PATRIOT ENGINEERING AND ENVIRONMENTAL, INC., PHASE II ... · Goodwill Industries Property,...

6330 East 75th Street, Suite 216, Indianapolis, Indiana 46250 (317) 576‐8058 (317) 576‐1965 FAX www.patrioteng.com

Offices in Indianapolis, Evansville, Fort Wayne, Lafayette, and Terre Haute, IN, Louisville, KY, Dayton / Cincinnati, OH, Nashville, TN, Carmi, IL, and New Orleans, LA

February 16, 2015 Mr. E. Sean Griggs Barnes and Thornburg LLP 11 South Meridian Street Indianapolis, Indiana 46204-3535 RE: Phase II Limited Subsurface Investigation

Goodwill Industries Property Southwest Corner of West Michigan Street and White River Parkway Indianapolis, Indiana 46222 Patriot Project No. 1-14-1903

Dear Mr. Griggs:

In accordance with the authorization by the Barnes and Thornburg LLP, Patriot Engineering and Environmental, Inc. (Patriot) has completed the Phase II Limited Subsurface Investigation (LSI) at the above-referenced location. The Phase II LSI was conducted to address potential recognized environmental conditions (RECs) identified by Patriot during a Phase I Environmental Site Assessment and to address recommendations provided by the Indiana Department of Environmental Management (IDEM) regarding the site. This report details the scope of work and presents a summary of our findings and conclusions relative to the property. We appreciate the opportunity to have provided you with our environmental services. If you have any questions regarding this report, or if we can be of further service, please do not hesitate to contact the undersigned at (317) 576-8058.

Respectfully submitted,

Patriot Engineering and Environmental, Inc.

Michael F. Casper, LPG Richard Kraft, CEM, CRS Principal Principal Engineer Environmental Group Manager

Reference 47

Phase II Limited Subsurface Investigation Patriot Project Number 1-14-1903 Goodwill Industries Property, Indianapolis, Indiana February 16, 2015

Patriot Engineering and Environmental Inc.

PHASE II LIMITED SUBSURFACE INVESTIGATION GOODWILL INDUSTRIES PROPERTY

SOUTHWEST CORNER OF WEST MICHIGAN STREET AND WHITE RIVER PARKWAY INDIANAPOLIS, INDIANA 46222

PATRIOT PROJECT NUMBER 1-14-1903

INTRODUCTION

Patriot Engineering and Environmental, Inc. (Patriot) was retained by the Barnes and

Thornburg LLP to conduct a Phase II Limited Subsurface Investigation (LSI) for the

property located at southwest corner of West Michigan Street and White River Parkway

in Indianapolis, Marion County, Indiana (herein referred to as the Site). The location of

the Site is depicted on the Site Location Map included as Figure 1 (Attachment A).

The Phase II LSI was conducted to address the Recognized Environmental Conditions

(RECs) identified by Patriot during a Phase I Environmental Site Assessment (ESA)

performed at the Site in December 2014 and in accordance with recommendations

provided by the Indiana Department of Environmental Management (IDEM) regarding

the Site. This report details the scope of work and presents a summary of our findings

and conclusions relative to the Site.

SCOPE OF WORK

Limited Subsurface Investigation

Patriot mobilized to the Site on December 30 and 31, 2014 and

January 27 and 28, 2015 to conduct the Phase II LSI activities. Prior to the start of the

field activities, underground utilities were marked by the Indiana Underground Plant

Protection Service. A site specific Health and Safety Plan was reviewed and signed by

the field personnel and subcontractors before the initiation of the field activities. The

approximate locations of the soil borings are depicted on the Boring Location Map

provided as Figure 2 (Attachment A).

Eight soil borings were advanced at the Site using a Geoprobe Direct-Push Dual Tube

Sampling System (Geoprobe). Boring SB-5 was advanced in the northeast corner of

property at the location of a historic gasoline service station, and borings SB-7 and SB-8

were advanced on the southeast corner of the property at the location of a second

historic gasoline service station. The remaining borings were advanced in locations that

Reference 47 Page 2



would provide data on potential impacts to the Site from historic usage and/or off-site

sources. The borings were advanced to depths that ranged from 47 feet below surface

grade (ft-bsg) to 56 ft-bgs. Soil samples from each boring were screened in the field for

evidence of contamination, and soil samples were collected from three boring locations

(SB-5, SB-7, and SB-8) for laboratory analysis. Groundwater samples were collected

from each boring location for laboratory analysis.

Soil Sampling and Field Screening Methodology

All sampling was performed in accordance with standard United States Environmental

Protection Agency (US EPA) and IDEM protocols for environmental investigations. All

equipment coming into contact with the samples designated for analysis was

decontaminated before use by cleaning with a non-phosphate detergent wash and

distilled water rinses. Soil samples from the borings were obtained using a 2-inch

diameter, stainless steel core barrel sampler equipped with an acetate liner. Soil

samples were collected by pushing the core sampler in 4-foot intervals to terminal

depths. Undisturbed soil collected within the acetate liner was then recovered by

removing the core barrel. The used liner was removed and replaced with a new acetate

liner prior to the collection of subsequent samples.

Following collection, the lithology of each soil sample was visually classified according

to the Unified Soil Classification System (USCS) and field screened for odor, staining,

the presence of fill material, and the presence of volatile organic compounds (VOCs)

using a photoionization detector (PID). A PID measures the headspace concentration

of total photoionizable vapors (TPVs) emitted from the samples. It should be noted that

headspace analysis is used for comparative purposes only and that TPVs recorded in

the field do not indicate actual VOC concentrations reported by laboratory analyses.

The field screening procedure is typically used to determine if elevated levels of volatile

contaminants are present in the soil samples. In order to prepare the samples for

headspace analysis, the samples were contained in a sealed zip-lock bag, the

concentration of TPVs within the bag was allowed to equilibrate for approximately five to

fifteen minutes before the bag was punctured with the PID monitoring probe and the

maximum instrument response was recorded in the field notes as the TPV level. The

soil lithology and field screening results from each boring were recorded on boring logs

provided as Attachment B.

Reference 47 Page 3



On the basis of odor, staining, and TPV response, one soil sample was selected from

each of the borings that was advanced at the historic gasoline service stations locations

(SB-5, SB-7 and SB-8) at the interval exhibiting the greatest potential for impacts.

Samples were placed in appropriate sample containers, labeled, placed on ice in a

cooler, and delivered to Pace Analytical, Inc. (Pace) using proper chain-of-custody

documentation. The soil samples were submitted for analysis of VOCs by US EPA SW-

846 Method 8260, polynuclear aromatic hydrocarbons (PAHs) by US EPA SW-846

Method 8270, and lead by US EPA SW-846 Method 6010. The samples analyzed for

VOCs were collected using Terra Core samplers in accordance with US EPA Method

5035. No soil samples were submitted for laboratory analysis from the remaining

borings.

Groundwater Sampling Methodology

The groundwater samples were collected through the Geoprobe equipment or

temporary PVC piezometers using a check valve and polyethylene tubing to draw a

sample to the surface. A shallow groundwater sample was collected from each boring,

generally at 30 ft-bgs. Additionally, a deep groundwater sample was collected from each

boring location at the terminal depth, which ranged between 47 and 55 ft-bgs. Following

groundwater sample collection, the equipment and tubing were removed and the

boreholes were backfilled with bentonite.

The groundwater samples were collected and placed in appropriate sample containers,

labeled, placed on ice in a cooler, and delivered to Pace using proper chain-of-custody

documentation. The groundwater samples were submitted for analysis of VOCs by US

EPA SW-846 Method 8260 and PAHs by US EPA SW-846 Method 8270. Groundwater

samples collected at borings SB-5, SB-7, and SB-8 were also analyzed for total and

dissolved lead by US EPA SW-846 Method 6010.

SUBSURFACE INVESTIGATION RESULTS

Field Screening Results

Based on the field observations made during the Phase II LSI, the subsurface materials at

the Site generally consisted of silty clay with varying amounts of sand and gravel,

overlaying sand and gravel. Saturated soil conditions were generally encountered during

the Phase II LSI at depths which ranged between 22 and 28 ft-bsg. The TPV

Reference 47 Page 4



responses in the soil samples screened ranged between 0.0 and 251 parts per million.

The lithologic descriptions, results of the field screening, and soil and groundwater

sampling depths are provided on the boring logs included in Attachment B.

Soil Analytical Results

The soil analytical results were compared against the Soil Exposure Screening Levels

established by IDEM in the IDEM Remediation Closure Guide (RCG) dated July 22,

2012 (updated March 2014). The soil analytical results revealed the following:

Benzo(a)pyrene and dibenzo(a,h)anthracene were detected at concentrations

slightly above the IDEM RCG Residential Direct Contact Screening Level

(RDCSL) in the soil sample collected from boring SB-5 (8-10 ft-bgs).

Tetrachloroethene was detected in soil sample collected from boring

SB-5 (8-10 ft-bgs) above the RCG Migration to Groundwater Screening

Level (MGSL).

A summary of the soil laboratory analytical results is presented in Table

1 (Attachment C) and the laboratory analytical report is presented in Attachment D.

Groundwater Analytical Results

Laboratory analytical results for groundwater were compared to the Ground Water (tap

water and vapor exposure) Screening Levels found in the IDEM RCG and default

closure levels found in IDEM’s Risk Integrated System of Closure (RISC) program. The

groundwater analytical results revealed the following:

No PAH constituents were identified in the groundwater samples above

laboratory reporting limits.

Tetrachloroethene (PCE) was detected in all groundwater samples at

concentrations above the IDEM RISC industrial default closure level (IDCL),

except the groundwater samples collected from borings SB-5 (31 ft-bgs and 55

ft-bgs), SB-7 (30 ft-bgs and 55 ft-bgs), and SB-8 (30 ft-bgs). Additionally, PCE

was detected in the groundwater samples collected from borings SB-7 (30 ft-bgs

and 55 ft-bgs) and SB-8 (30 ft-bgs) above the IDEM RISC residential default

closure level (RDCL).

Reference 47 Page 5



Trichloroethene was detected in the groundwater samples collected from borings

SB-2 (47 ft-bgs) and SB-6 (30 ft-bgs and 55 ft-bgs) above the IDEM RISC IDCL,

and above the IDEM RISC RDCL in the groundwater sample collected from

boring SB-4 (30 ft-bgs).

Vinyl chloride was detected in the groundwater samples collected from boring

SB-5 (31 ft-bgs and 55 ft-bgs) above the IDEM RISC IDCL.

No other VOC constituents were identified above the RISC or RCG screening

levels in the groundwater samples

Total lead was detected in the groundwater samples collected from boring

SB-5 (31 ft-bgs), SB-7 (30 ft-bgs), and SB-8 (30 ft-bgs) above the IDEM RISC

IDCL. However, dissolved lead analysis of these groundwater samples reported

no detectable concentrations of dissolved lead above the laboratory reporting

limit.

A summary of the groundwater laboratory analytical results is presented in

Table 2 (Attachment C) and the laboratory analytical report is presented in

Attachment D.

CONCLUSIONS

Based on the analytical data, there may be residual impacts to the soil at the location of

the former gasoline service station on the northeast corner of the Site (SB-5), as

evidenced by the low concentrations of PAHs detected in the sample. None of the

PAHs were present at concentrations that exceed the RCG industrial, excavation or

migration to groundwater screening levels, which would likely be applicable to the Site.

The laboratory did not indicate that the Site has been impacted by the former gasoline

fueling operations performed on the southeast corner of the Site. The laboratory data

indicate that the groundwater beneath most of the Site appears to be impacted from an

off-site upgradient source of chlorinated chemical constituents.

QUALIFICATIONS OF ASSESSMENT

This Phase II LSI was intended to investigate the Site for the presence or absence of

chemicals of concern associated with the RECs identified by Patriot during a Phase I

ESA completed for the Site and was not intended to fully delineate the extent of

potential impacts. Patriot was not made aware of any other potential environmental

concerns. Patriot is not responsible for identifying any soil and/or ground water

contamination, areas of environmental impact or any other areas of environmental

Reference 47 Page 6



concern located on other portions of the Site, and caused by any unidentified or

undisclosed activities.

All environmental assessments are inherently limited in the sense that conclusions are

drawn and recommendations developed from information obtained from limited

investigations and research.

Reference 47 Page 7

ATTACHMENT A

FIGURES

Reference 47

APPROXIMATE SITE LOCATION

Site Location Map

Source Map: Indianapolis West 1998 USGS Topographic Quadrangle Map

Project No.Figure 11-14-1903

Goodwill Industries PropertySouthwest Corner of West Michigan Street and

White River ParkwayIndianapolis, Indiana

Reference 47

Project No. Figure 2 1-14-1903

= Proposed Soil Boring-Soil and Groundwater

Former

Gasoline

Station

Former

Gasoline

Station

Approximate

Site

Boundaries

Legend: = Soil Boring - Groundwater Only

= Approximate Location of USTs

= Soil Boring - Soil and Groundwater

SB-2

SB-1

SB-3

SB-5

SB-4

SB-6

SB-7 SB-8

Soil Boring Map

Goodwill Industries Property

Southwest Corner of West Michigan Street and

White River Parkway

Indianapolis, Indiana

Reference 47

ATTACHMENT B

BORING LOGS

Reference 47

RECORD OF SUBSURFACE INVESTIGATION

BORING IDENTIFICATION: SB-1

Page 1 of 3

Client: Barnes and Thornburg LLP Drilling Method: GeoProbe® Direct Push

Project Number: 1-14-1903 Logged By: Alex Stephens

Project Name: Goodwill Industries Driller Name: SCS

Site Location: W Michigan & White River Pkwy Indpls IN License Number:

Start Date: 12/30/2014 Finish Date: 12/30/2014

Lithology Description DTW Depth (ft bsg)

TPV (ppm)

Recovery Comments

Asphalt

0.0

40%

CLAY; with sand/gravel, brown, firm, plastic, moist 1 2

0.0

3 4 trace gravel, with silt, soft, moist

0.0

40%

5 6

0.0

7 8 Firm

0.0

50%

9 10 Some sand at 10.0 ft

0.0

11 SAND; brown/tan, loose, fine to medium grained, dry 12 Trace fine gravel

0.0

60%

13 14

0.3

15 16

0.4

60%

17 18

0.4

19

20 DTW = Depth To Water TVP = Total Photoionizable Vapors PPM = 0Parts Per Million

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Page 2 of 3







TPV (ppm)

Recovery Comments

0.0

60%

21 22

0.0

Medium to coarse grained with fine/coarse gravel, saturated

23

24

0.0

80%

25 26 Increasing gravel content

0.0

27 28 GRAVEL; with sand, fine, saturated

0.0

95%

29 30

0.0

31 32 SAND; brown/tan, loose, medium to coarse grained,

0%

Liner stuck for 32’ to 36’ No Recovery

saturated 33 34

35 36 With fine gravel

0.0

60%

37 38

0.0

39

40

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Page 3 of 3







TPV (ppm)

Recovery Comments

0.0

80%

41 42

0.0

43 44

0.0

90%

45 GRAVEL; with sand, fine to coarse, saturated 46

0.0

47 48 SAND; brown/tan, loose, medium to coarse grained,

0.0

90%

saturated, with fine/coarse gravel 49 50

0.0

51 52

0.0

90%

53 54

0.0

55 SB-1 GW sample collected at 30’ 56 SB-1 GW sample collected at 56’ Refusal @ 56’

EOB @ 56 ft 57 58

59

60

Reference 47



Page 1 of 3







TPV (ppm)

Recovery Comments

Gravel

0.0

60%

CLAY; brown, soft plastic, dry, with organics 1 2

0.0

3 4 Slightly firm, slightly moist

0.0

60%

5 6

0.0

7 8 Sandy

0.0

40%

9 10

0.0

11 SAND; tan/brown, fine to medium grained, trace fine gravel, loose, dry 12

0.0

70%

13 14

0.0

15 16 Fine to coarse grained

0.0

70%

17 18

0.0

19


Reference 47



Page 2 of 3





Start Date: 12/30/2014 Finish Date/Time: 12/30/2014


TPV (ppm)

Recovery Comments

With fine gravel

0.0

60%

21 22

0.0

23 24 Saturated

0.0

60%

25 26

0.0

27 28

0.0

70%

29 30

0.0

31 32

20%

33 34

35 36

0.0

0%

No recovery 36’ – 40’ 37 38

0.0

39

40

Reference 47



Page 3 of 3



Project Name: Goodwill Industriees Driller Name: SCS


Start Date/Time: 12/30/2014, 2:30pm Finish Date/Time: 12/30/2014


TPV (ppm)

Recovery Comments

0.0

0%

No recovery 40’ – 44’ 41 42

0.0

43 44

0.0 100%

No recovery 44’ – 47’ 45 46

0.0 SB-2 GW sample collected at 27’

47 SB-2 GW sample collected at 47’ Refusal at 47’

EOB at 47’

48

49 50

51 52

53 54

55 56

57 58

59

60

Reference 47



Page 1 of 3







TPV (ppm)

Recovery Comments

Topsoil

0.0

40%

CLAY; trace sand, brown, firm, plastic, slightly moist 1 2

0.0

3 Brick/debris from 3.0-3.5 ft 4

0.0

60%

5 6

0.0

7 8

0.0

70%

9 10

0.0

11 12

0.0

70%

13 14 SAND; trace fine gravel, brown/tan, slightly firm,

0.0

medium to coarse grained, moist 15 16

0.0

80%

17 18

0.0

19


Reference 47



Page 2 of 3





Start Date/Time: 12/31/2014, 9:55am Finish Date/Time: 12/31/2014


TPV (ppm)

Recovery Comments

0.0

70%

21 22 Saturated at 22’

0.0

23 24 Fine to medium grained sand

0.0

80%

25 Medium to coarse grained sand, with fine gravel 26

0.0

27 28

1.0

40%

29 30

0.1

31 32

0.0

40%

33 34

0.0

35 36

0.0

30%

37 38

0.0

39

40

Reference 47



Page 3 of 3





Start Date/Time: 12/31/2014, 9:55am Finish Date/Time: 12/31/2014


TPV (ppm)

Recovery Comments

Gray

0.0

25%

41 42

0.0

43 44

0.0 80%

45 46

0.0

47

0.0

90%

48 49

0.0

50 51

0.0

10%

52 53

0.0

54 SB-3 GW sample collected at 30’ 55 SB-3 GW sample collected at 55’ Refusal @ 55’

EOB @ 55’ 56 57 58 59

60

Reference 47



Page 1 of 3







TPV (ppm)

Recovery Comments

Gravel

0.0

60%

CLAY; brown, firm, plastic, slightly moist 1 2

0.0

3 4

0.0

50%

5 6

0.0

7 with coarse sand 8 SAND; tan/brown, fine to coarse grained, loose, dry,

0.0

50%

trace fine gravel 9 10

0.0

11 12

0.0

40%

13 14

0.0

15 Tan, fine grained, slightly moist 16

0.0

60%

17 18 Some fine gravel

0.0

19


Reference 47



Page 2 of 3





Start Date/Time: 12/31/2014 Finish Date/Time: 12/31/2014


TPV (ppm)

Recovery Comments

0.0

40%

21 22

0.0

23 24 Saturated

0.0

80%

25 26

0.0

27 28

1.0

90%

29 30

0.1

31 32

0.0

60%

33 34 Fine gravel

0.0


0.0

70%

37 38

0.0

39

40

Reference 47



Page 3 of 3





Start Date/Time: 12/31/2014 Finish Date/Time: 12/31/2014


TPV (ppm)

Recovery Comments

0.0

80%

41 42

0.0

43 SB-4 GW sample collected at 30’ SB-4 GW sample collected at 50’ 44 Refusal @ 44’

EOB @ 44’ 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59

60

Reference 47



Page 1 of 3







TPV (ppm)

Recovery Comments

Asphalt

0.0

30%

CLAY; with sand, brown, plastic, firm, slightly moist 1 2

0.0

3 4

0.0

20%

5

6

0.0

7 8

0.0

60%

9

10

0.0

11

12

0.0

60%

13 14

0.0

15 SAND; tan/brown, fine to medium grained, dense, slightly moist 16

0.0

60%

17 18

0.0

19


Reference 47



Page 2 of 3





Start Date/Time: 1/27/2015 Finish Date: 1/27/2015


TPV (ppm)

Recovery Comments

0.0

60%

21

22

0.0

23 24

0.0

70%

25 26

0.0

27 28 Saturated, fine to coarse grained

0.0

80%

29 30

0.0

31 32

0.0

80%

33 34

0.0

35 36

0.0

50%

37 38

0.0

39

40

Reference 47



Page 3 of 3







TPV (ppm)

Recovery Comments

0.0

90%

41 42

0.0

43 44

0.0 90%

45 46

0.0

47

0.0

90%

48 49

0.0

50 51

0.0

90%

52 53

0.0


EOB @ 55’ 56 57 58 59

60

Reference 47



Page 1 of 3







TPV (ppm)

Recovery Comments

Topsoil

0.0

40%

CLAY; sandy, dark brown/black, slightly moist, loose 1 2

0.0

3 4

0.0

10%

5 6

0.0

7 8

0.0

50%

9 Brown, soft, plastic, trace sand SB-7 sample collected at 8-10’ 10

0.7

11 12

1.1

60%

13 14

0.0

15 SAND; tan/brown, fine to medium grained, loose, 16 slightly moist

0.0

60%

17 18

0.0

19


Reference 47



Page 2 of 3







TPV (ppm)

Recovery Comments

0.0

60%

21

22

0.0

23 24

0.0

70%

25 26

0.0

27 28 Saturated, fine to coarse grained, trace fine gravel

0.0

80%

29 30

0.0

31 32

0.0

90%

33 34

0.0


0.0

90%

37 Gravel with sand 38

0.0

39

40

Reference 47



Page 3 of 3





Start Date/Time: 1/27/2015 2:50pm Finish Date: 1/27/2015


TPV (ppm)

Recovery Comments

Sand with gravel

0.0

90%

41 42

0.0

43 44

0.0

90%

45 46

0.0

47 48

0.0

90%

49 50

0.0

51 SB-7 GW sample collected at 30’ SB-7 GW sample collected at 55’ 52 Refusal at 52’

EOB @ 52’ 53 54 55 56 57 58 59

60

Reference 47



Page 1 of 3







TPV (ppm)

Recovery Comments

Asphalt

0.0

30%

CLAY; with sand, brown, plastic, firm, slightly moist 1 2

0.0

3 4

0.0

20%

5

6

0.0

7 8

0.0

60%

9 SB-8 sample collected at 8-10’

10

0.0

11

12 Soft

0.0

60%

13 14

0.0

15 SAND; tan/brown, fine to medium grained, dense, slightly moist 16

0.0

60%

17 18

0.0

19


Reference 47



Page 2 of 3







TPV (ppm)

Recovery Comments

0.0

60%

21

22

0.0

23 24

0.0

70%

25 26

0.0

27 28 Saturated, fine to coarse grained

0.0

80%

29 30

0.0

31 32 With fine gravel

0.0

80%

33 34

0.0

35 36

0.0

50%

37 38

0.0

39

40

Reference 47



Page 3 of 3







TPV (ppm)

Recovery Comments

0.0

90%

41 42

0.0


0.0 90%

45 46

0.0

47

0.0

90%

48 49

0.0

50 51

0.0

90%

52 53

0.0


EOB @ 55’ 56 57 58 59

60

Reference 47

ATTACHMENT C

TABLES

Reference 47

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SB-5 8-10' 01/28/2015 <0.0056 <0.0056 <0.0056 0.19 <0.0056 <0.0056 <0.0056 <0.011 <0.0056 BRL 0.021 0.032 0.027 0.12 0.14 0.73 0.62 0.64 0.44 0.51 0.84 0.22 1.1 0.035 0.4 0.076 0.5 1.1 BRL 6.8

SB-7 8-10' 01/27/2015 <0.0044 <0.0044 <0.0044 <0.0044 <0.0044 <0.0044 <0.0044 <0.0088 <0.0044 BRL <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 <0.0061 BRL 13

SB-8 8-10' 01/27/2015 <0.0062 <0.0062 <0.0062 <0.0062 <0.0062 <0.0062 <0.0062 <0.012 <0.0062 BRL 0.017 0.02 0.033 0.026 0.26 0.26 0.2 0.21 0.13 0.17 0.38 0.066 0.46 0.042 0.12 0.034 0.37 0.42 BRL 42.4

15 76 600 120 820 6.2 0.84 260 210 Varies 220 320 4,800 NE 24,000 2.1 0.21 2.1 NE 21 210 0.21 3,200 3,200 2.1 50 NE 2,400 Varies 400

54 270 2,200 170 820 20 17 260 690 Varies 530 2,200 33,000 NE 100,000 21 2.1 21 NE 210 2,100 2.1 22,000 22,000 21 180 NE 17,000 Varies 800

750 480 8,900 170 820 34 660 260 1,200 Varies 33,000 3,700 55,000 NE 100,000 1,300 130 1,300 NE 13,000 100,000 130 37,000 37,000 1,300 1,000 NE 28,000 Varies 1,000

0.051 16 0.54 0.045 14 0.036 0.014 200 0.59 Varies 1 2.8 82 NE 860 2.1 4.7 7 NE 68 210 2.2 1,400 81 40 0.092 NE 190 Varies 270

BOLD

BOLD

BOLD

BOLD

BOLD

IDEM RCG Industrial DCSL's

IDEM RCG Excavation DCSL's

IDEM RCG Residential MTGSL's

Notes

SampleIdentification

Southwest Corner of West Michigane Street and White River Parkway

TABLE 1Summary of Soil Analytical Restuls - Goodwill Industries Phase II

Indianapolis, IndianaPatriot Project No.: 1-14-1903

= Constituent detected above Laboratory Reporting Limit

DateCollected

Volatile Organic Compounds (VOCs) Polynuclear Aromatic Hydrocarbons (PAHs)

IDEM RCG Residential DCSL's

IDEM = Indiana Department of Environmental Management

DCSL = Direct Contact Screening Level

MTGSL = Migration to Groundwater Screening Level

RCG = Remediation Closure Guide

= Constituent detected above IDEM RCG Residential DCSL's

= Constituent detected above IDEM RCG Industrial DCSL's

= Constituent detected above IDEM RCG Excavation DCSL's

= Constituent detected above IDEM RCG Residential MTGSL's

All results reported in milligrams per kilogram (mg/kg)

Reference 47

PAHs

Tetr

ach

loro

eth

en

e (

PC

E)

Tri

ch

loro

eth

en

e (

TC

E)

cis

-1,2

-Dic

hlo

roeth

en

e

tran

s-1

,2-D

ich

loro

eth

en

e

Vin

yl ch

lori

de

All R

em

ain

ing

VO

Cs

All P

AH

s

Lead

Lead

, D

isso

lved

SB-1 GW 30' 12/30/2014 249 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-1 GW 55' 12/30/2014 87.5 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-2 GW 27' 12/31/2014 304 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-2 GW 47' 12/31/2014 243 7.3 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-3 GW 30' 12/31/2014 582 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-3 GW 55' 12/31/2014 210 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-4 GW 30' 1/27/2015 124 5.5 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-4 GW 55' 1/27/2015 299 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-5 GW 31' 1/28/2015 <5.0 <5.0 9.1 <5.0 5.9 BRL BRL 1,020 <10.0

SB-5 GW 55' 1/28/2015 <5.0 <5.0 15.5 <5.0 4.3 BRL BRL NA NA

SB-6 GW 30' 1/28/2015 144 11.8 10.3 <5.0 <2.0 BRL BRL NA NA

SB-6 GW 55' 1/28/2015 73.3 10.2 11.9 <5.0 <2.0 BRL BRL NA NA

SB-7 GW 30' 1/27/2015 5.2 <5.0 <5.0 <5.0 <2.0 BRL BRL 984 <10.0

SB-7 GW 55' 1/27/2015 17.1 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

SB-8 GW 30' 1/27/2015 9.6 <5.0 <5.0 <5.0 <2.0 BRL BRL 649 <10.0

SB-8 GW 55' 1/27/2015 55.4 <5.0 <5.0 <5.0 <2.0 BRL BRL NA NA

5 5 70 100 2 Varies Varies 15 15

55 7.2 1000 2000 4 Varies Varies 42 42

5 5 70 100 2 Varies Varies 15 15

110 9.1 NE NE 2 Varies Varies NE NE

470 38 NE NE 35 Varies Varies NE NE

BOLD

BOLD

BOLD

BOLD

BOLD

BOLD

RISC = Risk Integrated System of Closure

DCL = Default Closure Level

Lead

NA = Not Analyzed

Sample

Identification

Date

Collected

IDEM RISC Residential DCLs

TABLE 2Summary of Groundwater Analytical Results - Goodwill Industries Phase II

Southwest Corner of West Michigan Street and White River Parkway

Patriot Project No.: 1-14-1903

IDEM RISC Industrial DCLs

RCG = Remediation Closure Guide

TWSL = Tap Water Screening Level

VESL = Vapor Exposure Screening Level

All results reported in micrograms per liter (ug/L)

Notes

Constituent detected above IDEM RCG Industrial VESL's

NE = No Screening Level Established for Constituent

IDEM = Indiana Department of Environmental Management

BRL - Below Laboratory Reporting Limit

Indianapolis, Indiana

Constituent detected above Laboratory Reporting Limit

Constituent detected above IDEM RISC RDCLs

Constituent detected above IDEM RISC IDCLs

Constituent detected above IDEM RCG Residential TWSL's

Constituent detected above IDEM RCG Residential VESL's

VOCs

IDEM RCG Residential TWSLs

IDEM RCG Residential VESLs

IDEM RCG Industrial VESLs

Reference 47

ATTACHMENT D

LABORATORY ANALYTICAL REPORT

Reference 47

#=CL#

January 13, 2015

LIMS USE: FR - ANTHONY NICKELS

LIMS OBJECT ID: 50110120

50110120

Project:

Pace Project No.:

RE:

Mr. Anthony NickelsPatriot Engineering and Environmental6330 E 75th StIndianapolis, IN 46250

Goodwill Industries

Dear Mr. Nickels:

Enclosed are the analytical results for sample(s) received by the laboratory on January 02, 2015.The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Tina Sayer

[email protected]

Project Manager

Enclosures

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.

7726 Moller Road

Indianapolis, IN 46268

(317)228-3100


Not NELAP Accredited

4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 1 of 40

Reference 47

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

50110120

Goodwill Industries

Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074Indiana Certification #: C-49-06Kansas Certification #: E-10247

Kentucky UST Certification #: 0042Louisiana/NELAP Certification #: 04076Ohio VAP Certification #: CL-0065West Virginia Certification #: 330





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Reference 47

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

50110120

Goodwill Industries

Lab ID Sample ID Matrix Date Collected Date Received

50110120001 SB-1 GW 30' Water 12/30/14 14:10 01/02/15 12:20

50110120002 SB-1 GW 55' Water 12/30/14 14:15 01/02/15 12:20

50110120003 SB-2 GW 27' Water 12/31/14 09:45 01/02/15 12:20

50110120004 SB-2 GW 47' Water 12/31/14 09:50 01/02/15 12:20

50110120005 SB-3 GW 30' Water 12/31/14 11:20 01/02/15 12:20

50110120006 SB-3 GW 55' Water 12/31/14 11:25 01/02/15 12:20





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Reference 47

#=SA#

SAMPLE ANALYTE COUNT

Pace Project No.:

Project:

50110120

Goodwill Industries

Lab ID Sample ID Method

Analytes

ReportedAnalysts

50110120001 SB-1 GW 30' EPA 6010 1LLB

EPA 8270 by SIM LVE 20CEM

EPA 8260 72RSW

50110120002 SB-1 GW 55' EPA 6010 1LLB


EPA 8260 72RSW

50110120003 SB-2 GW 27' EPA 6010 1LLB


EPA 8260 72RSW

50110120004 SB-2 GW 47' EPA 6010 1LLB


EPA 8260 72RSW

50110120005 SB-3 GW 30' EPA 6010 1LLB


EPA 8260 72RSW

50110120006 SB-3 GW 55' EPA 6010 1LLB


EPA 8260 72RSW





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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries

Sample: SB-1 GW 30' Lab ID: 50110120001 Collected: 12/30/14 14:10 Received: 01/02/15 12:20 Matrix: Water

Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit

Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP

Lead 1830 ug/L 01/06/15 11:53 7439-92-101/04/15 19:5050.0 1

Analytical Method: EPA 8270 by SIM LVE Preparation Method: EPA 35108270 MSSV PAHLV

Acenaphthene ND ug/L 01/05/15 22:31 83-32-901/05/15 09:081.2 1

Acenaphthylene ND ug/L 01/05/15 22:31 208-96-801/05/15 09:081.2 1

Anthracene ND ug/L 01/05/15 22:31 120-12-701/05/15 09:080.12 1

Benzo(a)anthracene ND ug/L 01/05/15 22:31 56-55-301/05/15 09:080.12 1

Benzo(a)pyrene ND ug/L 01/05/15 22:31 50-32-801/05/15 09:080.12 1

Benzo(b)fluoranthene ND ug/L 01/05/15 22:31 205-99-201/05/15 09:080.12 1

Benzo(g,h,i)perylene ND ug/L 01/05/15 22:31 191-24-201/05/15 09:080.12 1

Benzo(k)fluoranthene ND ug/L 01/05/15 22:31 207-08-901/05/15 09:080.12 1

Chrysene ND ug/L 01/05/15 22:31 218-01-901/05/15 09:080.62 1

Dibenz(a,h)anthracene ND ug/L 01/05/15 22:31 53-70-301/05/15 09:080.12 1

Fluoranthene ND ug/L 01/05/15 22:31 206-44-001/05/15 09:081.2 1

Fluorene ND ug/L 01/05/15 22:31 86-73-701/05/15 09:081.2 1

Indeno(1,2,3-cd)pyrene ND ug/L 01/05/15 22:31 193-39-501/05/15 09:080.12 1

1-Methylnaphthalene ND ug/L 01/05/15 22:31 90-12-001/05/15 09:081.2 1


Naphthalene ND ug/L 01/05/15 22:31 91-20-301/05/15 09:081.2 1

Phenanthrene ND ug/L 01/05/15 22:31 85-01-801/05/15 09:081.2 1

Pyrene ND ug/L 01/05/15 22:31 129-00-001/05/15 09:081.2 1

Surrogates2-Fluorobiphenyl (S) 33 %. 01/05/15 22:31 321-60-801/05/15 09:0821-114 1

p-Terphenyl-d14 (S) 52 %. 01/05/15 22:31 1718-51-001/05/15 09:0825-131 1

Analytical Method: EPA 82608260 MSV

Acetone ND ug/L 01/06/15 20:02 67-64-1100 1

Acrolein ND ug/L 01/06/15 20:02 107-02-850.0 1

Acrylonitrile ND ug/L 01/06/15 20:02 107-13-1100 1

Benzene ND ug/L 01/06/15 20:02 71-43-25.0 1

Bromobenzene ND ug/L 01/06/15 20:02 108-86-15.0 1

Bromochloromethane ND ug/L 01/06/15 20:02 74-97-55.0 1

Bromodichloromethane ND ug/L 01/06/15 20:02 75-27-45.0 1

Bromoform ND ug/L 01/06/15 20:02 75-25-25.0 1

Bromomethane ND ug/L 01/06/15 20:02 74-83-95.0 1

2-Butanone (MEK) ND ug/L 01/06/15 20:02 78-93-325.0 1

n-Butylbenzene ND ug/L 01/06/15 20:02 104-51-85.0 1

sec-Butylbenzene ND ug/L 01/06/15 20:02 135-98-85.0 1

tert-Butylbenzene ND ug/L 01/06/15 20:02 98-06-65.0 1

Carbon disulfide ND ug/L 01/06/15 20:02 75-15-010.0 1

Carbon tetrachloride ND ug/L 01/06/15 20:02 56-23-55.0 1

Chlorobenzene ND ug/L 01/06/15 20:02 108-90-75.0 1

Chloroethane ND ug/L 01/06/15 20:02 75-00-35.0 1

Chloroform ND ug/L 01/06/15 20:02 67-66-35.0 1

Chloromethane ND ug/L 01/06/15 20:02 74-87-35.0 1

2-Chlorotoluene ND ug/L 01/06/15 20:02 95-49-85.0 1



without the written consent of Pace Analytical Services, Inc..Date: 01/13/2015 08:53 AM


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4860 Blazer Parkway

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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries





Dibromochloromethane ND ug/L 01/06/15 20:02 124-48-15.0 1

1,2-Dibromoethane (EDB) ND ug/L 01/06/15 20:02 106-93-45.0 1

Dibromomethane ND ug/L 01/06/15 20:02 74-95-35.0 1

1,2-Dichlorobenzene ND ug/L 01/06/15 20:02 95-50-15.0 1



trans-1,4-Dichloro-2-butene ND ug/L 01/06/15 20:02 110-57-6100 1

Dichlorodifluoromethane ND ug/L 01/06/15 20:02 75-71-85.0 1

1,1-Dichloroethane ND ug/L 01/06/15 20:02 75-34-35.0 1


1,1-Dichloroethene ND ug/L 01/06/15 20:02 75-35-45.0 1

cis-1,2-Dichloroethene ND ug/L 01/06/15 20:02 156-59-25.0 1

trans-1,2-Dichloroethene ND ug/L 01/06/15 20:02 156-60-55.0 1

1,2-Dichloropropane ND ug/L 01/06/15 20:02 78-87-55.0 1



1,1-Dichloropropene ND ug/L 01/06/15 20:02 563-58-65.0 1

cis-1,3-Dichloropropene ND ug/L 01/06/15 20:02 10061-01-55.0 1

trans-1,3-Dichloropropene ND ug/L 01/06/15 20:02 10061-02-65.0 1

Ethylbenzene ND ug/L 01/06/15 20:02 100-41-45.0 1

Ethyl methacrylate ND ug/L 01/06/15 20:02 97-63-2100 1

Hexachloro-1,3-butadiene ND ug/L 01/06/15 20:02 87-68-35.0 1

n-Hexane ND ug/L 01/06/15 20:02 110-54-35.0 1

2-Hexanone ND ug/L 01/06/15 20:02 591-78-625.0 1

Iodomethane ND ug/L 01/06/15 20:02 74-88-410.0 1

Isopropylbenzene (Cumene) ND ug/L 01/06/15 20:02 98-82-85.0 1

p-Isopropyltoluene ND ug/L 01/06/15 20:02 99-87-65.0 1

Methylene Chloride ND ug/L 01/06/15 20:02 75-09-25.0 1

4-Methyl-2-pentanone (MIBK) ND ug/L 01/06/15 20:02 108-10-125.0 1

Methyl-tert-butyl ether ND ug/L 01/06/15 20:02 1634-04-44.0 1

n-Propylbenzene ND ug/L 01/06/15 20:02 103-65-15.0 1

Styrene ND ug/L 01/06/15 20:02 100-42-55.0 1

1,1,1,2-Tetrachloroethane ND ug/L 01/06/15 20:02 630-20-65.0 1


Tetrachloroethene 249 ug/L 01/06/15 20:02 127-18-45.0 1

Toluene ND ug/L 01/06/15 20:02 108-88-35.0 1

1,2,3-Trichlorobenzene ND ug/L 01/06/15 20:02 87-61-65.0 1


1,1,1-Trichloroethane ND ug/L 01/06/15 20:02 71-55-65.0 1


Trichloroethene ND ug/L 01/06/15 20:02 79-01-65.0 1

Trichlorofluoromethane ND ug/L 01/06/15 20:02 75-69-45.0 1

1,2,3-Trichloropropane ND ug/L 01/06/15 20:02 96-18-45.0 1

1,2,4-Trimethylbenzene ND ug/L 01/06/15 20:02 95-63-65.0 1


Vinyl acetate ND ug/L 01/06/15 20:02 108-05-450.0 1





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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries




Vinyl chloride ND ug/L 01/06/15 20:02 75-01-42.0 1

Xylene (Total) ND ug/L 01/06/15 20:02 1330-20-710.0 1

SurrogatesDibromofluoromethane (S) 103 %. 01/06/15 20:02 1868-53-7 HS,pH79-116 1

4-Bromofluorobenzene (S) 95 %. 01/06/15 20:02 460-00-480-114 1

Toluene-d8 (S) 97 %. 01/06/15 20:02 2037-26-581-110 1





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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries




Lead 5420 ug/L 01/06/15 11:56 7439-92-101/04/15 19:50100 1










Chrysene ND ug/L 01/05/15 22:49 218-01-901/05/15 09:080.83 1



Fluorene ND ug/L 01/05/15 22:49 86-73-701/05/15 09:081.7 1






Pyrene ND ug/L 01/05/15 22:49 129-00-001/05/15 09:081.7 1


p-Terphenyl-d14 (S) 59 %. 01/05/15 22:49 1718-51-001/05/15 09:0825-131 1


Acetone ND ug/L 01/06/15 20:35 67-64-1100 1

Acrolein ND ug/L 01/06/15 20:35 107-02-850.0 1


Benzene ND ug/L 01/06/15 20:35 71-43-25.0 1




Bromoform ND ug/L 01/06/15 20:35 75-25-25.0 1

















7726 Moller Road


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4860 Blazer Parkway

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Page 8 of 40

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries



























n-Hexane ND ug/L 01/06/15 20:35 110-54-35.0 1

2-Hexanone ND ug/L 01/06/15 20:35 591-78-625.0 1








Styrene ND ug/L 01/06/15 20:35 100-42-55.0 1



Tetrachloroethene 87.5 ug/L 01/06/15 20:35 127-18-45.0 1

Toluene ND ug/L 01/06/15 20:35 108-88-35.0 1















7726 Moller Road


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4860 Blazer Parkway

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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries








Toluene-d8 (S) 101 %. 01/06/15 20:35 2037-26-581-110 1





7726 Moller Road


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4860 Blazer Parkway

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Page 10 of 40

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries




Lead 3390 ug/L 01/06/15 11:59 7439-92-101/04/15 19:5050.0 1










Chrysene ND ug/L 01/06/15 04:42 218-01-901/05/15 12:580.50 1



Fluorene ND ug/L 01/06/15 04:42 86-73-701/05/15 12:581.0 1






Pyrene ND ug/L 01/06/15 04:42 129-00-001/05/15 12:581.0 1


p-Terphenyl-d14 (S) 82 %. 01/06/15 04:42 1718-51-001/05/15 12:5825-131 1


Acetone ND ug/L 01/06/15 21:07 67-64-1100 1

Acrolein ND ug/L 01/06/15 21:07 107-02-850.0 1


Benzene ND ug/L 01/06/15 21:07 71-43-25.0 1




Bromoform ND ug/L 01/06/15 21:07 75-25-25.0 1

















7726 Moller Road


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4860 Blazer Parkway

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Page 11 of 40

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries



























n-Hexane ND ug/L 01/06/15 21:07 110-54-35.0 1

2-Hexanone ND ug/L 01/06/15 21:07 591-78-625.0 1








Styrene ND ug/L 01/06/15 21:07 100-42-55.0 1




Toluene ND ug/L 01/06/15 21:07 108-88-35.0 1















7726 Moller Road


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Page 12 of 40

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries








Toluene-d8 (S) 105 %. 01/06/15 21:07 2037-26-581-110 1





7726 Moller Road


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4860 Blazer Parkway

Dublin, OH 43017

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Page 13 of 40

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries




Lead 4480 ug/L 01/06/15 12:02 7439-92-101/04/15 19:50100 1










Chrysene ND ug/L 01/06/15 05:00 218-01-901/05/15 12:581.0 1



Fluorene ND ug/L 01/06/15 05:00 86-73-701/05/15 12:582.0 1






Pyrene ND ug/L 01/06/15 05:00 129-00-001/05/15 12:582.0 1


p-Terphenyl-d14 (S) 78 %. 01/06/15 05:00 1718-51-001/05/15 12:5825-131 1


Acetone ND ug/L 01/06/15 21:40 67-64-1100 1

Acrolein ND ug/L 01/06/15 21:40 107-02-850.0 1


Benzene ND ug/L 01/06/15 21:40 71-43-25.0 1




Bromoform ND ug/L 01/06/15 21:40 75-25-25.0 1

















7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 14 of 40

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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries



























n-Hexane ND ug/L 01/06/15 21:40 110-54-35.0 1

2-Hexanone ND ug/L 01/06/15 21:40 591-78-625.0 1








Styrene ND ug/L 01/06/15 21:40 100-42-55.0 1




Toluene ND ug/L 01/06/15 21:40 108-88-35.0 1





Trichloroethene 7.3 ug/L 01/06/15 21:40 79-01-65.0 1










7726 Moller Road


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4860 Blazer Parkway

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Page 15 of 40

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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries








Toluene-d8 (S) 102 %. 01/06/15 21:40 2037-26-581-110 1





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 16 of 40

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

Goodwill Industries




Lead 634 ug/L 01/06/15 12:05 7439-92-101/04/15 19:5010.0 1










Chrysene ND ug/L 01/06/15 05:17 218-01-901/05/15 12:580.50 1



Fluorene ND ug/L 01/06/15 05:17 86-73-701/05/15 12:581.0 1






Pyrene ND ug/L 01/06/15 05:17 129-00-001/05/15 12:581.0 1


p-Terphenyl-d14 (S) 77 %. 01/06/15 05:17 1718-51-001/05/15 12:5825-131 1


Acetone ND ug/L 01/06/15 22:13 67-64-1100 1

Acrolein ND ug/L 01/06/15 22:13 107-02-850.0 1


Benzene ND ug/L 01/06/15 22:13 71-43-25.0 1




Bromoform ND ug/L 01/06/15 22:13 75-25-25.0 1

















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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

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n-Hexane ND ug/L 01/06/15 22:13 110-54-35.0 1

2-Hexanone ND ug/L 01/06/15 22:13 591-78-625.0 1








Styrene ND ug/L 01/06/15 22:13 100-42-55.0 1




Toluene ND ug/L 01/06/15 22:13 108-88-35.0 1















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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

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Toluene-d8 (S) 107 %. 01/06/15 22:13 2037-26-581-110 1





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Reference 47

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ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

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Lead 1590 ug/L 01/06/15 12:26 7439-92-101/04/15 19:5050.0 1










Chrysene ND ug/L 01/06/15 05:35 218-01-901/05/15 12:580.50 1



Fluorene ND ug/L 01/06/15 05:35 86-73-701/05/15 12:581.0 1






Pyrene ND ug/L 01/06/15 05:35 129-00-001/05/15 12:581.0 1


p-Terphenyl-d14 (S) 79 %. 01/06/15 05:35 1718-51-001/05/15 12:5825-131 1


Acetone ND ug/L 01/07/15 02:01 67-64-1100 1

Acrolein ND ug/L 01/07/15 02:01 107-02-850.0 1


Benzene ND ug/L 01/07/15 02:01 71-43-25.0 1




Bromoform ND ug/L 01/07/15 02:01 75-25-25.0 1

















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Reference 47

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ANALYTICAL RESULTS

Pace Project No.:

Project:

50110120

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n-Hexane ND ug/L 01/07/15 02:01 110-54-35.0 1

2-Hexanone ND ug/L 01/07/15 02:01 591-78-625.0 1








Styrene ND ug/L 01/07/15 02:01 100-42-55.0 1




Toluene ND ug/L 01/07/15 02:01 108-88-35.0 1















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Reference 47

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ANALYTICAL RESULTS

Pace Project No.:

Project:

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Toluene-d8 (S) 100 %. 01/07/15 02:01 2037-26-581-110 1





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Reference 47

#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

50110120

Goodwill Industries

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

MPRP/15013

EPA 3010

EPA 6010

6010 MET

Associated Lab Samples: 50110120001, 50110120002, 50110120003, 50110120004, 50110120005, 50110120006

Parameter Units

Blank

Result

Reporting

Limit Qualifiers

METHOD BLANK: 1217590

Associated Lab Samples: 50110120001, 50110120002, 50110120003, 50110120004, 50110120005, 50110120006

Matrix: Water

Analyzed

Lead ug/L ND 10.0 01/06/15 11:45

Parameter Units

LCS

Result

% Rec

Limits Qualifiers% RecConc.

1217591LABORATORY CONTROL SAMPLE:

LCSSpike

Lead ug/L 9611000 96 80-120

Parameter Units

MS

Result

% Rec

Limits Qual% RecConc.

1217592MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpike

Result

50110120005

1217593

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L M01000 74 75-12578 3 201000634 1370 1410





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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

Goodwill Industries


QC Batch:

QC Batch Method:

Analysis Method:


MSV/72552

EPA 8260

EPA 8260

8260 MSV

Associated Lab Samples: 50110120001, 50110120002, 50110120003, 50110120004, 50110120005

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/06/15 13:29

1,1,1-Trichloroethane ug/L ND 5.0 01/06/15 13:29



1,1-Dichloroethane ug/L ND 5.0 01/06/15 13:29

1,1-Dichloroethene ug/L ND 5.0 01/06/15 13:29

1,1-Dichloropropene ug/L ND 5.0 01/06/15 13:29

1,2,3-Trichlorobenzene ug/L ND 5.0 01/06/15 13:29

1,2,3-Trichloropropane ug/L ND 5.0 01/06/15 13:29


1,2,4-Trimethylbenzene ug/L ND 5.0 01/06/15 13:29

1,2-Dibromoethane (EDB) ug/L ND 5.0 01/06/15 13:29

1,2-Dichlorobenzene ug/L ND 5.0 01/06/15 13:29


1,2-Dichloropropane ug/L ND 5.0 01/06/15 13:29






2-Butanone (MEK) ug/L ND 25.0 01/06/15 13:29

2-Chlorotoluene ug/L ND 5.0 01/06/15 13:29

2-Hexanone ug/L ND 25.0 01/06/15 13:29


4-Methyl-2-pentanone (MIBK) ug/L ND 25.0 01/06/15 13:29

Acetone ug/L ND 100 01/06/15 13:29

Acrolein ug/L ND 50.0 01/06/15 13:29

Acrylonitrile ug/L ND 100 01/06/15 13:29

Benzene ug/L ND 5.0 01/06/15 13:29

Bromobenzene ug/L ND 5.0 01/06/15 13:29

Bromochloromethane ug/L ND 5.0 01/06/15 13:29

Bromodichloromethane ug/L ND 5.0 01/06/15 13:29

Bromoform ug/L ND 5.0 01/06/15 13:29

Bromomethane ug/L ND 5.0 01/06/15 13:29

Carbon disulfide ug/L ND 10.0 01/06/15 13:29

Carbon tetrachloride ug/L ND 5.0 01/06/15 13:29

Chlorobenzene ug/L ND 5.0 01/06/15 13:29

Chloroethane ug/L ND 5.0 01/06/15 13:29

Chloroform ug/L ND 5.0 01/06/15 13:29

Chloromethane ug/L ND 5.0 01/06/15 13:29

cis-1,2-Dichloroethene ug/L ND 5.0 01/06/15 13:29





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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

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Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

cis-1,3-Dichloropropene ug/L ND 5.0 01/06/15 13:29

Dibromochloromethane ug/L ND 5.0 01/06/15 13:29

Dibromomethane ug/L ND 5.0 01/06/15 13:29

Dichlorodifluoromethane ug/L ND 5.0 01/06/15 13:29

Ethyl methacrylate ug/L ND 100 01/06/15 13:29

Ethylbenzene ug/L ND 5.0 01/06/15 13:29

Hexachloro-1,3-butadiene ug/L ND 5.0 01/06/15 13:29

Iodomethane ug/L ND 10.0 01/06/15 13:29

Isopropylbenzene (Cumene) ug/L ND 5.0 01/06/15 13:29

Methyl-tert-butyl ether ug/L ND 4.0 01/06/15 13:29

Methylene Chloride ug/L ND 5.0 01/06/15 13:29

n-Butylbenzene ug/L ND 5.0 01/06/15 13:29

n-Hexane ug/L ND 5.0 01/06/15 13:29

n-Propylbenzene ug/L ND 5.0 01/06/15 13:29

p-Isopropyltoluene ug/L ND 5.0 01/06/15 13:29

sec-Butylbenzene ug/L ND 5.0 01/06/15 13:29

Styrene ug/L ND 5.0 01/06/15 13:29

tert-Butylbenzene ug/L ND 5.0 01/06/15 13:29

Tetrachloroethene ug/L ND 5.0 01/06/15 13:29

Toluene ug/L ND 5.0 01/06/15 13:29

trans-1,2-Dichloroethene ug/L ND 5.0 01/06/15 13:29

trans-1,3-Dichloropropene ug/L ND 5.0 01/06/15 13:29

trans-1,4-Dichloro-2-butene ug/L ND 100 01/06/15 13:29

Trichloroethene ug/L ND 5.0 01/06/15 13:29

Trichlorofluoromethane ug/L ND 5.0 01/06/15 13:29

Vinyl acetate ug/L ND 50.0 01/06/15 13:29

Vinyl chloride ug/L ND 2.0 01/06/15 13:29

Xylene (Total) ug/L ND 10.0 01/06/15 13:29

4-Bromofluorobenzene (S) %. 100 80-114 01/06/15 13:29

Dibromofluoromethane (S) %. 98 79-116 01/06/15 13:29

Toluene-d8 (S) %. 101 81-110 01/06/15 13:29

Parameter Units

LCS

Result

% Rec



LCSSpike

1,1,1,2-Tetrachloroethane ug/L 51.650 103 61-135

1,1,1-Trichloroethane ug/L 50.150 100 71-129



1,1-Dichloroethane ug/L 47.150 94 75-130

1,1-Dichloroethene ug/L 50.250 100 68-127

1,1-Dichloropropene ug/L 54.350 109 78-130

1,2,3-Trichlorobenzene ug/L 62.950 126 70-130

1,2,3-Trichloropropane ug/L 55.450 111 58-142





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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

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Parameter Units

LCS

Result

% Rec



LCSSpike


1,2,4-Trimethylbenzene ug/L 50.450 101 69-127

1,2-Dibromoethane (EDB) ug/L 51.550 103 76-125

1,2-Dichlorobenzene ug/L 50.650 101 75-123


1,2-Dichloropropane ug/L 53.150 106 74-121






2-Butanone (MEK) ug/L 276250 110 58-139

2-Chlorotoluene ug/L 49.750 99 74-122

2-Hexanone ug/L 300250 120 54-140


4-Methyl-2-pentanone (MIBK) ug/L 255250 102 58-138

Acetone ug/L 354250 142 49-150

Acrolein ug/L 2510 L31000 251 41-200

Acrylonitrile ug/L 9931000 99 63-137

Benzene ug/L 48.150 96 74-122

Bromobenzene ug/L 52.050 104 72-127

Bromochloromethane ug/L 50.550 101 63-132

Bromodichloromethane ug/L 51.250 102 62-136

Bromoform ug/L 55.450 111 44-134

Bromomethane ug/L 69.050 138 22-181

Carbon disulfide ug/L 96.0100 96 59-132

Carbon tetrachloride ug/L 54.350 109 56-137

Chlorobenzene ug/L 49.550 99 78-123

Chloroethane ug/L 53.850 108 60-144

Chloroform ug/L 50.350 101 78-126

Chloromethane ug/L 51.050 102 42-134

cis-1,2-Dichloroethene ug/L 51.950 104 75-122

cis-1,3-Dichloropropene ug/L 55.550 111 64-126

Dibromochloromethane ug/L 54.850 110 58-128

Dibromomethane ug/L 48.550 97 73-125

Dichlorodifluoromethane ug/L 53.950 108 35-181

Ethyl methacrylate ug/L 211200 105 69-133

Ethylbenzene ug/L 51.150 102 66-133

Hexachloro-1,3-butadiene ug/L 53.450 107 59-145

Iodomethane ug/L 99.8100 100 21-170

Isopropylbenzene (Cumene) ug/L 52.950 106 69-124

Methyl-tert-butyl ether ug/L 96.3100 96 69-122

Methylene Chloride ug/L 52.150 104 68-132

n-Butylbenzene ug/L 59.950 120 70-126

n-Hexane ug/L 49.050 98 51-125

n-Propylbenzene ug/L 52.850 106 71-122

p-Isopropyltoluene ug/L 54.050 108 72-132





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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

Goodwill Industries


Parameter Units

LCS

Result

% Rec



LCSSpike

sec-Butylbenzene ug/L 52.450 105 70-128

Styrene ug/L 52.650 105 74-126

tert-Butylbenzene ug/L 40.250 80 51-118

Tetrachloroethene ug/L 50.450 101 69-130

Toluene ug/L 51.750 103 72-122

trans-1,2-Dichloroethene ug/L 45.750 91 72-124

trans-1,3-Dichloropropene ug/L 55.550 111 64-121

trans-1,4-Dichloro-2-butene ug/L 225200 112 56-133

Trichloroethene ug/L 54.150 108 76-126

Trichlorofluoromethane ug/L 60.150 120 76-149

Vinyl acetate ug/L 210200 105 45-151

Vinyl chloride ug/L 45.550 91 59-126

Xylene (Total) ug/L 152150 101 70-124

4-Bromofluorobenzene (S) %. 100 80-114

Dibromofluoromethane (S) %. 99 79-116

Toluene-d8 (S) %. 98 81-110





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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

Goodwill Industries


QC Batch:

QC Batch Method:

Analysis Method:


MSV/72553

EPA 8260

EPA 8260

8260 MSV

Associated Lab Samples: 50110120006

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed























2-Hexanone ug/L ND 25.0 01/06/15 13:29



Acetone ug/L ND 100 01/06/15 13:29

Acrolein ug/L ND 50.0 01/06/15 13:29


Benzene ug/L ND 5.0 01/06/15 13:29




Bromoform ug/L ND 5.0 01/06/15 13:29













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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

Goodwill Industries


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed













n-Hexane ug/L ND 5.0 01/06/15 13:29




Styrene ug/L ND 5.0 01/06/15 13:29



Toluene ug/L ND 5.0 01/06/15 13:29











Toluene-d8 (S) %. 101 81-110 01/06/15 13:29

Parameter Units

LCS

Result

% Rec



LCSSpike














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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

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Parameter Units

LCS

Result

% Rec



LCSSpike












2-Butanone (MEK) ug/L 276250 110 58-139


2-Hexanone ug/L 300250 120 54-140



Acetone ug/L 354250 142 49-150

Acrolein ug/L 2510 L31000 251 41-200


Benzene ug/L 48.150 96 74-122




Bromoform ug/L 55.450 111 44-134






Chloroform ug/L 50.350 101 78-126










Iodomethane ug/L 99.8100 100 21-170





n-Hexane ug/L 49.050 98 51-125







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Reference 47

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Pace Project No.:

Project:

50110120

Goodwill Industries


Parameter Units

LCS

Result

% Rec



LCSSpike


Styrene ug/L 52.650 105 74-126



Toluene ug/L 51.750 103 72-122








Xylene (Total) ug/L 152150 101 70-124



Toluene-d8 (S) %. 98 81-110





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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

Goodwill Industries


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/37956

EPA 3510

EPA 8270 by SIM LVE

8270 Water PAH LV by SIM MSSV

Associated Lab Samples: 50110120001, 50110120002

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

1-Methylnaphthalene ug/L ND 1.0 01/05/15 17:31


Acenaphthene ug/L ND 1.0 01/05/15 17:31

Acenaphthylene ug/L ND 1.0 01/05/15 17:31

Anthracene ug/L ND 0.10 01/05/15 17:31

Benzo(a)anthracene ug/L ND 0.10 01/05/15 17:31

Benzo(a)pyrene ug/L ND 0.10 01/05/15 17:31

Benzo(b)fluoranthene ug/L ND 0.10 01/05/15 17:31

Benzo(g,h,i)perylene ug/L ND 0.10 01/05/15 17:31

Benzo(k)fluoranthene ug/L ND 0.10 01/05/15 17:31

Chrysene ug/L ND 0.50 01/05/15 17:31

Dibenz(a,h)anthracene ug/L ND 0.10 01/05/15 17:31

Fluoranthene ug/L ND 1.0 01/05/15 17:31

Fluorene ug/L ND 1.0 01/05/15 17:31

Indeno(1,2,3-cd)pyrene ug/L ND 0.10 01/05/15 17:31

Naphthalene ug/L ND 1.0 01/05/15 17:31

Phenanthrene ug/L ND 1.0 01/05/15 17:31

Pyrene ug/L ND 1.0 01/05/15 17:31

2-Fluorobiphenyl (S) %. 38 21-114 01/05/15 17:31

p-Terphenyl-d14 (S) %. 62 25-131 01/05/15 17:31

Parameter Units

LCS

Result

% Rec



LCSSpike

1-Methylnaphthalene ug/L 5.010 50 29-112


Acenaphthene ug/L 5.010 50 39-117

Acenaphthylene ug/L 5.210 52 40-120

Anthracene ug/L 5.710 57 48-126

Benzo(a)anthracene ug/L 8.010 80 51-134

Benzo(a)pyrene ug/L 6.910 69 48-141

Benzo(b)fluoranthene ug/L 6.510 65 49-139

Benzo(g,h,i)perylene ug/L 6.010 60 44-134

Benzo(k)fluoranthene ug/L 6.710 67 48-140

Chrysene ug/L 7.610 76 53-136

Dibenz(a,h)anthracene ug/L 6.210 62 44-132

Fluoranthene ug/L 6.410 64 50-135

Fluorene ug/L 5.610 56 44-124

Indeno(1,2,3-cd)pyrene ug/L 6.410 64 45-132

Naphthalene ug/L 4.810 48 30-112





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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

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Parameter Units

LCS

Result

% Rec



LCSSpike

Phenanthrene ug/L 5.710 57 47-128

Pyrene ug/L 7.510 75 50-134

2-Fluorobiphenyl (S) %. 37 21-114

p-Terphenyl-d14 (S) %. 64 25-131

Parameter Units

MS

Result

% Rec



MSSpike

Result

50110077013

1217617

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

1-Methylnaphthalene ug/L 10 48 10-13541 16 2010ND 4.8 4.1


Acenaphthene ug/L 10 45 28-11639 14 2010ND 4.8 4.1

Acenaphthylene ug/L 10 49 34-11543 14 2010ND 4.9 4.3

Anthracene ug/L 10 47 39-12140 15 20100.23 5.0 4.3

Benzo(a)anthracene ug/L 10 63 31-12755 14 20100.42 6.8 5.9

Benzo(a)pyrene ug/L 10 38 10-12136 4 20100.13 3.9 3.8

Benzo(b)fluoranthene ug/L 10 40 10-11939 4 2010ND 4.1 3.9

Benzo(g,h,i)perylene ug/L 10 22 10-10820 9 2010ND 2.2 2.0

Benzo(k)fluoranthene ug/L 10 32 10-11833 3 2010ND 3.2 3.3

Chrysene ug/L 10 55 32-12748 13 20100.57 6.1 5.4

Dibenz(a,h)anthracene ug/L 10 24 10-10422 10 2010ND 2.4 2.2

Fluoranthene ug/L 10 54 38-13146 15 2010ND 5.5 4.8

Fluorene ug/L 10 50 33-12142 16 2010ND 5.4 4.6

Indeno(1,2,3-cd)pyrene ug/L 10 25 10-10823 6 2010ND 2.5 2.3

Naphthalene ug/L 10 46 16-11940 15 2010ND 4.6 4.0

Phenanthrene ug/L 10 48 32-13041 15 2010ND 4.8 4.1

Pyrene ug/L 10 61 39-13151 16 2010ND 6.7 5.7


p-Terphenyl-d14 (S) %. 45 25-13142





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Page 33 of 40

Reference 47

#=QC#


Pace Project No.:

Project:

50110120

Goodwill Industries


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/37960

EPA 3510

EPA 8270 by SIM LVE


Associated Lab Samples: 50110120003, 50110120004, 50110120005, 50110120006

Parameter Units

Blank

Result

Reporting

Limit Qualifiers


Associated Lab Samples: 50110120003, 50110120004, 50110120005, 50110120006

Matrix: Water

Analyzed











Chrysene ug/L ND 0.50 01/06/15 00:35



Fluorene ug/L ND 1.0 01/06/15 00:35




Pyrene ug/L ND 1.0 01/06/15 00:35


p-Terphenyl-d14 (S) %. 87 25-131 01/06/15 00:35

Parameter Units

LCS

Result

% Rec



LCSSpike











Chrysene ug/L 9.110 91 53-136



Fluorene ug/L 8.210 82 44-124







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Reference 47

#=QC#


Pace Project No.:

Project:

50110120

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Parameter Units

LCS

Result

% Rec



LCSSpike


Pyrene ug/L 9.110 91 50-134


p-Terphenyl-d14 (S) %. 77 25-131





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Reference 47

#=QL#

QUALIFIERS

Pace Project No.:

Project:

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DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.

ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

ANALYTE QUALIFIERS

Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS

Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0

Post-analysis pH measurement indicates insufficient VOA sample preservation.pH





7726 Moller Road


(317)228-3100



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(614)486-5421

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Reference 47

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

50110120

Goodwill Industries

Lab ID Sample ID QC Batch Method QC Batch Analytical Method

Analytical

Batch

50110120001 MPRP/15013 ICP/18033SB-1 GW 30' EPA 3010 EPA 6010






50110120001 OEXT/37956 MSSV/16938SB-1 GW 30' EPA 3510 EPA 8270 by SIM LVE






50110120001 MSV/72552SB-1 GW 30' EPA 8260

50110120002 MSV/72552SB-1 GW 55' EPA 8260

50110120003 MSV/72552SB-2 GW 27' EPA 8260

50110120004 MSV/72552SB-2 GW 47' EPA 8260

50110120005 MSV/72552SB-3 GW 30' EPA 8260

50110120006 MSV/72553SB-3 GW 55' EPA 8260





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Reference 47

of 40

Reference 47

#=CL#

February 04, 2015

LIMS USE: FR - ANTHONY NICKELS

LIMS OBJECT ID: 50111605

50111605

Project:

Pace Project No.:

RE:

Mr. Anthony NickelsPatriot Engineering and Environmental6330 E 75th StIndianapolis, IN 46250

Goodwill Phase

Dear Mr. Nickels:

Enclosed are the analytical results for sample(s) received by the laboratory on January 28, 2015.The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Tina Sayer

[email protected]

Project Manager

Enclosures





7726 Moller Road


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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 1 of 78

Reference 47

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

50111605

Goodwill Phase

Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074Indiana Certification #: C-49-06Kansas Certification #:E-10177/ E-10247Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana/NELAP Certification #: 04076

Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148Pennsylvania Certification #: 68-05340Texas Certification #: T104704355-15-8West Virginia Certification #: 330Wisconsin Certification #: 999788130





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Reference 47

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

50111605

Goodwill Phase

Lab ID Sample ID Matrix Date Collected Date Received

50111605001 SB-4 30' Water 01/27/15 09:30 01/28/15 14:50

50111605002 SB-4 55' Water 01/27/15 09:40 01/28/15 14:50

50111605003 SB-6 30' Water 01/28/15 12:00 01/28/15 14:50

50111605004 SB-6 55' Water 01/28/15 12:10 01/28/15 14:50

50111605005 SB-5 31' Water 01/28/15 10:50 01/28/15 14:50

50111605006 SB-5 55' Water 01/28/15 11:00 01/28/15 14:50

50111605007 SB-7 30' Water 01/27/15 16:50 01/28/15 14:50

50111605008 SB-7 55' Water 01/27/15 17:00 01/28/15 14:50

50111605009 SB-8 30' Water 01/27/15 14:20 01/28/15 14:50

50111605010 SB-8 55' Water 01/27/15 14:30 01/28/15 14:50

50111605011 SB-5 8-10' Solid 01/28/15 10:20 01/28/15 14:50

50111605012 SB-7 8-10' Solid 01/27/15 16:00 01/28/15 14:50

50111605013 SB-8 8-10' Solid 01/27/15 14:00 01/28/15 14:50

50111605014 Trip Blank Water 01/27/15 08:00 01/28/15 14:50





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Dublin, OH 43017

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Page 3 of 78

Reference 47

#=SA#


Pace Project No.:

Project:

50111605

Goodwill Phase


Analytes

ReportedAnalysts

50111605001 SB-4 30' EPA 8270 by SIM LVE 20CEM

EPA 8260 72DAE


EPA 8260 72DAE


EPA 8260 72DAE


EPA 8260 72DAE

50111605005 SB-5 31' EPA 6010 1JPK

EPA 6010 1FRW


EPA 8260 72DAE


EPA 8260 72DAE

50111605007 SB-7 30' EPA 6010 1JPK

EPA 6010 1FRW


EPA 8260 72DAE


EPA 8260 72DAE

50111605009 SB-8 30' EPA 6010 1JPK

EPA 6010 1FRW


EPA 8260 72DAE


EPA 8260 72DAE

50111605011 SB-5 8-10' EPA 6010 1JPK

EPA 8270 by SIM 20CEM

EPA 8260 73JLZ

ASTM D2974-87 1MLS

50111605012 SB-7 8-10' EPA 6010 1JPK


EPA 8260 73JLZ

ASTM D2974-87 1MLS

50111605013 SB-8 8-10' EPA 6010 1JPK


EPA 8260 73JLZ





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Dublin, OH 43017

(614)486-5421

Page 4 of 78

Reference 47

#=SA#


Pace Project No.:

Project:

50111605

Goodwill Phase


Analytes

ReportedAnalysts

ASTM D2974-87 1MLS

50111605014 Trip Blank EPA 8260 72DAE





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Dublin, OH 43017

(614)486-5421

Page 5 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase

Sample: SB-4 30' Lab ID: 50111605001 Collected: 01/27/15 09:30 Received: 01/28/15 14:50 Matrix: Water











Chrysene ND ug/L 01/29/15 23:15 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/29/15 23:15 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/29/15 23:15 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 57 %. 01/29/15 23:15 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/29/15 20:39 67-64-1100 1

Acrolein ND ug/L 01/29/15 20:39 107-02-850.0 1


Benzene ND ug/L 01/29/15 20:39 71-43-25.0 1




Bromoform ND ug/L 01/29/15 20:39 75-25-25.0 1



















without the written consent of Pace Analytical Services, Inc..Date: 02/04/2015 03:21 PM


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Page 6 of 78

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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase























n-Hexane ND ug/L 01/29/15 20:39 110-54-35.0 1

2-Hexanone ND ug/L 01/29/15 20:39 591-78-625.0 1








Styrene ND ug/L 01/29/15 20:39 100-42-55.0 1




Toluene ND ug/L 01/29/15 20:39 108-88-35.0 1













SurrogatesDibromofluoromethane (S) 94 %. 01/29/15 20:39 1868-53-7 HS79-116 1





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Page 7 of 78

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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase




Surrogates4-Bromofluorobenzene (S) 100 %. 01/29/15 20:39 460-00-480-114 1

Toluene-d8 (S) 102 %. 01/29/15 20:39 2037-26-581-110 1





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Page 8 of 78

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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase












Chrysene ND ug/L 01/29/15 23:32 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/29/15 23:32 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/29/15 23:32 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 65 %. 01/29/15 23:32 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/29/15 21:44 67-64-1100 1

Acrolein ND ug/L 01/29/15 21:44 107-02-850.0 1


Benzene ND ug/L 01/29/15 21:44 71-43-25.0 1




Bromoform ND ug/L 01/29/15 21:44 75-25-25.0 1





















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Dublin, OH 43017

(614)486-5421

Page 9 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase























n-Hexane ND ug/L 01/29/15 21:44 110-54-35.0 1

2-Hexanone ND ug/L 01/29/15 21:44 591-78-625.0 1








Styrene ND ug/L 01/29/15 21:44 100-42-55.0 1




Toluene ND ug/L 01/29/15 21:44 108-88-35.0 1













SurrogatesDibromofluoromethane (S) 94 %. 01/29/15 21:44 1868-53-7 HS79-116 1





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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Toluene-d8 (S) 101 %. 01/29/15 21:44 2037-26-581-110 1





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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 11 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase












Chrysene ND ug/L 01/30/15 01:36 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/30/15 01:36 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/30/15 01:36 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 90 %. 01/30/15 01:36 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 13:52 67-64-1100 1

Acrolein ND ug/L 01/30/15 13:52 107-02-850.0 1


Benzene ND ug/L 01/30/15 13:52 71-43-25.0 1




Bromoform ND ug/L 01/30/15 13:52 75-25-25.0 1





















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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 12 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase












cis-1,2-Dichloroethene 10.3 ug/L 01/30/15 13:52 156-59-25.0 1











n-Hexane ND ug/L 01/30/15 13:52 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 13:52 591-78-625.0 1








Styrene ND ug/L 01/30/15 13:52 100-42-55.0 1




Toluene ND ug/L 01/30/15 13:52 108-88-35.0 1













SurrogatesDibromofluoromethane (S) 97 %. 01/30/15 13:52 1868-53-779-116 1





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#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Toluene-d8 (S) 103 %. 01/30/15 13:52 2037-26-581-110 1





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Dublin, OH 43017

(614)486-5421

Page 14 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase












Chrysene ND ug/L 01/30/15 01:54 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/30/15 01:54 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/30/15 01:54 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 61 %. 01/30/15 01:54 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 14:25 67-64-1200 2

Acrolein ND ug/L 01/30/15 14:25 107-02-8100 2


Benzene ND ug/L 01/30/15 14:25 71-43-210.0 2




Bromoform ND ug/L 01/30/15 14:25 75-25-210.0 2





















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Dublin, OH 43017

(614)486-5421

Page 15 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase























n-Hexane ND ug/L 01/30/15 14:25 110-54-310.0 2

2-Hexanone ND ug/L 01/30/15 14:25 591-78-650.0 2








Styrene ND ug/L 01/30/15 14:25 100-42-510.0 2




Toluene ND ug/L 01/30/15 14:25 108-88-310.0 2










Vinyl acetate ND ug/L 01/30/15 14:25 108-05-4100 2



SurrogatesDibromofluoromethane (S) 92 %. 01/30/15 14:25 1868-53-7 2d79-116 2





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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Toluene-d8 (S) 99 %. 01/30/15 14:25 2037-26-581-110 2





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(614)486-5421

Page 17 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase




Lead 1020 ug/L 01/30/15 22:58 7439-92-101/30/15 07:1650.0 1

Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered

Lead, Dissolved ND ug/L 02/02/15 13:58 7439-92-102/02/15 07:2010.0 1










Chrysene ND ug/L 01/30/15 02:12 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/30/15 02:12 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/30/15 02:12 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 81 %. 01/30/15 02:12 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 14:58 67-64-1100 1

Acrolein ND ug/L 01/30/15 14:58 107-02-850.0 1


Benzene ND ug/L 01/30/15 14:58 71-43-25.0 1




Bromoform ND ug/L 01/30/15 14:58 75-25-25.0 1














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Dublin, OH 43017

(614)486-5421

Page 18 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase






























n-Hexane ND ug/L 01/30/15 14:58 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 14:58 591-78-625.0 1








Styrene ND ug/L 01/30/15 14:58 100-42-55.0 1



Tetrachloroethene ND ug/L 01/30/15 14:58 127-18-45.0 1

Toluene ND ug/L 01/30/15 14:58 108-88-35.0 1












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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase







Vinyl chloride 5.9 ug/L 01/30/15 14:58 75-01-42.0 1




Toluene-d8 (S) 105 %. 01/30/15 14:58 2037-26-581-110 1





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Dublin, OH 43017

(614)486-5421

Page 20 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase












Chrysene ND ug/L 01/30/15 02:30 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/30/15 02:30 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/30/15 02:30 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 78 %. 01/30/15 02:30 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 15:30 67-64-1100 1

Acrolein ND ug/L 01/30/15 15:30 107-02-850.0 1


Benzene ND ug/L 01/30/15 15:30 71-43-25.0 1




Bromoform ND ug/L 01/30/15 15:30 75-25-25.0 1





















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Dublin, OH 43017

(614)486-5421

Page 21 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase























n-Hexane ND ug/L 01/30/15 15:30 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 15:30 591-78-625.0 1








Styrene ND ug/L 01/30/15 15:30 100-42-55.0 1




Toluene ND ug/L 01/30/15 15:30 108-88-35.0 1











Vinyl chloride 4.3 ug/L 01/30/15 15:30 75-01-42.0 1







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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Toluene-d8 (S) 103 %. 01/30/15 15:30 2037-26-581-110 1





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Dublin, OH 43017

(614)486-5421

Page 23 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase




Lead 984 ug/L 01/30/15 23:00 7439-92-101/30/15 07:1650.0 1












Chrysene ND ug/L 01/29/15 23:50 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/29/15 23:50 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/29/15 23:50 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 59 %. 01/29/15 23:50 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 16:03 67-64-1100 1

Acrolein ND ug/L 01/30/15 16:03 107-02-850.0 1


Benzene ND ug/L 01/30/15 16:03 71-43-25.0 1




Bromoform ND ug/L 01/30/15 16:03 75-25-25.0 1














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Dublin, OH 43017

(614)486-5421

Page 24 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase






























n-Hexane ND ug/L 01/30/15 16:03 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 16:03 591-78-625.0 1








Styrene ND ug/L 01/30/15 16:03 100-42-55.0 1




Toluene ND ug/L 01/30/15 16:03 108-88-35.0 1












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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 25 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase











Toluene-d8 (S) 101 %. 01/30/15 16:03 2037-26-581-110 1





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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 26 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase












Chrysene ND ug/L 01/30/15 00:08 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/30/15 00:08 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/30/15 00:08 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 62 %. 01/30/15 00:08 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 16:36 67-64-1100 1

Acrolein ND ug/L 01/30/15 16:36 107-02-850.0 1


Benzene ND ug/L 01/30/15 16:36 71-43-25.0 1




Bromoform ND ug/L 01/30/15 16:36 75-25-25.0 1





















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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 27 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase























n-Hexane ND ug/L 01/30/15 16:36 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 16:36 591-78-625.0 1








Styrene ND ug/L 01/30/15 16:36 100-42-55.0 1




Toluene ND ug/L 01/30/15 16:36 108-88-35.0 1


















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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 28 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Toluene-d8 (S) 100 %. 01/30/15 16:36 2037-26-581-110 1





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Dublin, OH 43017

(614)486-5421

Page 29 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase




Lead 649 ug/L 01/30/15 23:02 7439-92-101/30/15 07:1650.0 1












Chrysene ND ug/L 01/30/15 01:01 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/30/15 01:01 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/30/15 01:01 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 59 %. 01/30/15 01:01 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 17:08 67-64-1100 1

Acrolein ND ug/L 01/30/15 17:08 107-02-850.0 1


Benzene ND ug/L 01/30/15 17:08 71-43-25.0 1




Bromoform ND ug/L 01/30/15 17:08 75-25-25.0 1














7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 30 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase






























n-Hexane ND ug/L 01/30/15 17:08 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 17:08 591-78-625.0 1








Styrene ND ug/L 01/30/15 17:08 100-42-55.0 1




Toluene ND ug/L 01/30/15 17:08 108-88-35.0 1












7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 31 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase











Toluene-d8 (S) 100 %. 01/30/15 17:08 2037-26-581-110 1





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Dublin, OH 43017

(614)486-5421

Page 32 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase












Chrysene ND ug/L 01/30/15 01:19 218-01-901/29/15 13:180.50 1



Fluorene ND ug/L 01/30/15 01:19 86-73-701/29/15 13:181.0 1






Pyrene ND ug/L 01/30/15 01:19 129-00-001/29/15 13:181.0 1


p-Terphenyl-d14 (S) 50 %. 01/30/15 01:19 1718-51-001/29/15 13:1825-131 1


Acetone ND ug/L 01/30/15 17:41 67-64-1100 1

Acrolein ND ug/L 01/30/15 17:41 107-02-850.0 1


Benzene ND ug/L 01/30/15 17:41 71-43-25.0 1




Bromoform ND ug/L 01/30/15 17:41 75-25-25.0 1





















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(614)486-5421

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ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase























n-Hexane ND ug/L 01/30/15 17:41 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 17:41 591-78-625.0 1








Styrene ND ug/L 01/30/15 17:41 100-42-55.0 1




Toluene ND ug/L 01/30/15 17:41 108-88-35.0 1


















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ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Toluene-d8 (S) 99 %. 01/30/15 17:41 2037-26-581-110 1





7726 Moller Road


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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase

Sample: SB-5 8-10' Lab ID: 50111605011 Collected: 01/28/15 10:20 Received: 01/28/15 14:50 Matrix: Solid

Results reported on a "dry-weight" basis



Lead 6.8 mg/kg 02/02/15 21:47 7439-92-101/31/15 07:351.0 1

Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM

Acenaphthene 0.027 mg/kg 01/30/15 02:36 83-32-901/29/15 10:380.0056 1

Acenaphthylene 0.12 mg/kg 01/30/15 02:36 208-96-801/29/15 10:380.0056 1

Anthracene 0.14 mg/kg 01/30/15 02:36 120-12-701/29/15 10:380.0056 1

Benzo(a)anthracene 0.73 mg/kg 01/30/15 02:36 56-55-301/29/15 10:380.0056 1

Benzo(a)pyrene 0.62 mg/kg 01/30/15 02:36 50-32-801/29/15 10:380.0056 1

Benzo(b)fluoranthene 0.64 mg/kg 01/30/15 02:36 205-99-201/29/15 10:380.0056 1

Benzo(g,h,i)perylene 0.44 mg/kg 01/30/15 02:36 191-24-201/29/15 10:380.0056 1

Benzo(k)fluoranthene 0.51 mg/kg 01/30/15 02:36 207-08-901/29/15 10:380.0056 1

Chrysene 0.84 mg/kg 01/30/15 02:36 218-01-901/29/15 10:380.0056 1

Dibenz(a,h)anthracene 0.22 mg/kg 01/30/15 02:36 53-70-301/29/15 10:380.0056 1

Fluoranthene 1.1 mg/kg 01/30/15 02:36 206-44-001/29/15 10:380.0056 1

Fluorene 0.035 mg/kg 01/30/15 02:36 86-73-701/29/15 10:380.0056 1

Indeno(1,2,3-cd)pyrene 0.40 mg/kg 01/30/15 02:36 193-39-501/29/15 10:380.0056 1

1-Methylnaphthalene 0.021 mg/kg 01/30/15 02:36 90-12-001/29/15 10:380.0056 1


Naphthalene 0.076 mg/kg 01/30/15 02:36 91-20-301/29/15 10:380.0056 1

Phenanthrene 0.50 mg/kg 01/30/15 02:36 85-01-801/29/15 10:380.0056 1

Pyrene 1.1 mg/kg 01/30/15 02:36 129-00-001/29/15 10:380.0056 1


p-Terphenyl-d14 (S) 87 %. 01/30/15 02:36 1718-51-001/29/15 10:3832-111 1

Analytical Method: EPA 82608260 MSV 5035A VOA

Acetone ND mg/kg 02/03/15 12:01 67-64-10.11 1

Acrolein ND mg/kg 02/03/15 12:01 107-02-80.11 1

Acrylonitrile ND mg/kg 02/03/15 12:01 107-13-10.11 1

Benzene ND mg/kg 02/03/15 12:01 71-43-20.0056 1

Bromobenzene ND mg/kg 02/03/15 12:01 108-86-10.0056 1

Bromochloromethane ND mg/kg 02/03/15 12:01 74-97-50.0056 1

Bromodichloromethane ND mg/kg 02/03/15 12:01 75-27-40.0056 1

Bromoform ND mg/kg 02/03/15 12:01 75-25-20.0056 1

Bromomethane ND mg/kg 02/03/15 12:01 74-83-90.0056 1

2-Butanone (MEK) ND mg/kg 02/03/15 12:01 78-93-30.028 1

n-Butylbenzene ND mg/kg 02/03/15 12:01 104-51-80.0056 1

sec-Butylbenzene ND mg/kg 02/03/15 12:01 135-98-80.0056 1

tert-Butylbenzene ND mg/kg 02/03/15 12:01 98-06-60.0056 1

Carbon disulfide ND mg/kg 02/03/15 12:01 75-15-00.011 1

Carbon tetrachloride ND mg/kg 02/03/15 12:01 56-23-50.0056 1

Chlorobenzene ND mg/kg 02/03/15 12:01 108-90-70.0056 1

Chloroethane ND mg/kg 02/03/15 12:01 75-00-30.0056 1

Chloroform ND mg/kg 02/03/15 12:01 67-66-30.0056 1

Chloromethane ND mg/kg 02/03/15 12:01 74-87-30.0056 1

2-Chlorotoluene ND mg/kg 02/03/15 12:01 95-49-80.0056 1





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ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase






Dibromochloromethane ND mg/kg 02/03/15 12:01 124-48-10.0056 1

1,2-Dibromoethane (EDB) ND mg/kg 02/03/15 12:01 106-93-40.0056 1

Dibromomethane ND mg/kg 02/03/15 12:01 74-95-30.0056 1

1,2-Dichlorobenzene ND mg/kg 02/03/15 12:01 95-50-10.0056 1



trans-1,4-Dichloro-2-butene ND mg/kg 02/03/15 12:01 110-57-60.11 1

Dichlorodifluoromethane ND mg/kg 02/03/15 12:01 75-71-80.0056 1

1,1-Dichloroethane ND mg/kg 02/03/15 12:01 75-34-30.0056 1


1,1-Dichloroethene ND mg/kg 02/03/15 12:01 75-35-40.0056 1

cis-1,2-Dichloroethene ND mg/kg 02/03/15 12:01 156-59-20.0056 1

trans-1,2-Dichloroethene ND mg/kg 02/03/15 12:01 156-60-50.0056 1

1,2-Dichloropropane ND mg/kg 02/03/15 12:01 78-87-50.0056 1



1,1-Dichloropropene ND mg/kg 02/03/15 12:01 563-58-60.0056 1

cis-1,3-Dichloropropene ND mg/kg 02/03/15 12:01 10061-01-50.0056 1

trans-1,3-Dichloropropene ND mg/kg 02/03/15 12:01 10061-02-60.0056 1

Ethylbenzene ND mg/kg 02/03/15 12:01 100-41-40.0056 1

Ethyl methacrylate ND mg/kg 02/03/15 12:01 97-63-20.11 1

Hexachloro-1,3-butadiene ND mg/kg 02/03/15 12:01 87-68-30.0056 1

n-Hexane ND mg/kg 02/03/15 12:01 110-54-30.0056 1

2-Hexanone ND mg/kg 02/03/15 12:01 591-78-60.11 1

Iodomethane ND mg/kg 02/03/15 12:01 74-88-40.11 1

Isopropylbenzene (Cumene) ND mg/kg 02/03/15 12:01 98-82-80.0056 1

p-Isopropyltoluene ND mg/kg 02/03/15 12:01 99-87-60.0056 1

Methylene Chloride ND mg/kg 02/03/15 12:01 75-09-20.023 1

4-Methyl-2-pentanone (MIBK) ND mg/kg 02/03/15 12:01 108-10-10.028 1

Methyl-tert-butyl ether ND mg/kg 02/03/15 12:01 1634-04-40.0056 1

Naphthalene ND mg/kg 02/03/15 12:01 91-20-30.0056 1

n-Propylbenzene ND mg/kg 02/03/15 12:01 103-65-10.0056 1

Styrene ND mg/kg 02/03/15 12:01 100-42-50.0056 1

1,1,1,2-Tetrachloroethane ND mg/kg 02/03/15 12:01 630-20-60.0056 1


Tetrachloroethene 0.19 mg/kg 02/03/15 12:01 127-18-40.0056 1

Toluene ND mg/kg 02/03/15 12:01 108-88-30.0056 1

1,2,3-Trichlorobenzene ND mg/kg 02/03/15 12:01 87-61-60.0056 1


1,1,1-Trichloroethane ND mg/kg 02/03/15 12:01 71-55-60.0056 1


Trichloroethene ND mg/kg 02/03/15 12:01 79-01-60.0056 1

Trichlorofluoromethane ND mg/kg 02/03/15 12:01 75-69-40.0056 1

1,2,3-Trichloropropane ND mg/kg 02/03/15 12:01 96-18-40.0056 1

1,2,4-Trimethylbenzene ND mg/kg 02/03/15 12:01 95-63-60.0056 1





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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase






Vinyl acetate ND mg/kg 02/03/15 12:01 108-05-40.11 1

Vinyl chloride ND mg/kg 02/03/15 12:01 75-01-40.0056 1

Xylene (Total) ND mg/kg 02/03/15 12:01 1330-20-70.011 1


Toluene-d8 (S) 120 %. 02/03/15 12:01 2037-26-571-128 1


Analytical Method: ASTM D2974-87Percent Moisture

Percent Moisture 10.9 % 02/02/15 10:050.10 1





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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Lead 13.0 mg/kg 02/02/15 21:49 7439-92-101/31/15 07:351.1 1


Acenaphthene ND mg/kg 01/29/15 17:17 83-32-901/29/15 10:380.0061 1

Acenaphthylene ND mg/kg 01/29/15 17:17 208-96-801/29/15 10:380.0061 1

Anthracene ND mg/kg 01/29/15 17:17 120-12-701/29/15 10:380.0061 1

Benzo(a)anthracene ND mg/kg 01/29/15 17:17 56-55-301/29/15 10:380.0061 1

Benzo(a)pyrene ND mg/kg 01/29/15 17:17 50-32-801/29/15 10:380.0061 1

Benzo(b)fluoranthene ND mg/kg 01/29/15 17:17 205-99-201/29/15 10:380.0061 1

Benzo(g,h,i)perylene ND mg/kg 01/29/15 17:17 191-24-201/29/15 10:380.0061 1

Benzo(k)fluoranthene ND mg/kg 01/29/15 17:17 207-08-901/29/15 10:380.0061 1

Chrysene ND mg/kg 01/29/15 17:17 218-01-901/29/15 10:380.0061 1

Dibenz(a,h)anthracene ND mg/kg 01/29/15 17:17 53-70-301/29/15 10:380.0061 1

Fluoranthene ND mg/kg 01/29/15 17:17 206-44-001/29/15 10:380.0061 1

Fluorene ND mg/kg 01/29/15 17:17 86-73-701/29/15 10:380.0061 1

Indeno(1,2,3-cd)pyrene ND mg/kg 01/29/15 17:17 193-39-501/29/15 10:380.0061 1

1-Methylnaphthalene ND mg/kg 01/29/15 17:17 90-12-001/29/15 10:380.0061 1

2-Methylnaphthalene ND mg/kg 01/29/15 17:17 91-57-601/29/15 10:380.0061 1

Naphthalene ND mg/kg 01/29/15 17:17 91-20-301/29/15 10:380.0061 1

Phenanthrene ND mg/kg 01/29/15 17:17 85-01-801/29/15 10:380.0061 1

Pyrene ND mg/kg 01/29/15 17:17 129-00-001/29/15 10:380.0061 1


p-Terphenyl-d14 (S) 75 %. 01/29/15 17:17 1718-51-001/29/15 10:3832-111 1


Acetone ND mg/kg 02/03/15 12:27 67-64-10.088 1

Acrolein ND mg/kg 02/03/15 12:27 107-02-80.088 1


Benzene ND mg/kg 02/03/15 12:27 71-43-20.0044 1





















7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 39 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase




























n-Hexane ND mg/kg 02/03/15 12:27 110-54-30.0044 1

2-Hexanone ND mg/kg 02/03/15 12:27 591-78-60.088 1









Styrene ND mg/kg 02/03/15 12:27 100-42-50.0044 1



Tetrachloroethene ND mg/kg 02/03/15 12:27 127-18-40.0044 1

Toluene ND mg/kg 02/03/15 12:27 108-88-30.0044 1













7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

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Page 40 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase










Toluene-d8 (S) 103 %. 02/03/15 12:27 2037-26-571-128 1








7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 41 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase





Lead 42.4 mg/kg 02/02/15 21:52 7439-92-101/31/15 07:351.1 1


Acenaphthene 0.033 mg/kg 01/29/15 18:11 83-32-901/29/15 10:380.0058 1

Acenaphthylene 0.026 mg/kg 01/29/15 18:11 208-96-801/29/15 10:380.0058 1

Anthracene 0.26 mg/kg 01/29/15 18:11 120-12-701/29/15 10:380.0058 1

Benzo(a)anthracene 0.26 mg/kg 01/29/15 18:11 56-55-301/29/15 10:380.0058 1

Benzo(a)pyrene 0.20 mg/kg 01/29/15 18:11 50-32-801/29/15 10:380.0058 1

Benzo(b)fluoranthene 0.21 mg/kg 01/29/15 18:11 205-99-201/29/15 10:380.0058 1

Benzo(g,h,i)perylene 0.13 mg/kg 01/29/15 18:11 191-24-201/29/15 10:380.0058 1

Benzo(k)fluoranthene 0.17 mg/kg 01/29/15 18:11 207-08-901/29/15 10:380.0058 1

Chrysene 0.38 mg/kg 01/29/15 18:11 218-01-901/29/15 10:380.0058 1

Dibenz(a,h)anthracene 0.066 mg/kg 01/29/15 18:11 53-70-301/29/15 10:380.0058 1

Fluoranthene 0.46 mg/kg 01/29/15 18:11 206-44-001/29/15 10:380.0058 1

Fluorene 0.042 mg/kg 01/29/15 18:11 86-73-701/29/15 10:380.0058 1

Indeno(1,2,3-cd)pyrene 0.12 mg/kg 01/29/15 18:11 193-39-501/29/15 10:380.0058 1



Naphthalene 0.034 mg/kg 01/29/15 18:11 91-20-301/29/15 10:380.0058 1

Phenanthrene 0.37 mg/kg 01/29/15 18:11 85-01-801/29/15 10:380.0058 1

Pyrene 0.42 mg/kg 01/29/15 18:11 129-00-001/29/15 10:380.0058 1


p-Terphenyl-d14 (S) 80 %. 01/29/15 18:11 1718-51-001/29/15 10:3832-111 1


Acetone ND mg/kg 02/03/15 12:52 67-64-10.12 1

Acrolein ND mg/kg 02/03/15 12:52 107-02-80.12 1


Benzene ND mg/kg 02/03/15 12:52 71-43-20.0062 1





















7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 42 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase




























n-Hexane ND mg/kg 02/03/15 12:52 110-54-30.0062 1

2-Hexanone ND mg/kg 02/03/15 12:52 591-78-60.12 1









Styrene ND mg/kg 02/03/15 12:52 100-42-50.0062 1



Tetrachloroethene ND mg/kg 02/03/15 12:52 127-18-40.0062 1

Toluene ND mg/kg 02/03/15 12:52 108-88-30.0062 1













7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 43 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase










Toluene-d8 (S) 113 %. 02/03/15 12:52 2037-26-571-128 1








7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 44 of 78

Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase

Sample: Trip Blank Lab ID: 50111605014 Collected: 01/27/15 08:00 Received: 01/28/15 14:50 Matrix: Water



Acetone ND ug/L 01/30/15 12:47 67-64-1100 1

Acrolein ND ug/L 01/30/15 12:47 107-02-850.0 1


Benzene ND ug/L 01/30/15 12:47 71-43-25.0 1




Bromoform ND ug/L 01/30/15 12:47 75-25-25.0 1




































n-Hexane ND ug/L 01/30/15 12:47 110-54-35.0 1

2-Hexanone ND ug/L 01/30/15 12:47 591-78-625.0 1







7726 Moller Road


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Reference 47

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

50111605

Goodwill Phase

Sample: Trip Blank Lab ID: 50111605014 Collected: 01/27/15 08:00 Received: 01/28/15 14:50 Matrix: Water








Styrene ND ug/L 01/30/15 12:47 100-42-55.0 1




Toluene ND ug/L 01/30/15 12:47 108-88-35.0 1















Toluene-d8 (S) 104 %. 01/30/15 12:47 2037-26-581-110 1





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

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Page 46 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/15217

EPA 3050

EPA 6010

6010 MET

Associated Lab Samples: 50111605011, 50111605012, 50111605013

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Lead mg/kg ND 1.0 02/02/15 21:17

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead mg/kg 52.250 104 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

50111604002

1230438

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead mg/kg 53.6 92 75-12594 6 20579.5 59.1 62.8





7726 Moller Road


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4860 Blazer Parkway

Dublin, OH 43017

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Page 47 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/15204

EPA 3010

EPA 6010

6010 MET


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 10.0 01/30/15 22:06

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 9921000 99 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

50111607010

1229770

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 1000 99 75-125100 1 201000ND 987 1000





7726 Moller Road


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4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 48 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/15228

EPA 3010

EPA 6010

6010 MET Dissolved


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead, Dissolved ug/L ND 10.0 02/02/15 13:52

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead, Dissolved ug/L 10501000 105 80-120

Parameter Units

MS

Result

% Rec


1231092MATRIX SPIKE SAMPLE:

MSSpike

Result

50111605005

Lead, Dissolved ug/L 10301000 103 75-125ND





7726 Moller Road


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4860 Blazer Parkway

Dublin, OH 43017

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Page 49 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


MSV/73171

EPA 8260

EPA 8260

8260 MSV


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed























2-Hexanone ug/L ND 25.0 01/29/15 12:31



Acetone ug/L ND 100 01/29/15 12:31

Acrolein ug/L ND 50.0 01/29/15 12:31


Benzene ug/L ND 5.0 01/29/15 12:31




Bromoform ug/L ND 5.0 01/29/15 12:31













7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

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Page 50 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed













n-Hexane ug/L ND 5.0 01/29/15 12:31




Styrene ug/L ND 5.0 01/29/15 12:31



Toluene ug/L ND 5.0 01/29/15 12:31











Toluene-d8 (S) %. 104 81-110 01/29/15 12:31

Parameter Units

LCS

Result

% Rec



LCSSpike














7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 51 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike












2-Butanone (MEK) ug/L 305250 122 58-139


2-Hexanone ug/L 256250 102 54-140



Acetone ug/L 448 L3250 179 49-150

Acrolein ug/L 15901000 159 41-200


Benzene ug/L 39.950 80 74-122




Bromoform ug/L 41.050 82 44-134






Chloroform ug/L 38.0 L050 76 78-126










Iodomethane ug/L 110100 110 21-170





n-Hexane ug/L 47.050 94 51-125







7726 Moller Road


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4860 Blazer Parkway

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Page 52 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike


Styrene ug/L 48.150 96 74-126



Toluene ug/L 42.050 84 72-122








Xylene (Total) ug/L 141150 94 70-124



Toluene-d8 (S) %. 105 81-110

Parameter Units

MS

Result

% Rec



MSSpike

Result

50111605002

1,1,1,2-Tetrachloroethane ug/L 29.750 59 50-132ND

1,1,1-Trichloroethane ug/L 33.650 67 60-138ND

1,1,2,2-Tetrachloroethane ug/L 41.750 83 55-128ND

1,1,2-Trichloroethane ug/L 43.550 87 61-139ND

1,1-Dichloroethane ug/L 38.150 76 57-147ND

1,1-Dichloroethene ug/L 37.650 75 55-145ND

1,1-Dichloropropene ug/L 37.850 76 55-147ND

1,2,3-Trichlorobenzene ug/L 35.750 71 31-141ND

1,2,3-Trichloropropane ug/L 44.250 88 58-133ND

1,2,4-Trichlorobenzene ug/L 33.550 67 25-143ND

1,2,4-Trimethylbenzene ug/L 43.550 87 18-149ND

1,2-Dibromoethane (EDB) ug/L 40.850 82 63-129ND

1,2-Dichlorobenzene ug/L 37.050 74 38-136ND

1,2-Dichloroethane ug/L 41.050 82 62-138ND

1,2-Dichloropropane ug/L 41.750 83 59-130ND

1,3,5-Trimethylbenzene ug/L 41.250 82 20-147ND





2-Butanone (MEK) ug/L 200250 80 37-156ND

2-Chlorotoluene ug/L 39.550 79 27-142ND

2-Hexanone ug/L 194250 78 44-143ND

4-Chlorotoluene ug/L 35.950 72 27-144ND

4-Methyl-2-pentanone (MIBK) ug/L 195250 78 46-144ND





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 53 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

MS

Result

% Rec



MSSpike

Result

50111605002

Acetone ug/L 217250 87 39-156ND

Acrolein ug/L 14501000 145 33-200ND

Acrylonitrile ug/L 7391000 74 48-149ND

Benzene ug/L 39.150 78 62-129ND

Bromobenzene ug/L 39.850 80 39-140ND

Bromochloromethane ug/L 41.150 82 49-142ND

Bromodichloromethane ug/L 34.450 69 50-142ND

Bromoform ug/L 30.650 61 36-125ND

Bromomethane ug/L 49.950 100 13-179ND

Carbon disulfide ug/L 75.7100 76 45-142ND

Carbon tetrachloride ug/L 26.750 53 46-142ND

Chlorobenzene ug/L 39.150 78 49-136ND

Chloroethane ug/L 49.050 98 47-160ND

Chloroform ug/L 37.350 75 54-150ND

Chloromethane ug/L 43.450 87 30-148ND

cis-1,2-Dichloroethene ug/L 38.850 78 60-135ND

cis-1,3-Dichloropropene ug/L 36.150 72 52-123ND

Dibromochloromethane ug/L 29.350 59 48-125ND

Dibromomethane ug/L 38.550 77 59-134ND

Dichlorodifluoromethane ug/L 34.850 70 24-197ND

Ethyl methacrylate ug/L 161200 81 55-139ND

Ethylbenzene ug/L 40.950 82 28-153ND

Hexachloro-1,3-butadiene ug/L 33.650 67 10-176ND

Iodomethane ug/L 105100 105 17-157ND

Isopropylbenzene (Cumene) ug/L 44.950 90 18-152ND

Methyl-tert-butyl ether ug/L 92.0100 92 63-130ND

Methylene Chloride ug/L 46.050 92 45-156ND

n-Butylbenzene ug/L 42.850 86 10-161ND

n-Hexane ug/L 32.850 66 33-144ND

n-Propylbenzene ug/L 40.550 81 16-150ND

p-Isopropyltoluene ug/L 40.950 82 10-163ND

sec-Butylbenzene ug/L 42.050 84 10-160ND

Styrene ug/L 42.150 84 36-139ND

tert-Butylbenzene ug/L 37.650 75 12-134ND

Tetrachloroethene ug/L 37350 149 33-151299

Toluene ug/L 39.250 77 50-132ND

trans-1,2-Dichloroethene ug/L 39.450 79 40-153ND

trans-1,3-Dichloropropene ug/L 34.350 69 48-122ND

trans-1,4-Dichloro-2-butene ug/L 150200 75 32-139ND

Trichloroethene ug/L 37.550 70 50-143ND

Trichlorofluoromethane ug/L 45.850 92 60-175ND

Vinyl acetate ug/L 171200 85 17-142ND

Vinyl chloride ug/L 38.650 77 44-145ND

Xylene (Total) ug/L 126150 84 29-145ND


Dibromofluoromethane (S) %. HS95 79-116

Toluene-d8 (S) %. 106 81-110





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 54 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

Dup

Result

Max

RPD QualifiersRPDResult

50111605001

1230166SAMPLE DUPLICATE:

1,1,1,2-Tetrachloroethane ug/L ND 20ND

1,1,1-Trichloroethane ug/L ND 20ND

1,1,2,2-Tetrachloroethane ug/L ND 20ND

1,1,2-Trichloroethane ug/L ND 20ND

1,1-Dichloroethane ug/L ND 20ND

1,1-Dichloroethene ug/L ND 20ND

1,1-Dichloropropene ug/L ND 20ND

1,2,3-Trichlorobenzene ug/L ND 20ND

1,2,3-Trichloropropane ug/L ND 20ND

1,2,4-Trichlorobenzene ug/L ND 20ND

1,2,4-Trimethylbenzene ug/L ND 20ND

1,2-Dibromoethane (EDB) ug/L ND 20ND

1,2-Dichlorobenzene ug/L ND 20ND

1,2-Dichloroethane ug/L ND 20ND

1,2-Dichloropropane ug/L ND 20ND

1,3,5-Trimethylbenzene ug/L ND 20ND





2-Butanone (MEK) ug/L ND 20ND

2-Chlorotoluene ug/L ND 20ND

2-Hexanone ug/L ND 20ND

4-Chlorotoluene ug/L ND 20ND

4-Methyl-2-pentanone (MIBK) ug/L ND 20ND

Acetone ug/L ND 20ND

Acrolein ug/L ND 20ND

Acrylonitrile ug/L ND 20ND

Benzene ug/L ND 20ND

Bromobenzene ug/L ND 20ND

Bromochloromethane ug/L ND 20ND

Bromodichloromethane ug/L ND 20ND

Bromoform ug/L ND 20ND

Bromomethane ug/L ND 20ND

Carbon disulfide ug/L ND 20ND

Carbon tetrachloride ug/L ND 20ND

Chlorobenzene ug/L ND 20ND

Chloroethane ug/L ND 20ND

Chloroform ug/L ND 20ND

Chloromethane ug/L ND 20ND

cis-1,2-Dichloroethene ug/L 1.9J 20ND

cis-1,3-Dichloropropene ug/L ND 20ND

Dibromochloromethane ug/L ND 20ND

Dibromomethane ug/L ND 20ND

Dichlorodifluoromethane ug/L ND 20ND

Ethyl methacrylate ug/L ND 20ND

Ethylbenzene ug/L ND 20ND





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 55 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

Dup

Result

Max


50111605001


Hexachloro-1,3-butadiene ug/L ND 20ND

Iodomethane ug/L ND 20ND

Isopropylbenzene (Cumene) ug/L ND 20ND

Methyl-tert-butyl ether ug/L ND 20ND

Methylene Chloride ug/L ND 20ND

n-Butylbenzene ug/L ND 20ND

n-Hexane ug/L ND 20ND

n-Propylbenzene ug/L ND 20ND

p-Isopropyltoluene ug/L ND 20ND

sec-Butylbenzene ug/L ND 20ND

Styrene ug/L ND 20ND

tert-Butylbenzene ug/L ND 20ND

Tetrachloroethene ug/L 124 0 20124

Toluene ug/L .3J 20ND

trans-1,2-Dichloroethene ug/L ND 20ND

trans-1,3-Dichloropropene ug/L ND 20ND

trans-1,4-Dichloro-2-butene ug/L ND 20ND

Trichloroethene ug/L 5.3 3 205.5

Trichlorofluoromethane ug/L ND 20ND

Vinyl acetate ug/L ND 20ND

Vinyl chloride ug/L ND 20ND

Xylene (Total) ug/L ND 20ND

4-Bromofluorobenzene (S) %. 101 1100

Dibromofluoromethane (S) %. 95 HS194

Toluene-d8 (S) %. 102 0102





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 56 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


MSV/73206

EPA 8260

EPA 8260

8260 MSV

Associated Lab Samples: 50111605003, 50111605004, 50111605005, 50111605006, 50111605007, 50111605008, 50111605009,50111605010, 50111605014

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed























2-Hexanone ug/L ND 25.0 01/30/15 11:42



Acetone ug/L ND 100 01/30/15 11:42

Acrolein ug/L ND 50.0 01/30/15 11:42


Benzene ug/L ND 5.0 01/30/15 11:42




Bromoform ug/L ND 5.0 01/30/15 11:42












7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 57 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed














n-Hexane ug/L ND 5.0 01/30/15 11:42




Styrene ug/L ND 5.0 01/30/15 11:42



Toluene ug/L ND 5.0 01/30/15 11:42











Toluene-d8 (S) %. 102 81-110 01/30/15 11:42

Parameter Units

LCS

Result

% Rec



LCSSpike












7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 58 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike














2-Butanone (MEK) ug/L 283250 113 58-139


2-Hexanone ug/L 239250 95 54-140



Acetone ug/L 410 L3250 164 49-150

Acrolein ug/L 14601000 146 41-200


Benzene ug/L 43.550 87 74-122




Bromoform ug/L 42.250 84 44-134






Chloroform ug/L 40.750 81 78-126










Iodomethane ug/L 111100 111 21-170





n-Hexane ug/L 50.450 101 51-125





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 59 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike




Styrene ug/L 51.150 102 74-126



Toluene ug/L 44.050 88 72-122








Xylene (Total) ug/L 153150 102 70-124



Toluene-d8 (S) %. 105 81-110





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 60 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


MSV/73289

EPA 8260

EPA 8260

8260 MSV 5035A Volatile Organics


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 02/03/15 09:06

1,1,1-Trichloroethane mg/kg ND 0.0050 02/03/15 09:06

1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 02/03/15 09:06

1,1,2-Trichloroethane mg/kg ND 0.0050 02/03/15 09:06

1,1-Dichloroethane mg/kg ND 0.0050 02/03/15 09:06

1,1-Dichloroethene mg/kg ND 0.0050 02/03/15 09:06

1,1-Dichloropropene mg/kg ND 0.0050 02/03/15 09:06

1,2,3-Trichlorobenzene mg/kg ND 0.0050 02/03/15 09:06

1,2,3-Trichloropropane mg/kg ND 0.0050 02/03/15 09:06

1,2,4-Trichlorobenzene mg/kg ND 0.0050 02/03/15 09:06

1,2,4-Trimethylbenzene mg/kg ND 0.0050 02/03/15 09:06

1,2-Dibromoethane (EDB) mg/kg ND 0.0050 02/03/15 09:06

1,2-Dichlorobenzene mg/kg ND 0.0050 02/03/15 09:06

1,2-Dichloroethane mg/kg ND 0.0050 02/03/15 09:06

1,2-Dichloropropane mg/kg ND 0.0050 02/03/15 09:06

1,3,5-Trimethylbenzene mg/kg ND 0.0050 02/03/15 09:06





2-Butanone (MEK) mg/kg ND 0.025 02/03/15 09:06

2-Chlorotoluene mg/kg ND 0.0050 02/03/15 09:06

2-Hexanone mg/kg ND 0.10 02/03/15 09:06

4-Chlorotoluene mg/kg ND 0.0050 02/03/15 09:06

4-Methyl-2-pentanone (MIBK) mg/kg ND 0.025 02/03/15 09:06

Acetone mg/kg ND 0.10 02/03/15 09:06

Acrolein mg/kg ND 0.10 02/03/15 09:06

Acrylonitrile mg/kg ND 0.10 02/03/15 09:06

Benzene mg/kg ND 0.0050 02/03/15 09:06

Bromobenzene mg/kg ND 0.0050 02/03/15 09:06

Bromochloromethane mg/kg ND 0.0050 02/03/15 09:06

Bromodichloromethane mg/kg ND 0.0050 02/03/15 09:06

Bromoform mg/kg ND 0.0050 02/03/15 09:06

Bromomethane mg/kg ND 0.0050 02/03/15 09:06

Carbon disulfide mg/kg ND 0.010 02/03/15 09:06

Carbon tetrachloride mg/kg ND 0.0050 02/03/15 09:06

Chlorobenzene mg/kg ND 0.0050 02/03/15 09:06

Chloroethane mg/kg ND 0.0050 02/03/15 09:06

Chloroform mg/kg ND 0.0050 02/03/15 09:06

Chloromethane mg/kg ND 0.0050 02/03/15 09:06

cis-1,2-Dichloroethene mg/kg ND 0.0050 02/03/15 09:06





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 61 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

cis-1,3-Dichloropropene mg/kg ND 0.0050 02/03/15 09:06

Dibromochloromethane mg/kg ND 0.0050 02/03/15 09:06

Dibromomethane mg/kg ND 0.0050 02/03/15 09:06

Dichlorodifluoromethane mg/kg ND 0.0050 02/03/15 09:06

Ethyl methacrylate mg/kg ND 0.10 02/03/15 09:06

Ethylbenzene mg/kg ND 0.0050 02/03/15 09:06

Hexachloro-1,3-butadiene mg/kg ND 0.0050 02/03/15 09:06

Iodomethane mg/kg ND 0.10 02/03/15 09:06

Isopropylbenzene (Cumene) mg/kg ND 0.0050 02/03/15 09:06

Methyl-tert-butyl ether mg/kg ND 0.0050 02/03/15 09:06

Methylene Chloride mg/kg ND 0.020 02/03/15 09:06

n-Butylbenzene mg/kg ND 0.0050 02/03/15 09:06

n-Hexane mg/kg ND 0.0050 02/03/15 09:06

n-Propylbenzene mg/kg ND 0.0050 02/03/15 09:06

Naphthalene mg/kg ND 0.0050 02/03/15 09:06

p-Isopropyltoluene mg/kg ND 0.0050 02/03/15 09:06

sec-Butylbenzene mg/kg ND 0.0050 02/03/15 09:06

Styrene mg/kg ND 0.0050 02/03/15 09:06

tert-Butylbenzene mg/kg ND 0.0050 02/03/15 09:06

Tetrachloroethene mg/kg ND 0.0050 02/03/15 09:06

Toluene mg/kg ND 0.0050 02/03/15 09:06

trans-1,2-Dichloroethene mg/kg ND 0.0050 02/03/15 09:06

trans-1,3-Dichloropropene mg/kg ND 0.0050 02/03/15 09:06

trans-1,4-Dichloro-2-butene mg/kg ND 0.10 02/03/15 09:06

Trichloroethene mg/kg ND 0.0050 02/03/15 09:06

Trichlorofluoromethane mg/kg ND 0.0050 02/03/15 09:06

Vinyl acetate mg/kg ND 0.10 02/03/15 09:06

Vinyl chloride mg/kg ND 0.0050 02/03/15 09:06

Xylene (Total) mg/kg ND 0.010 02/03/15 09:06



Toluene-d8 (S) %. 96 71-128 02/03/15 09:06

Parameter Units

LCS

Result

% Rec



LCSSpike

1,1,1,2-Tetrachloroethane mg/kg 0.051.05 103 62-123

1,1,1-Trichloroethane mg/kg 0.050.05 101 70-123

1,1,2,2-Tetrachloroethane mg/kg 0.052.05 104 65-124

1,1,2-Trichloroethane mg/kg 0.050.05 101 74-129

1,1-Dichloroethane mg/kg 0.050.05 99 73-130

1,1-Dichloroethene mg/kg 0.045.05 90 66-126

1,1-Dichloropropene mg/kg 0.050.05 100 78-125

1,2,3-Trichlorobenzene mg/kg 0.043.05 86 66-131





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 62 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike

1,2,3-Trichloropropane mg/kg 0.051.05 102 44-157

1,2,4-Trichlorobenzene mg/kg 0.039.05 78 68-129

1,2,4-Trimethylbenzene mg/kg 0.048.05 97 67-126

1,2-Dibromoethane (EDB) mg/kg 0.051.05 102 74-120

1,2-Dichlorobenzene mg/kg 0.046.05 92 73-122

1,2-Dichloroethane mg/kg 0.048.05 96 73-127

1,2-Dichloropropane mg/kg 0.052.05 104 75-118

1,3,5-Trimethylbenzene mg/kg 0.051.05 101 65-127





2-Butanone (MEK) mg/kg 0.23.25 93 59-139

2-Chlorotoluene mg/kg 0.046.05 92 72-121

2-Hexanone mg/kg 0.24.25 95 56-139

4-Chlorotoluene mg/kg 0.045.05 90 75-123

4-Methyl-2-pentanone (MIBK) mg/kg 0.26.25 106 63-136

Acetone mg/kg 0.22.25 87 46-156

Acrolein mg/kg 3.3 L31 333 47-200

Acrylonitrile mg/kg 1.01 103 67-130

Benzene mg/kg 0.051.05 101 74-119

Bromobenzene mg/kg 0.048.05 96 69-129

Bromochloromethane mg/kg 0.053.05 107 67-129

Bromodichloromethane mg/kg 0.049.05 98 68-121

Bromoform mg/kg 0.042.05 83 49-124

Bromomethane mg/kg 0.039.05 79 44-142

Carbon disulfide mg/kg 0.084.1 84 61-129

Carbon tetrachloride mg/kg 0.050.05 100 58-127

Chlorobenzene mg/kg 0.047.05 93 77-122

Chloroethane mg/kg 0.045.05 91 59-141

Chloroform mg/kg 0.050.05 101 75-124

Chloromethane mg/kg 0.039.05 78 46-133

cis-1,2-Dichloroethene mg/kg 0.050.05 101 72-122

cis-1,3-Dichloropropene mg/kg 0.043.05 86 68-115

Dibromochloromethane mg/kg 0.041.05 83 60-121

Dibromomethane mg/kg 0.048.05 96 72-124

Dichlorodifluoromethane mg/kg 0.031.05 63 26-186

Ethyl methacrylate mg/kg 0.17.2 87 63-130

Ethylbenzene mg/kg 0.050.05 101 72-123

Hexachloro-1,3-butadiene mg/kg 0.045.05 90 55-139

Iodomethane mg/kg 0.10.1 102 38-149

Isopropylbenzene (Cumene) mg/kg 0.053.05 107 65-123

Methyl-tert-butyl ether mg/kg 0.10.1 104 68-120

Methylene Chloride mg/kg 0.046.05 92 57-142

n-Butylbenzene mg/kg 0.045.05 91 68-125

n-Hexane mg/kg 0.045.05 91 57-117

n-Propylbenzene mg/kg 0.049.05 98 68-122





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 63 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike

Naphthalene mg/kg 0.056.05 111 67-131

p-Isopropyltoluene mg/kg 0.048.05 96 66-133

sec-Butylbenzene mg/kg 0.054.05 107 64-131

Styrene mg/kg 0.053.05 105 70-126

tert-Butylbenzene mg/kg 0.044.05 88 46-124

Tetrachloroethene mg/kg 0.045.05 91 72-126

Toluene mg/kg 0.049.05 99 71-121

trans-1,2-Dichloroethene mg/kg 0.048.05 97 69-123

trans-1,3-Dichloropropene mg/kg 0.041.05 82 66-114

trans-1,4-Dichloro-2-butene mg/kg 0.13.2 66 61-124

Trichloroethene mg/kg 0.050.05 100 74-123

Trichlorofluoromethane mg/kg 0.050.05 99 72-146

Vinyl acetate mg/kg 0.21.2 103 57-131

Vinyl chloride mg/kg 0.040.05 80 55-128

Xylene (Total) mg/kg 0.15.15 101 66-124



Toluene-d8 (S) %. 97 71-128





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 64 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/38201

EPA 3510

EPA 8270 by SIM LVE


Associated Lab Samples: 50111605001, 50111605002, 50111605003, 50111605004, 50111605005, 50111605006, 50111605007,50111605008, 50111605009, 50111605010

Parameter Units

Blank

Result

Reporting

Limit Qualifiers


Associated Lab Samples: 50111605001, 50111605002, 50111605003, 50111605004, 50111605005, 50111605006, 50111605007,50111605008, 50111605009, 50111605010

Matrix: Water

Analyzed











Chrysene ug/L ND 0.50 01/29/15 20:00



Fluorene ug/L ND 1.0 01/29/15 20:00




Pyrene ug/L ND 1.0 01/29/15 20:00


p-Terphenyl-d14 (S) %. 85 25-131 01/29/15 20:00

Parameter Units

LCS

Result

% Rec



LCSSpike











Chrysene ug/L 8.510 85 53-136



Fluorene ug/L 7.010 70 44-124





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 65 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike




Pyrene ug/L 8.210 82 50-134


p-Terphenyl-d14 (S) %. 77 25-131

Parameter Units

MS

Result

% Rec



MSSpike

Result

50111573002

1229880

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.



Acenaphthene ug/L 10 65 28-11672 10 2010ND 6.5 7.2

Acenaphthylene ug/L 10 70 34-11576 9 2010ND 7.0 7.6

Anthracene ug/L 10 74 39-12183 12 2010ND 7.4 8.3

Benzo(a)anthracene ug/L R110 63 31-12781 25 2010ND 6.3 8.1

Benzo(a)pyrene ug/L R110 34 10-12152 42 2010ND 3.4 5.2

Benzo(b)fluoranthene ug/L R110 29 10-11949 50 2010ND 2.9 4.9

Benzo(g,h,i)perylene ug/L R110 19 10-10828 38 2010ND 1.9 2.8

Benzo(k)fluoranthene ug/L R110 34 10-11852 42 2010ND 3.4 5.2

Chrysene ug/L R110 62 32-12779 24 2010ND 6.2 7.9

Dibenz(a,h)anthracene ug/L R110 19 10-10428 40 2010ND 1.9 2.8

Fluoranthene ug/L 10 68 38-13182 20 2010ND 6.8 8.2

Fluorene ug/L 10 68 33-12177 12 2010ND 6.8 7.7

Indeno(1,2,3-cd)pyrene ug/L R110 20 10-10830 39 2010ND 2.0 3.0

Naphthalene ug/L 10 66 16-11970 6 2010ND 6.6 7.0

Phenanthrene ug/L 10 62 32-13071 13 2010ND 6.2 7.1

Pyrene ug/L R110 71 39-13187 21 2010ND 7.1 8.7


p-Terphenyl-d14 (S) %. 58 25-13163





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(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 66 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/38193

EPA 3546

EPA 8270 by SIM

8270 MSSV PAH by SIM


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

1-Methylnaphthalene mg/kg ND 0.0050 01/29/15 19:59


Acenaphthene mg/kg ND 0.0050 01/29/15 19:59

Acenaphthylene mg/kg ND 0.0050 01/29/15 19:59

Anthracene mg/kg ND 0.0050 01/29/15 19:59

Benzo(a)anthracene mg/kg ND 0.0050 01/29/15 19:59

Benzo(a)pyrene mg/kg ND 0.0050 01/29/15 19:59

Benzo(b)fluoranthene mg/kg ND 0.0050 01/29/15 19:59

Benzo(g,h,i)perylene mg/kg ND 0.0050 01/29/15 19:59

Benzo(k)fluoranthene mg/kg ND 0.0050 01/29/15 19:59

Chrysene mg/kg ND 0.0050 01/29/15 19:59

Dibenz(a,h)anthracene mg/kg ND 0.0050 01/29/15 19:59

Fluoranthene mg/kg ND 0.0050 01/29/15 19:59

Fluorene mg/kg ND 0.0050 01/29/15 19:59

Indeno(1,2,3-cd)pyrene mg/kg ND 0.0050 01/29/15 19:59


Phenanthrene mg/kg ND 0.0050 01/29/15 19:59

Pyrene mg/kg ND 0.0050 01/29/15 19:59


p-Terphenyl-d14 (S) %. 84 32-111 01/29/15 19:59

Parameter Units

LCS

Result

% Rec



LCSSpike

1-Methylnaphthalene mg/kg 0.22.33 65 40-102


Acenaphthene mg/kg 0.24.33 72 43-108

Acenaphthylene mg/kg 0.25.33 76 44-110

Anthracene mg/kg 0.26.33 77 44-112

Benzo(a)anthracene mg/kg 0.28.33 83 43-124

Benzo(a)pyrene mg/kg 0.22.33 65 44-124

Benzo(b)fluoranthene mg/kg 0.22.33 65 44-123

Benzo(g,h,i)perylene mg/kg 0.20.33 61 44-118

Benzo(k)fluoranthene mg/kg 0.19.33 58 42-122

Chrysene mg/kg 0.26.33 77 44-124

Dibenz(a,h)anthracene mg/kg 0.22.33 66 44-119

Fluoranthene mg/kg 0.26.33 77 45-119

Fluorene mg/kg 0.27.33 81 44-113

Indeno(1,2,3-cd)pyrene mg/kg 0.22.33 66 44-119






7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 67 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike

Phenanthrene mg/kg 0.24.33 71 44-113

Pyrene mg/kg 0.27.33 81 45-123


p-Terphenyl-d14 (S) %. 83 32-111

Parameter Units

MS

Result

% Rec



MSSpike

Result

50111584001

1229758

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

1-Methylnaphthalene mg/kg .36 72 20-11672 0 20.36ND 0.26 0.26


Acenaphthene mg/kg .36 74 25-11772 1 20.36ND 0.26 0.26

Acenaphthylene mg/kg .36 81 27-12375 6 20.36ND 0.29 0.27

Anthracene mg/kg .36 84 20-12379 5 20.36ND 0.30 0.29

Benzo(a)anthracene mg/kg .36 80 23-12478 2 20.36ND 0.30 0.29

Benzo(a)pyrene mg/kg .36 63 23-12062 1 20.36ND 0.24 0.23

Benzo(b)fluoranthene mg/kg .36 65 24-11765 0 20.36ND 0.24 0.24

Benzo(g,h,i)perylene mg/kg .36 57 12-12255 1 20.36ND 0.21 0.21

Benzo(k)fluoranthene mg/kg .36 60 14-12359 2 20.36ND 0.22 0.22

Chrysene mg/kg .36 74 22-12473 0 20.36ND 0.28 0.28

Dibenz(a,h)anthracene mg/kg .36 64 26-11362 2 20.36ND 0.23 0.23

Fluoranthene mg/kg .36 78 21-12579 2 20.36ND 0.29 0.30

Fluorene mg/kg .36 76 19-12777 3 20.36ND 0.27 0.28

Indeno(1,2,3-cd)pyrene mg/kg .36 65 15-12162 4 20.36ND 0.23 0.22

Naphthalene mg/kg 1d.36 80 15-12570 12 20.36ND 0.29 0.25

Phenanthrene mg/kg .36 77 10-13974 3 20.36ND 0.28 0.27

Pyrene mg/kg .36 77 17-13278 2 20.36ND 0.29 0.30


p-Terphenyl-d14 (S) %. 82 32-11178





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 68 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/38194

EPA 3546

EPA 8270 by SIM

8270 MSSV PAH by SIM


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed



Acenaphthene mg/kg ND 0.0050 01/29/15 16:41

Acenaphthylene mg/kg ND 0.0050 01/29/15 16:41

Anthracene mg/kg ND 0.0050 01/29/15 16:41

Benzo(a)anthracene mg/kg ND 0.0050 01/29/15 16:41

Benzo(a)pyrene mg/kg ND 0.0050 01/29/15 16:41

Benzo(b)fluoranthene mg/kg ND 0.0050 01/29/15 16:41

Benzo(g,h,i)perylene mg/kg ND 0.0050 01/29/15 16:41

Benzo(k)fluoranthene mg/kg ND 0.0050 01/29/15 16:41

Chrysene mg/kg ND 0.0050 01/29/15 16:41

Dibenz(a,h)anthracene mg/kg ND 0.0050 01/29/15 16:41

Fluoranthene mg/kg ND 0.0050 01/29/15 16:41

Fluorene mg/kg ND 0.0050 01/29/15 16:41

Indeno(1,2,3-cd)pyrene mg/kg ND 0.0050 01/29/15 16:41


Phenanthrene mg/kg ND 0.0050 01/29/15 16:41

Pyrene mg/kg ND 0.0050 01/29/15 16:41


p-Terphenyl-d14 (S) %. 91 32-111 01/29/15 16:41

Parameter Units

LCS

Result

% Rec



LCSSpike



Acenaphthene mg/kg 0.23.33 70 43-108

Acenaphthylene mg/kg 0.24.33 73 44-110

Anthracene mg/kg 0.26.33 78 44-112

Benzo(a)anthracene mg/kg 0.28.33 84 43-124

Benzo(a)pyrene mg/kg 0.22.33 66 44-124

Benzo(b)fluoranthene mg/kg 0.23.33 68 44-123

Benzo(g,h,i)perylene mg/kg 0.18.33 55 44-118

Benzo(k)fluoranthene mg/kg 0.19.33 58 42-122

Chrysene mg/kg 0.26.33 79 44-124

Dibenz(a,h)anthracene mg/kg 0.21.33 62 44-119

Fluoranthene mg/kg 0.26.33 79 45-119

Fluorene mg/kg 0.25.33 76 44-113

Indeno(1,2,3-cd)pyrene mg/kg 0.20.33 60 44-119






7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 69 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


Parameter Units

LCS

Result

% Rec



LCSSpike

Phenanthrene mg/kg 0.24.33 72 44-113

Pyrene mg/kg 0.27.33 80 45-123


p-Terphenyl-d14 (S) %. 81 32-111

Parameter Units

MS

Result

% Rec



MSSpike

Result

50111605012

1229762

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.



Acenaphthene mg/kg .4 77 25-11774 4 20.4ND 0.31 0.30

Acenaphthylene mg/kg .4 82 27-12378 5 20.4ND 0.33 0.31

Anthracene mg/kg .4 78 20-12377 3 20.4ND 0.32 0.31

Benzo(a)anthracene mg/kg .4 75 23-12475 0 20.4ND 0.30 0.30

Benzo(a)pyrene mg/kg .4 58 23-12059 1 20.4ND 0.23 0.23

Benzo(b)fluoranthene mg/kg .4 59 24-11761 3 20.4ND 0.24 0.24

Benzo(g,h,i)perylene mg/kg .4 48 12-12249 2 20.4ND 0.19 0.20

Benzo(k)fluoranthene mg/kg .4 51 14-12353 2 20.4ND 0.21 0.21

Chrysene mg/kg .4 75 22-12477 3 20.4ND 0.30 0.31

Dibenz(a,h)anthracene mg/kg .4 59 26-11359 1 20.4ND 0.24 0.24

Fluoranthene mg/kg .4 74 21-12575 1 20.4ND 0.30 0.30

Fluorene mg/kg .4 81 19-12777 6 20.4ND 0.33 0.31

Indeno(1,2,3-cd)pyrene mg/kg .4 54 15-12155 2 20.4ND 0.22 0.22

Naphthalene mg/kg .4 72 15-12576 5 20.4ND 0.29 0.30

Phenanthrene mg/kg .4 73 10-13971 2 20.4ND 0.29 0.29

Pyrene mg/kg .4 74 17-13276 3 20.4ND 0.30 0.31


p-Terphenyl-d14 (S) %. 76 32-11177





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 70 of 78

Reference 47

#=QC#


Pace Project No.:

Project:

50111605

Goodwill Phase


QC Batch:

QC Batch Method:

Analysis Method:


PMST/10303

ASTM D2974-87

ASTM D2974-87

Dry Weight/Percent Moisture


Parameter Units

Dup

Result

Max


50111608017


Percent Moisture % 10.1 R134 514.2





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 71 of 78

Reference 47

#=QL#

QUALIFIERS

Pace Project No.:

Project:

50111605

Goodwill Phase

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.

ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

ANALYTE QUALIFIERS

Due to the extract's physical characteristics, the analysis was performed at dilution. CEM 01/30/151d

Sample diluted due to high volume of sediment in sample vials. DAE 02/02/152d

Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS

Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0

Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

RPD value was outside control limits.R1





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 72 of 78

Reference 47

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

50111605

Goodwill Phase

Lab ID Sample ID QC Batch Method QC Batch Analytical Method

Analytical

Batch

50111605011 MPRP/15217 ICP/18411SB-5 8-10' EPA 3050 EPA 6010



50111605005 MPRP/15204 ICP/18391SB-5 31' EPA 3010 EPA 6010






50111605001 OEXT/38201 MSSV/17135SB-4 30' EPA 3510 EPA 8270 by SIM LVE










50111605011 OEXT/38193 MSSV/17137SB-5 8-10' EPA 3546 EPA 8270 by SIM



50111605001 MSV/73171SB-4 30' EPA 8260

50111605002 MSV/73171SB-4 55' EPA 8260

50111605003 MSV/73206SB-6 30' EPA 8260

50111605004 MSV/73206SB-6 55' EPA 8260

50111605005 MSV/73206SB-5 31' EPA 8260

50111605006 MSV/73206SB-5 55' EPA 8260

50111605007 MSV/73206SB-7 30' EPA 8260

50111605008 MSV/73206SB-7 55' EPA 8260

50111605009 MSV/73206SB-8 30' EPA 8260

50111605010 MSV/73206SB-8 55' EPA 8260

50111605014 MSV/73206Trip Blank EPA 8260

50111605011 MSV/73289SB-5 8-10' EPA 8260

50111605012 MSV/73289SB-7 8-10' EPA 8260

50111605013 MSV/73289SB-8 8-10' EPA 8260

50111605011 PMST/10303SB-5 8-10' ASTM D2974-87

50111605012 PMST/10303SB-7 8-10' ASTM D2974-87

50111605013 PMST/10303SB-8 8-10' ASTM D2974-87





7726 Moller Road


(317)228-3100



4860 Blazer Parkway

Dublin, OH 43017

(614)486-5421

Page 73 of 78

Reference 47

of 78

Reference 47

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