PGE Topock - RFI/RI v1: Apndx C Lab Data 1992 Pt. 6...L90256026 MOLYBDEIWM (EPA 6010) 1.0 eng/kg 89....

... -

Page 304 of 442

---------------,-----------------a;:"I:'----~'=,U I::It.'UJ

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DHS certificate 1157

Matrix Spike/Hat~ix spike Duplicate Repoit·Cross-Reference

QC Batch Date .Ptt&neter (Method) Sample Noa.------------- ----------- ---------------------------------------- -------------

MOLYBDENUM (BPA 6010)

_.~

Reviewed

NICKEL (EPA 6010)

SILVER (EPA 6010)

"l'HALLIUH (EPA 6010)

G-9024220-00l1C-9024220-022G-902422OP-0230-9024220-024G-9024220-025G-9024220-0260-9024220-027G-9024220-0260-9024220-0290-9024220-030G-9024220-0320-9024220-0340-9024220-036G-9024220-036G-9024220-0406-9024220-021G-9024220-022G-9024220-o23G-9024220-0240-9024220-0250-9024220-026G-9024220-0270-9024220-0280-9024220-029G-9024220-0300-9024220-0320-9024220-0340-9024220-0360-9024220-038G-9024220-0400-9024220-0210-9024220-022G-9024220-0230":9024220-024G-9024220-02SG-9024220-026G-9024220-027G-9024220~028

G-9024220-029G-9024220-030G-9024220-032G-9024220-034G-9024220-036G-9024220-038G-9024220-04DG-9024220-0210-9024220-022G-9024220-023G-90;Z4220-024G:-9024220-o2S

p~COBlJSOI06127

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DHS certificate #157

..__~__--~~a_t-r-i-x-spike/HatrixSpike Duplicate Report Cross-ReferenceQC Batch Date Parameter (Method) Sample No••

------------- ----------- ---------------------------------------- -------------

RevIeWed

VANAD!UM (EPA 6010)

ZINC (EPA 6010)

ARSENIC (EPA 7061)

G-9024220-026C-9024220-027G-9024220-028G-9024220-029G-9024220-030G-9024220-032G-9024220-o340-9024220-0360-9024220-038G-90242:20-040G-90:24220-021G-9024220-022G-9024220-023G-9024220-024G-9024220-025G-9024220-02.6G-9024220-027C-9024220-028G-90242~0-029

G-9024220-o30G-9024220-032G-9024220-0340'-9024220-036C-9024220-038C-90242:20-040G-9024220-021C-9024220-022G-9024220-023C-9024220-024G-9024220-0250-9024220-026C-9024220-027C-9024220-028C-9024220-029G-9024220-030G-9024220-032C-9024220-034G-9024220-0360-9024220-038G-9024220-040G-9024220-0210-9024220-022G-9024220-023C-9024220-024G-9024220-0250-9024220-026C-9024220-027G-9024220-028C-9024220-029G-9024220-030G-9024220-032G-9024220-034

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CHS certificate #157

Matrix Spike/Matrix Spike Dup~icat8 Report cross-Referen=-

C-9024220-021G-9024220-022c-902422o-0230-9024220-024G-9024220-025G-9024220-026G-9024220-021

of 442•• ~ _. __ _ •• ~ •••••• •••• __ • - _ •••_ _ 0 •••••_ 0 ••

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DHS Cort1f1cate #157

Matrix SpikejMatrLx Spike Duplicate Report cr~••-Refer.nce

QC Batch Date Sample 110••-----~------- ----------- ----------~----------------------------

G-9024220-o180-9024220-019G-9024220-0200-9024220-017G-9024220-0180-9024220-0190-9024220-0200-9024220-0170-9024220-0180-9024220-019G-90:24220-0200-51024220-017G-9024220-0180-9024220-0190-51024220-0200-9024220-017G-9024220-o18G-9024220-o19G-9024220-020C-9024220-017G-9024220-o180-9024220-0190-9024220-020G-9024220-0170-9024220-0180-9024220-0190-9024220-020G-9024220-0170-9024220-018G-9024220-0190-9024220-0200-9024220-0170-9024220-019G-9024220-0190-9024220-020G-9024220-o17G-9024220-01BG-9024220-o19G-9024220-0200-9024220-017G-9024220-o18C-9024220-019G-9024220-o200-9024220-017C-9024220-0180-9024220-019C-9024220-020

."

CADMIUM (EPA 6010)

BERYLLIUM (EPA 6010)

COPPER (EPA 6010)

" . ~LEAD (BPA 6010) fl\'?

MOLYBDENUM (EPA 6010)

NICKEL (EPA 6010)

SILVER (EPA 6010)

Reviewed

PMCOBUSOI06131

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DHS Certificate #151

. Matrix Spike/Matrix Spike Duplicate Report Croas-Reference

2C Batch Date

9025027-004 18-SEP-1990

:.r • ....;.;. i H. 4',.2 Pl¥ li} .....il0fiir...... :ccv4J!,.

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-----------------"'=---------------~lEnseco0;;::'

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Laboratory Report~-------------------------------'e== e?-------------------------------------------

MITTELHAUSER"CORP An~lysia NO.2 0-9024220-001/031/;23272 MILL CREEK JU) .. STE 300 Data sampled: 2S-AUG-1990

LAGUNA HILLS, CA 92653 29-AUC-1990. ATTN: MR. DAVE DORN D~tD Sample Rec'd: 30-AUC-1990

~. sample Type: SOLIDPro~ect: (1352) PG ~ E - TOPOCK

-----------------------------------------~--------------------------------------------Laboratery COntrol SAmple Report:

Avg. Rel.QC Amt:. Spike Acceptable Pet. AcceptableBatch Parameter (Method} Spik~HJ UnitB Recev. Range Diff. .Range

----------- ------------------------- ------ ---------- ------ ---------- ----- ----------L90254002 TDS/STLC-DI (EPA 160.1) 270.9 mg/L 115. 70-120 2. 30L90254003 TDS/STLC-DI (EPA 160.1) 270.9 mg/L 115. 70-120 8. 30L90254004 TDS!STLC-DI (EPA 160.1) 270.9 mglL 120. 70-120 9. 30L90250034 FLUORIDE, STLC (EPA 2.00 mg/L 96. 69-125 6. 17

340.2)mg/LL90250033 FLUORIDE, STLC (EPA 2.00 96. 69-125 2. 17

340.2)L90250035 FLUORIDE, STLC (EPA 2.00 mgjL 94. 69-125 3. 17

340.2)L90.257024 AllTIMONY (EPA 5010) 1.0 mglxg 98. 60-125 2. 25L90256026 ANTIMONY (EPA 6010) 1.0 mqJkg 91. 60-125 3. 25L90256020 ANTIMONY (EPA 6010) 1.0 m

of 442

---------------------------~';Enseco-- .~e.--r..


Laboratory Report

---------------------------------------------------------------------------------------MITTELHAUSER CORP Analysis No.: G-9024220-001/03723272 HILL CREEK RD, STE 300 pate sampled: 28-AUG-1990LAGUNA HILLS, CA 92653 29-AUG-1990ATTN: HR. DAVE CORN Date sample Rec'd: 30-AUG-1990

proje~t:sample Type: SOLID

(1352) PG « E - TOPOCK-------------------------------------------------------------------------

Laboratory Control sample Report

Avg. ReI.QC Amt. Spike Acceptable Pet. AcceptableBatch Para.'Ileter (Method) Spiked Units Reeov. Range Oiff. Range.----------- ------------------------- ------ ---------- ------ ---------- ----- ----------

L9025S012 LEAD (EPA 6010) 1.0 mg/kg 9~ 61-126 2_ 30L90256020 MOLYBDENUM (EPA 6010) 1.0 mg/kg 102. 61-126 2. 32L90257024 MOL¥BOEUUM (EPA 6010) 1.0 mg/kg 94. 61-126 3_ 32L90256026 MOLYBDEIWM (EPA 6010) 1.0 eng/kg 89. 61-126 2. 32 'L9025S012 MOLYBDErWM (EPA 6010) 1.0 mg/kg 92. 61-126 1. 32L90257024 NICKEL (EPA 6010) 1.0 mg/kg 95. 61-126 3. 25L90256020 NICKEL (EPA 6010) 1.0 mg/kg 107. 61-126 1. 25L90256026 NICKEL (EPA 6010) 1.0 lng/kg 92. 61-126 2. 25L90255012 NICKEL (EPA 6010) 1.0 mg/kg 96. 61-126 O. 25L90256026 SILVER (EPA 6010) 1.0 mg/kg 81- 60-126 2. 30L90256020 SILVER (EPA 6010) 1.0 mg/kg 92_ 60-ns L 30L90257024 SILVER (EPA 6010) 1.0 trig/kg 94. 60-126 O. 30L90255012 SILVER (EPA 6010) 1.0 mg/kg 8B. 60-125 o. 30L90256026 THALLIUM (EPA 6010) 1,0 mg/kg 91. 60-126 2. 30L90257024 THALLIUM (EPA 6010) 1.0 mg/kg 90. 60-126 2. 30L90256020 THALLIUM (BPA 6010) 1.0 mg/kg 103. 60-126 2. 30L9025S012 THALLIUM (EPA 6010) 1.0 rng/kg 92. 60-126 1. 30L90257024 VANADIUM (EPA 6010) 1.0 mg/kg 91. 60-126 1. 25L90256026 VAliADIUH (EPA 6010) 1.0 mg/kg 87. 60-126 2. 25L90256020 VANADIUM (EPA 6010) 1.0 mg/kg 97. 60-126 2. 25L90255012 VANADIUM (EPA ,6010) 1.0 rng/kg a9. 60-126 o. 25L90256020 ZINC (EPA 6010) 1.0 mg/kg 102. 60-.126 o. 30L90256026 ZINC (EPA 6010) 1.0 mg/kg 87. 60-126 3_ 30L90257024 ZINC (EPA 6010) 1.0 mg/kg 92. 60-126 4. 30L90255012 ZINC (EPA 6010) 1.0 mg/kg 91. 60-126 1. 30L90257019 ANTIMorrr (EPA 6010-L) 2.0 mg/L 88. 70-130 8_ 30L90257023 ANTIMOnY' (EPA 6010-L) 2.0 mg/I. 94_ 70-130 9. 30L90257022 ANTIMOliY (EPA 6010-I.) 2.0 mg/L 96. 70-130 3. 30L90257023 CHROMIUM (EPA 6010-L) 2.0 mq/L 94. 71-123 8. 20L90257019 CHROMIUM (EPA 6010-L) 2.0 mg/L 89. 71.-123 5. 20L90257022 CHROMIUM (EPA 6010-L) 2.0 mg/L 96. 71-123 2. 20L90257019 COPPER (EPA 6010-I.) 2.0 mgjL 96. 62-126 5. 30L90257023 COPPER (EPA 6010-L) 2.0 mg/L 96. 6:2-126 5. 30L90257022 COPPER (EPA 6010-L) 2.0 mg/L 90. 62-126 6. 30L90257023 MOLYBDENUM (EPA 6010-L) 2.0 mgJL 94. 69-124 8. 20L90257019 MO~YBDE~UM (EPA 6010-L) 2.0 mg/L 88. 69-124 4. 20L902S70:22 MOLYBDENUM (EPA GOlD-I.) 2.0 mg/L 95. 69-124 1_ 20L90257019 ZINC (EPA 6010-L) 2_0 mg/L 80_ 10-128 7. 20L90257023 ZINC (EPA 6010-L) 2.0 mgjL as. 70-128 10. 20L90257022 ZINC (EPA 6010-L) 2.0 mg/L 83_! 70-128 3. 20

.« -d$fL~Reviewed

PMCOBUSOlO6134....4. i. r : ;A5_:4WS'iM IUik91Jf::pctXQitlftLi....."..:;; ,,\,.i .•";::"4G:,.•,,,1f'CI

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- "- """' -- ------------------------~Enseco....,.....,.-.

DBS Certificate #157

Laboratory COntrol Sample Report erc••-Rafetene.

QC Batch DAt. 'Parameter (Method)------------------------- -------C-9024220-012c-9024220-014G-9024220-015G-9024220-016

L90250009

L90250010

L90250011

J:,9025001Z

..... , :: ..... J3\( 1';" $id A II

6-SEP-1990 PH (BPA 9045)

6-SEP-1990 PH (EPA 9045)

6-SEP-1990 P.B (EPA 90(5)

6-SEP-1990 PB/S~-DX (EPA 9045)

-.

""" ••,.".,. ,>OF '. , ."

0-9024220-001G-9024220-oo20-9024220-003G-9024220-0040-9024220-005c-9024220-0060-9024220-0070-9024220-008C-9024220-009.G-9024220-010a-9024220-011C-9024220-0120-9024220-013G-9024220-014G-90.24.220-0~S

C-9024220-016C-9024220-0170-9024220-018G-9024220-o1.9G-9024220-020

G-9024220-021G-9024220-022G-9024220-023G-9024220-024G-9024220-02SG-9024220-026C-9024220-027G-9024220-028G-9Q24220-029C-9024220-030

G-9024220-032G-9024220-034G-9024220-036G-9024220-040G-9024220-042G-9024220-045

C-9024220-oo1C-9024220-Q02G-9024220-003c-9024220-Q04C-9024220-00SG-902422o-D06

. ,G-9024220-007

P~C()BlJSOI06136

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Page 314 of 442••••• n.". _ •••••••• _ •. n. _. .. • .. •• 0 on. _... ..,

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DRS certificate #157

Laborat~COntrolSample Report CroBs-BHfermnC.'

QC Batch Date .Parl!Jlletcrr (Method) Sample NOli.

L902500l3

•

6-SEP-1990 PHjSTLC-DI (EPA 9045)

G-90242:20-0080-9024220-0090-9024220-0100-9024220-011G-9024220-012G-9024220-013C-9024220-0140-9024220-015G-9024220-0160-9024220-0170-9024220-0180-9024220-0190-9024220-020

0-9024220-0210-9024220-0220-9024220-0230-9024220-0240-9024220-0250-9024220-0260-9024220-0270-9024220-0280-9024220-0290-9024220-030

L90250014 6-SEP-1990 PHjSTLc-DI (EPA 9045)

:~

--L90250P33 7-SEP-1990 FLUORIDE, Sn.c (EPA 340.2)

G-9024220-0320-9024220-0340-9024220-036G-9024220~038

C-9024220-040G-9024220-0420-9024,220-045

0-9024220-0010-9024220-0020-9024220-003G-9024220-004G-9024220-005G-9024220-006G-9024220-007G-9024220-00a0-9024220-009G-9024220-010G-9024220-011C;-9024220-012G-9024220-0n0-9024220-014G-9024220-o15C-9024220-016G-9024220-011G-9024220-018

Reviewed.

PA{COBtTSOI06137

.,La.

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II•

QC Batch

L90250034

L902500J5

L.90250039

L90252003

Date Parameter (Method)----------- ----------------------------------------

1-SEP-1990 FLUORIDE, STLC (EPA 340.2)

7-SEP-1990 FLUORIDE, STLC (EPA 340.2)

7-SEP-1990 SELENIUM (EPA 7741)

9-SEP-1990 ARSENIC (EPA 7061)

_-3,..-------d=9024220-019~,,"9024220-020

U..9024220-o:21U-90 2 4 22 0 - 0 2 2d=90242~O-023

(1w!1024220-0240-lJ024220-025(1-9024220-0260-9024220-0270-9024220-028o~ '1024220-029a~IJ024220-030

a~')024220-032

g.') 024220-0340-')024220-036a-'J024220-038O...·J024220-0~O

0 ... •• ;a:,'" _.... k ..... PYSA[ .44j • ......,.... sz'.·. Ii P f '",. 4.1,1

PMCOBUS0106138

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---------,,----------------·~EnsecoA """"'-0_

DRS certifica~g #157

Labor.tO:')' control Sample Report Croee-Rllf'erence

QC Batch Date 'Parameter (Method) Sampl. Ifoe._____________ _ M_~ - ____

0-9024220-0270-9024220-028C-9024220-029G-9024220-030G-9024220-032G-9024220-034

. 0-9024220-036G-9024220-0380-9024220-040

L902S'4007 lO-SEP-1990 ARSENIC (EPA 7061) 0-9024220-017C-9024220-018G-9024220-019G-9024220-0200-9024220-042G-9024220-045

L90254033 11-SEP-1990 JmRCURY (EPA 7471)' 0-9024220-017G-9024220-018

J . .. ..... G-9024220-019f G-9024220-020G-9024220-D42

G-9024220-o45

L90255008 1l-SEP-1990 SELENIUM (EPA 7741) 0-9024220-0170-9024220-0180-9024220-019G-9024220-0200-9024220-042G-9024220-045

L90255009 1l-SEP-1990 SELENIUM (EPA 7141) 0-9024220-0210-9024220-0220-9024220-0230-9024220-024G-9024220-025G-9024220-026G-9024220-027G-9024220-028G-902422o-029G-9024220-030G-9024220-032G-9024220-03f0-9024220-0360-9024220-038C-9024220-o40

L9025S01~_ 1l-SEP-1990 ANTIMONY (EPA 6010) G-902422o-D42G-9024220-oU

BARICH (EPA 6010) C-9024220-0f2cr-902422Q-On

d ~AtfLdt&Rev.iewed

PMCOBUSOI06140

if.' .' J , i. 4C.

PMCOBUS0106140

.. . , _- _ _ " •• • • p, _ ••• ~•••Page 318 of 442

........ ~ .rn-.r:--:"' 0 •••• _ •

-- '"---------------------'----------~Enseco

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DRS certi~lcat. #157

Laboratory COntro1 Sample Il.eport cro••-Ref.~c.

QC Batch D~t. . Parllllleter (Method) S~l. Ho••

------------- ----------- ---------------------------------------- -------------

L90256020


CADHIUH (EPA 6010)

CHROMIUH (EPA 6010)

COaALT (EPA 6010)

COPPER (EPA 6010)

LEAD (EPA -6010)


NICKEL (EPA 6010)

SILVER (EPA 6010)

THALLIUM (.EPA 6010)

VANADIUM. (~PA 6010)

ZINC (EPA 6010)-

7-SEP-1990 ANTIMONY (EPA 6010)

BARItJK (EPA 6010)

G-9024220-o420-9024220-045G-9024220-o420-9024220-045G-9024220-042G-9024220-045G-9024220-Q.I2G-9024220-045G-9024220-o42G-9024220-045G-9024220-042G-9024220-045G-9024220-0420-9024220-045G-9024220-042G'-9024220-045G-9024220-0420-9024220-0450-9024220-0420-9024220-0450-9024220-042G-9024220-o45

of 442

.- _ " .r'wl"eU '''fM' ;;'O;,:;t;.;.;;.:;;;;;·; ... ·{ 11 b·"·"tiie'g -

. ...~ -.. '

*,",'.00· 'id .t.l • pt"tcW

-------------------------------------~'Enseco=' "~e--.DHS ca~ifi~ate 1151

Lllboratory Control Sample Report CroBIf-Referenc.--.

QC Batch

Reviewed

Date . Parameter (Method)

--------------------------------------

•BERYLLltm (EPA 6010)

CADKIOM (ZPA 6010)

CHROHIUH (EPA 6010)

G-9024220-011G-9024220-012G-9024220-013G-9024220-014G-9024220-015G-9024220-016G-9024220-001G-9024220-002G-9024220-003G-9024220-004G-9024220-005G-9024220-006G-90242Z0-007G-9024220-00SG-9024220-009G-9024220-010G-9024220-0110-9024220-012G-9024220-013G-9024220-014G-9024220-015G-9024220-016G-90U220-001G-9024220-002G-9024220-0030-9024220-0040-9024220-0050-9024220-006G-9024220-007G-9024220-008G-9024220-00~

G-~024220-010

C-9024220-011G-9024220-012G-9024220-013G-51024220-014G-9024220-015G-9024220-016G-9024220-001G-9024220-002G-9024220-003G-902422D-004C-9024220-005G-9024220-006G-9024220-o07'G-902422Q-008G-9024220-009C-9024220-0100-9024220-011G-9Q2422 0-012

. G-9024220-013

JEf"" '" '4"1 .... :pos;:j .. , ...G, .. $ .'\P4i _ PQt*;C*4 " ... ,S.• 1.).;:P "';. Y;l. "t""'.....

P~COB1JSOI06142

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Page 320 of 442• o' • ..... .._... • ......_~••

--------------.:..-------------~Enseco.~,,=,e:...-.,.


Laboratory COntrol Sample Report Cross-Reference

QC Ba1:ch Date ~arameter (Method) Sample No••------------- ----------- ---------------------------------------- -------------

,~Reviewed

PMCOBUSOI06143

::w ... C"'O •• P

PMCOBUS0106143

of 442

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--------------------------~Enseco""""""""'-

DHS certifica~. 1157

Laboratory. COntrol Sample Report Croll.-Refer.nc.

QC Batch Date .l'al:'ameter (Method) ~ampl. lCo._

L9025G02G

VANADIUM (EPA 6010)

.-

ZINC (EPA 6010)

7-SEP-1990 ANTIMONY (EPA 6010)

C-9024220-OO40-9024220-005G-9024220-oo60-9024220-0070-9024220-0080-9024220-0090-9024220-010G-9024220-013-0-9024220-0120-9024220-013G-9024220-0140-9024220.,.0150-9024220-0J.Ei0-9024220-001G-9024220-002G-9024220-0030-9024220-004G-9024220-00SG-9024220-o060-9024220-0070-9024220-0080-9024220-009C-9024220-01.0G-9024220-0110-9024220-012G-9024220-0U0-9024220-0140-9024220-0150-9024220-0160-9024220-001G-9024220-0020-9024220-0030-9024220-004G-9024220-0050-9024220-006 'G-902422 0-007G-9024220-008G-9024220-o09G-9024220-o10G-9024220-011G-9024220-012G-9024220-013G-902422o-014G-9024220-015C-902-4220-016

«:-9024220-017G-9024220-018C-9024220-019G-9024220-o20

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2C Batc::b Date . Parameter (Hethoda Sample .0..------------- ----------- ---------------------------------------- ------------

::

BARJ:UH (EPA 6010)

BERYLLIUM (BPA 6010)

CADMIUM (EPA 6010)

.+

CHROMIUM (BPA 6010)

COBALT (EPA 6010)

COPPER (EPA 6010)

LEAD (EPA (010)


NICKEL (EPA 6010)

SILVER (EPA 60l0)

THALLIOH (EPA 6010)

VAHADIDH (EPA 6010)

zmc (EPA 6010)

C-9024220-0170-9024220-018G-9024220-019G-9024220-020G-9024220-0170-9024220-0180-9024220-019G-9024220-0200-9024220-0170-9024220-0180-9024220-0190-9024220-0200-9024220-0170-9024220-018G-9024220-019G-9024220-Q200-9024220-0170-9024220-018G-9024220-0.19G-9024220-0200-9024220-017G-9024220-o180-9024220-0190-9024220-0200-9024220-0170-9024220-0186-9024220-0190-9024220-0200-9024220-0170-9024220-0180-9024220-0196-9024220-020Q-9024220-o170-9024220-0180-9024220-0190-9024220-020G-9024220-o170-9024220-018G-9024220-019G-9024220-o20G-9024220-0170-9024220-018G-9024220-0190-9024220-0200-9024220-017G-9024220-018G~9024220-o19

0-9024220-020G-9024220-o170-9024220-018a-9024220-019

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QC Batch Date Pllri!ll'llElter (Hethod) Sample No••

G-902422o-013G-902422 0-014C-9024220-015G-9024220-016G-9024220-017G-9024220-018G-902422 0-019G-9024220-020

L90257014 13-SEP-1990 CHROMIUH.BEX!STLC-DI H2O (EPA 7196) 6-9024220-025G-9024220-026G-9024220-021G-9024220-0280-9024220-029G-9024220-030G-9024220-0310-9024220-0320-9024220-0330-9024220-034G-9024220-03S0-9024220-0:360-9024220-037G-9024220-0380-9024220-039G-9024220-0400-9024220-041G-9024220-0420-9024220-043G-9024220-044

L9025701S 13-SEP-1990 CHROMIUM HEX!STLC Dr H2o (EPA 7196) G-9024220-021C-9024220-022G-9024220-023C-9024220-0Z4G-9024220-045G-9024220-o46

L90257019 13-SEP-1990

Revi"ewed

ANTIHONY (EPA 6010-L} G-9024220-001G-9024220-002G-9024220-003G-9024220-004G-9024220-005G-9024220-006G-902422D-007G-9024220-008G-902422D-009G-902422O-010G-902422D-OllG-9024220-012C-9D24220-013G-9024220-014G-9024220-01SG":9024220-016G-902422D-017C-9024220-o18G-9024220-019C-9024220-020

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QC Batch Date ParWlleter (Method) sampl_ No••

------------- ----------- ---------------------------------------- -------------CHROMIOH (EPA 6010-L)

COPPER (EPA 6010-L)

G-9024220-001G-9024220-002G-9024220-003G-9024220-0040-9024220-005G-9024220-006G-9024220-007G-9024220-008G-9024220-009G-9024220-010C-9024220-011G-9024220-012G-9024220-013G-9024220-014G-9024220-015G-9024220-016G-9024220-017G-9DZ4220-018G-9024220-019G-9024220-020G-9024220-001C-9024220-002G-9024220-003C-9024220-0040-9024220-005G-9024220~006

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QC Batch Pate pa,rameter (MBthod) SaJDPle Jfo_.------------- ----------- ----------------~----------------------- ------------

L90257022

MOLYBDENUM (EPA 6010-L)

ZINC (EPA 6010-L)

13-SEP-J.990 ANTIMONY (EPA 6010-L)

CHROMIUM (EPA 6010-L)

COPPER (EPA 6010-L)


ZINC [EPA 6010-L)

0-9024220-0010-9024220-002G-9024220-003G-902422o-00-lG-9024220-OO56-9024220-006G-9024220-007G-9024220-008G-9024220-009G-9024220-010G-9024220-0110-9024220-0120-9024220-013G-9024220-0140-9024220-0150-9024220-016G-9024220-0170-9024220-018G-9024220-o19G-9024220-020G-9024220-o01G-9024220-0020-9024220-003G-9 02422 0-004-G-9024220-o05G-9024220-o060-9024220-007G-9024220-o080-9024220-009G-9024220-0100-9024220-011G-9024220-o12G-9024220-013G-902422G-OUG-9024220-01SG-9024220-016G-9024220-o17G-902422o-0J.8G-9024220-019G-902422D-020

G-902422D-042G-9024220-04SG-9024220-042G-9024220-045

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------------------------~Enseco"'"......,-DHS certificat. #151

Laboratory Control Sample Report Cro_s-ReferIUlc.

QC Batch Date .parameter (Hethod)

Reviewed.

L90257023 13-SEP-1990 AN'lIHONY (EPA 6010-L)

CHROHIOM (EllA 6010-L)

COPPER (EPA 6010-L)

HOLYBDENtJH (EPA 6010-L)

A

0-9024220-021G-902422o-0220-9024220-023G-9024220-024G-9024220-0250-9024220-026G-9024220-0270-9024220-0280-9024220-0290-9024220-030G-9024220-0320-9024220-0340-9024220-036Q-~02"22o-038

G-9024220-o400-9024220-0210-9024220-022G-9024220-0230-9024220-02.4G-9024220-o250-9024220-026G-9024220-0270-9024220-0280-9024220-029G-9024220-o300-9024220-0320-9024220-0340-9024220-036G-9024220-0380-9024220-0010G-9024220-0210-9024220-022G-9024220-0230-9024220-024G-9024220-025G-9024220-026G-9024220-027G-9024220-0280-9024220-D29G-9024220-030G-902422Q-032G-9024220-0301G-9024220-036G-9024220-0380-9024220-040G-902422o-021C-902422Q-022G-902422G-023e-9024220-024G-9024220-025

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QC Batch Data Parameter (Method)

------------- ----------- ----------~------------------------~--

ZINC (EPA 601o-L)

sample No••

G-9024220-026G-9024220-0270-9024220-028G-9024220-029G-9024220-0300-9024220-032G-9024220-034G-9024220-0360-9024220-0380-9024220-040G-9024220-0210-9024220-0220-9024220-0230-9024220-0240-9024220-0250-9024220-026G-9D24220-027G-9024220-0280-9024220-029G-9024220.0300-9024220-0320-9024220-034G-"90:24220-0360-9024220-038G-9024220-0.0

L90257024 12-SEP-1990 ~IMONY (EPA 6010)

BARICH (EPA 6010)

0-9024220-021G-9024220-022G-9024220-023G-9024220-024G-9024220-025G-9024220-026G-9024220-027G-S024220-028G-9024220-029G-9024220-0300-5024220-032(;-9024220-0340-9024;220-036C-9024220-0380-90;24220-040C-9024220-021G-9024220-022G-9024220-0230-9024220-0240-9024220-025G-9024220-026C-9024220-027G-9024220-0280-9024220-029G-902422o-030

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-DRS certificate #157

Labo~atory COnt;o~ sample Report Cross-Reference

QC Batch Date Parameter '(Method) Sample ~o••

•

Reviewed

G-9024220-032G-9024220-034G-9024220-036G-9024220-038G-9024220-040

BER~~UH (EPA 6010) C-9024220-021G-9024220-022G-9024220-023G-9024220-024G-9024220-025C-9024220-026G-9024220-027G-9024220-028G-9024220-029G-9024220-030G-9024220-032G-9024220-034G-9024220-036C-9024220-038G-9024220-040

CADMIUM (EPA 6010) C-9024220-021G-9024220-022C-9024220-023C-9024220-024G-9024220-025C-9024220-026C-9024220-027G-9024220-028G-9024220-029G-9024220-030G-9024220-032G-9024220-034G-9024220-036G-9024220-038G-9024220-040

CHROMIUM (EPA 6010) G-9024220-021G-9024220-022G-9024220-D23G-9024220-024G-9024220-025G-9b24220-026C-9024220-027G-9024220-028C-9024220-029G-9024220-030G-9024220-032C-9024220-034G-9024220-036C-9024220-o38G-9024220-040

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DRS Certificate #157

Laboratory control sample Report Cross-~eferenca

QC Batch Date ·Parameter (Method) sample NOB.

Reviewed

COBAL~ (EPA GOlO)

COPPER (EPA 6010)

LEAD (EPA 6010)

MOL1!BPENUK (EPA 6010)

G-9024220-021G-9024220-022G-9024220-023G-9024220-024G-9024220-025G-9024220-026G-9024220-021G-9024220-028G-9024220-029G-9024220-030G-9024220-032G-9024220-0340-9024220-036G-9024220-038G-9024220-040G-9024220-021G-9024220-022C-9024220-023G-9024220-024G-9024220-025G-9024220-026G-9024220-027G-9024220-026G-9024220-029G-9024220-030G-9024220-032G-9D24220-034G-9024220-036G-9024220-0JBG-9024220-040G-9024220-021G-9024220-022G-9024220-023C-9024220-024G-9024220-025G-9024220-026G-9024220-027G-9024220-028G-9024220-029G-9024220-030G-9024220"'03~

G-9024220-034G-S024220-036G-9024220-038G-90Z4220-040G-9024220-0;i!1G-9024220-022C-9024220-023G-9024220-024G-9024220-025G-9024220-026

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Laboratory Control ~ample Report cross-Reference

QC Batch D~te ,Parameter (Hethod) Sample !ro••

0-9024220-027C-9024220-0280-9024220-0290-9024220-030G-9024220-o320-9024220-03"C-9024220-o36C-9024220-0380-9024220-040G-9024220-0210-9024220-022G-9024220-023C-9024220-024G-9024220-025G-9024220-0260-9024220-027G-9024220-o26C-9024220-0290-9024220-030G-9024220-032G-9d:;l4220-0340-9024220-0360-9024220-03BG-9024220-o40G-9024220-021G-9024220-0220-9024220-023

. G-9024220-0240-9024220-0250-9024220-0260-9024220-027C-9024220-028G-9024220-o290-9024220-030G-9024220-032G-9024220-o34G-9024220-o36G-902.4220-o38G-9024220-Q40G-902422o-021G-902422Q-022G-9024220-023G-9024220-024G-902422.0-025G-9024220-0260-9024220-027G-9024220-028G-9024220-o29C-9024220-030G-9024220-o32

'G-'9024220-oU

DRS certifica~e #157

NICKEL (EPA 6010)

SILVER (EPA 6010)

TRALLIOH (EPA 6010)

Reviewed

PhfC{)BllSOl06155

PMCOBUS0106155

....- , _.. _....•-. •• _ _ ". _ •• _ MPage 333 of 442

------------------------~FJlSeCO• .-0.-..


Laboratory Control SUlple Report Cro••-Ref.rene.

2C Batch Date ParUlGter (Method)

------------- ----------- -------------------_._.-------------------- ----_.-------

L90260001

VANADIUM (EPA 6010)

ZINC (EPA 60iO»

10-SEP-1990 HERCURY (EPA 7471)

0-902.. 220-D360-9024220-038G-9024220-Q40G-9024220-0210-9024220-0220-9024220-0230-9024220~0240-9024220-0250-9024220-0250-9024220-0270-9024220-028G-902"'220-02~

0-9024220-0300-9024220-0320-9024220-0340-9024220-0360-9024220-038G-9024220-().lOG-9024220-0210-9024220-0220-9024220-0230-9024220-0240-9024220-025G-9024220-026G-902=+.. e....(4 ......,s:W%J44Ah ~J. p.)

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Laboratory COntrol sample ft~port cro••~Ref8renc.

'2C Batch Date Parameter (Method) Sampl. lto••---------_.-- ----------- ---------------~~=~--------------------- -------------L902610~9 18-SEP-~990 CHROMIUM, EEx/TtL§ (EPA 7196) 0-9024220-001

0-9024220-002G-9024220~003

0-9024220-0040-9024220-0050-9024220-0060-9024220-007G~902422o-008

0-9024220-0090-9024220-0100-9024220-0~1

0-9024220-0120-9024220-0130-9024220-0140-9024220-0150-9024220-0160-9024220-0110-9024220-0160-9024220-0190-9024220-020

L90251020 lS-SEP-1990 CHROMIUM, BEX1TTL~ (EPA 7196) 0-9024220-0210-9024220-0220-9024220-0230-9024220-0240-9024220-0250-9024220-0260-9024220-0270-9024220-0280-9024220-0290-9024220-0300-9024220-0320-9024220-0340-9024220-036G-9024220-o380-9024220-040

L90261021 18-SEP-1990 CHROMIUM, HEX/xrte (EPA 7196) 0-9024220-042:;-9024220-0.&5

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------------------------------~EnsecoA.~.c....-.

DRS Cert£~~cate 1157

Laboratory Report

------------------~------------------------- ----~ --q----------MITTELHAUSER CORP23272 MILL CREEK RD, STE 300LAGUNA HILLS, CA 92653ATTN: MR. DAVE OORN

Project: (li52) PG & E - TOPOCK

Analysis No.= G-9024220-031/039,Date Sampled: 29-AUG-1990Date Sample Rec'd: 30-AUG-1990sample Type: SLUDGB

Matrix spike/Matrix Spike Duplicate Report

ObservedSample concentration Amt. , Recovery tNumber Parameter (Method) units sample . HS HSD Spiked HS MSD Avg. RPD

------------- ------------------------ ------- ------ ------ ------ ------ ---- ---- ----9024220-027 FLUORIDE (EPA 340.2) mq/L 10.2 ,31.5 31.7 20.0 1.07 lOB 107 19024220-046 FLUORIDE (EPA 340.2) mg/L 38.5 58.9 59.2 20.0 102 104 103 29024220-021 ANTIMONY (EPA 6010) mg/kg 0.072 230 219 250·

~90 5

9024220-017 ANTIMONY (EPA 6010) mg/kg NO 179 167 250 69 79024220-021 BARIUM (EPA 6010) mg/kg 41.8 957 931 1000 92 89 90 39024220-017 BARIUM (EPA 6010) mg/kg 197 982 944 1000 79 75 77 59024220-021 BERYLLIUM (EPA 6010) mg/kg 0.0967 25.0 24.0 25 100 96 98 4

I 9024220-017 BERYLLIUM (EPA 6010) mg/kg 0.122 20.2 19.9 25 aD 79 80 2

I9024220-021 CADMIUM (EPA 6010) mg/kg ND 21.4 20.6 25 86 82 84 49024220-017 CADMIUM (EPA 6010) mg/kg O.O9~1 16.6 16.8 25 e66 61;:; 56 1·9024220-021 CHROMIUM (EPA SOlO) mgjkg 2.78 87.2 83.5 100 84 81 83 5

19024220-017 CHROMIUM (EPA 6010) mg/kg 7.21 79_9 75.3 100 ~~ 70 79024220-021 COBALT (EPA 6010) mg/kg 1.44 218 20B 250 87 83 85 5

1 9024220-017 COBALT (EPA 6010) mg/kg 4.00 175 174 250 CSa_6.S) 68 1J

9024220-021 COPPER (EPA 6010) mg/kg 2.68 120 118 125 94 92 93 29024220-017 COPPER (EPA 6010) mg/kg 7.03 III 109 125 83 82 82 2

I 9024220-021 LEAD (EPA 6010) a1g/kg 1.94 214 203 250 8.5_80 B3 5

I 9024220-017 LEAD (EPA 6010) mg/kg 1.22 161 160 250 C64- 61> 64- 19024220-0:21 MOLYBDENUM (EPA 6010) rngjkg 0.340 112 106 125 8..9_8.5 87 69024220-017 MO~YBDENUM (EPA 6010) Illg/kg 0.581 91.5 90.0 125 C'-3- 72) 72 21

f

9024220-021 NICKEL (EPA 6010) IllS/kg 3.36 21B 207 250 85 82 84 59024220-017 NICKEL (EPA 6010) mg/kg 5.40 176 176 250 a8~ 68 09024220-021 SILVER (EPA 6010) mg/kg 0.059 20 19.3 25 eo 77 78 4

1 9024220-017 SILVER (EPA 6010) mg/kg 0.261 17.8 H.5 25 ~6» 70 19024220-021 THALLIUM (EPA 6010) mg/kg 1.72 22.4 21.6 25 8.3_80 81 4{ 9024220-017 THALLIUM (EPA 6010) mg/kg 6.08 24.3 24.4 2S ~-3- 73) 73 1

I 9024220-021 VANADIUM (EPA 6010) mg/kg 4.52 226 217 250 89 85 87 49024220-017 VANADIUM (EPA 6010) mg/kg 17.6 204 203 250 75 74 74 19024220-021 ZINC (EPA 6010) mg/kg 8.22 232 .220 250 9o_85 87 69024220-017 ZINC (EPA 6010) mg/kg 22.2 197 199 250 Cio iv 70 19024220-017 ARSENIC (EPA 7061) rng/kg 2.2 20.0 20.0 25.0 CtL W 71 09024220-021 ARSENIC (EPA 7061) mg/kg 0.50 18.5 16.5 :25.0 G7..~-=6~~ 68 129025027-004 CHROMIUM, HEX/TTLC (EPA mg/kg NO 0.32 0.35 0.50 (64 70· 67 9

7196)

6iJ09024220-032 CHROMIUM. HEX/TTLC (EPA mq/kg ND 0.37 0.35 0.50 72 67196)

9024220-021 MERCURY (EPA 7471) mglkg 0.007 0.178 0.186 0.175 9B 102 100 59024220-017 MERCURY (EPA 7471) mg/kg NO 0.175 0.172 0.175 100 98 99 .29024220-0:i!l SELENIUM (EPA 7741) rag/kg NO 9.75 B.SO 12.5 78 68 73 149024220-017-- SELENIUM (EPA 7741) mg/kg NO 10.25 8.25 12.5 .82 66 74 22

-« y4wL 1$!!.&L-l(8VlfiW8(1 Ap eel

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--------------------------------------~Enseco,.~~~


Matrix spike/Matrix Spike Duplicate Report Cross-Reference

QC Batch

9024220-027

Dato Parameter (Method)

7-SE:P-~~90 FLUORIDE (EPA 340.2)

G-9024220-039

C-9024220-D31G-9024220-033C-9024220-035C-9024220-037G-902422o-039

18-SEP-1990 CHROMIUM.. HEX/TTLC (EPA 7196) tll,1O9024220-032

9024220-046

9025027-004

7-SEP-1990

~8-SEP-1990

FLUORIDE (EPA 340.2)

CHROMIUM.. HEX!TTLC (EPA 7196}

C-9024220-031C-9024220-033G-9024220-035G-9024220-037G-9024220-039

G-9024220-041G-9024220-043G-9024220-044C-90.24220-046

C-9024220-041G-9024220-043G-9024220-044C-9024220-046

Reviewed

PMCOBUSOI061S9

~........~ **" ~l "$. ".4f'!N s::;es:g;a;,CJ'I';R'Z».iCEL A.lJ '*'" j!L\'l1 tN'h..\ 'C'¢H:X>.,

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• • _ __ •• ' _a a 40

Page 337 of 442

---~-------------------------~Ensecoo-.oסס. .......


'#_- -'. - "-. -~~----.J!Matrixspike/Matrix spike DupH.cate Report CrOSl:I-RGfercanca

&-9024220-0410-9024220-043G-9024220-0440-90242.20-046G-9024220~041

G-9024220-043G-9024220-044C-9024220-0460-9024220-041a-9024220-043G-9024220-044G-9024220-0460-9024220-041G-9024220-043G-9024220-0440-9024220-046G-9024220-'...... "))';y

MOLYBDENUM (EPA 6010) '::t

SILVER (BPA 6010)

VANADXUK (EPA 6010)

Date

1l-SEP-1990

QC Batch

9024220-017

~eviewed

F~COBlJS0106160I!- fJ :;5 •• 1 , I. i ..... ' •. _ .to ;. .... 1, , , .f}

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------------------~~

DRS certificate 1157

Matrix Spike/Matrix spike Duplicate Report Cros.-Reference

QC Batch Dato , . Parameter (Huthod)

------------- ----------- ---------------------------------------ZINC (:ePA 6010)

ARSENIC (ZPA 7061)

MERCURY (EPA 7471)

SELENIUM (EPA 7741)

"

Sample .~.

0-9024220-0460-9024220-0410-9024220-0430-9024220-0440-9024220-0460-9024220-0410-9024220-0430-90242~0-044

0-9024220-0460-9024220-041C-9024220-043G-9024220-044G-9624220-0460-9024220-0.11-G-9024220-043c.-9024220-0UG-9024220-o46

9024220-021 14-SEP-1990 AN~IMONY (EPA 6010)

SARICH (EPA 6010)

BER:iL!..IOH (EPA 6010)

CADMIUM (EPA 6010)

CHROHIDH (EPA 6010)

COBALT (BPI. 6010)

COPPER (EPA 6010)

G-9024220-Q310-9024220-033G-9024220-o35G-9024220-0370-9024220-039G-9024220-0310-9024220-033G-9024220-035G-9024220-037G-9024220-039G-9024220-031G-9024220-o33G-9024220-0350-9024220-037G-9024220-0390-9024220-0310-9024220-033G-9024220-035G-9024220-o37G-9024220-039C-9024220-0310-9024220-0330-9024220-035G-9024220-037G-9024220-0390-9024220-031G-9024220-o33G-9024220-035G-9024220-o37G-9024220-039G-9024220-031 .G-9024220-033G-9024220-o3$

.ssP,.... >:0:0 '(.4tdl."a:;'"+::'3awe~}564",.•• =:Ja... ILH.

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PMCOBUS0106161

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Page 339 of 442

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DRS eerti,ticate #157

Matrix sp.1.:Jce/Matrix spike Duplicate Report Cross-Reference

OC Batch Date . Parameter (Hetbod) Sample lfo••

.~

Reviewed

LEAD (BPI. 6010) .

MOLYBDENtrK {EPA 6010)

NICKEL (EPA 6010)

SILVER (:SPA (010)

THALLIUM (EPA (010)

Vl.NAOIOM (EPA 6010)

tun (EPA 6010)

MERCURY (EPA 7471)

SELENIOH (EPA 7741)

0-9024220-037G-9024220-039G-5024220-0310-9024220-033G-9024220-0350-9024220-037G-9024220-o39G-9024220-0310-9024220-033G-9024220...035G-9024220-037G-902422Q-0390-9024220-0:310-9024220-033G-9024220-0350-9024220-0370-9024220-0390-9024220-on0-9024220-033G-9024220-0350-9024220-037G-9024220-0390-9024220-031G-9024220-033G-9024220-o350-9024220-037G-9024220-G39G-9024220-031c-9024220-0330-9024220-0350-9024220-0370-9024220-039G-9024220-031G-9024220-0:33G-9024220-035G-9024220-037G-9024220-039G-9024220-031G-9024220-0336-9024220-035G-9024220-037G-90242.20-039G-9024220-031G-9024220-033G-9024220-0350-9024220-037G-9024220-039G-902422Q-031e-9024220-033G-9024220-035G-9024220-031

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L~'t:ory Report * • ' '--------------------------------------------------------------------------------------MITTELHAUSER CORP23272 HILL CREEK RD, STE 300LAGUNA HILLS, CA 92653ATTN: HR. DAVE CORN

Project: (1352) PG G E - TOPOUK

Analysis No.: G-9024220-031/039Date Sampled: 29-AUG-1990Date Sample Rec'd: 30-AUG-1990Sample '1'ype: SLUDGE

------------------------------------------------------------------------------------Labo~atory control Sample Report

Avg. ReI.QC Amt. Spi.ke Acceptable Pet. AcceptableEatch Parameter (Method) Sp.iked Un.its Recov. flange Dlff. Range

----------- ------------------------- ------ --------- ------ ---------- ----- ----------L90254004 TDS{STLC-DI (EPA 160.1) 270.9 mg(L 120. 70-120 9. 30L90250034 FLUORIDE, STLC (EPA 2.00 mg/L 96. 69-125 6. 17

340.2)L902Sa035 FLUORIDE, STLC {EPA 2.00 mg/L 94. 69-125 3. 17

340.2}L90262003 ANTIMONY (EPA 6010) 1.0 mg/kg 101. 60-125 11. 25L902S7024 ANTIMONY (EPA 6010) 1.0 mg/kg 99. 60-125 2. 25L9025S012 ANTIMONY (EPA 60l0) 1.0 mg/kg 95. 60-125 1. 25L90257024 BARIUM (EPA 60~OJ 1.0 mg/kg 98. 65-125 1. 30L90262003 BARIUM (EPA 6010) 1.0 l'llg{kg lOS. 65-125 10. 30L90255012 BARIUM (EPA 6010) 1.0 mq/kg 95. 65-125 o. 30L90262003 BERYLLIUM (EPA 6010) 1.0 mg/kg 103. 60-126 11. 30L90257024 BERYLLIUM (EPA 6010) 1.0 mg/kg 96. 60-126 2. 30L90255012 BERYLLIUM (EPA (010) 1.0 mg/kg 95. 60-1.26 1. 30L90257024 CADMIUM (EPA 6010) 1.0 rng!kg 86. 63-126 2. 25L90262003 CADMIUM (EPA 6010) l.0 mg/k{J 95. 63-126 11. 25L902550l2 CADMIUM {EPA GOIO} 1.0 mg{kg 91. 63-126 O. 25L9026200J CHROMIUM (EPA 6010) l.O mg!kg 97. 63-126 9. 30L90257024 CHROMIUM (EPA 6010) l.0 mg/kg 98. 63-126 2. 30L90255012 CHROMIUM (EPA 6010) 1..0 mg/kg 95. 63-126 o. 30L90251024 COBALT (EPA 6010) 1.0 rngjkg 91. 63-126 4. 35L90262003 COBALT (EPA 6010) 1.0 'tMJ/kg 95. 63-126 10. 35I.90255012 COBALT (EPA 6010) 1.0 rng/kg 91. 63-126 o. 35L90262003 COPPER (EPA 6010) 1.0 mg/kg 103. 62-126 9. 30L90257024 COPPER (EPA 60l0) 1.0 mgjkg 100. 62-126 O. 30L90255012 COPP~R (EPA 6010) 1.0 mgJkg 94. 62-126 o. 30L90257024 LEAD (EPA 6010) 1.0 mgjkg 92. 61-l26 4. 30L90262003 LEAD (EPA 6010) l.O mg/kg 94. 61-126 12. 30L902SS012 LEAD (EPA 6010) 1.0 lDSl/kg 91. 61-126 2. .!I0L90262003 MOLYBDENUM (EPA 6010) 1.0 mg/kg 97. 61-126 10. 32L90257024 MOLYBDENUM (EPA 6010) 1.0 'l'f!9/k g 94. 61-126 3. 32L902SS012 MOLYBDENUM (EPA 6010) 1.0 mg/kg 92. 61-126 1. 32L90257024 NICKEL (EPA 6010J 1.0 mqjkg 95. 61-126 3. 2SL90262003 nICKEL (EPA 6010) 1.0 mgjkg 100. 61-126 10. 25L9025S012 NICKEL (EPA 6010) 1.0 mgjkg 96. 61-126 o. 2SL90262003 SILVER (EPA 6010) 1..0 ~/kg 86. 60-126 12. 30L9025,024 SILVER (EPA 6010) 1.0 mg{kg 94. 60-126 o. 30L9025S012 SILVER (EPA 6010) 1.0 mq/kg 88. 60-126 o. 30L9025,024 THALLIUM (EPA 6010) 1.0 mg{kg 90. 60-126 2. 30L9026200J THALLIUM (EPA 6010) 140 mg/kg 95. 60-126 12. 30L90255012 'tHALLIUM (EPA 6010) 1.0 mglkIJ 92., 60-126 14 30

/4 dmL~ReviewedPMCOBUSOI06163

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~as certificate #151

Laboratory Report

MI'l"!'ELHAUSER CORP23272 HILL CREEK RD, STE 300LAGUNA HILLS, CA 92653ATTN; HR. DAVE DOM

Project: (1352) PG & E - TOPOCK

Analyg~s No.: C-9024220-031/DJ9Date Sampled: 29-AUG-199QDate Sample Rec'd: 30-AUG-1990S;smple Xype: SLUDGE

Laboratory control Sample Report

QCBatch Parameter (Method)

Amt.Spiked Unite

Avg.spikeRecov.

Rel.Acceptable pct.

Range Diff.Acceptable

Ranqe

I

l

L90262003L90257024L9025S012L90257024L90262003L90255012L90257023L90257022L90257D23L90257022L90257D23L90257022L90257023L9D257022L90257023L90257022L90254006L90254007L90256028L90255029L90261021

L90261020

L90260DOlL90254033L90255009L902550DBL90250011L90250014L90249012L90249011

VANADIUH (EPA 6010~VAl,ADIUH (BPA 60l0)VAllADIUM (EPA 6010)ZINC (EPA 6010)ZINC (EPA 6010)ZINC (EPA 6010)ANTIMONY (EPA 6010-L)lINTIMONY (EPA 6010-L)CHROMIUM (EPA 6010-L)CHROMIUM (EPA 6010-L)COPPER (EPA 50l0-L)COPPER (EPA 6010-L)MOLYBDENUM (EPA 6010-L)MOLYBDENUM (EPA 6010-L)ZINC (EPA 6010-L)ZINC (EPA 6010-L)ARSENIC (EPA 7061)ARSENIC (EPA 7061)ARSENIC (EPA 7061-L)ARSENIC (EPA 7061-L)CHROMIUM, HEX/TrLC (EPA7196)CHROMIUM, HEX!TTLC (EPA7196)MERCURY (EPA 7471)MERCURY (EPA 7471)SELENIUM (EPA 7741)SELENIUM (EPA 7741)PH (EPA 9045)PH/STLC-DI (EPA 9045)CONDUCTIVITY (BPA 9050)CONDUCTIVITY (EPA 9050)

Reviewed

1.01.01.01.01.01.02.02.02.02.02.02.02.02.02.02.0

1.001.002.02.0

1.00

1.0

0.002• 00201.001.00

9.1839.18314651465

mgjkgmy/kgmg/kgmy/kgmy/kgmg/kg

mg/Lrng/LmgjLmg/Lmg/Lmg/Lrng/Lf!lg/Lmg/Lmg/L

mg/kgmg/kg

mg/LmgjL

mg/kg

mg/kg

mg/kglng/kgmg!kgmg/kgunitsunits

uohlll/cmuobmjcm

95.91.69.92.95.91.94.96.94.96.96.90.94.95.aB.83.86.85.93.

100.100.

97.

108.95 •84.92.

101.101.96.95.,

60-12660-12660-12660-12660-12660-12670-13070-13071-12371-12362-~26

62-12669-12469-12470-12B70-12650-12750-12778-12078-12060-130

60-J.30

51-12551-12545-12B45-1289B-10298-10280-12080-120

10.1.o.4.

u.1.9.3.8.2.s.6.8.1-

J.D.3.5.7.o.o.2.

9.

5.11.8.1.o.o.O.1.

2!i2525303030303020203030202020202525202040

40

42424040112020

...

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Page 342 of 442

---------...,.------------------~iEn.seco..-,r ....~.e::.-.-.,

DHS ce;tifleate #151---.:_- -Laboratory COntrol Sample Report C~olJll-Raf.-C'am:.

QC Batch

1.90249011

1.90249012

1.902500J.1

1.9025001.4

Date

6-SEP-1990

6-SEP-1990

6-SEP-1990

6-5EP-1990

P4r.'UIster {Method)

CONDUC'rIVITY CEPA 9050)

CONDUCTIVITY (EPA 9050)

PH (EPA 9045)

PH!STLC-DI (EPA 9045)

0-9024220-0310-9024220-033

0-g02.f220-0350-9024220-037G-9024220-0390-9024220-041C':'9024220-0430-9024220-0440-9024220-046

0-9024220-0310-9024220-033G-9024220-0350-9024220-037

of 442..- _. ~ .....

.f6'Kt b '? .. ,Lu·,.·o&ri....ifitfrOfeXo·, .,.-. eN .te.....-

-----------------------~Enseco.~ ........

DHS cartLfieate #157

1.abara.tcry Contl:ol Sample Report era••-RfrfeJ:eace

------------- ----------- ----------------------------_.----------~ Ba~ch Date 'Parameter CHet:bod)

1.90254006

1.90254007

1.9025-4033

1.90255008

1.90255009

1.90255012

10-SEP-1990 ARSENIC (EPA 7061)

10-SEP-1990 ARSENIC (BPA 7061)

11-SEP-1990 KERCUR~ (EPA 7471)

11-SEP-1990 SELENIUM (ZPA 7741)

n-SEP-1990 SELlmltIH tEPA 7741}

11-SEP-1990 ANTIMONY" (EPA 6010)

B1IRIUH (EPA 6010)


CADKIUH (EPA 6010)

CHROHItIH (SPA 6010)

COBALT (EPA 6010)

0-902"220-031.0-9024220-0330-9024220-035G-9024220-0370-9024220-039

0-9024220-041G-9024220-043G-902422C-0440-9024220-046

0-9024220-041G-9024220-0430-9024220-0440-9024220-046.0-9024220-041G-9024220-0430-90:24220-044 .....:_0-9024220-046

0-9024220-0310-9024220-0330-9024220-0350-9024220-0370-9024220-039

0-9024220-0410-9024220-0430-9024220·0440-9024220-046G-9Q24220-0410-9024220-043G-9024220-0~4

G-9024220-o46G-9024220-04lG-90242~0-043

G-9024220-0"40-9024220-0&6a-9024220-0410-9024220-043G-9024220-044G-9024220-o46(;-9024220-041C-9024220-0430-9024220-0440-9024220-0460-9024220-041G-90242:20-043G-9024220-044-

Rev.iewed

P~COB1JSOI06166

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PMCOBUS0106166

." 6+.. ,+~. __ •• • 01... .. .. . ..........__ .Page 344 of 442

.. .. ' ..~ ..

.... ....,..--------------------------------~Enseco

.~-

pas certificate #~57

Laboratory COntrol Sample Report Cro••-Re~erenc:e

QC Batch Date PArl1Jl)CJter (Method) Sample no••

------------- ----------- ---------------------------------------- --------------,

L90256028

L90256029

L90257022

COPPER (EPA 6010)

LEAD (EPA 6010)

MOLYBDENUM (BPA 6010)

NlexEI. (EPA 6010»

SILVER (EPA 6010)

1'HALLItIH (EPA 6010)

VANADIUH (EPA 6010)

ZINC (EPA 6010)

12-SEP-1990 ARSENIC (EPA 7061-L)

12-SEP-1990 ARSENIC (EPA 7061-L)

13-SEP-1990 ANTIMONY (EPA 6010-L)

CHROHnm (EPA 6010-L)

G-9024.220-o46G-9024220-o41G-9024220-0430-9024220-0440-9024220-0460-9024220-0410-9024220-0430-9024220-044G-9024220-046G-9024220-041G-90;24220-043C-9024220-0440-9024220-046'G-9024220-0n0--9024220-0430-9024220-0440-9024220-046G-9024220-Q410-9024220-0430-9024220-044G-9024220-o460-9024220-0410-9024220-0430-9024220-044G-9024220-o46G-9024220-041G-9024220-0430-9024220-044G-9024220-0.60-9024220-0nG-902422Q-0,U0-9024220-0140-9024220-046'

G-9024220-0310-9024220-0330-9024220-0350-9024220-0370-9024220-039

0-9024220-041G-9024220-0430-9024220-0440-9024220-046

G-902422Q-0410-9024220-0,13C-9024220-044G-9024220-o46G-9024220-o410-902422o-Gf3

I

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Page 345 of 442.... .- ...- ......

~ ... ..r-'-

----------------------------,Fb~Enseco::I.~-

DHB certificate #157

Laboratory Control Sample Report Croas-Ref.rence-OC Ullt:c:h Dat. . Parameter (Method) Sample lfo••

L90257023

L902S7024

COPPER (EPA 6!,10-L) •

MOLYBDENUM (BPA 6010-L)

ZINC (EPA 6010-L)

13-SEP-1990 ANTIMONY (EPA 6010-L)

CHROMIUM (EPA 6010-L)

COPPER (EPA 6010-L)


ZINC (gp~ 6010-L)

12-SEP-1990 ANTIMONY (BPA 6010)

BARtOK (EPA 6010)

BERYLLIOK (EPA 6010)

C-9024220-0440-9024220-046a-9024220-041G-9024220-043G-9024220-044G-9024220-046G-902422o-0nG-9024220-043G-9024220-044G-9024220-046G-9024220-041G-9024220-043G-9024220-044G-9024220-046

G-9024220-0310-9024220-033G-9024220-o35G-90242'20-037G-9024220-o351(;-9024220-031G-9024220-0330-9024220-035G-9024220-037G-9024220-039G-9024220-031G-9024220-033G-9024220-035G-9024220-037G-9024220-039G-9024220-031G-9024220-0330-9024220-035G-9024220-037G-9024220-0J9G-9024220-031G-9024220-033G-9024220-0350-9024220-031G-902422o-039

G-9024220-031G-9024220-0330-9024220-035G-9024220-037G-9024220-031G-9024220-033G-9024220-035C-9024220-037G-9024220-o31C-9024220-033

'.~Reviewed

P~C()BlJSOI06168

PMCOBUS0106168

M- ...j..1tPage 346 of 442

_.1 - -- ~ ............'-------------------------------r-t··Enseco

~/I~""~.


Laboratory Control Sample Report CroslJ-Referenca

QC Batc::h Date ~arameter (Methoo) Sample No••------------- ----------- ---------------------------------------- -------------

001

CADMIUM. {EPA 60~O)

CHROMIUM (EPA 6010)

COBALT (EPA 6010)

COPPER (EPA 6010)

LEAD (EPA 6010)

MOLYBDENUM (EPA 60101

NICKEL (EPA 6010)

SILVER (EPA 6010)

THALLIUM (EPA 6010)

VANADIOH (EPA 6010)

ZINC (EPA 6010)

lO-SEP-1990 H?RCORY (EPA 7471)

Rev~ewed. Approved.

G-9024220~035

G-9024220-037G-90~4220-031

G-9024220-033G-9024220-035G-9014220-037G-9024220-031G-9024220-033G-9024220-035G-9024220-0370-9024220-031G-9024220-033G-90242.20-0350-9024220-037G-9024220-031G-9024220-033G-9024220-035G-9024220-0370-9024220-031G-5I'024220-033G-9024220-035G-9024220-037G-9024220-031G-9024220-0330-9024220-035G-9024220-037G-9024220-031G-9024220-033G-9024220-0350-9024220-037G-9024220-031G-9024220-033G-9024220-035G-9024220-037G-9024220-031G-9024220-0330-9024220-035G-9024220-0370-9024220-0310-9024220-033G-9024220-035G-9024220-031G-9024220-031G-9024220-033G-9024220-035G-9024220-o37

G-9024220-031,0-9024220-033G-9024220-035c-9024220-Q31

p~COB1JSOI06169

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~\Io'" .~ .. ,

Page 347 of 442• ~ a •

...",,,' ., ,l' , ... :w'":::~':~~~=:'~'~~'~,9 M '0"'W4d_'-

---------------~----------~Enseoo" ..........-

OHS certi~ic~te 1157

Labor4tory-;t~'ofSample Repore CrasB-Rater.nea

QC Batch Date Parameter (Method) Sample Hes.------------- ----------- ---------------------------------------- ------------

G-9024220-o39

L90261020'

L90261021

18-S£1'-1990 CHROMIUM. HEX!XTLC (EPA 7196)

18-SE1'-2990 CHROMIUM, HEX/TTLC (EPA 7196)

G-9024220-031G-9024220-033

.. ....... ...... ...... .. ., ~ _ .._. ~ ..' hU_"'_· .•...........................

Page 348 of 442

Analytical Report

t' T

'. -d

'"Hr. KevIn DoddsEnseco7440 Lincoln VayGarden Grove, California 92641

LOG NO: E90~09-001

Receiveds 04 SEP 90Reported: 24 SBP 90

Requjsltlon~ G-9024220Project: Hittelbauser #1352

LOG NO

09-001-109-001-209-001-309-001-409-001-5

REPORT OF ANALYTICAL RESULTS

SAMPLE DESCRIPTION. SOIL SAMPLES

G-9024Z20-001 B-I-lG-9024220-002 B-1-2G-9024220-003 R-I-3G-9024220-004 B-1-4G-9024220-005 B-1-5

Page 1

DATE SAMPLED,

28 AUG 9028 AUG 9028 AUG 9028 AUG 9028 AUG 90

PARAMETER 09-001-1 09-001-2 09-001-3 09-001-4 09-001-5

Total Fluorides, mg/kg 150 130 180 210 130

P~~()BlJSOI06171

........... ..... "..::[1...... 0,;BC~- .

............._--PMCOBUS0106171

of 442................................._ _ .

Analytiea&eport

lco' 'ft'? t, ~·""~I'bolt·)

LOG NO: E90-09-001

Received: 04 SEP 90Reported; 24 SEP 90

Hr. KeviJl DoddsEnsec:.o7440 Lincoln YayGarden Grove, California 92641

REPORT OF ANALYTICAL RESULTS

Requisition: G-9024220Project: Kittelhauser /1352

Page 2

LOG NO

09-001-609-001-709-001-809-001-909-001-10

SAMPLE DESCRIPTION, SOIL SAMPLES

G-9024220-006 B-I-6G-9024220-007 B-I-7G-9024220-00B B-2-1G-9024220-009 B-2-2G-9024220-010 B-2-3

DATE SAMPLED

28 AUG 9028 AUG 9028 AUG 9028 AUG 9028 AUG 90

PARAMETER 09-001-6 09-001-7 09-001-8 09-001-9 09-001-10

Total Fluorides, mg/kg 110 280 110 190 200

............ ........==0 s c»....,....

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PMCOBUS0106172

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PGE Topock - RFI/RI v1: Apndx C Lab Data 1992 Pt. 6...L90256026 MOLYBDEIWM (EPA 6010) 1.0 eng/kg 89....

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