125.378.7Copper

"10100 25.0 14400 35.8-164.669.8Iron

"74.4 0.500 92.3 70-13080.6Lead

"1650 5.00 2300 61.7-137.871.8Magnesium

"526 0.500 677 78.1-12277.7 Low BiasManganese

"47.3 1.00 59.8 70.1-130.179.1Nickel

"1490 5.00 2030 59.1-140.973.2Potassium

"26.5 2.50 42.0 55.7-144.563.0Selenium

"30.2 0.500 40.3 69.2-130.874.9Silver

"138 50.0 139 36.1-163.399.6Sodium

"58.2 2.50 83.1 65.3-146.870.1Thallium

"69.3 1.00 96.9 67-133.171.6Vanadium

"269 2.50 369 69.9-130.172.9Zinc

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Mercury by EPA 7000/200 Series Methods - Quality Control Data


Flag

7000/200 Series Methods EPA 7473[TOC]

Batch BI01370 - EPA 7473 soil


mg/kg wetND 0.0300Mercury

Duplicate (BI01370-DUP1) Prepared & Analyzed: 09/24/2020*Source sample: 20I0806-16 (TP-04 0-2)

mg/kg dry0.373 0.0332 0.406 358.52Mercury

Matrix Spike (BI01370-MS1) Prepared & Analyzed: 09/24/2020*Source sample: 20I0806-16 (TP-04 0-2)

mg/kg0.794 0.500 0.367 75-12585.3Mercury

Reference (BI01370-SRM1) Prepared & Analyzed: 09/24/2020

mg/kg3.3701 3.71 65-13590.8Mercury

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Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Wet Chemistry Parameters - Quality Control Data


Flag

et Chemistry Parameters EPA 7196A[TOC]

Batch BI01367 - EPA SW846-3060


mg/kg wetND 0.500Chromium, Hexavalent


mg/L35.2 92.5 25.95-196.7638.1Chromium, Hexavalent

Batch BI01452 - Analysis Preparation Soil


mg/kg wetND 0.500Cyanide, total


ug/mL94.8 96.2 42.41-156.9698.5Cyanide, total

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Volatile Analysis Sample Containers

Volatile Sample ContainerClient Sample IDLab ID

20I0806-01 40mL Vial with Stir Bar-Cool 4° CTP-01 2





20I0806-06 40mL Vial with Stir Bar-Cool 4° CTP-06 1.5







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[TOC_1]Notes and Specific Data Flags[Sample and Data Qualifiers Relating to This Work Order

S-GC Two surrogates are used for this analysis. One surrogate recovered within control limits therefore the analysis is acceptable.

S-08 The recovery of this surrogate was outside of QC limits.

QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The LCS and/or LCSD were

within acceptance limits showing that the laboratory is in control and the data are acceptable.

QL-02 This LCS analyte is outside Laboratory Recovery limits due the analyte behavior using the referenced method. The reference method

has certain limitations with respect to analytes of this nature.

M-SRD1 The serial dilution for this element was outside control limits.

M-CRL The RL check for this element recovered outside of control limits.

J Detected below the Reporting Limit but greater than or equal to the Method Detection Limit (MDL/LOD) or in the case of a TIC,

the result is an estimated concentration.

CCV-L The value reported is estimated due to its behavior during continuing calibration verification (>20% difference for average RF or

>20% drift for linear or quadratic fit.) This value may be biased low.

CCV-H The value reported is estimated due to its behavior during continuing calibration verification (>20% difference for average RF or

>20% drift for linear or quadratic fit.) This value may be biased high.

CCV-E The value reported is ESTIMATED. The value is estimated due to its behavior during continuing calibration verification (>20%

Difference for average Rf or >20% Drift for quadratic fit).

B Analyte is found in the associated analysis batch blank. For volatiles, methylene chloride and acetone are common lab contaminants.

Relative Percent DifferenceRPD

Not reportedNR

NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND

Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note

that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias

conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.

Low Bias

High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take

note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias


High Bias

Wet The data has been reported on an as-received (wet weight) basis

REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.

METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a

99% confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA

600 and 200 series methods.

RL

MDL

*

LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the

lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is

based upon NELAC 2009 Standards and applies to all analyses.

LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably

detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.

Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located

above the LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and

semi-volatile target compounds only.

Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .

Definitions and Other Explanations

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Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is

outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high

due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.

If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet

and cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two. For this

reason, York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as

Diphenylamine.

If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and

1268 which are non-target aroclors for some regulatory lists.

2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user

should take note.

Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.

Certification for pH is no longer offered by NYDOH ELAP.

For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a

verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.

Corrective Action: Herbicide, Cr+6 and cyanide analysis added to TP-03, TP-07 and TP-11 composites per Victoria Panico email on 9/23/20.

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of 166

Technical Report

prepared for:

Gallagher Bassett - Poughkeepsie, NY22 IBM Road, Suite 101






CT Cert. No. PH-0723 New Jersey Cert. No. CT005 and NY037 PA Cert. No. 68-04440

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New York Cert. Nos. 10854 and 12058

132-02 89th AVENUE RICHMOND HILL, NY 11418

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Page 1 of 31


SV-0120I0814-01 Soil Vapor 09/17/2020 09/17/2020

SV-0220I0814-02 Soil Vapor 09/17/2020 09/17/2020

SV-0320I0814-03 Soil Vapor 09/17/2020 09/17/2020

SV-0520I0814-05 Soil Vapor 09/17/2020 09/17/2020

SV-0620I0814-06 Soil Vapor 09/17/2020 09/17/2020






22 IBM Road, Suite 101

Gallagher Bassett - Poughkeepsie, NY

Purpose and Results

This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory on

September 17, 2020 and listed below. The project was identified as your project: 20-0683.

The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data summary

tables.

All samples were received in proper condition meeting the customary acceptance requirements for environmental samples except

those indicated under the Sample and Analysis Qualifiers section of this report.

All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags, the

meaning of which are explained in the Sample and Data Qualifiers Relating to This Work Order section of this report and case

narrative if applicable.

The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the following

pages.

Please contact Client Services at 203.325.1371 with any questions regarding this report.

[TOC_1] Introduction and Sample Cross Reference [

Page 2 of 31

General Notes for York Project (SDG) No.: 20I0814

1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to

the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest

standard utilized for the calibration where applicable.

2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.

3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .

4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.

5. All analyses conducted met method or Laboratory SOP requirements. See the Sample and Data Qualifiers Section for further

information.

6. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.

7. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.

8. Analyses conducted at York Analytical Laboratories, Inc. Stratford, CT are indicated by NY Cert. No. 10854; those conducted at York

Analytical Laboratories, Inc., Richmond Hill, NY are indicated by NY Cert. No. 12058.

Approved By:

Laboratory Director

Date: 09/24/2020

Benjamin Gulizia

OC_2]General Notes Relating to this Report[TOC]

Page 3 of 31

SV-01


20I0814

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:


September 17, 2020 12:36 pmSoil Vapor20-0683

[TOC_2]SV-01[TOC]

09/17/2020

20I0814-01

[TOC_3]Volatile Organic Compounds in Air by GC/MS[TOC]

Sample Prepared by Method: EPA TO15 PREP



LOQ

Reported to

Volatile Organics, EPA TO15 Full List

ND ug/m³ 1.752630-20-6 LLJ09/17/2020 14:00 09/18/2020 20:201.2 EPA TO-15* 1,1,1,2-TetrachloroethaneCertifications:

ND ug/m³ 1.75271-55-6 LLJ09/17/2020 14:00 09/18/2020 20:200.96 EPA TO-151,1,1-TrichloroethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75279-34-5 LLJ09/17/2020 14:00 09/18/2020 20:201.2 EPA TO-151,1,2,2-TetrachloroethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75276-13-1 LLJ09/17/2020 14:00 09/18/2020 20:201.3 EPA TO-151,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: NELAC-NY12058,NJDEP-Queens


ND ug/m³ 1.75275-34-3 LLJ09/17/2020 14:00 09/18/2020 20:200.71 EPA TO-151,1-DichloroethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75275-35-4 LLJ09/17/2020 14:00 09/18/2020 20:200.69 EPA TO-151,1-DichloroethyleneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.752120-82-1 LLJ09/17/2020 14:00 09/18/2020 20:201.3 EPA TO-151,2,4-TrichlorobenzeneCertifications: NELAC-NY12058,NJDEP-Queens

42 ug/m³ 1.75295-63-6 LLJ09/17/2020 14:00 09/18/2020 20:200.86 EPA TO-151,2,4-Trimethylbenzene

Certifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.752106-93-4 LLJ09/17/2020 14:00 09/18/2020 20:201.3 EPA TO-151,2-DibromoethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75295-50-1 LLJ09/17/2020 14:00 09/18/2020 20:201.1 EPA TO-151,2-DichlorobenzeneCertifications: NELAC-NY12058,NJDEP-Queens


ND ug/m³ 1.75278-87-5 LLJ09/17/2020 14:00 09/18/2020 20:200.81 EPA TO-151,2-DichloropropaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75276-14-2 LLJ09/17/2020 14:00 09/18/2020 20:201.2 EPA TO-151,2-DichlorotetrafluoroethaneCertifications: NELAC-NY12058,NJDEP-Queens



ND ug/m³ 1.752106-99-0 LLJ09/17/2020 14:00 09/18/2020 20:201.2 EPA TO-151,3-ButadieneCertifications: NELAC-NY12058,NJDEP-Queens


ND ug/m³ 1.752142-28-9 LLJ09/17/2020 14:00 09/18/2020 20:200.81 EPA TO-15* 1,3-DichloropropaneCertifications:


ND ug/m³ 1.752123-91-1 LLJ09/17/2020 14:00 09/18/2020 20:201.3 EPA TO-151,4-DioxaneCertifications: NELAC-NY12058,NJDEP-Queens

1.3 ug/m³ 1.75278-93-3 LLJ09/17/2020 14:00 09/18/2020 20:200.52 EPA TO-152-Butanone


ND ug/m³ 1.752591-78-6 LLJ09/17/2020 14:00 09/18/2020 20:201.4 EPA TO-15* 2-HexanoneCertifications:

[TOC_1]Sample Results[TOC]

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20I0814

York Sample ID:

Sample Information

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Client Sample ID:


September 17, 2020 12:36 pmSoil Vapor20-0683 09/17/2020

20I0814-01




LOQ

Reported to


ND ug/m³ 1.752107-05-1 LLJ09/17/2020 14:00 09/18/2020 20:202.7 EPA TO-153-ChloropropeneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.752108-10-1 LLJ09/17/2020 14:00 09/18/2020 20:200.72 EPA TO-154-Methyl-2-pentanoneCertifications: NELAC-NY12058,NJDEP-Queens

22 ug/m³ 1.75267-64-1 LLJ09/17/2020 14:00 09/18/2020 20:200.83 EPA TO-15Acetone


ND ug/m³ 1.752107-13-1 LLJ09/17/2020 14:00 09/18/2020 20:200.38 EPA TO-15AcrylonitrileCertifications: NELAC-NY12058,NJDEP-Queens

0.67 ug/m³ 1.75271-43-2 LLJ09/17/2020 14:00 09/18/2020 20:200.56 EPA TO-15Benzene


ND ug/m³ 1.752100-44-7 LLJ09/17/2020 14:00 09/18/2020 20:200.91 EPA TO-15Benzyl chlorideCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75275-27-4 LLJ09/17/2020 14:00 09/18/2020 20:201.2 EPA TO-15BromodichloromethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75275-25-2 LLJ09/17/2020 14:00 09/18/2020 20:201.8 EPA TO-15BromoformCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75274-83-9 LLJ09/17/2020 14:00 09/18/2020 20:200.68 EPA TO-15BromomethaneCertifications: NELAC-NY12058,NJDEP-Queens

0.93 ug/m³ 1.75275-15-0 LLJ09/17/2020 14:00 09/18/2020 20:200.55 EPA TO-15Carbon disulfide


ND ug/m³ 1.75256-23-5 LLJ09/17/2020 14:00 09/18/2020 20:200.28 EPA TO-15Carbon tetrachlorideCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.752108-90-7 LLJ09/17/2020 14:00 09/18/2020 20:200.81 EPA TO-15ChlorobenzeneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75275-00-3 LLJ09/17/2020 14:00 09/18/2020 20:200.46 EPA TO-15ChloroethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75267-66-3 LLJ09/17/2020 14:00 09/18/2020 20:200.86 EPA TO-15ChloroformCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75274-87-3 LLJ09/17/2020 14:00 09/18/2020 20:200.36 EPA TO-15ChloromethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.752156-59-2 LLJ09/17/2020 14:00 09/18/2020 20:200.69 EPA TO-15cis-1,2-DichloroethyleneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75210061-01-5 LLJ09/17/2020 14:00 09/18/2020 20:200.80 EPA TO-15cis-1,3-DichloropropyleneCertifications: NELAC-NY12058,NJDEP-Queens

27 ug/m³ 1.752110-82-7 LLJ09/17/2020 14:00 09/18/2020 20:200.60 EPA TO-15Cyclohexane


ND ug/m³ 1.752124-48-1 LLJ09/17/2020 14:00 09/18/2020 20:201.5 EPA TO-15DibromochloromethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75275-71-8 LLJ09/17/2020 14:00 09/18/2020 20:200.87 EPA TO-15DichlorodifluoromethaneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.752141-78-6 LLJ09/17/2020 14:00 09/18/2020 20:201.3 EPA TO-15* Ethyl acetateCertifications:

11 ug/m³ 1.752100-41-4 LLJ09/17/2020 14:00 09/18/2020 20:200.76 EPA TO-15Ethyl Benzene


ND ug/m³ 1.75287-68-3 LLJ09/17/2020 14:00 09/18/2020 20:201.9 EPA TO-15HexachlorobutadieneCertifications: NELAC-NY12058,NJDEP-Queens

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SV-01


20I0814

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0814-01




LOQ

Reported to


18 ug/m³ 1.75267-63-0 LLJ09/17/2020 14:00 09/18/2020 20:200.86 EPA TO-15Isopropanol


0.79 ug/m³ 1.75280-62-6 LLJ09/17/2020 14:00 09/18/2020 20:200.72 EPA TO-15Methyl Methacrylate


ND ug/m³ 1.7521634-04-4 LLJ09/17/2020 14:00 09/18/2020 20:200.63 EPA TO-15Methyl tert-butyl ether (MTBE)Certifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75275-09-2 LLJ09/17/2020 14:00 09/18/2020 20:201.2 EPA TO-15Methylene chlorideCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75291-20-3 LLJ09/17/2020 14:00 09/18/2020 20:209.2 EPA TO-15* NaphthaleneCertifications: NJDEP-Queens

1.9 ug/m³ 1.752142-82-5 LLJ09/17/2020 14:00 09/18/2020 20:200.72 EPA TO-15n-Heptane


0.99 ug/m³ 1.752110-54-3 LLJ09/17/2020 14:00 09/18/2020 20:200.62 EPA TO-15n-Hexane


14 ug/m³ 1.75295-47-6 LLJ09/17/2020 14:00 09/18/2020 20:200.76 EPA TO-15o-Xylene


31 ug/m³ 1.752179601-23-1 LLJ09/17/2020 14:00 09/18/2020 20:201.5 EPA TO-15p- & m- Xylenes


35 ug/m³ 1.752622-96-8 LLJ09/17/2020 14:00 09/18/2020 20:200.86 EPA TO-15* p-Ethyltoluene

Certifications:

ND ug/m³ 1.752115-07-1 LLJ09/17/2020 14:00 09/18/2020 20:200.30 EPA TO-15* PropyleneCertifications:

ND ug/m³ 1.752100-42-5 LLJ09/17/2020 14:00 09/18/2020 20:200.75 EPA TO-15StyreneCertifications: NELAC-NY12058,NJDEP-Queens

7.1 ug/m³ 1.752127-18-4 LLJ09/17/2020 14:00 09/18/2020 20:200.30 EPA TO-15Tetrachloroethylene


ND ug/m³ 1.752109-99-9 LLJ09/17/2020 14:00 09/18/2020 20:201.0 EPA TO-15* TetrahydrofuranCertifications:

12 ug/m³ 1.752108-88-3 LLJ09/17/2020 14:00 09/18/2020 20:200.66 EPA TO-15Toluene


ND ug/m³ 1.752156-60-5 LLJ09/17/2020 14:00 09/18/2020 20:200.69 EPA TO-15trans-1,2-DichloroethyleneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75210061-02-6 LLJ09/17/2020 14:00 09/18/2020 20:200.80 EPA TO-15trans-1,3-DichloropropyleneCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75279-01-6 LLJ09/17/2020 14:00 09/18/2020 20:200.24 EPA TO-15TrichloroethyleneCertifications: NELAC-NY12058,NJDEP-Queens

1.6 ug/m³ 1.75275-69-4 LLJ09/17/2020 14:00 09/18/2020 20:200.98 EPA TO-15Trichlorofluoromethane (Freon 11)


ND ug/m³ 1.752108-05-4 LLJ09/17/2020 14:00 09/18/2020 20:200.62 EPA TO-15Vinyl acetateCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.752593-60-2 LLJ09/17/2020 14:00 09/18/2020 20:200.77 EPA TO-15Vinyl bromideCertifications: NELAC-NY12058,NJDEP-Queens

ND ug/m³ 1.75275-01-4 LLJ09/17/2020 14:00 09/18/2020 20:200.45 EPA TO-15Vinyl ChlorideCertifications: NELAC-NY12058,NJDEP-Queens


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20I0814

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0814-01




LOQ

Reported to




460-00-4

SV-02


20I0814

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]SV-02[TOC]

09/17/2020

20I0814-02




LOQ

Reported to


















8.8 ug/m³ 1.88108-67-8 LLJ09/17/2020 14:00 09/18/2020 21:150.92 EPA TO-151,3,5-Trimethylbenzene


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SV-02


20I0814

York Sample ID:

Sample Information

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20I0814-02




LOQ

Reported to











ND ug/m³ 1.88108-10-1 LLJ09/17/2020 14:00 09/18/2020 21:150.77 EPA TO-154-Methyl-2-pentanoneCertifications: NELAC-NY12058,NJDEP-Queens















1.1 ug/m³ 1.8867-66-3 LLJ09/17/2020 14:00 09/18/2020 21:150.92 EPA TO-15Chloroform


0.39 ug/m³ 1.8874-87-3 LLJ09/17/2020 14:00 09/18/2020 21:150.39 EPA TO-15Chloromethane



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SV-02


20I0814

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



20I0814-02




LOQ

Reported to











9.8 ug/m³ 1.8867-63-0 LLJ09/17/2020 14:00 09/18/2020 21:150.92 EPA TO-15Isopropanol
















Certifications:

ND ug/m³ 1.88115-07-1 LLJ09/17/2020 14:00 09/18/2020 21:150.32 EPA TO-15* PropyleneCertifications:


4.7 ug/m³ 1.88127-18-4 LLJ09/17/2020 14:00 09/18/2020 21:150.32 EPA TO-15Tetrachloroethylene






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SV-02


20I0814

York Sample ID:

Sample Information

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20I0814-02




LOQ

Reported to



ND ug/m³ 1.8879-01-6 LLJ09/17/2020 14:00 09/18/2020 21:150.25 EPA TO-15TrichloroethyleneCertifications: NELAC-NY12058,NJDEP-Queens









460-00-4

SV-03


20I0814

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:



[TOC_2]SV-03[TOC]

09/17/2020

20I0814-03




LOQ

Reported to













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SV-03


20I0814

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20I0814-03




LOQ

Reported to




1.2 ug/m³ 1.807107-06-2 LLJ09/17/2020 14:00 09/18/2020 22:100.73 EPA TO-151,2-Dichloroethane













3.1 ug/m³ 1.807591-78-6 LLJ09/17/2020 14:00 09/18/2020 22:101.5 EPA TO-15* 2-Hexanone

Certifications:


0.89 ug/m³ 1.807108-10-1 LLJ09/17/2020 14:00 09/18/2020 22:100.74 EPA TO-154-Methyl-2-pentanone













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LOQ

Reported to





ND ug/m³ 1.80767-66-3 LLJ09/17/2020 14:00 09/18/2020 22:100.88 EPA TO-15ChloroformCertifications: NELAC-NY12058,NJDEP-Queens

0.49 ug/m³ 1.80774-87-3 LLJ09/17/2020 14:00 09/18/2020 22:100.37 EPA TO-15Chloromethane TO-LCS

-H Certifications: NELAC-NY12058,NJDEP-Queens



























Certifications:

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LOQ

Reported to


3.3 ug/m³ 1.807115-07-1 LLJ09/17/2020 14:00 09/18/2020 22:100.31 EPA TO-15* Propylene

Certifications:


160 ug/m³ 1.807127-18-4 LLJ09/17/2020 14:00 09/18/2020 22:100.31 EPA TO-15Tetrachloroethylene







0.39 ug/m³ 1.80779-01-6 LLJ09/17/2020 14:00 09/18/2020 22:100.24 EPA TO-15Trichloroethylene










460-00-4

SV-05


20I0814

York Sample ID:

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[TOC_2]SV-05[TOC]

09/17/2020

20I0814-05




LOQ

Reported to




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SV-05


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20I0814-05




LOQ

Reported to
















8.5 ug/m³ 1.784108-67-8 LLJ09/20/2020 03:00 09/20/2020 08:350.88 EPA TO-151,3,5-Trimethylbenzene













9.8 ug/m³ 1.78467-64-1 LLJ09/20/2020 03:00 09/20/2020 08:350.85 EPA TO-15Acetone


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LOQ

Reported to









ND ug/m³ 1.78475-15-0 LLJ09/20/2020 03:00 09/20/2020 08:350.56 EPA TO-15Carbon disulfideCertifications: NELAC-NY12058,NJDEP-Queens




















ND ug/m³ 1.78480-62-6 LLJ09/20/2020 03:00 09/20/2020 08:350.73 EPA TO-15Methyl MethacrylateCertifications: NELAC-NY12058,NJDEP-Queens


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LOQ

Reported to













Certifications:


Certifications:

1.8 ug/m³ 1.784100-42-5 LLJ09/20/2020 03:00 09/20/2020 08:350.76 EPA TO-15Styrene



















460-00-4

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SV-06


20I0814

York Sample ID:

Sample Information

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[TOC_2]SV-06[TOC]

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20I0814-06




LOQ

Reported to

























14 ug/m³ 1.59978-93-3 LLJ09/20/2020 03:00 09/20/2020 09:300.47 EPA TO-152-Butanone


2.8 ug/m³ 1.599591-78-6 LLJ09/20/2020 03:00 09/20/2020 09:301.3 EPA TO-15* 2-Hexanone

Certifications:


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LOQ

Reported to













ND ug/m³ 1.59975-15-0 LLJ09/20/2020 03:00 09/20/2020 09:300.50 EPA TO-15Carbon disulfideCertifications: NELAC-NY12058,NJDEP-Queens




















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20I0814-06




LOQ

Reported to






10 ug/m³ 1.59991-20-3 LLJ09/20/2020 03:00 09/20/2020 09:308.4 EPA TO-15* Naphthalene

Certifications: NJDEP-Queens










Certifications:


Certifications:



















460-00-4

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Analytical Batch Summary

[TOC_1]Quality Batch Summary[TOC]

Batch ID: Preparation Method: Prepared By:BI00940 EPA TO15 PREP AS


20I0814-01 SV-01 09/17/20

20I0814-02 SV-02 09/17/20

20I0814-03 SV-03 09/17/20

BI00940-BLK1 Blank 09/17/20

BI00940-BS1 LCS 09/17/20

Batch ID: Preparation Method: Prepared By:BI01130 EPA TO15 PREP AS


20I0814-05 SV-05 09/20/20

20I0814-06 SV-06 09/20/20

BI01130-BLK1 Blank 09/20/20

BI01130-BS1 LCS 09/20/20

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[TOC_1]QA/QC Summary Data[TOC]

Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Volatile Organic Compounds in Air by GC/MS - Quality Control Data


Flag

olatile Organic Compounds in Air by GC/MS EPA TO-15[TOC]

Batch BI00940 - EPA TO15 PREP


ug/m³ND 0.691,1,1,2-Tetrachloroethane




113)




"0.74 0.741,2,4-Trichlorobenzene






"ND 0.701,2-Dichlorotetrafluoroethane


"ND 0.661,3-Butadiene




"ND 0.721,4-Dioxane

"ND 0.292-Butanone

"ND 0.822-Hexanone

"ND 1.63-Chloropropene


"ND 0.48Acetone


"ND 0.32Benzene

"ND 0.52Benzyl chloride


"ND 1.0Bromoform






"ND 0.49Chloroform




"ND 0.34Cyclohexane



"ND 0.72Ethyl acetate



"ND 0.49Isopropanol

"ND 0.41Methyl Methacrylate


"ND 0.69Methylene chloride

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



ug/m³ND 5.2Naphthalene

"ND 0.41n-Heptane

"ND 0.35n-Hexane

"ND 0.43o-Xylene


"ND 0.49p-Ethyltoluene

"ND 0.17Propylene

"ND 0.43Styrene


"ND 0.59Tetrahydrofuran

"ND 0.38Toluene




"ND 0.56Trichlorofluoromethane (Freon 11)

"ND 0.35Vinyl acetate

"ND 0.44Vinyl bromide


ppbv 10.0 70-130Surrogate: SURR: p-Bromofluorobenzene 78.07.80


ppbv10.0 10.0 70-1301001,1,1,2-Tetrachloroethane

"11.0 10.0 70-1301101,1,1-Trichloroethane

"9.87 10.0 70-13098.71,1,2,2-Tetrachloroethane

"9.99 10.0 70-13099.91,1,2-Trichloro-1,2,2-trifluoroethane (Freon

113)

"9.46 10.0 70-13094.61,1,2-Trichloroethane

"10.1 10.0 70-1301011,1-Dichloroethane

"9.58 10.0 70-13095.81,1-Dichloroethylene

"9.62 10.0 70-13096.21,2,4-Trichlorobenzene

"10.3 10.0 70-1301031,2,4-Trimethylbenzene

"10.5 10.0 70-1301051,2-Dibromoethane

"12.4 10.0 70-1301241,2-Dichlorobenzene

"9.94 10.0 70-13099.41,2-Dichloroethane

"9.30 10.0 70-13093.01,2-Dichloropropane

"12.7 10.0 70-1301271,2-Dichlorotetrafluoroethane

"9.80 10.0 70-13098.01,3,5-Trimethylbenzene

"13.0 10.0 70-1301301,3-Butadiene

"9.23 10.0 70-13092.31,3-Dichlorobenzene



"9.50 10.0 70-13095.01,4-Dioxane

"10.3 10.0 70-1301032-Butanone

"11.1 10.0 70-1301112-Hexanone

"10.5 10.0 70-1301053-Chloropropene

"9.65 10.0 70-13096.54-Methyl-2-pentanone

"11.1 10.0 70-130111Acetone

"9.93 10.0 70-13099.3Acrylonitrile

"10.0 10.0 70-130100Benzene

"8.66 10.0 70-13086.6Benzyl chloride

"9.77 10.0 70-13097.7Bromodichloromethane

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



ppbv12.0 10.0 70-130120Bromoform

"11.0 10.0 70-130110Bromomethane

"10.4 10.0 70-130104Carbon disulfide

"10.4 10.0 70-130104Carbon tetrachloride

"10.4 10.0 70-130104Chlorobenzene

"10.9 10.0 70-130109Chloroethane

"10.4 10.0 70-130104Chloroform

"13.1 10.0 70-130131 High BiasChloromethane

"9.78 10.0 70-13097.8cis-1,2-Dichloroethylene

"10.3 10.0 70-130103cis-1,3-Dichloropropylene

"10.4 10.0 70-130104Cyclohexane

"10.5 10.0 70-130105Dibromochloromethane

"12.7 10.0 70-130127Dichlorodifluoromethane

"10.3 10.0 70-130103Ethyl acetate

"9.98 10.0 70-13099.8Ethyl Benzene

"9.69 10.0 70-13096.9Hexachlorobutadiene

"10.8 10.0 70-130108Isopropanol

"9.95 10.0 70-13099.5Methyl Methacrylate

"10.6 10.0 70-130106Methyl tert-butyl ether (MTBE)

"11.0 10.0 70-130110Methylene chloride

"9.32 10.0 70-13093.2Naphthalene

"9.86 10.0 70-13098.6n-Heptane

"10.5 10.0 70-130105n-Hexane

"9.93 10.0 70-13099.3o-Xylene

"18.7 20.0 70-13093.7p- & m- Xylenes

"11.6 10.0 70-130116p-Ethyltoluene

"10.6 10.0 70-130106Propylene

"11.2 10.0 70-130112Styrene

"9.34 10.0 70-13093.4Tetrachloroethylene

"10.5 10.0 70-130105Tetrahydrofuran

"9.18 10.0 70-13091.8Toluene

"10.1 10.0 70-130101trans-1,2-Dichloroethylene

"10.4 10.0 70-130104trans-1,3-Dichloropropylene

"9.40 10.0 70-13094.0Trichloroethylene

"10.4 10.0 70-130104Trichlorofluoromethane (Freon 11)

"10.2 10.0 70-130102Vinyl acetate

"11.1 10.0 70-130111Vinyl bromide

"15.5 10.0 70-130155 High BiasVinyl Chloride


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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



ug/m³ND 0.691,1,1,2-Tetrachloroethane




113)










"ND 0.701,2-Dichlorotetrafluoroethane


"ND 0.661,3-Butadiene




"ND 0.721,4-Dioxane

"ND 0.292-Butanone

"ND 0.822-Hexanone

"ND 1.63-Chloropropene


"ND 0.48Acetone


"ND 0.32Benzene

"ND 0.52Benzyl chloride


"ND 1.0Bromoform






"ND 0.49Chloroform




"ND 0.34Cyclohexane



"ND 0.72Ethyl acetate



"ND 0.49Isopropanol

"ND 0.41Methyl Methacrylate


"ND 0.69Methylene chloride

"ND 5.2Naphthalene

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



ug/m³ND 0.41n-Heptane

"ND 0.35n-Hexane

"ND 0.43o-Xylene


"ND 0.49p-Ethyltoluene

"ND 0.17Propylene

"ND 0.43Styrene


"ND 0.59Tetrahydrofuran

"ND 0.38Toluene




"ND 0.56Trichlorofluoromethane (Freon 11)

"ND 0.35Vinyl acetate

"ND 0.44Vinyl bromide


ppbv 10.0 70-130Surrogate: SURR: p-Bromofluorobenzene 74.67.46


ppbv9.80 10.0 70-13098.01,1,1,2-Tetrachloroethane

"10.9 10.0 70-1301091,1,1-Trichloroethane

"9.64 10.0 70-13096.41,1,2,2-Tetrachloroethane

"9.78 10.0 70-13097.81,1,2-Trichloro-1,2,2-trifluoroethane (Freon

113)

"9.26 10.0 70-13092.61,1,2-Trichloroethane

"10.0 10.0 70-1301001,1-Dichloroethane

"9.43 10.0 70-13094.31,1-Dichloroethylene

"9.02 10.0 70-13090.21,2,4-Trichlorobenzene

"10.1 10.0 70-1301011,2,4-Trimethylbenzene

"10.2 10.0 70-1301021,2-Dibromoethane

"12.2 10.0 70-1301221,2-Dichlorobenzene

"9.66 10.0 70-13096.61,2-Dichloroethane


"12.4 10.0 70-1301241,2-Dichlorotetrafluoroethane

"9.84 10.0 70-13098.41,3,5-Trimethylbenzene

"12.5 10.0 70-1301251,3-Butadiene




"9.25 10.0 70-13092.51,4-Dioxane

"10.2 10.0 70-1301022-Butanone

"10.8 10.0 70-1301082-Hexanone

"10.2 10.0 70-1301023-Chloropropene

"9.42 10.0 70-13094.24-Methyl-2-pentanone

"10.8 10.0 70-130108Acetone

"9.90 10.0 70-13099.0Acrylonitrile

"9.83 10.0 70-13098.3Benzene

"8.58 10.0 70-13085.8Benzyl chloride

"9.50 10.0 70-13095.0Bromodichloromethane

"11.7 10.0 70-130117Bromoform

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte



Flag



ppbv10.9 10.0 70-130109Bromomethane

"10.2 10.0 70-130102Carbon disulfide

"10.1 10.0 70-130101Carbon tetrachloride

"10.2 10.0 70-130102Chlorobenzene

"10.8 10.0 70-130108Chloroethane

"10.1 10.0 70-130101Chloroform

"12.7 10.0 70-130127Chloromethane

"9.56 10.0 70-13095.6cis-1,2-Dichloroethylene

"10.2 10.0 70-130102cis-1,3-Dichloropropylene

"10.2 10.0 70-130102Cyclohexane

"10.3 10.0 70-130103Dibromochloromethane

"12.5 10.0 70-130125Dichlorodifluoromethane

"10.1 10.0 70-130101Ethyl acetate

"9.83 10.0 70-13098.3Ethyl Benzene

"9.37 10.0 70-13093.7Hexachlorobutadiene

"10.7 10.0 70-130107Isopropanol

"9.69 10.0 70-13096.9Methyl Methacrylate

"10.4 10.0 70-130104Methyl tert-butyl ether (MTBE)

"10.8 10.0 70-130108Methylene chloride

"8.86 10.0 70-13088.6Naphthalene

"9.71 10.0 70-13097.1n-Heptane

"10.4 10.0 70-130104n-Hexane

"9.79 10.0 70-13097.9o-Xylene

"18.5 20.0 70-13092.4p- & m- Xylenes

"11.2 10.0 70-130112p-Ethyltoluene

"10.7 10.0 70-130107Propylene

"11.1 10.0 70-130111Styrene

"9.23 10.0 70-13092.3Tetrachloroethylene

"10.5 10.0 70-130105Tetrahydrofuran

"9.04 10.0 70-13090.4Toluene

"9.96 10.0 70-13099.6trans-1,2-Dichloroethylene

"10.2 10.0 70-130102trans-1,3-Dichloropropylene

"9.15 10.0 70-13091.5Trichloroethylene

"10.2 10.0 70-130102Trichlorofluoromethane (Freon 11)

"9.89 10.0 70-13098.9Vinyl acetate

"10.9 10.0 70-130109Vinyl bromide

"15.0 10.0 70-130150 High BiasVinyl Chloride


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[TOC_1]Notes and Specific Data Flags[Sample and Data Qualifiers Relating to This Work Order

TO-LCS-H The result reported for this compound may be biased high due to its behavior in the analysis batch LCS where it recovered greater

than 130% of the expected value.

TO-CCV The value reported is ESTIMATED for this compound due to its behavior during continuing calibration verification (>30%

Difference from initial calibration).

B Analyte is found in the associated analysis batch blank. For volatiles, methylene chloride and acetone are common lab

contaminants.

Relative Percent DifferenceRPD

Not reportedNR

NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND

Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note

that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias


Low Bias

High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take

note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias


High Bias

Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is

outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high due to

either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.

Wet The data has been reported on an as-received (wet weight) basis

REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.

METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a 99%

confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA 600 and 200

series methods.

RL

MDL

If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet and

cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two. For this reason, York

reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as Diphenylamine.

If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and 1268

which are non-target aroclors for some regulatory lists.

2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user should

take note.

Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.

Certification for pH is no longer offered by NYDOH ELAP.

*

LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the lowest

point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is based upon

NELAC 2009 Standards and applies to all analyses.

LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably detect.

This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.

Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located above the

LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and semi-volatile

target compounds only.

Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .

Definitions and Other Explanations

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For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a verified

LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.

Corrective Action: SV-04 sample received with valve upon receipt at air lab.

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PHASE II ENVIRONMENTAL SITE ASSESSMENT

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Transcript of PHASE II ENVIRONMENTAL SITE ASSESSMENT