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Laboratory Nawal Analytical Laboratories, Plot No. 100, New SIDCO Industrial Estate, Srinagar, Hosur, Tamil Nadu

Accreditation Standard ISO/IEC 17025: 2005

Certificate Number TC-5834(in lieu of T-1615, T-1192 & T-2635) of 105

Validity 05.04.2016 to 04.04.2018 Last Amended on 08.05.2017

Sl. Product / Material of Test

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

BIOLOGICAL TESTING

I. FOOD AND AGRICULTURAL PRODUCTS

1. Fruit & Fruit Products, Vegetable & Vegetable Products

Total Aerobic Microbial Count/ Aerobic Plate Count/ Total Plate Count/ Standard Plate Count/ Total Bacterial Count

IS 5402 ≥10 cfu/gISO 4833:(Part-1) ≥10 cfu/gSOP/NAL/M/031

Coliform IS 5401 (Part 1) ≥10 cfu/gISO 4832,SOP/NAL/M/033

≥10 cfu/g

Escherichia coli IS 5887 (Part 1) Qualitative(Present or Absent)/g or 0.1 g

ISO 16649(Part-2) ≥10 cfu / gSOP/NAL/M/035 <3 to >1100 MPN/g

Staphylococcus aureus IS 5887 (Part 2) Qualitative(Present or Absent)/25 g

ISO 6888(Part-1) ≥10 cfu / gSOP/NAL/M/037 ≥10 cfu / g

Faecal streptococci IS 5887 (Part 2) ≥10 cfu/g

Salmonella spp. IS 5887 (Part 3) Qualitative(Present or Absent)/25 g

ISO 6579 Qualitative(Present or Absent)/25 g

SOP/NAL/M/032 Qualitative (Present or Absent)/25 g

Shigella spp. IS 5887 (Part 7) Qualitative(Present or Absent)/25 g

Ashutosh D. TatwawadiConvenor

N. VenkateswaranProgram Director









ISO 21567 Qualitative (Present or Absent)/25 g

SOP/NAL/M/036 Qualitative (Present or Absent)/25 g

Bacillus cereus IS 5887 (Part 6) ≥10 cfu/gClostridium perfringens APHA (4th Edition) Cl.

34.71) Chapter 34Qualitative(Present or Absent)/25g

ISO 7937 ≥10 cfu / gSOP/NAL/M/042 Qualitative (Present or

Absent)/25 gYeast and mould IS 5403 ≥10 cfu/g

ISO 21527-1 ≥10 cfu/gSOP/NAL/M/040 ≥10 cfu/g

Listeria monocytogenes FDA BAM, Chapter 10 Qualitative(Present or Absent)/25g

ISO 11290-1 Qualitative(Present or Absent)/25 g

SOP/NAL/M/041 Qualitative (Present or Absent)/25g

Vibrio cholerae ISO 21872-1 Qualitative(Present or Absent) / 25g

SOP/NAL/M/038 Qualitative(Present or Absent) / 25g

Vibrio parahaemolyticus ISO 21872-1 Qualitative(Present or Absent) /25g

SOP/NAL/M/039 Qualitative(Present or Absent) /25g

2. Milk and Dairy Products (Raw and Processed)Milk, Milk powder, Skimmed milk

Total Aerobic Microbial Count/Aerobic Plate Count/Total Plate Count/ Standard Plate Count/ Total Bacterial Count

IS 5402 ≥10 cfu/gISO 4833:(Part-1) ≥10 cfu/gSOP/NAL/M/031 ≥1 cfu/mlFDA BAM, Chapter 3 ≥10 cfu/g

≥1 cfu/ml











powder, Partially skimmed milk powder,Infant milk powder, Cereal based complementary food, Butter,Ghee,Milk fats,Khoya, Panner,Cream, Cream powder , Malai, Chesse, Dahi/ Curd, Ice cream, Dry ice cream, Kulfi,Chocolate ice cream etc

Coliform IS 5401 (Part 1) ≥10 cfu/g≥1 cfu/ml

APHA (4th Edition) Cl. 8.71,8.73 & 8.74 Chapter 8

≥10 cfu/g≥1 cfu/mlMPN 3/g or ml ;<3 to >1100

SOP/NAL/M/033 ≥1 cfu/mlISO 4832 ≥10 cfu/g

Enterobacteriaceae APHA (4th Edition)(Cl. 8.62) Chapter 8

≥10 cfu/g≥1 cfu/ml

Escherichia coli IS 5887 (Part-1) Qualitative(Present or Absent)/g or ml/ 0.1 g or 0.1 ml

ISO 16649(Part-2) ≥10 cfu/g≥1 cfu/ml

SOP/NAL/M/035 <3 to >1100 MPN/g/mlAPHA (4th Edition)(Cl. 8.91) Chapter 8

<3 to >1100 MPN/g/ml

Faecal coliforms APHA (4th Edition) Cl. 8.81) Chapter- 8

MPN 3/g or ml;<3 to >1100

Staphylococcus aureus IS 5887 (Part- 2) Qualitative(Present or Absent)/25 g or 25 ml≥10 cfu/g≥1 cfu/ml

ISO 6888(Part-1) ≥10 cfu/g≥1 cfu/ml

FDA BAM Chapter 12 ≥10 cfu/g≥1 cfu/ml

SOP/NAL/M/037 ≥10 cfu/g≥1 cfu/ml

Faecal streptococci IS 5887 (Part 2) ≥10 cfu/g≥1 cfu/ml











Salmonella spp. IS 5887 (Part 3) Qualitative(Present or Absent)/25 g or 25 ml

ISO 6579 Qualitative(Present or Absent)/25 g or 25 ml

FDA BAM ,Chapter 5 Qualitative(Present or Absent)/25 g or 25 ml

SOP/NAL/M/035 Qualitative(Present or Absent)/25 g or 25 ml

Shigella spp. IS 5887 (Part 7) Qualitative(Present or Absent)/25 g or 25 ml

ISO 21567 Qualitative(Present or Absent)/25 g or 25 ml

FDA BAM, Chapter 6 Qualitative(Present or Absent)/25 g or 25 ml


Bacillus cereus IS 5887 (Part 6) ≥10 cfu/g≥1 cfu/ml

APHA (4th Edition), (Cl. 32.21) Chapter 32


Clostridium perfringens/ Anerobic Spore CountClostridium perfringens/ Sulfite ReducingClostridia

IS 5887 (Part 4) ≥10 cfu/g≥1 cfu/ml

ISO 7937 ≥10 cfu/g≥1 cfu/ml

ISO 15213 ≥10 cfu/g≥1 cfu/ml

APHA (4th Edition) Qualitative(Present or Absent)/25 g or 25 ml

SOP/NAL/M/042 Qualitative (Present or Absent)/25 g/25ml

Thermophillic bacteria SMEDP, APHA (17th Edition)Chapter 8












(Cl. 8.040)Thermoduric bacteria SMEDP, APHA (17th

Edition)Chapter 8 (Cl. 8.030)


Lactic acid bacteria SMEDP, APHA (17th Edition):(Cl.8.071)Chapter-8


Yeast and mould IS 5403 ≥10 cfu/g≥1 cfu/ml

ISO 21527-1 ≥10 cfu/g≥1 cfu/ml

APHA (4th Edition) (Cl.20.51) Chapter 20



Vibrio cholerae ISO 21872-1 Qualitative(Present or Absent)/25 g or 25 ml

APHA (4th Edition)(Cl. 40.51) Chapter 40

Qualitative(Present or Absent)/25 g or 25 ml


Vibrio parahaemolyticus ISO 21872-1 Qualitative(Present or Absent)/25 g or 25 ml


MPN 3/g or ml <3 to >1100


Vibrio vulnificus APHA (4th Edition)(Cl. 40.53) Chapter 40

MPN 3/g or ml <3 to >1100

Listeria monocytogenes IS 14988(Part-2) ≥10 cfu/g≥1 cfu/ml

IS14988 (Part 1) Qualitative(Present or











Absent)/ g or mlISO 11290-1 Qualitative(Present or

Absent)/25 g or 25 mlFDA BAM, Chapter 10 Qualitative(Present or

Absent)/25 g or 25 mlSOP/NAL/M/041 Qualitative(Present or

Absent)/25 g or 25 ml3. Meat & Meat

Products (Raw and Processed)

Total Aerobic Microbial Count / Aerobic Plate Count/ Total Plate Count/ Standard Plate Count/ Total Bacterial Count

IS 5402 ≥10 cfu/g

Coliform IS 5401 (Part 1) ≥10 cfu/gEscherichia coli IS 5887 (Part 1) Qualitative(Present or

Absent)/g or 0.1 gStaphylococcus aureus IS 5887 (Part 2) Qualitative(Present or

Absent)/25 gFaecal streptococci IS 5887 (Part 2) ≥10 cfu/gSalmonella spp. IS 5887 (Part 3) Qualitative

(Present or Absent)/25 gShigella spp. IS 5887 (Part 7) Qualitative(Present or

Absent)/25 gBacillus cereus IS 5887 (Part 6) ≥10 cfu/gClostridium perfringens APHA (4th Edition)(Cl.

34.71) Chapter 34Qualitative(Present or Absent)/25 g

Yeast and mould IS 5403 ≥10 cfu/gListeria monocytogenes FDA BAM Chapter 10 Qualitative

(Present or Absent)/25 g4. Canned and

Processed FoodsTotal Aerobic Microbial Count /Aerobic Plate Count/Total Plate Count/ Standard Plate Count/

IS 5402 ≥10 cfu/g











Total Bacterial CountColiform IS 5401 (Part 1) ≥10 cfu/gEscherichia coli IS 5887 (Part 1) Qualitative(Present or

Absent)/g or 0.1 gStaphylococcus aureus IS 5887 (Part 2) Qualitative(Present or

Absent)/25 gFaecal streptococci IS 5887 (Part 2) ≥10 cfu/gSalmonella spp. IS 5887 (Part 3) Qualitative(Present or

Absent)/25 gShigella spp. IS 5887 (Part 7) Qualitative(Present or

Absent)/25 gBacillus cereus IS 5887 (Part 6) ≥10 cfu/gClostridium perfringens APHA (4th Edition)(Cl.


Yeast and mould IS 5403 ≥10 cfu/gListeria monocytogenes FDA BAM, Chapter 10 Qualitative(Present or

Absent)/25 g

5. Fruit juices and pulps

Total Aerobic Microbial Count/ Aerobic Plate Count/Total Plate Count/ Standard Plate Count/ Total Bacterial Count

IS 5402 ≥1 cfu/ml

Coliform IS 5401 (Part 1) ≥1 cfu/mlEscherichia coli IS 5887 (Part 1) Qualitative(Present or

Absent)/ml or 0.1 mlStaphylococcus aureus IS 5887 (Part 2) Qualitative(Present or

Absent)/25 mlFaecal streptococci IS 5887 (Part 2) ≥1 cfu/mlSalmonella spp. IS 5887 (Part 3) Qualitative(Present or

Absent)/25 ml











Shigella spp. IS 5887 (Part 7) Qualitative(Present or Absent)/25 ml

Bacillus cereus IS 5887 (Part 6) ≥1 cfu/mlClostridium perfringens APHA (4th Edition)(Cl.

34.71) Chapter 34Qualitative(Present or Absent)/25 ml

Yeast and mould IS 5403 ≥1 cfu/mlListeria monocytogenes FDA BAM, Chapter 10 Qualitative(Present or

Absent)/25 mlAciduric flat sour spore formers

SOP/NAL/M/030 ≥ 1 cfu/ ml

6. Nut & Nut Products


IS 5402 ≥10 cfu/gISO 4833:(Part-1) ≥10 cfu/g

Coliform IS 5401 (Part 1) ≥10 cfu/gISO 4832 ≥10 cfu/g

Escherichia coli IS 5887 (Part 1) Qualitative (Present or Absent)/g or 0.1 g

ISO 16649(Part-2) ≥10 cfu / gStaphylococcus aureus ISO 6888(Part-1) ≥10 cfu / gSalmonella spp. IS 5887 (Part-3) Qualitative

(Present or Absent)/25 gISO 6579 Qualitative (Present or

Absent)/25 gShigella spp. ISO 21567 Qualitative (Present or

Absent)/ 25gYeast and Mould IS 5403 ≥10 cfu/g

ISO 21527-2 ≥10 cfu/gClostridium perfringens ISO 7937 ≥10 cfu / gVibrio cholerae ISO 21872-1 Qualitative(Present or











Absent) / 25gVibrio parahaemolyticus ISO 21872-1 Qualitative(Present or

Absent) / 25gListeria monocytogenes

ISO 11290-1Qualitative(Present or Absent) / 25g

7. Other Specified Food Items, raw and processed (Cereals And Pulses ,Food Grains)



Yeast and Mould IS 5403 ≥10 cfu/gISO 21527-2 ≥10 cfu/g

Staphylococcus aureus IS 5887 (Part- 2) Qualitative(Present or Absent)/25 g

ISO 6888(P-1) ≥10 cfu / gClostridium perfringens APHA (4th Edition)(Cl.


ISO 7937 ≥10 cfu / gColiform IS 5401 (Part -1) ≥10 cfu/g

ISO 4832 ≥10 cfu/gSalmonella spp. IS 5887 (Part- 3) Qualitative(Present or

Absent)/25 gISO 6579 Qualitative(Present or

Absent)/25 gEscherichia coli IS 5887 (Part -1) Qualitative(Present or

Absent)/g or 0.1 gISO 16649(Part-2) ≥10 cfu / g

Shigella spp. ISO 21567 Qualitative(Present or Absent) / 25g

Vibrio cholerae ISO 21872-1 Qualitative(Present or Absent) / 25g











Vibrio parahaemolyticus ISO 21872-1 Qualitative(Present or Absent) / 25g

Listeria monocytogenes ISO 11290-1 Qualitative(Present or Absent) / 25g

8. Bakery & Confectionery Products


IS 5402 ≥10 cfu/g

Yeast and Mould IS 5403 ≥10 cfu/gStaphylococcus aureus IS 5887 (Part- 2) Qualitative

(Present or Absent)/25 gClostridium perfringens APHA (4th Edition)(Cl.


Coliform IS 5401 (Part -1) ≥10 cfu/gSalmonella spp. IS 5887 (Part- 3) Qualitative

(Present or Absent)/25 gEscherichia coli IS 5887 (Part- 1) Qualitative

(Present or Absent)/g or 0.1 g

9. Spice & Spice Products, Herbals And Condiments

Salmonella spp. IS 5887 (Part -3) Qualitative(Present or Absent)/25 g


Total Aerobic Microbial Count/ Aerobic Plate Count/ Total Plate Count/ Standard Plate Count/ Total Bacterial Count

IS 5402 ≥10 cfu/gISO 4833 ≥10 cfu/g

Coliform ISO 4832 ≥10 cfu/gStaphylococcus aureus IS 5887 (Part -2) Qualitative











(Present or Absent)/25 gISO 6888(Part-1) ≥10 cfu / g

Yeast &mould count IS 5403 ≥10 cfu/gISO 21527-2 ≥10 cfu/g

Escherichia coli IS 5887 (Part- 1) Qualitative(Present or Absent)/g or 0.1 g

ISO 16649(Part-2) ≥10 cfu / gPseudomonas aeruginosa

SOP/NAL/M/029 Qualitative(Present or Absent)/25 g

Clostridium perfringens ISO 7937 ≥10 cfu / gBacillus cereus APHA 4th Edition,Chapter-

32(Cl.32.21)≥10 cfu / g

Enterobacteriaceae IS/ISO/7402 ≥10 cfu / gListeria monocytogenes ISO 11290-1 Qualitative(Present or

Absent) / 25g10. Coffee & Cocoa

productsYeast and Mould IS 5403 ≥10 cfu/g

ISO 21527-2 ≥10 cfu/gTotal Aerobic Microbial Count / Aerobic Plate Count/ Total Plate Count/ Standard Plate Count/ Total Bacterial Count


Coliform IS 5401 (Part 1) ≥10 cfu/gISO 4832 ≥10 cfu/g

Salmonella spp. IS 5887 (Part 3) Qualitative(Present or Absent)/25 g


Escherichia coli IS 5887 (Part 1) Qualitative(Present or Absent)/g or 0.1 g

ISO 16649(Part-2) ≥10 cfu/g











Staphylococcus aureus ISO 6888(Part-1) ≥10 cfu / gClostridium perfringens ISO 7937 ≥10 cfu / gBacillus cereus APHA 4TH Edition

Chapter-32(Cl.32.21)≥10 cfu / g

Enterobacteriaceae IS/ISO/7402 ≥10 cfu / gListeria monocytogenes ISO 11290-1 Qualitative

(Present or Absent) / 25g

11. Tea Yeast and Mould IS 5403 ≥10 cfu/gISO 21527-2 ≥10 cfu/g

Total Aerobic Microbial Count/Aerobic Plate Count/ Total Plate Count/ Standard Plate Count/ Total Bacterial Count


Coliform IS 5401 (Part -1) ≥10 cfu/gISO 4832 ≥10 cfu/g

Salmonella spp. IS 5887 (Part -3) Qualitative(Present or Absent)/25 g



ISO 16649(Part-2) ≥10 cfu/gStaphylococcus aureus ISO 6888(Part-1) ≥10 cfu / gClostridium perfringens ISO 7937 ≥10 cfu / gBacillus cereus APHA 4TH Edition

Chapter-32(Cl.32.21)≥10 cfu / g

Enterobacteriaceae IS/ISO/7402 ≥10 cfu / gListeria monocytogenes ISO 11290-1 Qualitative

(Present or Absent) /











25g12. Ready To Eat

Foods (Snacks And Instant Mixes)


IS 5402 ≥10 cfu/g

Escherichia coli IS 5887 (Part-1) Qualitative (Present or Absent)/g or 0.1g

Staphylococcus aureus IS 5887 (Part -2) Qualitative(Present or Absent)/25 g

Bacillus cereus IS 5887 (Part -6) ≥10 cfu/gSalmonella IS 5887 (Part -3) Qualitative

(Present or Absent)/25 g13. Beverages

(Alcoholic And Non Alcoholic)


IS 5402 ≥1 cfu/ml

Coliform IS 5401 (Part -1) ≥1 cfu/mlYeast and mould IS 5403 ≥1 cfu/ml

14. Cooked Food( White Rice, Sambar, Rasam, Veg Curry, Chicken Curry, Mutton Curry, Pulavo, Curd. Chapathi, Poori, Poriyal, Payasam)

Total Aerobic Microbial Count/Aerobic Plate Count/ Total Plate Count/ Standard Plate Count/ Total Bacterial Count

IS 5402 ≥10 cfu/g≥1 cfu/ml

Coliform IS 5401 (Part -1) ≥10 cfu/g≥1 cfu/ml

Staphylococcus aureus IS 5887 (Part- 2) Qualitative(Present or Absent)/25 g or 25 ml

Escherichia coli IS 5887 (Part- 1) Qualitative(Present or











Absent)/g or ml/ 0.1 g or 0.1 ml

Salmonella spp. IS 5887 (Part- 3) Qualitative(Present or Absent)/25 g or 25 ml

Yeast and mould IS 5403 ≥10 cfu/g≥1 cfu/ml

15. Food Additives And Preservatives

Total Aerobic Microbial Count /Aerobic Plate Count/Total Plate Count/ Standard Plate Count/ Total Bacterial Count

IS 5402 ≥10 cfu/g≥1 cfu/ml


Coliform IS 5401 (Part -1) ≥10 cfu/g≥1 cfu/ml


Escherichia coli IS 5887 (Part -1) Qualitative(Present or Absent)/g or ml/ 0.1 g or 0.1 ml

SOP/NAL/M/035 <3 to >1100 MPN/g/mlSalmonella spp. IS 5887 (Part- 3) Qualitative(Present or

Absent)/25 g or 25 mlSOP/NAL/M/032 Qualitative(Present or

Absent)/25 g or 25 mlYeast and mould IS 5403 ≥10 cfu/g

≥ 1 cfu/mlSOP/NAL/M/040 ≥10 cfu/g

≥ 1 cfu/mlBacillus cereus SOP/NAL/M/034 ≥10 cfu/g

≥1 cfu/mlShigella SOP/NAL/M/036 Qualitative(Present or

Absent)/ 25 g / 25mlStaphylococcus aureus SOP/NAL/M/037 ≥10 cfu/g











≥1 cfu/mlVibrio cholera SOP/NAL/M/038 Qualitative(Present or

Absent) / 25 g / 25mlVibrio parahaemolyticus SOP/NAL/M/039 Qualitative(Present or

Absent) / 25 g / 25mlListeria monocytogenes SOP/NAL/M/041 Qualitative (Present or

Absent) / 25g / 25mlClostridium perfringens SOP/NAL/M/042 Qualitative(Present or

Absent)/ 25 g / 25 ml

II MARINE / AQUA CULTURE FOOD PRODUCTS

1. Prawn & Prawn Products, Fish & Fish Products, Shrimps

Total Aerobic Microbial Count/Aerobic plate count/total plate count/ Standard plate count/ Total bacterial count

IS 5402 ≥10 cfu/gISO 4833 ≥10 cfu/gFDA BAM, Chapter 3 ≥10 cfu/gSOP/NAL/M/031 ≥10 cfu/g

Enterobacteriaceae APHA (4th Edition), (Cl. 8.6) Chapter 8

≥10 cfu/g

Coliforms IS 5401 (Part- 1) ≥10 cfu/gISO 4832 ≥10 cfu/gAPHA (4th Edition),(Cl. 8.71, 8.72&8.73)Chapter 8

≥10 cfu/g MPN 3/g or ml <3 to >1100

SOP/NAL/M/033 ≥10 cfu/gFaecal coliforms APHA (4th Edition), (Cl.

8.81) Chapter 8MPN 3/g or ml <3 to >1100


ISO 16649(Part-2) ≥10 cfu / gFDA BAM Chapter 4 <1.8 to >1600












MPN 3/g<3 to >1100 /1.8/g

SOP/NAL/M/035 <3 to >1100 MPN/gStaphylococcus aureus IS 5887 (Part -2) Qualitative

(Present or Absent)/25 gISO 6888(Part-1) ≥10 cfu / gFDA BAM , Chapter 12 ≥10 cfu / gSOP/NAL/M/037 ≥10 cfu / g

Faecal streptococci IS 5887 (Part- 2) ≥10 cfu/gSalmonella spp. IS 5887 (Part -3) Qualitative

(Present or Absent)/25 gISO 6579 Qualitative

(Present or Absent)/25 gFDA BAM, Chapter 5 Qualitative

(Present or Absent)/25 gSOP/NAL/M/032 Qualitative

(Present or Absent)/25 gShigella spp. IS 5887 (Part- 7) Qualitative

(Present or Absent)/25 gISO 21567 Qualitative

(Present or Absent)/25 gFDA BAM , Chapter 6 Qualitative

(Present or Absent)/25 gSOP/NAL/M/036 Qualitative

(Present or Absent)/25 gBacillus cereus IS 5887 (Part -6) ≥10 cfu/g

APHA (4th Edition) (Cl. 32.21) Chapter 32

≥10 cfu/g

Clostridium perfringens ISO 7937 ≥10 cfu/gAPHA (4th Edition) (Cl. 34.71) Chapter 34

Qualitative(Present or Absent)/25 g

SOP/NAL/M/042 Qualitative











(Present or Absent)/25 gYeast and mould IS 5403 ≥10 cfu/g

ISO 21527-1 ≥10 cfu/gAPHA (4th Edition),(Cl. 20.51) Chapter 20

≥10 cfu/g

FDA BAM, Chapter18 ≥10 cfu/gSOP/NAL/M/040 ≥10 cfu/g

Vibrio cholerae IS 5887 (Part- 5) Qualitative(Present or Absent)/25 g



Qualitative(Present or Absent)/25 g

FDA BAM Chapter 9 Qualitative(Present or Absent)/25 g


Vibrio parahaemolyticus IS 5887 (Part- 5) Qualitative(Present or Absent)/25 g



MPN 3/g<3 to >1100


Vibrio vulnificus APHA (4th Edition), (Cl. 40.53) Chapter 40

MPN 3/g;<3 to >1100

Listeria monocytogenes FDA BAM Chapter 10 Qualitative(Present or Absent)/25 g


SOP/NAL/M/041 Qualitative











(Present or Absent)/25 gIII WATER

1. Packaged Drinking Water, Packaged Natural Mineral Water

Total Aerobic Microbial Count/Aerobic Plate Count/Total Plate Count/ Standard Plate Count/ Total Bacterial Count@37 and 20-22 degree

IS 5402 ≥ 1 cfu/ ml

Coliform IS 15185 Qualitative(Present or Absent)/250ml

IS 5401 (Part- 1) ≥ 1 cfu/ mlEscherichia coli IS 15185 Qualitative

(Present or Absent)/250ml

IS 5887 (Part -1) Qualitative(Present or Absent)/250ml

Faecal streptococci IS 15186 Qualitative(Present or Absent)/250ml

IS 5887 (Part -2) Qualitative(Present or Absent)/250ml

Staphylococcus aureus IS 5887 (Part-2) Qualitative(Present or Absent)/250ml

Salmonella spp. IS 15187 Qualitative(Present or Absent)/250 ml











Shigella spp. IS 5887 (Part -7) Qualitative(Present or Absent)/250ml

Pseudomonas aeruginosa

IS 13428 Qualitative(Present or Absent)/250ml

Sulphite reducing anaerobes

IS 13428 (Annexure C) Qualitative(Present or Absent)/50 ml

Vibrio cholerae IS 5887 (Part- 5) Qualitative(Present or Absent)/250 ml

Vibrio parahaemolyticus IS 5887 (Part- 5) Qualitative(Present or Absent)/250 ml

Yeast and Mould IS 5403 Qualitative(Present or Absent)/250 ml

2. Drinking Water. (Raw water, Bore well water, Treated water, Waste water)


IS 1622 ≥ 1cfu/ ml

Coliform IS 1622 (<2 MPN to >1600 MPN)/100 ml(<1 to >161 MPN)/ 100ml

Thermotolerent Coliform(Faecal Coliform)

IS 1622 (<2 MPN to > 1600 MPN)/100 ml(<1 to >161 MPN) / 100ml











Escherichia coli IS 1622 (<2 MPN to >1600 MPN)/100 ml(<1 to >161 MPN )/ 100ml

3. Water For Processed Food Industry

Proteolytic organism IS 4251(Appendix A) ≥ 1 cfu/mlLipolytic organism IS 4251(Appendix A) ≥ 1 cfu/ml

Thermophilic bacteria count

IS 4251(Appendix B) ≥ 1 cfu/ml

4. Water As Per (98/83/EC)


APHA (22nd Edition) 9215B ≥ 1 cfu/ml

Total Aerobic Microbial Count/Aerobic Plate Count/Total Plate Count/ Standard Plate Count/ Total Bacterial Count @ 37˚C & 22˚C

ISO 6222 ≥ 1Cfu/ ml

Coliform IS 15185 (ISO 9308-1) Qualitative(Present or Absent)/250ml

ISO 9308-1 Qualitative(Present or Absent)/250ml≥ 1Cfu/ ml

Escherichia coli IS 15185 (ISO 9308-1) Qualitative(Present or Absent)/250ml

ISO 9308-1 Qualitative (Present or











Absent)/250ml≥ 1Cfu/ ml

Enterococci(Faecal streptococci)

IS 15186 (ISO 7899-2) Qualitative(Present or Absent)/250ml

ISO 7899-2 Qualitative (Present or Absent)/250ml≥ 1Cfu/ ml

Salmonella IS 15187(ISO 6340)

Qualitative(Present or Absent)/250ml

Pseudomonas aeruginosa

IS 13428 (Annexure D) Qualitative(Present or Absent)/250ml

ISO 16266 Qualitative(Present or Absent)/250ml≥ 1Cfu/ ml

Clostridium perfringens(Including spores)

IS 13428 (Annexure C) Qualitative(Present or Absent)/50 ml

ISO 14189 Qualitative (Present or Absent)/250ml≥ 1Cfu/ ml

IV ENVIRONMENT AND POLLUTION

1. Air(Air Sampling-Settle Plate, Air

Total Aerobic Microbial Count/Aerobic Plate Count/

SOP/NAL/M/007 ≥ 1Cfu/L≥ 1Cfu/m3











sampler)Environmental Monitoring)

Total Plate Count/ Standard Plate Count/ Total Bacterial CountTotal yeast and mould count

SOP/NAL/M/007 ≥ 1Cfu/L≥ 1Cfu/m3

2. Bio Burden Estimation of Classified and Non Classified Areas (Machineries,Personnel Swab,Hand Swab,Contact Plate (Finger Dab Meth-od), Uniform Swab, Equipment Swab, Sanitization Effic-iency Of Equip-ments, Machine Parts Used in Production Area,Material Swab,Cooking Plat-forms, Cooking Accessories, Floor Swab


SOP/NAL/M/024 ≥1 cfu/cm2

≥1 cfu /swab

Coliform SOP/NAL/M/024 ≥1 cfu/cm2

≥1 cfu /swabEscherichia coli SOP/NAL/M/024 Qualitative

(Present or Absent)/10 cm2or swab

Yeast and Mould SOP/NAL/M/024 ≥1 cfu/cm2

≥1 cfu /swab











CHEMICAL TESTING

I ATMOSPHERIC POLLUTION

1 Ambient Air SPM (Suspended Particulate Matter)

IS 5182 (Part -4) 5.0 to 1500 μg/m3

Sulphur Dioxide as SO2 IS 5182 (Part -2) 3.0 to 100 μg/m3

Nitrogen Dioxide as NO2 IS 5182 (Part- 6) 9.0 to100 μg/m3

RPM (PM10)Particulate matter (Size less than10 µm)

IS 5182 (Part- 23) 5.0 to 250 μg/m3

PM 2.5 Particulate matter(Size less than 2.5 µm)

BS EN 14907 10.0 to 100 μg/m3

Ozone as O3 IS 5182 (Part -9) 10.0 to 200 μg/m3

Lead as Pb BS EN 14902 0.05 to 100 µg/m3

Arsenic as As BS EN 14902 2.0 to 15 ng/m3

Nickel as Ni BS EN 14902 2.0 to 30 ng/m3

Carbon monoxide as CO IS 5182 (Part-10) Cl. 6 (Electrochemical Method)

115 to 2520 µg/m3

Ammonia as NH3 Methods of Air Sampling and Analysis (3rd Edition), 401

20 to 500 µg/m3

Benzene as C6H6 IS 5182 (Part -11) Cl. 4 0.1 to 30 μg/m3

Toluene IS 5182 ( Part -11) Cl. 4 0.1 to 500 μg/m3

Xylene IS 5182 (Part -11) Cl. 4 0.1 to 500 μg/m3

Benzo (α) Pyrene IS 5182 (Part -12) 0.04 to 25 ng/m3

VOCs ASTM D 3685 & ASTM D 3687

1.0 to 1000 mg/m3

2 Stack Emission Particulate Matter IS 11255 (Part -1) 5.0 to 5000mg/Nm3

Sulphur Dioxide as SO2 IS 11255 (Part- 2) 3.0 to 200 mg/Nm3

Oxides of Nitrogen (NOx) IS 11255 (Part -7) 9.0 to 300 mg/Nm3











as NO2 Lead (in Particulate Matter) (in Particulate Matter)

BS EN 14902 0.1 to 50 mg/m3

Carbon Monoxide as CO NAL/SOP/STA/005 10.0 to 500 mg/m3

Velocity of flue Gas IS 11255 (Part 3) 1.0 to 60 m/sNon Methyl hydro carbon(NMHC)

IS 5182 (Part 21) 1.0 to 50 mg/m3

3 Volatile Organic Compounds

Acetone

NAL/SOP/STA/013

0.1 to 10000 mg/m3

Benzene 0.1 to 10000 mg/m3

Cyclohexane 0.1 to 20000 mg/m3

Ethanol 0.1 to 10000 mg/m3

Ethyl Acetate 0.1 to 10000 mg/m3

Heptane 0.1 to 10000 mg/m3

Toluene 0.1 to 10000 mg/m3

Xylene 0.1 to 10000 mg/m3

Hexane 0.1 to 10000 mg/m3

N-Butyle Acetate 0.1 to 10000 mg/m3

Methyl Ethyl Ketone 0.1 to 10000 mg/m3

Carbondisulphide 0.1 to 10000 mg/m3

Carbon tetra chloride 0.1 to 10000 mg/m3

Phenol 0.1 to 10000 mg/m3

Methanol 0.1 to 10000 mg/m3

II POLLUTION & ENVIRONMENT

1 Waste Water (Effluents/ Sewage)

pH IS 3025 (Part 11) 1 to 14Total Solids IS 3025 (Part 15) 2.5 to 20000 mg/lTemperature IS 3025 (Part 9) Ambient to 60°CTotal Dissolved Solids IS 3025 (Part 16) 2.5 to 20000 mg/lTotal Suspended Solids IS 3025 (Part 17) 5.0 to 1000 mg/lResidual Chlorine IS 3025 (Part 26), Cl. 3,4 0.01 to 100mg/l











Sulphate as SO4 IS 3025 (Part- 24),Cl. 2,4 5.0 to 2500 mg/lChloride as Cl IS 3025 (Part -32), Cl. 2 1.0 to 2500 mg/lSulphide as H2S IS 3025 (Part -29), Cl. 2,3 0.05 to 10 mg/lOil & Grease IS 3025 (Part -39), Cl. 5 2.0 to 200 mg/lAmmonical Nitrogen as NH3-N

IS 3025 (Part- 34), Cl. 2.2, 2.3

0.05 to 100 mg/l

COD (Chemical Oxygen Demand)

IS 3025 (Part- 58) 4.0 to 25000 mg/l

BOD at 27°C for 3 days (Biological Oxygen Demand)

IS 3025 (Part -44) 2.5 to 5000 mg/l

Residual Sodium Carbonate

IS 11624 By Calculation

Hexavalent Chromium as Cr6+

IS 3025 (Part -52) 0.05 to 25 mg/l

Cyanide as CN IS 3025 (Part- 27),Cl. 2 0.1 to 1 mg/lPhenolic compounds as C6H5OH

IS 3025 (Part -43),Cl. 5,6 0.001 to 10 mg/l

Free Ammonia as NH3 IS 3025 (Part -34),Cl. 2.2, 2.3

0.1 to 100 mg/l

Percent Sodium IS 11624 By CalculationBoron as B IS 13428,Annexure H 0.05 to 10 mg/lTotal Kjeldahl Nitrogen as N

IS 3025 (Part- 34),Cl. 5.3 0.5 to 250 mg/l

Reactive Silica as SiO2 IS 3025 (Part- 35),Cl. 3 1.0 to 100 mg/lFluoride as F IS 3025 (Part -60) 0.02 to 10 mg/lCopper as Cu IS 3025 (Part-42), Cl. 6 0.05 to 25 mg/lNickel as Ni IS 3025 (Part -54) 0.05 to 25 mg/lZinc as Zn IS 3025 (Part -49) 0.01 to 25 mg/lLead as Pb IS 3025 (Part -47) 0.05 to 50 mg//lSodium as Na IS 3025 (Part -45),Cl. 5 1.0 to 500 mg/lPotassium as K IS 3025 (Part- 45),Cl. 5 1.0 to 500 mg/l











Sodium Absorption Ratio IS 3025 (Part -45), Cl. 5 By CalculationPhosphate as PO4/P2O5 IS 3025 (Part -31),Cl. 4 0.05 to 100 mg/lTotal Chromium as Cr IS 3025(Part -52),Cl. 7 0.05 to 40 mg/lArsenic as As IS 3025 (Part -37),Cl. 2 0.001 to 100 mg/lCadmium as Cd IS 3025 (Part -41),Cl. 3 0.01 to 10 mg/lIron as Fe IS 3025 (Part -53),Cl. 6, 7 0.05 to 25 mg/l Mercury as Hg IS 3025 (Part- 48) 0.001 to 10 mg/lSelenium as Se IS 3025 (Part- 56) 0.001 to 10 mg/lManganese as Mn IS 3025 (Part-59) 0.05 to 25 mg/lAluminium as Al IS 3025 (Part -55) 0.05 to 25 mg/l

2 Soil/Sediments pH IS 2720 (Part -26) 1 to 14Electrical Conductivity IS 14767 2.5 to 2000 μS/cmOrganic Matter IS 2720 (Part -22) By CalculationAvailable Sodium as Na USEPA 3050 B Rev. 2 &

USEPA 7000B Rev. 21.0 to 1000 mg/kg

Available Potassium as K USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1.0 to 500 mg/kg

Available Phosphorus IS 10158 1 to 500 mg/kgAvailable Nitrogen as N NAL/SOP/SAS/008 1 to 500 mg/kgCalcium as Ca USEPA 3050 B Rev. 2 &

USEPA 7000B Rev. 21 to 5000 mg/kg

Magnesium as Mg USEPA 3050 B Rev. 2: & USEPA 7000B Rev. 2

1 to 500 mg/kg

Copper as Cu SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 20 mg/kg

Cation Exchange Capacity

USEPA 9080-1 1to 50 meq/100g

Moisture IS 2720 (Part- 2) 0.1 to 90 g/100g Organic carbon IS 2720 (Part -22) 0.05 to 50 g/100g Barium SW- 846/USEPA 3050 B

Rev. 2 &0.5 to 200 mg/kg











USEPA 7000B Rev. 2Iron as Fe SW- 846/USEPA 3050 B

Rev. 2 & USEPA 7000B Rev. 2

1 to 10000 mg/kg

Lead as Pb SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg

Total Chromium as Cr SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg

Nickel as Ni SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg

Zinc as Zn SW- 846/USEPA 3050 B Rev. 2 &USEPA 7000B Rev. 2

0.2 to 5000 mg/kg

3 Wastes(Liquid/Slurry/Sludge/Solid/ Semi-Solid)

Iron as Fe SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

0.05 to 5 g/100 g

Total Chromium as Cr SW- 846/USEPA 3050 BRev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg

Nickel As Ni SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg


1 to 200 mg/kg

Arsenic as As USEPA 3050 B Rev. 2 & USEPA 7062B

0.1 to 100 mg/kg

Antimony as Sb USEPA 3050 B Rev. 2 & USEPA 7000B-1 Rev. 2

0.1 to 100 mg/kg

Selenium as Se USEPA 3050 B Rev. 2 & 0.1 to 100 mg/kg











USEPA 7740-1 Rev.0Ash content/Non Volatile matter

ASTM D 3174IS 10158

1 % to 25 %

Moisture ASTM D 3173-11IS 9235

1 % to 60 %

Volatile matter ASTM D 3175-11,IS 10158 1 % to 15 % Fixed Carbon ASTM D 3172-13 1 % to 25 % Gross Calorific Value IS 10158 100 to 9000 k.Cal/kgNitrogen as N NAL/SOP/SAS/008 1 to 500 mg/kgPhosphorus IS 10158 1 to 500 mg/kgPotassium as K USEPA 3050 B Rev. 2 &

USEPA 7000B-1 Rev. 21 to 500 mg/kg

Calcium as Ca USEPA 3050 B Rev. 2 & USEPA 7000B -1 Rev. 2

1 to 5000 mg/kg

Magnesium as Mg USEPA 3050 B Rev. 2 & USEPA 7000B -1 Rev. 2

1 to 500 mg/kg

Sodium as Na USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 500 mg/kg

Copper as Cu SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg

Cadmium as Cd SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

0.5 to 50 mg/kg

Zinc as Zn USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

0.2 to 5000 mg/kg

Mercury as Hg USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

0.1 to 1000 mg/kg


IS 3025(Part -52) 0.05 to 1000 mg/kg

4 Municipal Solid wastes

Iron as Fe SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

0.05 to 5 g/100 g











Total Chromium as Cr SW- 846/USEPA 3050 BRev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg

Nickel As Ni SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 200 mg/kg


1 to 200 mg/kg

Arsenic as As USEPA 3050 B Rev. 2 & USEPA 7062B

0.1 to 100 mg/kg

Antimony as Sb USEPA 3050 B Rev. 2 & USEPA 7000B-1 Rev. 2

0.1 to 100 mg/kg

Selenium as Se USEPA 3050 B Rev. 2 & USEPA 7740-1 Rev.0,

0.1 to 100 mg/kg

Ash content/Non Volatile matter

ASTM D 3174,IS 10158 1 % to 25 %

Moisture ASTM D 3173-11, IS 9235 1 % to 60 %Volatile matter ASTM D 3175-11, IS 10158 1 % to 15 % Fixed Carbon ASTM D 3172-13 1 % to 25 % Gross Calorific Value IS 10158 100 to 9000 k.Cal/kgNitrogen as N NAL/SOP/SAS/008 1 to 500 mg/kgPhosphorus as P IS 10158 1 to 500 mg/kgPotassium as K USEPA 3050 B Rev. 2 &

USEPA 7000B-1 Rev. 21 to 500 mg/kg

Calcium as Ca USEPA 3050 B Rev. 2 & USEPA 7000B -1 Rev. 2

1 to 5000 mg/kg

Magnesium as Mg USEPA 3050 B Rev. 2 & USEPA 7000B -1 Rev. 2

1 to 500 mg/kg

Sodium as Na USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

1 to 500 mg/kg

Copper as Cu SW- 846/USEPA 3050 B Rev. 2 & USEPA 7000B

1 to 200 mg/kg











Rev. 2Cadmium as Cd SW- 846/USEPA 3050 B

Rev. 2 & USEPA 7000B Rev. 2

0.5 to 50 mg/kg

Zinc as Zn USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

0.2 to 5000 mg/kg

Mercury as Hg USEPA 3050 B Rev. 2 & USEPA 7000B Rev. 2

0.1 to 1000 mg/kg


IS 3025(Part 52) 0.05 to 1000 mg/kg

5 Effluents toxicity[Toxicity Characteristic Leaching Procedure(TCLP)]

Arsenic as As APHA (22nd Edition) 3114-C: Page. 3-38/USEPA 1311-1

0.1 to 1000 mg/l

Cadmium as Cd APHA (22nd Edition) 3111-B: Page. 3-18/USEPA 1311-1

0.1 to 1000 mg/l

Chromium as Cr APHA (22nd Edition) 3500 Cr-A USEPA 1311-1

0.1 to 1000 mg/l


APHA (22nd Edition) 3500 Cr-B: Page.3-69/USEPA 1311-1

0.1 to 1000 mg/l

Nickel as Ni APHA (22nd Edition) 3111-B: Page.3-18/USEPA 1311-1

0.1 to 1000 mg/l

Selenium as Se APHA (22nd Edition) 3114-C: Page. 3-38/USEPA 1311-1

0.1 to 1000 mg/l

Silver as Ag APHA (22nd Edition) 3111-B: 2 Page. 3-18/USEPA 1311-1

0.1 to 1000 mg/l

Barium as Ba APHA (22nd Edition) 3111-D: Page. 3:20/USEPA 1311-1

0.1 1000 mg/l

Mercury as Hg APHA (22nd Edition) 3112-B: 0.1 to 1000 mg/l











Page. 3-23/USEPA 1311-1Zinc as Zn APHA (22nd Edition) 3111-B:

Page. 3-18/USEPA 1311-10.1 to 1000 mg/l

Copper as Cu APHA (22nd Edition) 3111-B: Page. 3-18/USEPA 1311-1

0.1 to 1000 mg/l

Lead as Pb APHA (22nd Edition) 3111-B: Page. 3-18/USEPA 1311-1

0.1 to 1000 mg/l

III WATER

1. Water (Packaged Drinking Water Other Than Packaged Natural Mineral Water & Packaged Natural Mineral Water Other Than Packaged Drinking Water , Drinking Water, Water (EU Council Directive 98/83/EC Of 3 November 1998) On The Quality Of Water Intended For Human Consumption, Raw Water, Bore Well Water, Ro Processed Water, Product Water,

Colour IS 3025 (Part- 4) 1 to 75 HazenOdour IS 3025 (Part- 5) QualitativeTaste IS 3025 (Part -8) QualitativeElectrical Conductivity IS 3025 (Part -14) 1 to 10000 µS/cmTurbidity IS 3025 (Part- 10) 0.5 to 4000 NTUTotal Hardness as CaCO3

IS 3025 (Part- 21) 1 to 1000 mg/l

Total Dissolved Solids IS 3025 (Part -16) 5 to 2000 mg/lpH IS 3025(Part-11), Cl. 2 1 to 14Nitrate as NO3 IS 3025(Part -34),Cl. 3.3 1 to 55.0 mg/lNitrite as NO2 IS 3025 (Part- 34), Cl. 4 0.01 to 10 mg/lFluoride as F IS 3025 (Part -60) 0.02 to 10.0mg/lAmmonia (as Total Ammonia-N)

IS 3025 (Part -34) 0.25 to 2.5.mg/l

Chloride as Cl IS 3025 (Part -32),Cl. 2 1 to 1000 mg/lSulphate as SO4 IS 3025 (Part- 24),Cl. 2, 4 5 to 400 mg/lTotal Alkalinity as CaCO3

IS 3025(Part -23) 1 to 500 mg/l

Calcium as Ca IS 3025 (Part- 40),Cl. 5 1 to 1000 mg/lMagnesium as Mg IS 3025 (Part- 46),Cl. 6 0.5 to 1000 mg/lSodium as Na IS 3025 (Part -45),Cl. 5 1.0 to 1000 mg/lResidual Free Chlorine IS 3025 (Part -26),Cl. 3,4 0.02 to 5 mg/l











Swimming Pool Water, Product Water, Ground Water, Surface Water)

Mineral Oil IS 3025 (Part- 39),Cl. 6 0.01 to 10 mg/l Anionic surface Active agents as MBAS

IS 13428,Annexure K 0.1 to 1.0 mg/l

Sulphide as H2S IS 3025 (Part- 29),Cl. 2,3 0.05 to 25 mg/lBorates as B IS 13428,Annexure H 0.05 to 25 mg/lChloramines as Cl2 IS 3025 (Part -26),Cl. 3,4 0.1 to 10.0 mg/lTotal organic carbon (TOC)

APHA (22nd Edition) 5310 0.5 to 25 mg/l

Bromates as BrO3 ISO 15061 0.005 to 1 mg/l

IV RESIDUES IN WATER

1. Water Pesticides2, 4 DDT (O,P DDT) USEPA 525.2,Rev 2.0,

USEPA 8141A, Rev. 1,USEPA 515.1, Rev. 4.1,USEPA 532 ,Rev. 1,USEPA 507, Rev. 2.1,AOAC (19th Edition) 990.06:Chapter 10, Page. 27

0.025 to 100 µg/l4, 4 DDT (P,P DDT) 0.025 to 100 µg/l2, 4 DDE (O,P DDE) 0.025 to 100 µg/l4, 4 DDE (P,P DDE) 0.025 to 100 µg/l2, 4 DDD (O,P DDD) 0.025 to 100 µg/l4,4 DDD (P,P DDD) 0.025 to 100 µg/l

- HCH (Lindane) USEPA 525.2,Rev 2.0,USEPA 8141A, Rev. 1,USEPA 515.1, Rev. 4.1,USEPA 532 ,Rev. 1,USEPA 507, Rev. 2.1,AOAC (19th Edition) 990.06:Chapter 10, Page. 27

0.025 to 100 µg/l - HCH 0.025 to 100 µg/l - HCH 0.025 to 100 µg/l - HCH 0.025 to 100 µg/lEndosulfan 0.025 to 100 µg/lEndosulfan 0.025 to 100 µg/lEndosulfan sulphate 0.025 to 100 µg/lMonocrotophos 0.025 to 100 µg/lEthion 0.025 to 100 µg/lChlorpyrifos 0.025 to 100 µg/l











Phorate 0.025 to 100 µg/lButachlor 0.025 to 100 µg/lPhorate sulphone 0.025 to 100 µg/lAlachlor 0.025 to 100 µg/lAtrazine 0.025 to 100 µg/lMethyl parathion 0.025 to 100 µg/lMethyl Paraoxon 0.025 to 100 µg/lMalathion 0.025 to 100 µg/lMalaoxon 0.025 to 100 µg/lAldrin 0.025 to 100 µg/lDieldrin 0.025 to 100 µg/lPhorate sulphoxide 0.025 to 100 µg/lIsoproturon 0.025 to 100 µg/l2, 4 – D 0.025 to 100 µg/lAcrylamide USEPA 8032A-1,Rev. 1 0.1 to 100 µg/lEpichlorohydrin USEPA 8260B-1,Rev. 2 0.1 to 100 µg/l1,2-dichloroethane

USEPA 5030C-2,Rev. 3

0.1 to 100 µg/lTrichloroethene 0.1 to 100 µg/lTetra chloroethane 0.1 to 100 µg/lBromoform 0.1 to 100 µg/lDibromochloromethane 0.1 to 100 µg/lBromodichloromethane 0.1 to 100 µg/lChloroform 0.1 to 100 µg/lVinyl chloride 0.1 to 100 µg/lBenzene 0.1 to 100 µg/lTrace Metals ElementsCopper as Cu IS 3025 (Part- 42),Cl. 6/

APHA (22nd Edition)/ USEPA 200.8 Rev.5.4

0.01 to 5.0 mg/l

Iron as Fe IS 3025 (Part- 53),Cl. 6,APHA (22nd Edition) 3500- Fe B

0.05 to 15.0 mg/l











Manganese as Mn IS 3025 (Part -59),APHA (22nd Edition)

0.05 to 15.0 mg/l

Selenium as Se IS 3025 (Part- 56), IS 15303, Cl. 7

0.001 to 1 mg/l

Antimony as Sb IS 13428,IS 15303Annexure G

0.001 to 1.5 mg//l

Barium as Ba IS 13428 Annexure F/APHA (22nd Edition) 3125B/USEPA 200.8 Rev. 5.4: /IS 15302

0.05 to 10.0 mg/l

Mercury as Hg IS 3025 (Part- 48) 0.0005 to 1 mg/lCadmium as Cd IS 3025 (Part- 41) 0.001 to 5 mg/lArsenic as As IS 3025 (Part -37) 0.001 to 1 mg/lCyanide as CN IS 3025 (Part- 27) 0.001 to 5 mg/lLead as Pb IS 3025 (Part -47),

Clause 70.005 to 5 mg/l

Chromium as Cr IS 13428,Annexure J 0.01 to 5 mg/lNickel as Ni IS 13428,Annexure L 0.01 to 2.0 mg/lZinc as Zn IS 3025 (Part -49) 0.01 to 10 mg/LSilver as Ag IS 13428, Annexure J 0.005 to 1 mg/lAluminium as Al IS 3025 (Part- 55),

Clause 5,6/IS 153020.01 mg/l to 1 mg/l

Molybdenum as Mo IS 3025 (Part 2) 0.02 to 1 mg/lPhenolsPhenolic Compounds IS 3025(Part- 43), Cl. 5,6 0.001 to 1 mg/lPoly Aromatic Hydrocarbons (PAHs)Acenaphthene APHA (22nd Edition) 6440 0.01 to 100 µg/lAcenaphthylene 0.01 to 100 µg/lAnthracene 0.01 to 100 µg/lBenz (a) anthracene 0.01 to 100 µg/lBenzo (b) fluranthene 0.01 to 100 µg/lBenzo (k) fluranthene 0.01 to 100 µg/l











Benzo (g,h,i) perylene 0.01 to 100 µg/lBenzo (a) pyrene 0.01 to 100 µg/lChrysene 0.01 to 100 µg/lDibenz (a,h) anthracene 0.01 to 100 µg/lFluoranthene 0.01 to 100 µg/lFluorene 0.01 to 100 µg/lIndeno (1,2,3-cd) pyrene 0.01 to 100 µg/lNaphthalene 0.01 to 100 µg/lPhenanthrene 0.01 to 100 µg/lPyrene 0.01 to 100 µg/lPoly Chlorinated Biphenyls (PCBs)2,4,4’ Trichloro biphenyl

IS 13428,Annexure M

0.01 to 100 µg/l2, 2,5,5’ Tetra chloro biphenyl

0.01 to 100 µg/l

2, 2’, 3,4,4’, 5’ Hexachlorobiphenyl

0.01 to 100 µg/l

2,2’,4,4’,5,5’ Hexa chloro biphenyl

0.01 to 100 µg/l

2,2’,3,4,4’,5,5’ Hepta chloro biphenyl

0.01 to 100 µg/l

2,6’ Di chloro biphenyl 0.01 to 100 µg/l

V. FOOD & AGRICULTURAL PRODUCTS

1 Fruit & fruit productsIncluding Raw/Frozen/Dried/Cooked/Canned/Processed

Moisture NAL/SOP/FOOD/001 0.5 to 90.0 g/100 g Total Solids AOAC (19th Edition)

920.151,Chapter 371 to 99 g/100 g

Total Soluble Solids IS 13815 5 to 85 g/100 gTotal Ash AOAC (19th Edition) 940.26,

Chapter 370.1 to 5.0 g/100 g

pH AOAC (19th Edition) 981.12, Chapter 42

2.0 to 14.0











Salinity as NaCl IS 2860 0.1 to 20g/100g Total Protein IS 7219 0.1 to 20g/100g Total Fat NAL/SOP/F/014 0.1 to 10g/100g Crude Fiber NAL/SOP/F/015 0.1 to 10g/100g Calcium as Ca IS 5949,IS 2860 0.1 to 5 g/100gMineral Impurities IS 13816 0.05 % to 10 %Acid insoluble Ash IS 13846 0.01 to 3 g/100g Magnesium as Mg IS 5949 10 to 2000 mg/kgSodium as Na AOAC (19th Edition) 966.16,

Chapter 3710 to 2000 mg/kg

Brix IS 2860 4˚ to 85˚Sugar AOAC (19th Edition)

925.35,Chapter 371 to 90g/100g

Alcohol as Ethanol AOAC (19th Edition), Chapter 37,IS 15096

0.01 to 10g/100g

Volatile Acidity IS 3752 0.1 to 10g/100g Starch AOAC (19th Edition) 925.38

Chapter 37Qualitative

Sulphur dioxide AOAC (19th Edition) 990.28 Chapter 47

10 to 5000 mg/kg

Rodent Contamination IS 6261 QualitativeAdded Coloring Matter NAL/SOP/FOOD/002 QualitativeAdded Wax Coating NAL/SOP/F/270 QualitativeInorganic Bromide AOAC (19th Edition) 956.03

Chapter 32,IS 14626 NAL/SOP/F/305

5 to 200 mg/kg

Benzoic acid AOAC (19th Edition) 994.11 10 to 600 mg/kgFruit Content NAL/SOP/FOOD/003 1 % to 50 %Potassium AOAC (19th Edition)

965.30,Chapter 3710 to 2000 mg/kg

Rotting NAL/SOP/FOOD/004 QualitativePatulin AOAC (19th Edition) 995.10 10 to 500 µg/kg











Chapter 49Sorbic Acid IS 12014 (Part- 3) 5 to 360 mg/lDrained Weight AOAC (20th Edition):

953.15 IS: 2860,NAL/SOP/FOOD/022

1 to 99 g/100g

Titrable Acidity IS 2860 /AOAC (20th Edition) 37.1.37/942.15/p.10 NAL/SOP/FOOD/022

0.05 to 12.5 g/100g

Reducing sugar NAL/SOP/FOOD/022 1 to 80 g/100gSand NAL/SOP/FOOD/004 QualitativeGrit NAL/SOP/FOOD/004 QualitativeInsect NAL/SOP/FOOD/004 QualitativeFungal Infection NAL/SOP/FOOD/004 QualitativeExtraneous Matter NAL/SOP/FOOD/004 QualitativeMineral Acid NAL/SOP/FOOD/022 QualitativeDamaged Matter IS 4333 (Part -1) 0.01 to 10g/100gInsect Damaged Units IS 4333 (Part-1) 0.01 to 5 g/100gForeign Matter IS 4333 (Part -1) 0.01 to 25 g/100gLiving and Dead Insects IS 6261 QualitativeFungal Infection NAL/SOP/FOOD/004 Qualitative

2 Vegetable & Vegetable Productsa Including

Raw/Frozen/Dried/Cooked/Canned/Processed

Moisture NAL/SOP/FOOD/001 0.5 to 90.0 g/100 g Total Solids AOAC (19th Edition)

920.151,Chapter 371 to 99 g/100 g

Total Soluble Solids IS 13815 5 to 85 g/100 gTotal Ash AOAC (19th Edition) 940.26

Chapter 370.1 to 5.0 g/100 g

pH AOAC (19th Edition) 981.12Chapter 42

2.0 to 14.0

Salinity as NaCl IS 2860 0.1 to 20g/100g Total Protein IS 7219 0.1 to 20g/100g











Total Fat NAL/SOP/F/014 0.1 to 10g/100g Crude Fiber NAL/SOP/F/015 0.1 to 10g/100g Calcium as Ca IS 5949,IS 2860 0.1 to 5 g/100gMineral Impurities IS 13816 0.05 % to 10 %Acid insoluble ash IS 13846 0.01 to 3 g/100g Magnesium as Mg IS 5949 10 to 2000 mg/kgSodium as Na AOAC (19th Edition) 966.16


Brix IS 2860 4˚ to 85˚Sugar AOAC (19th Edition) 925.35

Chapter 371 to 90g/100g

Alcohol as Ethanol AOAC (19th Edition), Chapter 37,IS 15096

0.01 to 10g/100g

Volatile Acidity IS 3752 0.1 to 10g/100g Starch AOAC (19th Edition)

925.38,Chapter 37Qualitative

Sulphur dioxide AOAC (19th Edition) 990.28Chapter 47

10 to 5000 mg/kg

Rodent Contamination IS 6261 QualitativeAdded Coloring Matter NAL/SOP/FOOD/002 QualitativeAdded Wax Coating NAL/SOP/F/270 QualitativeInorganic Bromide AOAC (19th Edition) 956.03

Chapter 32,IS 14626NAL/SOP/F/305

5 to 200 mg/kg

Benzoic Acid AOAC (19th Edition) 994.11,Chapter 37

10 to 600 mg/kg

Fruit Content NAL/SOP/FOOD/003 1 % to 50 %Potassium AOAC (19th Edition)

965.30,Chapter 3710 to 2000 mg/kg

Rotting NAL/SOP/FOOD/004 QualitativePatulin AOAC (19th Edition)

995.10,Chapter 4910 to 500 µg/kg

Sorbic Acid IS 12014 (Part 3) 5 to 360 mg/l











Drained Weight AOAC (20th Edition), 953.15 IS 2860),NAL/SOP/FOOD/022

1 to 99 g/100g

Titrable Acidity IS 2860,AOAC (20th Edition) 37.1.37/942.15, NAL/SOP/FOOD/022

0.05 to 12.5 g/100g

Reducing Sugar NAL/SOP/FOOD/022 1 to 80 g/100gSand NAL/SOP/FOOD/004 QualitativeGrit NAL/SOP/FOOD/004 QualitativeInsect NAL/SOP/FOOD/004 QualitativeFungal infection NAL/SOP/FOOD/004 QualitativeExtraneous Matter NAL/SOP/FOOD/004 QualitativeMineral Acid NAL/SOP/FOOD/022 QualitativeDamaged Matter IS 4333 (Part -1) 0.01 to 10g/100gInsect Damaged Units IS 4333 (Part -1) 0.01 to 5 g/100gForeign Matter IS 4333 (Part- 1) 0.01 to 25 g/100gLiving and Dead Insects IS 6261 QualitativeFungal Infection NAL/SOP/FOOD/004 Qualitative

3 Cereals, pulses & cereal productsa. Wheat Atta,

Fortified Atta, Protein Rich Atta, Maida, Fortified Maida, Protein Rich Maida,Rawa, Suji, Besant, Pearl Barley, Whole Meal Barley, Corn Flour, Custard Food Grains Wheat, Maize, Jawa, Rice,

Moisture IS 4333 (Part 2) 1.0 to 25 g/100 gTotal Ash IS 1155 0.05 to 10 g/100 gAsh insoluble in dil.HCl IS 1155 0.01 to 5.0 g/100 gGluten IS 1155 1.0 to 20 g/100 gAlcoholic Acidity IS 1009 0.02 to 2.0g/100g Crude fibre IS 1155 0.5 to 25.0 g/100 gCalcium as CaCO3 AOAC (19th Edition) 944.03


Total Protein IS 7219 1 to 95 g/100 gTotal Fat AOAC (19th Edition) 922.06

Chapter 321 to 25 g/100 g

Granularity IS 1155 0.5 % to 100 %











Millet, Ragi, Rye, Masur Whole, Moong Whole, Chana Whole, Dal Moong, Urd, Arhar, Chana, Cornflour, Cornflakes, Macroni Products, Custared Powder, Rolled Oats, Solvent Extracted Flours, Starchy Foods, Food Grains (Malted & Malt Based Foods Processed Cereal Based Complimentary Foods

Foreign Matter/ Extraneous Matter

IS 4333 (Part- 1) 0.01 % to 10 %

Damaged Grains IS 4333 (Part -1) 0.01 % to 40 %

Weevilled Grains IS 4333 (Part- 1) 0.01 % to 50 % Uric Acid IS 4333 (Part 5)

NAL/SOP/F/040 1 to 100 mg/kg

Argemone Seeds IS 2323 QualitativeKhesari Dal IS 2400 Qualitative Mineral Matter NAL/SOP/FOOD/005 0.01 % to 10 %Organic Matter NAL/SOP/FOOD/005 0.01 % to 10 %Insect Damaged Grains IS 4333 (Part -1) 0 to 25 %Other Edible grains IS 4333 (Part- 1) 0 to 25 %Insect IS 6261 QualitativeRodent Hair & Excreta AOAC (19th Edition) 941.16


Inorganic Bromide AOAC (19th Edition) 956.03Chapter 32,IS 14626NAL/SOP/F/305

5 to 1000 mg/kg

Hydrocyanic Acid as HCN

AOAC (19th Edition) 915.03,Chapter-49

1 to 1000 mg/kg

Hydrogen phosphide as AlP

IS 6438,NAL/SOP/F/306 0 to 1000 mg/kg

Bulk Density IS 1797 0.16 to 2g/cm3

Added Coloring Matter NAL/SOP/FOOD/002 QualitativeWet Gluten IS 8162 10 % to 50 % Sedimentation Index IS 13864 1 to 80 mlDeoxynivalenol (DON) NAL/SOP/INS/005 10 to 200 mg/kgMould NAL/SOP/FOOD/004 QualitativeMusty odour IS 1656 QualitativeRancidity NAL/SOP/FOOD/014 Qualitative











Dirt NAL/SOP/FOOD/004 Qualitative

Potassium Bromate AOAC (20th Edition)956.03 1 to 100 mg/kgFungus NAL/SOP/FOOD/004 QualitativeLarva NAL/SOP/FOOD/004 QualitativeSulphur dioxide AOAC (20th Edition)990.28


Total Ash excluding Salt IS 1158 0.01 to 20 g/100gSolubility IS 1806 QualitativeFree Gossypol NAL/SOP/FOOD/023 0.01 to 1 g/100gTotal Gossypol NAL/SOP/FOOD/023 0.01 to 2 g/100g

4 Nuts & nut productsa. Raw And

Processed-(Including Peanut And Peanut Products/ Pistachios/ Almonds/ Walnuts/Paprika/ Coconut & Coconut Products/Cashew Nuts)

Moisture AOAC (19th Edition) 925.40,Chapter 40,

1 % to 25.0 %

Crude Protein AOAC (19th Edition) 950.48,1 Chapter 40

1 % to 30 %

Crude Fat AOAC (19th Edition) 948.22 Chapter 40

0.1 % to 75 %

Crude Fiber NAL/SOP/F/015 0.1 % to 15 %Sulphur dioxide AOAC (19th Edition) 990.28


Extraneous matter IS 4333 (Part-1) 0.1 % to 10 %Insects Fragments IS 6261 QualitativeRodent Hair& Excreta AOAC (19th Edition) 941.16


Acidity of Extracted Fat as Oleic Acid

IS 15271 0.1 to 5 g/100 g

Sodium AOAC (19th Edition) 956.01,Chapter 3.0

0.01 to 1 g/100g

Potassium AOAC (19th Edition) 956.01,Chapter 3.0

0.01 to 1 g/100g

Magnesium AOAC (19th Edition) 920.09 ,Chapter 3.0

0.02 to 5 g/100g











Calcium AOAC (19th Edition) 910.01Chapter 3.0

0.02 to 5 g/100g

Ash IS 966,AOAC (19th Edition) 950.49, Chapter 40

0.1 to 5.0 g/100g

Sodium Chloride as NaCl AOAC (19th Edition) 950.52,Chapter 40

0.1 to 20 g/100g

Fungal Infection NAL/SOP/FOOD/004 QualitativeStones NAL/SOP/FOOD/004 QualitativeDirt Clay NAL/SOP/FOOD/004 QualitativeDamaged Kernel /Slightly Damaged Kernel

IS 4333 0.01 to 10%

Mineral Oil IS 15642 QualitativeDamaged Raisins NAL/SOP/FOOD/039 0.01 to 10 g/100gBlemished / Damaged Units

NAL/SOP/FOOD/039 0.01 to 10 g/100g

Mustiness NAL/SOP/FOOD/040 QualitativeRancidity NAL/SOP/FOOD/014 QualitativeHydrocyanic Acid as HCN/ Hydrogen Cyanide

AOAC (20th Edition)915.03 Chapter 49

1 to 1000 mg/kg

Inorganic Bromide NAL/SOP/F/305 5 to 1000 mg/kgHydrogen Phosphide NAL/SOP/FOOD/306 0 to 1000 mg/kg

5 Herbs, spices & condimentsa. (Whole &

Ground)Caraway, Cardamom, Chillies & Capsicum,Cinnamon, Cassia, Cloves, Coriander, Cumin, Fennel, Fenugreek, Ginger, Mace,

Extraneous Matter IS 4333 (Part-1) 0.01 % to 20 %Non volatile Ether Extract IS 1797 1 % to 30 %Rodent Hair & Excreta AOAC (19th Edition) 941.16

Chapter 16Qualitative(Present or Absent)

Damaged/Discolored Unit IS 4333 (Part-1),IS 3579 0.01 % to 20 %Tendrils IS 4404 0.01 % to 10.0 %Mother Cloves IS 4404 0.01 % to 10.0 %Khokar Cloves IS 4404 0.1 % to 10 %Headless Cloves IS 4404 0.01 % to 20 %Insect Fragment IS 4333 (Part-1) Qualitative











Mustard, Nutmeg,Pepper Black,Poppy, Saffron,Turmeric, Curry Powder, Mixed Powder, Aniseed, Ajwain, Dried Mango Slice, Dried Mango Powder, Pepper White, Garlic, Celery, Dehydrated Onion, Asafoetida,Tamarind, Tamarind Concentrate, Garam Masala, Large Cardamom, Amchur, Raw Mango Mangifera Indica Powder, Dehydrated Garlic, Dehydrated Onion, Ajowan,Celery Seeds, Ginger

Insect Damaged Cloves IS 4333 (Part -) 0 to 5 %Damaged/Discolored Cloves

IS 4333 (Part-1) 0.01 % to 20 %

Insect Damaged Matter IS 4333 (Part-1) 0.01 % to 10 %Live & Dead Insects Fragments

IS 4333 (Part-1) Qualitative

Nutmeg in Mace NAL/SOP/FOOD/004 1 % to 5 %Inorganic Bromide IS 14626,NAL/SOP/F/305 5 to 200 mg/kgEmpty/Malformed Capsules

IS 4333 (Part-1) 0.01 % to 50 %

Immature and Shriveled Capsules

IS 4333 (Part -1) 0.01 % to 20 %

Broken Tendrils IS 4333 (Part -1) 0.01 % to 20 %Split Fruits IS 4333 (Part -1) 0.01 % to 5 %Moisture IS 1797 0.1 % to 50 %Total Ash IS 1797 0.1 % to 30 % Ash insoluble in dilute HCl

IS 1797 0.01 % to 5 %

Volatile Oil IS 1797 1 % to 10 %Mineral Oil IS 548 (Part-2),

NAL/SOP/FOOD/014 Qualitative

Crude Fiber IS 1797 0.1 % to 30 %Cold Water Soluble Extract

IS 1797 0.01 % to 20 %

Calcium as Calcium Oxide

IS 1797 0.1 % to 20 %

Water Soluble Ash IS 1797 0.5 % to 5 %Alcohol Soluble Extract IS 1797 1 % to 25 %Starch IS 4706 (Part -2) 1 % to 60 %Bulk Density IS 1797 0.3 to 2.0 g/cm3

Piperine Content in Pepper

AOAC (19th Edition) 987.07 Chapter 43

1 % to 10 %











Lead Chromate in Turmeric

IS 3576 Qualitative

Curcuminoid Content in Turmeric

IS 10925 1.0 to 10

Peroxidase Test NAL/SOP/FOOD/006 QualitativeAllyl iso thiocyanate NAL/SOP/F/239 1.0 % to 25 %p-hydroxyl benzyl iso thiocyanate

NAL/SOP/F/240

2.5 % to 50 %

Argemone seed IS 2323 QualitativeKokum Seed Content IS 13644 0.25 % to 10.0 %Salt as NaCl IS 1797 1 % to 50 %Total Soluble Solids IS 5955 10 % to 50 %Total insoluble Pulp IS 5955 1 % to 50 %Total Reducing Sugar IS 5955 1 % to 70 %Added Coloring Matter NAL/SOP/FOOD/002 QualitativeTurmeric in Chilli and Coriander


Papaya Seeds in Black Pepper


Protein IS 7219 1 % to 50 %Mould NAL/SOP/FOOD/004 QualitativeOrganic Matter NAL/SOP/FOOD/005 QualitativeInorganic Matter NAL/SOP/FOOD/005 QualitativeExtraneous Flavor NAL/SOP/FOOD/040 QualitativeMustiness NAL/SOP/FOOD/040 QualitativeLight seeds/Brown/Red seeds

IS 13446 0.01to 10g/100g

Odour IS 13446,NAL/SOP/FOOD/040

Qualitative

Rancidity NAL/SOP/FOOD/014 QualitativeSulphur dioxide AOAC (20th Edition) 990.28 10 to 5000 mg/kg











Chap.47Defective Seeds IS 3576 0.01 to 10 g/100gArgemone Oil NAL/SOP/FOOD/014 QualitativeLight Berries NAL/SOP/FOOD/029 0.01 to 10 g/100gPinheads or broken Berries

IS 1798 0.01 to 10 g/100g

Other foreign Edible Seeds

IS 4333(Part -1) 0.01 to 10 g/100g

Floral Waste IS 5453 (Part-2) Clause 6 0.05 to 10 g/100gBitterness (Absorbance of picrocine)

IS 5453(part-2),NAL/SOP/FOOD/041

20.0 % to 80.0 %

Flavor(Absorbance of safranal)

IS 5453 (Part-2) 20 to 50 at 330 nm

Coloring strength (Absorbance of crocine)

IS 5453 (Part-2) 50.0 % to 300.0 %

Defective rhizomes IS 3576 Physical Method 0.01 to 10 g/100gBlack berries/Black Pepper

IS 1798 Qualitative

Peroxidase Test NAL/SOP/FOOD/029 QualitativeForeign Resin IS 7807 QualitativeColophony Resin IS 7807 QualitativeGalbanum Resin IS 7807 QualitativeAmmoniaccum Resin IS 7807 QualitativeMineral Pigment ASTA (4th Edition)

Method 14.11 to 10 No

6 Meat & meat products

a. Beef, Canned luncheon Meat, Canned Cooked Ham, Canned Chopped Meat,

Total Volatile Base – N NAL/SOP/FOOD/010 0.5 to 100 mg/100g Total Fat IS 5960 (Part -3) 1 % to 35 %Total Nitrogen IS 5960 (Part -1) 1 % to 50 %Total Ash IS 5960 (Part -2) 1 % to 50 %pH IS 5960 (Part -0) 3 to 12











Canned Chicken, Canned Mutton and Goat Meat, Frozen Mutton, Chicken, Goat and Buffalo

Moisture IS 5960 (Part-5) 5 % to 90 %Mould NAL/SOP/FOOD/004 QualitativeLiving and dead insects IS 6261 QualitativeInsect fragments IS 6261 QualitativeRodent contamination AOAC (20th Edition) 941.16 QualitativeSodium metabisulphite AOAC (20th Edition) 990.28 10 to 5000 mg/kgSodium Nitrite NAL/SOP/FOOD/024,

AOAC (20th Edition) 973.31IS 11747

10 to 1000 mg/kg

Bones NAL/SOP/FOOD/004 QualitativeDetached cartilage ligaments


Blood Clots NAL/SOP/FOOD/004 QualitativeSkin NAL/SOP/FOOD/004 QualitativeHair NAL/SOP/FOOD/004 QualitativeStrings NAL/SOP/FOOD/004 QualitativeFibrous Tissue NAL/SOP/FOOD/004 Qualitative

7 Milk & dairy productsa. Raw Milk &

Processed Milk & Milk ProductsLiquid Milk Condensed/Evaporated Milk(Sweetened Unsweetened)Milk Powder(Whole, Skimmed And Partly Skimmed Milk Powder) CheeseCurd KhoaIce Cream

Solids Not Fat AOAC (19th Edition) 990.21 Chapter 33, IS 12333IS 1479 (Part -2)

5 % to 80 %

Milk Fat AOAC (19th Edition) 989.05,Chapter 33 AOAC (19th Edition)932.06, Chapter 33,IS 3507IS 10484,IS 2785,IS 2802IS 11721,IS 1479 (Part- 2)

1 % to 80 %

Sucrose IS 4079 ,IS 2802IS 1479 (Part -2)

0.5 % to 80 %

Titratable Acidity IS 1166,IS 11766 0.1 % to 3 %Milk Protein AOAC (19th Edition) 991.20,

Chapter 3,AOAC (19th

Edition) 930.29, Chapter 33

1 % to 50 %











Sterilized Milk Ghee/ButterPaneer

IS 7219Moisture AOAC (19th Edition) 927.05

Chapter 33,IS 3508,IS 3507IS 10484,IS 2785,IS 11623

1 % to 50 %

Total Ash AOAC (19th Edition) 930.30 Chapter 33,IS 1479 (Part-2)

0.1 % to 10 %

Total Solids IS 12333, IS 2802IS 1479 (Part- 2),IS 11623

10 % to 99 %

Insolubility Index IS 12759,IS 3568 0.5 to 5 mlRefractive Index IS 3508 1.33 to 1.80Free Fatty Acid as Oleic Acid

IS 3508 0.01 % to 5 %

Peroxide Value IS 3508 0 to 250 meq O2/kgSalt as NaCl IS 2785,IS 3507 1 % to 10 %Acidity as Lactic Acid IS 2802,IS 3507

IS 3508,IS 1479 (Part-1)0.1 % to 10 %

Scorched Particles IS 13500 7.5 to 32.5 mgButyro Refractometer reading

IS 3508 10 to 80

Reichert-meissel Value IS 3508 10 to 35Polenske Value IS 3508 0.1 to 10Baudouins Test IS 3508 QualitativepH IS 1479 (Part -2) 3 to 12Lactose IS 1479 (Part -2) 1 % to 20 %Acid insoluble ash IS 14433 0.01 % to 3 % Potassium AOAC (19th Edition) 990.23

Chapter 33 0.01 % to 3 %

Sodium AOAC (19th Edition) 990.23,Chapter-33

0.01 % to 3 %

Calcium IS 1479 (Part -2)IS 5949

0.1 % to 3 %

Magnesium IS 1479 (Part -2),IS 5949 0.005 % to 3 %Curd IS 3507 0.2 % to 5.0 %











Melamine IS 16195 1 to 10 µg/kgFilthy NAL/SOP/FOOD/004 QualitativePutrid NAL/SOP/FOOD/040

Issue. 01, Issue Dated. 26.05

Qualitative

Rotten NAL/SOP/FOOD/004 QualitativeDecomposed /diseased animal substance / vegetable substance


Coloring Matter NAL/SOP/FOOD/002 QualitativeWorms NAL/SOP/FOOD/004 QualitativeWeevils /Insects NAL/SOP/FOOD/004 QualitativeDetergents NAL/SOP/FOOD/012 QualitativeAdded Preservative(SO2)


10 to 5000 mg/kg

Mineral oil IS 15642 (Part-2) NAL/SOP/FOOD/012

Qualitative

Lactate content IS 11202 0.1 to 5.0 mg/gVegetable oil IS 15642 (Part-2)

IS 1479(Part-1)Qualitative

Moisture if low fat Paneer IS 10484, Appendix A 5 to 90 g/100gMilk fat paneer or chana IS 10484,Appendix B 5 to 80g/100gRancidity NAL/SOP/FOOD/014 QualitativeWeight / Volume (gms/l) IS 2802 250 to 1000 g/lSolubility Percent NAL/SOP/FOOD/017 90 to 100 g/100gIodine as Iodide IS 7224, Cl. A2 QualitativeLumps IS 1165 QualitativeAnimal body Fat NAL/SOP/FOOD/017 QualitativeCasein in protein NAL/SOP/FOOD/017 80 to 100 g/100gAsh including P2O5 NAL/SOP/FOOD/017 1 to 10 g/100gCurd Content IS 3507 0.1 to 10 g/100gPhosphates in Ice Cream NAL/SOP/FOOD/017 Qualitative











b. Adulterants, Preservative & Neutralizers in Dairy Products

Cane Sugar NAL/SOP/FOOD/012IS 1479 (Part -1)

Qualitative

Starch NAL/SOP/FOOD/012IS 1479 (Part -1)

Qualitative

Cellulose NAL/SOP/FOOD/012 QualitativeUrea NAL/SOP/FOOD/012

IS 1479 (Part -1)Qualitative

Ammonium Compounds NAL/SOP/FOOD/012 IS 1479 (Part -2)

Qualitative

Sulphates NAL/SOP/FOOD/012 QualitativeGlucose NAL/SOP/FOOD/ 012 QualitativeSodium Chloride NAL/SOP/FOOD/012 QualitativeNitrates NAL/SOP/FOOD/012

IS 1479 (Part- 2)Qualitative

Neutralizers NAL/SOP/FOOD/012 ,IS 1479 (Part 2), IS 1479 (Part -1)

Qualitative

Formalin NAL/SOP/FOOD/012 IS 1479 (Part -2)IS 1479 (Part- 1)

Qualitative

Hydrogen Peroxide NAL/SOP/FOOD/012 IS 1479 (Part-1)

Qualitative

Boric Acid & Borate NAL/SOP/FOOD/012 QualitativeSalicylic acid NAL/SOP/FOOD/012

IS 1479 (Part-1)Qualitative

8 Beverages (Alcoholic / Non-alcoholic)a. Alcoholic

Beverages/Non Alcoholic Beverages (Gin,Vodka, Whisky,Premix Vodka,Malt Grain

Aldehydes IS 3752 (1 g to 500 g)/100 lAlcohol as Ethanol IS 3752 (1 g to 60 g)/100 gEsters IS 3752 (1 g to 750 g)/100 lTotal Acidity IS 3752 (1 g to 5000 g)/100 lResidue on Evaporation IS 3752 1 % to 90 %Volatile acidity IS 3752 (1 g to 200 g)/100 lAsh IS 3752 0.01 % to 2 %











Blended Whisky,Grape Brandy, Blended Grape Brandy, Rum,White Rum, Premix/Flavored Rum, Plain Country Spirit, Blended Country Spirit,Spiced Country Spirit) Beer,Draught Beer ,Low Alcoholic Beverages

Fixed acidity IS 3752 (1 g to 1000 g)/100 lFurfural IS 3752 (1 g to 20 g)/100 lHigher alcohols IS 3752 (1 g to 800 g)/100 lMethyl alcohol IS 3752 (1 g to 50 g)/100 l pH AOAC (19th Edition) 981.12

Chapter 42 ,IS 38652 to 10

Sugar AOAC (19th Edition) 925.35 Chapter 37

0.5 % to 50 %

Total Sulphur dioxide IS 7585 1 to 1000 mg/lFree Sulphur dioxide IS 7585 1 to 1000 mg/lExtraneous matter IS 4333 (Part -1) 0.01 to 10g/100gLive & dead insects NAL/SOP/FOOD/004 QualitativeInsect fragment NAL/SOP/FOOD/004 QualitativeRodent contamination AOAC (20th Edition) 941.16 QualitativeTest for chloral hydrate IS 8538 QualitativeTest for paraldehyde IS 8538 QualitativeHydrocyanic Acid as HCN


1 to 1000 mg/kg

Colour NAL/SOP/FOOD/004 QualitativeOdour NAL/SOP/FOOD/040 QualitativeTaste NAL/SOP/FOOD/040 Qualitative

9 Starch & starch productsa. Edible Starch And

Starch ProductsMoisture IS 4706 (Part -1) 1 % to 50 %Total ash IS 4706 (Part -2) 0.1 % to 5 %Cold water soluble IS 4706 (Part- 1) 0.05 % to 70 %Starch IS 4706 (Part -2 ) 1 % to 99 %Protein IS 4706 (Part- 2) 1 % to 25 %pH IS 4706 (Part -2) 2 to 10Free Acidity IS 4706 (Part- 2) 0.05 % to 10 %Sulphur Dioxide IS 4706 (Part -2) 10 to 2500 mg/kgCrude Fiber IS 4706 (Part- 2) 0.1 % to 25 %Sulphated ash IS 4706 (Part -2) 0.1 % to 10 %











Alcoholic acidity IS 4706 (Part -2) 0.01 % to 5 %Dietary fiber AOAC (19th Edition) 985.29

Chapter-450.1 % to 20 %

Gelling power IS 1007 QualitativeAcid insoluble ash IS 4706 (Part -2) 0.01 % to 2 %

10 Sugar & sugar productsa. Sweets &

Confectionary, Chocolates, Sweetening Agents, Chewing Gum, Bubble Gum, Sugar, Refined Sugar, Khandesi Sugar, Icing Sugar, Cube Sugar, Jaggery, Dextrose, Golden Syrup, Dried Glucose Syrup, Saccharin

Sulphated Ash IS 15279 0.01 % to 5 %Total Ash AOAC (19th Edition) 900.02

Chapter 44 ,IS 49410.1 % to 5 %

Total fat IS 6287 0.1 % to 40 % Milk Fat IS 1163 0.1 % to 40 %Milk solids not fat IS 1163 1 % to 50 %Acid Insoluble ash IS 6287 0.01 % to 5 %Sulphur dioxide AOAC (19th Edition) 990.28


Moisture AOAC (19th Edition) 925.45Chapter 44,IS 4941

0.1 % to 30 %

Reducing Sugar NAL/SOP/FOOD/013 IS 4941

0.1 % to 15 %

Sucrose NAL/SOP/FOOD/013, IS 4941

1 % to 90 %

Colour IS 15279 5 to 45000 ICUMSADietary Fibre AOAC (19th Edition) 985.29

Chapter-450.1 % to 5 %

Specific Gravity IS 4941 1.0 g/cm3 to 1.9 g/cm3

Fructose and Glucose Ratio (F/G Ratio)

IS 4941 0.5 to 2

Acidity IS 4941 0.1 % to 5 %Brix (Total Soluble solids) IS 13815 5˚ to 80˚Acidity of extracted fat IS 2650 0.01 % to 2 %

pH AOAC (19th Edition) 981.12 Chapter 42

2 to 10











Mould NAL/SOP/FOOD/004 QualitativeLiving and dead insects IS 6261 QualitativeInsect fragments IS 6261 QualitativeRodent contamination AOAC (20th Edition) 941.16 QualitativeTalc IS 1008 QualitativeMineral oil IS 15642 (Part-1 & 2)

NAL/SOP/FOOD/012Qualitative

Gum content NAL/SOP/FOOD/028 1 to 20 g/100gRancidity NAL/SOP/FOOD/014 QualitativeVegetable fat NAL/SOP/FOOD/012 QualitativeCocoa Solids NAL/SOP/FOOD/028 0.5 to 5 g/100gDirt NAL/SOP/FOOD/004 QualitativeFilth NAL/SOP/FOOD/004 QualitativeIron fillings NAL/SOP/FOOD/028 10 to 500 mg/kgExtraneous Matter IS 433 (Part -1) 0.01 to 10 g/100gSpecific Conductivity (106mhos/cm2)

IS 13953, NAL/SOP/FOOD/042

50 to 400 106mhos/cm2

Calcium oxide (mg/100gms)

IS 13953,NAL/SOP/FOOD/043

30 to 300 mg/100g

Total Starch IS 1152,IS 15279 0.5 to 10 g/100g Extraneous matter insoluble in water

IS 12923 0.01 to 5 g/100g

Solubility at 20˚C in 1.5 parts of water and 50 parts of alcohol (95%)

IS 5345 60 to 101 g/100g

Melting point IS 6385 0 ˚C to 250 ˚CSolubility IS 15970 Qualitative

11 Honey & honey products

Specific gravity at 27˚C IS 4941 1 to 1.9 g/cm3

Moisture IS 4941 1 to 30 g/100gTotal reducing sugars IS 4941 5 to 98 g/100gSucrose IS 4941 1 to 20 g/100gFructose and Glucose IS 4941 0.5 to 2











ratio (F/G Ratio)Ash IS 4941 0.1 to 2 g/100gAcidity expressed as Formic Acid

IS 4941 0.01 to 1g/100g

Fiehe’s Test IS 4941 QualitativeHydroxy Methyl Furfural (HMF)

IS 4941 5 to 200 mg/kg

Optical Density at 660 nm

IS 4941 0.01 to 0.8

pH AOAC (19th Edition)981.12 Chapter 42

3.0 to 6.5

Dirt IS 4941 QualitativeScum IS 4941 QualitativePieces of Beeswax NAL/SOP/FOOD/004

Issue. 01,IS 4941Qualitative

Fragments of Bees NAL/SOP/FOOD/004 QualitativeInsects NAL/SOP/FOOD/004 QualitativeRodent contamination AOAC (20th Edition) 941.16 Qualitative

12 Bakery & confectionery products

Acid insoluble Ash IS12711 0.01 % to 5 %Acidity of Extracted Fat(as Oleic Acid)

IS12711 0.05 % to 5 %

Total Solids IS 12711 10 % to 98 %Crude Fiber IS 12711 0.1 % to 25 %Fat IS 12711 1 % to 40 %Moisture IS 12711 0.5 % to 40 %Sulphur dioxide AOAC (19th Edition) 990.28,


Sugar NAL/SOP/FOOD/013 0.5 % to 50 %Protein IS 7219 0.5 % to 25 %Alcoholic acidity NAL/SOP/F/238 0.01 % to 2 % Dietary Fibre AOAC (19th Edition) 985.29,

Chapter-450.1 % to 10 %











Peroxide Value IS 12711 0.1 to 10.0 meq/kgSulphated Ash IS 6287 0.12 % to 5 %

13 Stimulant Foodsa. Including Black

Tea/Green Tea/ Coffee/Cocoa And By Products/ Coffee Powder/ Chicory/Tea/Roasted Coffee/ Ground Coffee/ Soluble Coffee Powder/ Instant Coffee, White Tea

Total Ash IS 3077,IS 13854 1 % to 25 %Acid Insoluble Ash IS 3077,IS 13857 0.01 % to 5 %Water Soluble Ash IS 3077,IS 13855

AOAC (19th Edition) 920.100Chapter 30

1 % to 90 %

Alkalinity of Soluble Ash IS 3077,IS 13856 0.1 % to 10 %Moisture IS 3077

IS 138530.01 % to 25 %

Solubility in Boiling Water IS 2791 QualitativeSolubility In Cold Water IS 2791 QualitativePetroleum Ether Extract IS 3077 0.05 % to 25 %Water Soluble Extract IS 13862 ,IS 3077 20 % to 70 %Crude Fiber NAL/SOP/F/236 1.0 % to 25 %Ochratoxin A AOAC (19th Edition)

2000.09Chapter 49

5 to 100 µg/kg

Caffeine Content IS 2791 0.01 % to 10 %Extraneous Matter IS 4333 0.01 to 10 g/100gLive and dead Insects NAL/SOP/FOOD/004 QualitativeMould NAL/SOP/FOOD/004 QualitativeRodent Contamination AOAC (20th Edition)

941.16Qualitative

Odour NAL/SOP/FOOD/040 QualitativeTaint NAL/SOP/FOOD/004 QualitativeMustiness NAL/SOP/FOOD/040 QualitativeIron Fillings IS 3633 10 to 500 mg/kgTotal Polyphenols NAL/SOP/FOOD/292 5 to 25 g/100 gRancid/Obnoxious NAL/SOP/FOOD/040 Qualitative



http://www.standardsbis.in/Gemini/search/BasicSearch.action









FlavorChicory NAL/SOP/FOOD/004 QualitativeHydrocyanic Acid as HCN

AOAC (20th Edition) 915.03:Chapter 49

1 to 1000 mg/kg

Sulphur dioxide AOAC (20th Edition) 990.28 10 to 5000 mg/kgInorganic bromide NAL/SOP/F/305 5 to 200 mg/kgCarbohydratesXylose

NAL/SOP/INS/035

0.5 to 2.5 %Glucose 0.5 to 2.5 %Fructose 0.5 to 2.5 %Sucrose 0.5 to 2.5 %Total Catechins IS 15344, ISO 14502-2

NAL/SOP/F/2921.0 to 20 %

14 Edible oils & fatsa. Coconut Oil,

Cottonseed Oil, Groundnut Oil, Linseed Oil, Mustard Oil, Safflower Seed Oil, Sunflower Oil, Till Oil, Niger Seed Oil, Soyabean Oil, Maize Oil (Corn Oil), Fish Oil,Olive Oil (Virgin, Extra Virgin), Olive Pomace Oil, Palm Oil, Palmolein Oil, Palm Kernel Oil, Ricebran Oil, Almond Oil,

Refractive index IS 548 (Part -1) 1.3 to 1.8Saponification value IS 548 (Part -1) 168 to 300Iodine Value IS 548 (Part -1) 7.5 to 250Unsaponifiable Matter IS 548 (Part -1) 0.1 to 15 g/100 gAcid Value IS 548 (Part -1) 0.01 to 20.0Peroxide value IS 548 (Part-1) 0 to 50meq/kgRancidity NAL/SOP/FOOD/014

IS 548 (Part -1)Qualitative

Argemone oil NAL/SOP/FOOD/014 IS 548 (Part -2)IS 15642 (Part- 1&2)

Qualitative

Specific Gravity IS 548 (Part -1) 0.5 to 2 g/cm3

Karanja Oil IS 548 (Part -2 ) QualitativeNeem Oil IS 548 (Part -2 ) QualitativeHydrocyanic Acid IS 548 (Part -2 ) QualitativeMineral Oil IS 548 (Part- 2 ) QualitativeKusume Oil IS 548 (Part- 2 ) QualitativeCastor Oil IS 548 (Part -2 ) Qualitative











Vanaspathy Melting point AOAC (19th Edition),Chapter 41

30 ˚C to 100 ˚C

Flash point IS 1448 (Part -21) 40˚C to 400˚CPoly bromide test NAL/SOP/FOOD/014 QualitativeBellier Turbidity Test NAL/SOP/FOOD/014

IS 548 (Part-2 )10 ˚C to 100˚C

Cloud point NAL/SOP/FOOD/015 (-)10 ˚C to 50˚CMoisture & Volatile matter

IS 548 (Part -1) 0.01 to 2 g/100 g

Olive Pomace oil NAL/SOP/FOOD/014 IS 548 (Part -2 )

Qualitative

Propyl Gallate AOAC (19th Edition) 983.15 NAL/SOP/F/268

3 to 100 mg/kgEthyl Gallate 3 to 100 mg/kgOctyl Gallate 10 to 200 mg/kgDodecyl Gallate 10 to 200 mg/kgAscorbyl Palmitate 10 to 300 mg/kgBHA (Butylated Hydroxy Anisole)

AOAC (19th Edition) 983.15Chapter 47

3 to 200 mg/kg

BHT 3 to 200 mg/kgTBHQ 3 to 100 mg/kgColor IS 548 (Part -1) 0.1 to 70Free Fatty acid (as Oleic acid,Lauric acid,ricinoleic acid, Palmitic acid)

IS 548 (Part -1) 0.01 to 2g/100g

Linseed Oil (Hexabromide Test)

NAL/SOP/FOOD/014IS 548 (Part-2 )

Qualitative

Teaseed oil NAL/SOP/FOOD/014 AOAC (19th Edition) 936.14,Chapter 41

Qualitative

Sesame Oil(Baudouins Test)

NAL/SOP/FOOD/014 AOAC (19th Edition) 893.01 Chapter 41,IS 548 (Part- 2 )

Qualitative

Insoluble Impurities IS 548 (Part-1) 0.05 to 2 g/100g











Semi – Siccative Oil NAL/SOP/FOOD/014 QualitativeCotton seed Oil (Halphen’s Test)

NAL/SOP/FOOD/014 IS 548 (Part -2 ), AOAC (19th Edition) 897.02,Chapter 41

Qualitative

Reichert Meissel value IS 548 (Part -1) 2 to 30Polenske Value IS 548 (Part -1) 1 to 50Added Colouring Matter NAL/SOP/FOOD/002 QualitativeButyro –Refractometerreading

IS 548 (Part- 1) 10 to 80

Oryzanol Content IS 3448 1 to 2.5 g/100gHexane NAL/SOP/INS/018 1.0 to 10 mg/kg

15 Food additives & preservativesa. Common Salt,

Iodized Salt And Iron Fortified Common Salt

Chloride as NaCl IS 253,IS 7224 90 % to 99 %Matter soluble in water other than sodium chloride

IS 253,IS 7224 0.1 % to 5 %

Moisture IS 253, IS 7224 0.1 % to 5 %Water insoluble Matter IS 253, IS 7224 0.1 %to 5 %Magnesium IS 253,IS 7224 0.01 % to 1 %Iodine content IS 7224 1 to 100 mg/kgSulphate as SO4 IS 253, IS 7224 0.05 % to 1 %Calcium IS 253,IS 7224 0.01 % to 2 %Alkalinity as Na2CO3 IS 253, IS 7224 0.01 % to 1 %Potassium Ferro cyanide IS 253, IS 7224 QualitativepH IS 12981 4 to 14

b. Vinegar(Brewed Or Alcoholic Vinegar, Synthetic Or Wine Vinegar)

Phosphorus pentoxide IS 14703 0.01 % to 0.1 %Total Acidity IS 3752 1 % to 20 % Residual Alcohol IS 3752 0.1 % to 2 %Total Solids IS 14703 0.1 % to 10 %Total Ash IS 14703 0.01 % to 5 %Soluble Solids IS 14703 0.05 to1 g/100ml











c. Citric Acid Citric acid IS 5464 90 % to 100 %Sulphate IS 5464 QualitativeHalides (Chloride) IS 5464 QualitativeSulphated ash IS 5464 0.01 % to 1 %Oxalates IS 5464 QualitativeWater content IS 5464 0.1 % to 10 %Readily carbonizable substances

IS 5464 Qualitative

d. Ascorbic Acid Purity IS 5342 95 % to 100 %Loss on drying IS 4818 0.05 % to 1 %Sulphated ash IS 4750 0.05 % to 2 %

e. Monosodium Glutamate

Purity IS 9505 90 % to 100 %Loss on drying IS 1699 0.1 % to 5 %Chloride IS 9505 0.25 % to 10%pH IS 9505 4 to 8 Solubility IS 9505 QualitativeAppearance NAL/SOP/FOOD/004 Qualitative

f. Calcium Chloride Matter Insoluble in Water IS 1314 0.005 % to 1 %Calcium chloride IS 1314 90 % to 100 %Magnesium chloride IS 1314 0.01 % to 1 %Alkalinity as Ca(OH)2 IS 1314 0.001 % to 1 %Alkali Chlorides as NaCl IS 1314 0.1 % to 2 %Magnesium and alkali salts

IS 1314 0.1 % to 2.0 %

Oxidizing substance IS 1314 QualitativeSulphates IS 1314 0.001 % to 0.2 %Ammonium salts IS 1314 QualitativeMagnesium IS 1314 0.01 % to 2 %Potassium IS 1314 0.01 % to 2 %Sodium IS 1314 0.01 % to 2 %pH IS 1314 4.5 to 8.5











g. Acetic Acid Solubility in Water IS 695 QualitativeRelative density @ 27°C IS 82 1.0 to 1.6 g/cm3

Acetic acid content IS 695 95 % to 100 %Crystallizing point IS 695 10 °C to 25 °CResidue on Evaporation IS 695 0.001 % to 0.1 %Chlorides IS 695 QualitativeSulphates IS 695 1 to100 mg/kgFormic acid IS 695 0.01 % to 0.5 %Acetaldehyde IS 695 0.01 % to 0.5 %Oxidizable impurities IS 695 QualitativeWater content IS 695 0.05 % to 0.2 %

h. Potassium Meta Bisulphite

Purity IS 4751 90 % to 100 %Water Insoluble matter IS 4751 0.01 % to 0.1 %Thio sulphate IS 4751 QualitativepH IS 4751 3 to 8

i. Ammonium Bicarbonate

Purity IS 2697 90 % to 100 %Chloride as Cl IS 2697 0.1 % to 5 %Sulphate as SO4 IS 2697 Qualitative

j. Phosphoric Acid Purity IS 10508 90 % to 100 %Nitrates IS 10508 QualitativeVolatile Acid IS 10508 QualitativeChloride IS 10508 QualitativeSulphate IS 10508 QualitativeFluoride IS 10508 Qualitative

k. Flavours Colour NAL/SOP/FOOD/004 QualitativeSpecific Gravity AOAC (19th Edition)

920.127 Chapter 36, 0.8 to 2.0 g/cm3

Refractive Index AOAC (19th Edition) 920.141 Chapter 36

1.3 to 1.6

Moisture IS 5464 0.1 % to 90 %l. Baking Powder Extraneous matter IS 4333 (Part -1) 0.01 to 10 g/100g











Products, Catechu, Gelatin, Silver Leaf (Chand-Kiwarq), Pan Masala,Low And High Fat Cocoa Powder, Carob Powder

Live & Dead insects NAL/SOP/FOOD/004IS 6261

Qualitative

Mould NAL/SOP/FOOD/004 QualitativeRodent contamination AOAC (20th Edition) 941.16 QualitativeTartaric acid or its salts AOAC (20th Edition) 899.01

AOAC (20th Edition) 930.16Qualitative

Acid compounds of aluminium

AOAC (20th Edition) 925.06AOAC (20th Edition) 972.06

Qualitative

Sand NAL/SOP/FOOD/004 QualitativeEarth NAL/SOP/FOOD/004 QualitativeLoss on Drying IS 2962 1 to 25 g/100gWater insoluble residue(dried at 100°C)

IS 2962 1 to 40 g/100g

Alcohol insoluble residue in 90 % alcohol dried at 100°C

IS 2962 1 to 50 g/100g

Total ash on dry basis IS 5643,Cl. 6IS 5719,Annex C

0.05 to 15 g /100g

Ash insoluble in HCl IS 5643,Cl. 6 0.01 to 2 g/100gHydrocyanic Acid as HCN/ Hydrogen cyanide


1 to 1000 mg/kg

Moisture IS 5719,Annex A 1 to 20 g/100gGel strength IS 5719,Annex B QualitativeSulphur dioxide IS 5719,Annex D

AOAC (20th Edition) 990.2810 to 5000 mg/kg

Nitrogen (on dry basis) IS 5719,Annex E 5 to 30 g/100gHusk NAL/SOP/FOOD/004 QualitativeRancidity NAL/SOP/FOOD/014 QualitativeObnoxious flavor NAL/SOP/FOOD/040 QualitativeNeotame NAL/SOP/FOOD/002 QualitativeArtificial flavor NAL/SOP/FOOD/002 QualitativeSulphurdioxide AOAC (20th Edition) 990.28 10 to 5000 mg/kg











Total ash IS 7237 0.1 to 5 g/100gAcid insoluble matter IS 7237 0.1 to 5g/100gTannin content IS 7237 QualitativeHydrogen phosphide NAL/SOP/F/306 0 to 1000 mg/KgInorganic bromide NAL/SOP/F/305 5 to 1000 mg/kgClay NAL/SOP/FOOD/004 QualitativeGrit NAL/SOP/FOOD/004 QualitativeInsect fragments IS 6261 QualitativePhosphorous as P2O5 IS 16232 0.1 to 3500 mg/kgPotassium iodate as Iodine(I2)

IS 7224 1 to 200mg/kg

Methyl Mercury AOAC 20th Edition, 983.20 NAL/SOP/INS/011

0.05 to 50 µg/kg

16 Vitamin In Food And Complimentary Food Substances

Vitamin-A AOAC (19th Edition) 992.06 Chapter 50NAL/SOP/F/264

100 to 2500 µg RE

Vitamin-D AOAC (19th Edition) 992.06 Chapter 50,NAL/SOP/F/264

100 IU to 2500 IU

Pyridoxine - B6 AOAC (19th Edition), Chapter 50,NAL/SOP/F/265

10 to 500 mg/kg

Folic Acid- B9 NAL/SOP/F/265 10 to 500 mg/kgCyanocobalamin- B12 NAL/SOP/F/265 10 to 500 mg/kgRiboflavin- B2 AOAC (19th Edition) 985.31

Chapter 50,NAL/SOP/F/265 10 to 500 mg/kg

Thiamine-B1 AOAC (19th Edition) 986.27 Chapter 50,NAL/SOP/F/265

10 to 500 mg/kg

Niacin – B3 NAL/SOP/F/265 10 to 500 mg/kgAscorbic acid- Vitamin C NAL/SOP/F/265 10 to 500 mg/kgVitamin – E (Tocopherol) NAL/SOP/F/264 10 to 100 mg/kgVitamin – K NAL/SOP/F/264 0.5 to 100 mg/kgBeta Carotene NAL/SOP/F/265 0.5 to 100 mg/kgVitamin – B5 NAL/SOP/F/265 0.5 to 100 mg/kg











(Pantothenic acid)17 Follow- Up

Formula- Complementary Food

Moisture AOAC (19th Edition) 927.05 Chapter 33

1 % to 10 %

Total Milk Protein IS 7219 10 % to 50 % Total Fat IS 11721 15 % to 50 % Total ash IS 14433 1 % to 2 % Insolubility index IS 12759 0.5 ml to 5 mlSodium IS 9497 10 to 150 mg/100gPotassium IS 9497 100 to 500mg/100gChloride IS 2785 100 to 300mg/100gCalcium IS 5949 100 to 600mg/100gPhosphorus AOAC (19th Edition): 995.11

Chapter-45100 to 400 mg/100g

Magnesium IS 5949 10 to 50 mg/100g18 Nutritional parameters a. Food & Agri

ProductsRaw/ Processed/ Cooked/Frozen/Ready-To-Eat Foods/Feeds/Fruits & Vegetables (Grapes/Gherkins/Onions/Pomegranates/Mangoes) Processed Fruits & Vegetables/ Raw/Processed Foods/Supplementary Foods/Food Grains/Cereals &

Energy NAL/SOP/F/017 5 to 5000 kcal/100g Carbohydrate IS 1656

AOAC (19th Edition) 986.25Chapter 50,NAL/SOP/F/016

0.1 to 1000 g/100g

Fat NAL/SOP/F/014 IS 12711, AOAC (19th

Edition) 922.06, Chapter 32, AOAC (19th Edition),989.05 Chapter 33, IS 5960 (Part-3)

0.1 % to 40 %

Protein IS 7219 0.1 % to 80 %Crude Fibre NAL/SOP/F/236,IS 12711 0.1 % to 20 % Sodium IS 9497 0.01 % to 15 % Potassium IS 9497 0.01 % to 15 %Calcium AOAC (19th Edition) 944.03

Chapter 32,IS 7224,IS 59490.01 % to 15 %











Pulses/Dairy & Dairy Products/Seafood, Fishery & Fishery Products/Egg &Egg Products/Nut & Nut Products (Groundnut Etc.)/Oilseeds & Products/ Spices, Spice Products & Condiments/Meat & Meat Products/Poultry & Poultry Products/Sugar & Sugar Products/Stimulant Foods (Tea, Coffee & Related Products)/Bakery & Confectionery/Flavors, Seasonings & Food Additives/Pet Food/Beverages/Herbs, Health

Drinks & Mixes/ Infusion Foods

Magnesium IS 7224,IS 949,AOAC (19th Edition) 920.09 , Chapter 3.0

0.1 % to 15 %

Phosphorus AOAC (19th Edition) 995.11,Chapter 45

0.005 % to 9 %

Dietary Fibre AOAC (19th Edition) 985.29,Chapter-45

0.1 % to 50 %

Iron AOAC (19th Edition) 991.11 Chapter 9

0.25 to 500 mg/100g

Saturated fat AOAC (19th Edition) 996.06 NAL/SOP/INS/001

More than 0.1 %

Monounsaturated fat AOAC (19th Edition) 996.06 NAL/SOP/INS/001

More than 0.1 %

Polyunsaturated fat AOAC (19th Edition) 996.06 NAL/SOP/INS/001

More than 0.1 %

Trans fat AOAC (19th Edition) 996.06 NAL/SOP/INS/001

More than 0.1 %

Cholesterol AOAC (19th Edition) 994.10 Chapter 45,NAL/SOP/INS/002

> 1 mg/100g

19 Mycotoxin & Naturally Occuring Toxin In Food And Food Substancesa. Mycotoxins Aflatoxin B1 AOAC (19th Edition) 1.0 to 50 µg/kg











2005.08, Chapter 49NAL/SOP/INS/004

Aflatoxin B2 1.0 to 50 µg/kgAflatoxin G1 1.0 to 50 µg/kgAflatoxin G2 1.0 to 50 µg/kgOchratoxin A AOAC (19th Edition)

2000.09 Chapter 495.0 to 50 µg/kg

b. Naturally Occurring Toxin

Hypericine NAL/SOP/F/235 0.25 to 3.0 mg/kg

Saffrole NAL/SOP/F/236 1 to 20.0 mg/kgAgaric acid NAL/SOP/F/237 10 to 150 mg/kg

Hydrocyanic acid AOAC (19th Edition) 915.03 Chapter-49

1 to 100 mg/kg

20 Trace Metals And Minerals In Food And Food Substancesa. Raw & Processed Iron AOAC (19th Edition)

999.11,Chapter 90.25 to 30 mg/kg

Copper AOAC (19th Edition) 999.11 Chapter 9

0.25 to 30 mg/kg

Lead AOAC (19th Edition) 999.11 Chapter 9

0.25 to 20 mg/kg

Cadmium AOAC (19th Edition) 999.11 Chapter 9

0.1 to 10 mg/kg

Zinc AOAC (19th Edition) 999.11,Chapter 9

0.1 to 20 mg/kg

Arsenic AOAC (19th Edition) 963.21 Chapter 9

0.02 to 10 mg/kg

Mercury AOAC (19th Edition) 971.21 Chapter 9

0.02 to 0.5 mg/kg

Chromium AOAC (19th Edition) 2011.19,Chapter 50

0.25 to 20 mg/kg

Nickel AOAC (19th Edition) 975.34 Chapter 9

0.25 to 20 mg/kg

Tin AOAC (19th Edition) 980.19 Chapter 9

2.5 to 50 mg/kg











Selenium AOAC (19th Edition) 986.15 Chapter 9

0.02 to 20 mg/kg

Methyl Mercury AOAC 20th Edition, 983.20 NAL/SOP/INS/011

0.05 to 50 µg/kg

21. Test for added Natural colors & Test for synthetic colors for Food and Food Substancesa. Milk & Dairy

Products, Oils & Fats, Fruits &Vegetable Products, Nuts & Raisins, Cereals & Cereal Products, Meat & Meat Products, Fish & Marine Products, Sugar & Sugar Products (Sweets & Confectionery), Honey & Honey Products, Spice & Spice products, Stimulant foods, Beverages(Alcoholic/Nonalcoholic),

Curcumin NAL/SOP/FOOD/002 QualitativeRiboflavin QualitativeChlorophyl NAL/SOP/FOOD/002 QualitativeBeta Carotene QualitativeCarotene QualitativeAnnatto Extract (Bixin) QualitativeCaramel colours(Plain) QualitativeCaramel colours (Ammonium Sulphite process)

Qualitative

Ponceau 4R QualitativeCarmoisine QualitativeErythrosine QualitativeTartrazine QualitativeSunset Yellow FCF QualitativeSaffron QualitativeIndigo carmine QualitativeBrilliant blue FCF QualitativeFast green FCF Qualitative

22 Test for Artificial sweeteners Food and Food Substancesa. Aspartame

NAL/SOP/FOOD/002Qualitative

Acesulfame-K QualitativeSaccharin QualitativeSucralose Qualitative

23 Test for added Preservatives& Antioxidants in Food and Food Substancesa. Milk & Dairy

Products, Oils & Benzoic Acid NAL/SOP/INS/036 10 to 2500 mg/kgSorbic Acid NAL/SOP/INS/036 5 to 2500 mg/kg











Fats, Fruits&Vegetable Products, Nuts & Raisins, Cereals & Cereal Products, Meat & Meat Products, Fish & Marine Products, Sugar & Sugar Products (Sweets & Confectionery), Honey & Honey Products, Spice & Spice products, Stimulant foods, Beverages (Alcoholic/Nonalcoholic), Food Additives

BHA NAL/SOP/INS/037 3 to 500 mg/kg

TBHQ NAL/SOP/INS/037 3 to 500 mg/kg

VI ANIMAL FOOD & FEEDS

1. Animal Feed/Poultry Feed

Moisture IS 7874 (Part -1) 1 % to 20 %Acid insoluble ash IS 7874 (Part -1) 0.01 % to 5 %Total ash IS 7874 (Part- 1) 0.1 % to 50 %Crude Protein IS 7874 (Part -1) 1 % to 50 %Crude fiber IS 7874 (Part -1) 0.1 % to 30 %Crude fat IS 7874 (Part-1) 0.1 % to 25 %Urea nitrogen IS 7874 (Part -1) 0.1 % to 10 %Phosphorus IS 7874 (Part -2) 0.1 % to 5 %Calcium IS 13574 0.01 % to 10 %Salt as NaCl IS 7874 (Part -2) 0.1 % to 25 %Magnesium as Mg IS 13574 0.01 % to 10 %











Sodium as Na IS 9497 0.1 % to 25 % Potassium as K IS 9497 0.1 % to 25 % Fluoride IS 7874 (Part -2) 1 to 1000 mg/kgAmmoniacal Nitrogen IS 7874 (Part -1) 0.1 % to 5 %

VII MARINE /AQUA CULTURE FOOD PRODUCTS

1. Fish& Fish Products/ShrimpsFrozen ShrimpsOr Prawns, Frozen Lobster, Frozen Squid, Frozen Finfish, Frozen Fish Fillets OrMinced FishFlesh Or Mixtures,Dried Shark Fins, Salted Fish/DriedSalted Fish, Canned Finfish, Canned Shrimp, Canned SardinesOr Sardine TypeProducts, Canned Salmon, Canned Crab, Canned Tuna AndBonito

Acidity of Brine NAL/SOP/FOOD/009 0.01 % to 50 % Moisture IS 14950 5 % to 98 %Ash insoluble in dil.HCl IS 14950 0.1 % to 5 %Salt as NaCl IS 14950,


0.01 % to 15 %

Sulphur dioxide AOAC (19th Edition) 990.28 Chapter 47

10 to 50 mg/kg

Total Volatile Base-N NAL/SOP/FOOD/010 1 to 150 mg/100g Histamine NAL/SOP/F/233 10 to 100 mg/kgFat AOAC (19th Edition) 925.32

Chapter 341 % to 50 %

Phosphorous as PO4/P2O5

NAL/SOP/FOOD/011 AOAC (19th Edition) 995.11 Chapter 45

0.01 % to 10 %

Trimethylamine-nitrogen (TMA-N)


0.1 to 25 mg/100g

Sodium AOAC (19th Edition) 969.23 Chapter 35

2.5 to 1000 mg/kg

Potassium AOAC (19th Edition) 969.23,Chapter 35

2.5 to 1000 mg/kg

Boric Acid AOAC (19th Edition) 959.09 Chapter 47

0.1 to 10 g/100g

Mould NAL/SOP/FOOD/004 QualitativeLiving and dead insects IS 6261 QualitativeInsect fragments IS 6261 Qualitative











Rodent contamination AOAC (20th Edition) 941.16 QualitativeSodium metabisulphite AOAC (20th Edition) 990.28 10 to 5000 mg/kgSodium Nitrite NAL/SOP/FOOD/024 10 to 1000 mg/kgScales in Fish NAL/SOP/FOOD/004 QualitativeFish Head NAL/SOP/FOOD/004 QualitativeRaw Fish NAL/SOP/FOOD/004 QualitativeCooked Fish NAL/SOP/FOOD/004 QualitativeGills NAL/SOP/FOOD/004 Qualitative

VIII AYUSH PRODUCTS

a. Herbal & Ayurvedic Product

Energy NAL/SOP/F/017 5 to 5000 kcal/100g Carbohydrate NAL/SOP/F/016 0.1 to 1000 g/100gProtein IS 7219 0.1 % to 80 %Fat NAL/SOP/F/014,AOAC

(19th Edition) 922.06, Ch. 32AOAC (19th Edition) 989.05 Chapter 33 ,IS 5960 (Part -3)

0.1 % to 40 %

Cholesterol AOAC (19th Edition) 994.10 Ch. 45,NAL/SOP/INS/002

> 1 mg/100g

IX RESIDUES IN FOOD PRODUCTS

a. Fish and Fish Products, Prawn & Prawn Products, Shrimps

AntibioticsChloramphenicol NAL/SOP/INS/017 0.075 to 0.75 µg/kgFlorfenicol 0.075 to 0.75 µg/kgNitrofuran Metabolites Amino -Oxazolidinone (AOZ)

NAL/SOP/INS/018

0.05 to 3 µg/kg

3-Amino-5- morpholinomethyl-2-oxazolidinone (AMOZ)

0.05 to 3 µg/kg

Semicarbazide (SEM) 0.05 to 3 µg/kg











Aminnohydantation(AHD) 0.05 to 3 µg/kgNitrofuran parent drugsNitrofurazone (NFZ)

NAL/SOP/INS/028

1 to 5 µg/kgFurazolidone (FZD) 1 to 5 µg/kgNitrofurantoin (NFT 1 to 5 µg/kgFuraltadone (FTD) 1 to 5 µg/kgNitroimidazoleMetronidazole (MTZ) NAL/SOP/INS/019 1 to 5 µg/kgRonidazole (RNZ) 1 to 5 µg/kgQuinolones/Flouro-quinalonesOxolinic acid

NAL/SOP/INS/029

10 to 500 µg/kgDifloxacin 10 to 500 µg/kgSarafloxacin 10 to 500 µg/kgEnrofloxacin 10 to 500 µg/kgCiprofloxacin 10 to 500 µg/kgDanofloxacin 10 to 500 µg/kgFlumequine 10 to 500 µg/kgNorfloxacin 10 to 500 µg/kgNalidixic acid 10 to 500 µg/kgTetracyclinesTetracycline

NAL/SOP/INS/020

10 to 500 µg/kg4 –Epitetracycline 10 to 500 µg/kgOxytetracycline 10 to 500 µg/kg4- Epioxytetracycline 10 to 500 µg/kgChlortetracycline 10 to 500 µg/kg4 –Epichlortetracycline NAL/SOP/INS/020 10 to 500 µg/kgSulfonamidesSulfadiazine NAL/SOP/INS/031 10 to 500 µg/kgSulfamethoxazole 10 to 500 µg/kgSulfamethoxypyridazine 10 to 500 µg/kgSulfamethizole 10 to 500 µg/kg











Sulfamethazine 10 to 500 µg/kgSulfamerazine 10 to 500 µg/kgSulfapyridine 10 to 500 µg/kgSulfadimethoxine 10 to 500 µg/kgSulfachloropyradizine 10 to 500 µg/kgSulfathiazole-free acid 10 to 500 µg/kgPesticidesAldrin NAL/SOP/lNS/003

(LC MSMS & GC-MS MS)10 to 200 µg/kg

Dieldrin 10 to 200 µg/kgCis –Chlordane 10 to 200 µg/kgTrans chlordane 10 to 200 µg/kgDDE,o,p’ 10 to 200 µg/kgDDE,p,p’ 10 to 200 µg/kgDDT,o,p’ 10 to 200 µg/kgDDT,p,p’ 10 to 200 µg/kgDDD,o,p’ 10 to 200 µg/kgDDD,p,p’ 10 to 200 µg/kgFenitrothion 10 to 200 µg/kgHeptachlor 10 to 200 µg/kgHeptachlor epoxide 10 to 200 µg/kgAlpha –HCH 10 to 200 µg/kgBeta-HCH 10 to 200 µg/kgDelta-HCH 10 to 200 µg/kgGamma-HCH 10 to 200 µg/kgChlorpyrifos 10 to 200 µg/kg2,4 D 10 to 200 µg/kgEthion 10 to 200 µg/kgMonochrtophos 10 to 200 µg/kgParaquate dichloride 10 to 200 µg/kgTrichlorophon 10 to 200 µg/kgCarbendazim 10 to 200 µg/kgBenomyl 10 to 200 µg/kg











Carbofuron 10 to 200 µg/kgCypermethrin 10 to 200 µg/kgEdifenphos 10 to 200 µg/kgFenthion 10 to 200 µg/kgFenvalerate

NAL/SOP/lNS/003 (LC MSMS & GC-MS MS)

10 to 200 µg/kgPhenthoate 10 to 200 µg/kgPhorate 10 to 200 µg/kgPirimiphos-methyl 10 to 200 µg/kgEndosulfan alpha isomer 10 to 200 µg/kgEndosulfan beta isomer 10 to 200 µg/kgEndosulfan sulfate 10 to 200 µg/kgDiazinon 10 to 200 µg/kgMalathion 10 to 200 µg/kgMethyl parathion 10 to 200 µg/kgDichlorvos 10 to 200 µg/kgChlorfenvinfos 10 to 200 µg/kgCarbaryl 10 to 200 µg/kgEthoxyquin 10 to 200 µg/kgQuinolphos 10 to 200 µg/kgEndrin 10 to 500 µg/kgHCB 10 to 500 µg/kgMycotoxinsAflatoxin B1 NAL/SOP/INS/004 5.0 to 50 µg/kgAflatoxin B2 5.0 to 50 µg/kgTrace metal elementsCadmium IS 2237

AOAC (19th Edition) 999.110.01 to 10.0 mg/kg

Lead IS 2237AOAC (19th Edition) 972.23

0.01 to 10.0 mg/kg

Mercury IS 2237AOAC (19th Edition) 971.21

0.01 to 10.0 mg/kg

Arsenic IS 2237 0.02 to 10 mg/kg











AOAC (19th Edition) 963.21Copper IS 2237

AOAC (19th Edition) 999.110.25 to 20 mg/kg

Selenium AOAC (19th Edition) 986.15

0.02 to 10 mg/kg

Poly Chlorinated Biphenyl2,4,4′-TrichlorobiphenylPCB No 28

NAL/SOP/INS/007, AOAC (19th Edition), 970.52,( GC-MSMS )

20 to 200 µg/kg

2,2′,3,4,4′,5′-HexachlorobiphenylPCB 138

20 to 200 µg/kg

2,2′,4,5,5′-PentachlorobiphenylPCB 101

20 to 200 µg/kg

2,2′,3,4,4′,5,5′-HeptachlorobiphenylPCB 180

20 to 200 µg/kg

2,2′,4,4′,5,5′-HexachlorobiphenylPCB 153

20 to 200 µg/kg

2,2′,5,5′-TetrachlorobiphenylPCB 52

20 to 200 µg/kg

DyesMalachite Green

NAL/SOP/INS/034

0.5 to 5.0 µg/kgLeuco malachite Green 0.5 to 5.0 µg/kgCrystal Violet 0.5 to 5.0 µg/kgLeuco-crystal violet 0.5 to 5.0 µg/kg

b. Fruit and Fruit products/Vegetables & vegetable products

Pesticide Residue1-Naphthylacetic acid NAL/SOP/lNS/003


2,4-D 10 to 200 µg/kg4-bromo-2-chlorophenol 10 to 200 µg/kg











4 Chlorophenoxy acetic acid

10 to 200 µg/kg

6-Benzyl adenine 10 to 200 µg/kgAbamectin 10 to 200 µg/kgAcephate 10 to 200 µg/kgAcetamiprid 10 to 200 µg/kgAlachlor NAL/SOP/lNS/003


Aldrin 10 to 200 µg/kgDieldrin 10 to 200 µg/kgAllethrin/Bioallethrin 10 to 200 µg/kgAmetoctradin 10 to 200 µg/kgAtrazine 10 to 200 µg/kgAzadirachtin 10 to 200 µg/kgAzoxystrobin 10 to 200 µg/kgBenalaxyl and isomers 10 to 200 µg/kgBendiocarb 10 to 200 µg/kgBenfuracarb 10 to 200 µg/kgBenomyl 10 to 200 µg/kgBifenazate 10 to 200 µg/kgBifenthrin 10 to 200 µg/kgBitertenol 10 to 200 µg/kgBromophos 10 to 200 µg/kgButachlor 10 to 200 µg/kgBuprofezin 10 to 200 µg/kgCaptafol 10 to 200 µg/kgCaptan 10 to 200 µg/kgCarbaryl 10 to 200 µg/kgCarbendazim 10 to 200 µg/kgCarbofuran 10 to 200 µg/kg3-hydroxy-carbofuran 10 to 200 µg/kgCarbosulfan 10 to 200 µg/kgCarboxin 10 to 200 µg/kg











Cartap hydrochloride 10 to 200 µg/kgChlorantraniliprole 10 to 200 µg/kgCis-chlordane 10 to 200 µg/kgtrans-chlordane 10 to 200 µg/kgChlorfenopyr NAL/SOP/lNS/003


Chlorfenvinphos 10 to 200 µg/kgChlormequat chloride (CCC)

10 to 200 µg/kg

Chlorothalonil 10 to 200 µg/kgChlorobenzilate 10 to 200 µg/kgChlorpyrifos 10 to 200 µg/kgChlorpyrifos methyl 10 to 200 µg/kgClothianidin 10 to 200 µg/kgCyantranilirole 10 to 200 µg/kgCyazofamid 10 to 200 µg/kgCyfluthrin 1 10 to 200 µg/kgCyfluthrin 2 10 to 200 µg/kgCyfluthrin 3 10 to 200 µg/kgCyfluthrin 4 10 to 200 µg/kgCymoxanil 10 to 200 µg/kgCypermethrin 1 10 to 200 µg/kgCypermethrin 2 10 to 200 µg/kgCypermethrin 3 10 to 200 µg/kgCypermethrin 4 10 to 200 µg/kgDazomet 10 to 200 µg/kgp,p´-DDT 10 to 200 µg/kgo,p´-DDT 10 to 200 µg/kgp,p´-DDE 10 to 200 µg/kgp,p´-TDE (DDD) 10 to 200 µg/kgDeltamethrin 10 to 200 µg/kgDiafenthiuron 10 to 200 µg/kgDiazinon 10 to 200 µg/kg











Dichlorvos 10 to 200 µg/kgDicofol 10 to 200 µg/kgDifenoconazole


10 to 200 µg/kgDiflubenzuron 10 to 200 µg/kgDimethoate 10 to 200 µg/kgOmethoate 10 to 200 µg/kgDimethomorph 10 to 200 µg/kgDinocap 10 to 200 µg/kgDinotefuran 10 to 200 µg/kgDiquat 10 to 200 µg/kgDithianon 10 to 200 µg/kgMancozeb 10 to 200 µg/kgManeb 10 to 200 µg/kgPropineb 10 to 200 µg/kgThiram 10 to 200 µg/kgZineb 10 to 200 µg/kgZiram 10 to 200 µg/kgMetiram 10 to 200 µg/kgDiuron 10 to 200 µg/kg3,4-dichloroaniline 10 to 200 µg/kgDodine 10 to 200 µg/kgEdifenphos 10 to 200 µg/kgEmamectin Benzoate 10 to 200 µg/kgalpha-Endosulphan 10 to 200 µg/kgbeta-Endosulphan 10 to 200 µg/kgEndosulphan Sulphate 10 to 200 µg/kgEndrin 10 to 200 µg/kgEthephon 10 to 200 µg/kgEthion 10 to 200 µg/kgEthofenprox (Etofenprox) 10 to 200 µg/kgEtrimfos 10 to 200 µg/kgFamoxadone 10 to 200 µg/kg











Fenamidone


10 to 200 µg/kgFenarimol 10 to 200 µg/kgFenazaquin 10 to 200 µg/kgFenitrothion 10 to 200 µg/kgFenobucarb 10 to 200 µg/kgFenpropathrin 10 to 200 µg/kgFenpyroximate 10 to 200 µg/kgFenthion 10 to 200 µg/kgFenthion-sulfone 10 to 200 µg/kgFenthion-sulphoxide 10 to 200 µg/kgFenvalerate 10 to 200 µg/kgFenvalerate and Esfenvalerate

10 to 200 µg/kg

Fipronil 10 to 200 µg/kgFipronil sulfone 10 to 200 µg/kgFlonicamide 10 to 200 µg/kgTNFG 10 to 200 µg/kgTNFA 10 to 200 µg/kgFlubendiamide 10 to 200 µg/kgFluchloralin 10 to 200 µg/kgFlufenacate 10 to 200 µg/kgFlufenoxuron 10 to 200 µg/kgFlufenzine 10 to 200 µg/kgFlusilazole 10 to 200 µg/kgFluvalinate 10 to 200 µg/kgForchlorfenuron (CPPU) 10 to 200 µg/kgFormothion 10 to 200 µg/kgFosetyl-Al 10 to 200 µg/kgGibberellic acid 10 to 200 µg/kgGlufosinate-ammonium 10 to 200 µg/kgMPP NAL/SOP/lNS/003


NAG 10 to 200 µg/kg











Glyphosate 10 to 200 µg/kgalpha-HCH 10 to 200 µg/kgbeta-HCH 10 to 200 µg/kgGamma-HCH 10 to 200 µg/kgdelta-HCH 10 to 200 µg/kgHexachlorbenzene 10 to 200 µg/kgHeptachlor 10 to 200 µg/kgHeptachlor epoxide 10 to 200 µg/kgHexaconazole 10 to 200 µg/kgHexythiazox 10 to 200 µg/kgHomobrassinolide 10 to 200 µg/kgHydrogen Cyanamide 10 to 200 µg/kgImidacloprid 10 to 200 µg/kgIndoxacarb 10 to 200 µg/kgIodosulfuron-methyl 10 to 200 µg/kgIprobenphos 10 to 200 µg/kgIprodione 10 to 200 µg/kgIprovalicarb 10 to 200 µg/kgIsoprothioline 10 to 200 µg/kgIsoproturon 10 to 200 µg/kgKresoxim methyl 10 to 200 µg/kgLambda-cyhalothrin 10 to 200 µg/kgLinuron 10 to 200 µg/kgLufenuron 10 to 200 µg/kgMalathion 10 to 200 µg/kgMalaoxon 10 to 200 µg/kgMandipropamid 10 to 200 µg/kgMalic Hydrazide 10 to 200 µg/kgMepiquat Chloride NAL/SOP/lNS/003


Mevinphos 10 to 200 µg/kgMetalaxyl 10 to 200 µg/kgMetalaxyl-M 10 to 200 µg/kg











Methamidophos 10 to 200 µg/kgMethomyl 10 to 200 µg/kgMethyl chloro phenoxy acetic Acid (MPCA)

10 to 200 µg/kg

Thiodicarb 10 to 200 µg/kgMetasulfuron-methyl 10 to 200 µg/kgMethabenzthiazuron 10 to 200 µg/kgMetolachlor 10 to 200 µg/kgMetribuzin 10 to 200 µg/kgMilbemectin A3 10 to 200 µg/kgMilbemectin A4 10 to 200 µg/kgMonocrotophos 10 to 200 µg/kgMyclobutanil 10 to 200 µg/kgNovaluron 10 to 200 µg/kgOxadiazon 10 to 200 µg/kgOxycarboxin 10 to 200 µg/kgOxydemeton- methyl 10 to 200 µg/kgDemeton-S-methylsulfone

10 to 200 µg/kg

Oxyfluorfen 10 to 200 µg/kgPaclobutrazole 10 to 200 µg/kgParaquit dichloride 10 to 200 µg/kgParathion Methyl 10 to 200 µg/kgParaoxon methyl 10 to 200 µg/kgParathion ethyl 10 to 200 µg/kgPenconazole 10 to 200 µg/kgPencycuron NAL/SOP/lNS/003

(LC MSMS & GC-MS MS10 to 200 µg/kg

Pendimethalin 10 to 200 µg/kgcis-Permethrin 10 to 200 µg/kgtrans-Permethrin 10 to 200 µg/kgPhenthoate 10 to 200 µg/kgPhorate 10 to 200 µg/kg











Phorate-sulfone 10 to 200 µg/kgPhorate-sulfoxide 10 to 200 µg/kgPhosalone 10 to 200 µg/kgPhosphamidon 10 to 200 µg/kgPhosmet 10 to 200 µg/kgPirimiphos-methyl 10 to 200 µg/kgProfenofos 10 to 200 µg/kgPropamocarb 10 to 200 µg/kgPropanil 10 to 200 µg/kgPropagite 10 to 200 µg/kgPropetamphos 10 to 200 µg/kgPropiconazole 10 to 200 µg/kgPropoxur 10 to 200 µg/kgPyraclostrobin 10 to 200 µg/kgPyrethrins –I 10 to 200 µg/kgPyrethrins –II 10 to 200 µg/kgPyridaben 10 to 200 µg/kgPyriproxyfen 10 to 200 µg/kgQuinalphos 10 to 200 µg/kgSimazine 10 to 200 µg/kgSpinosad A 10 to 200 µg/kgSpinosad D 10 to 200 µg/kgSpirodiclofen 10 to 200 µg/kgSpiromesifen 10 to 200 µg/kgSulphur NAL/SOP/lNS/003

(LC MSMS & GC-MS MS10 to 200 µg/kg

tau- Fluvalinate 10 to 200 µg/kgTebuconazole 10 to 200 µg/kgTemephos 10 to 200 µg/kgTetraconazole 10 to 200 µg/kgThiacloprid 10 to 200 µg/kgThiamethoxam 10 to 200 µg/kgThiobencarb











Thiometon 10 to 200 µg/kgThiophanate-methyl 10 to 200 µg/kgTransfluthrin 10 to 200 µg/kgTriadimefon 10 to 200 µg/kgTriadimenol 10 to 200 µg/kgTriazophos 10 to 200 µg/kgTrichlorfon 10 to 200 µg/kgTricyclazole 10 to 200 µg/kgTridemorph 10 to 200 µg/kgTrifloxystrobin 10 to 200 µg/kgTrifluralin 10 to 200 µg/kgTriallate 10 to 200 µg/kgUracil 10 to 200 µg/kgVinclozolin 10 to 200 µg/kgPyrimethanil 10 to 500 µg/kg Imazalil 10 to 500 µg/kgFludioxonil 10 to 500 µg/kgThiabendazole 10 to 500 µg/kgCarpropamide 10 to 500 µg/kg Fluopicolide 10 to 500 µg/kgFluopyram 10 to 500 µg/kg Fluxapyroxad 10 to 500 µg/kgMeptyldinocap NAL/SOP/lNS/003

(LC MSMS & GC-MS MS) Metrafenone 10 to 500 µg/kgPicoxystrobin 10 to 500 µg/kgTriforine 10 to 500 µg/kgValidamycin 10 to 500 µg/kgChlorimuron ethyl 10 to 500 µg/kgDimethachlor 10 to 500 µg/kgImazethapyr 10 to 500 µg/kgQuizalofop 10 to 500 µg/kgPyridalyl 10 to 500 µg/kg











Spirotetramat and its metabolites

10 to 500 µg/kg

Etoxazole 10 to 500 µg/kgTebufenozide 10 to 500 µg/kgThiocyclamTolfenpyrad 10 to 500 µg/kgNereistoxin 10 to 500 µg/kgChlorpropham 10 to 500 µg/kgTrace metal elementsLead as Pb AOAC (20th Edition),999.11 0.01 to 0.1 mg/kgCadmium as Cd AOAC (20th Edition),999.11 0.01 to 0.1 mg/kg

c. Milk & dairy products

AntibioticsChloramphenicol NAL/SOP/INS/017 0.075 to 0.75 µg/kgFlorfenicol 0.075 to 0.75 µg/kgNitrofuran MetabolitesAmino-oxazolidinone(AOZ)

NAL/SOP/INS/022

0.5 to 3 µg/kg

Semicarbazide (SEM) 0.5 to 3 µg/kgAminohydantoin (AHD) 0.5 to 3 µg/kg3-Amino-5- morpholinomethyl - 2- oxazolidinone (AMOZ)

0.5 to 3 µg/kg

SulfonamidesSulfadimidine NAL/SOP/INS/021

10 to 500 µg/kg

Sulfadiazine 10 to 500 µg/kgSulfadoxine 10 to 500 µg/kgSulfadimethoxine 10 to 500 µg/kgSulfamethazine 10 to 500 µg/kgSulfamirazine 10 to 500 µg/kgSulfanilamide 10 to 500 µg/kgSulfamethoxypyridazine 10 to 500 µg/kgSulfamethiazole 10 to 500 µg/kg











Sulfathiazole 10 to 500 µg/kgEnrofloxacin 10 to 500 µg/kgCiprofloxacin 10 to 500 µg/kgMetronidazole NAL/SOP/INS/019 0.5 to 3 µg/kgRonidazole 0.5 to 3 µg/kgStreptomycin NAL/SOP/INS/032 10 to 500 µg/kgGentamicin

NAL/SOP/INS/019

10 to 500 µg/kgKanamycin 10 to 500 µg/kgNeomycin 500 to 5000 µg/kgSpectinomycin 10 to 500 µg/kgErythromycin 10 to 500 µg/kgSpiramycin 10 to 500 µg/kgTylosin 10 to 500 µg/kgTilmicosin 10 to 500 µg/kgTetracyclinesTetracycline

NAL/SOP/INS/020

10 to 500 µg/kg4-epi-Tetracycline 10 to 500 µg/kgOxytetracycline 10 to 500 µg/kg4-epi-Oxytetracycline 10 to 500 µg/kgChlorotetracycline 10 to 500 µg/kg4-epi-Chlorotetracycline NAL/SOP/INS/020 10 to 500 µg/kgDoxycycline 10 to 500 µg/kgAnthelminticsalbendazole sulphoxide

NAL/SOP/INS/025

25 to 300 µg/kgalbendazole sulphone 25 to 300 µg/kgalbendazole 2-amino sulphone

25 to 300 µg/kg

Fenbendazole 5 to 300 µg/kgIvermectin 5 to 300 µg/kgMorantel 15 to 300 µg/kgPesticides ResidueAbamectin NAL/SOP/INS/003 10 to 500 µg/kg











(LC-MS MS& GC MSMS)

Emamectin Benzoate 10 to 500 µg/kgAldrin 10 to 500 µg/kgCis-chlordane 10 to 500 µg/kg Dieldrin 10 to 500 µg/kgEndosulphan 10 to 500 µg/kgGamma-HCH (Lindane) 10 to 500 µg/kgHeptachlor 10 to 500 µg/kgHCH-Alfa 10 to 500 µg/kgHCH-Beta 10 to 500 µg/kgHCH-Delta 10 to 500 µg/kg o,p-DDD 10 to 500 µg/kg o,p-DDE 10 to 500 µg/kg o,p-DDT 10 to 500 µg/kg p,p-DDD 10 to 500 µg/kg p,p-DDE 10 to 500 µg/kg p,p-DDT 10 to 500 µg/kgTrans-chlordane NAL/SOP/INS/003

(LC-MS MS& GC MSMS)10 to 500 µg/kg

Chlorfenvinphos 10 to 500 µg/kgChlorpyrifos 10 to 500 µg/kgCypermethrin 10 to 500 µg/kgDiazinon 10 to 500 µg/kgEthion 10 to 500 µg/kgFenitrothion 10 to 500 µg/kgFenvalerate 10 to 500 µg/kgParathion Methyl 10 to 500 µg/kgPirimiphos-methyl 10 to 500 µg/kgPhorate 10 to 500 µg/kgEthoxychlor 10 to 500 µg/kgCarbofurans 10 to 500 µg/kgFenthion 10 to 500 µg/kgFenthion-sulfone 10 to 500 µg/kgFenthion-sulphoxide 10 to 500 µg/kg











Malathion 10 to 500 µg/kgMalaoxon 10 to 500 µg/kgMonocrotophos 10 to 500 µg/kgPhenthoate 10 to 500 µg/kgPhorate-sulfone 10 to 500 µg/kgPhorate-sulfoxide 10 to 500 µg/kgPhosalone 10 to 500 µg/kg2,4-D 10 to 500 µg/kgCarbendazim 10 to 500 µg/kgBenomyl 10 to 500 µg/kgEdifenphos 10 to 500 µg/kgMycotoxinsAflatoxin M1 AOAC (19th Edition)

Chapter 490.1 to 10 µg/kg

Trace metal elements Lead AOAC (20th Edition):

999.110.01 to 10 mg/kg

Cadmium 0.01 to 10 mg/kgd. Nut and Nut

ProductsPesticides Residue

Chlorothalonil NAL/SOP/INS/003 (LC-MS MS & GC MSMS)

10 to 500 µg/kgPermethrin I 10 to 500 µg/kgPermethrin II 10 to 500 µg/kgPyrethrin I 10 to 500 µg/kgPyrethrin II 10 to 500 µg/kgIndoxacarb 10 to 500 µg/kgProthioconazole 10 to 500 µg/kgTebuconazole 10 to 500 µg/kgTrifloxystrobin 10 to 500 µg/kgMetalaxyl 10 to 500 µg/kg Azoxystrobin 10 to 500 µg/kgCarbendazim 10 to 500 µg/kgAldicarb 10 to 500 µg/kg











Imidacloprid 10 to 500 µg/kge. Cereals, pulses &

cereal productsPesticide Residue Fenoxaprop-P-ethyl

NAL/SOP/INS/003 (LC-MS MS & GC MSMS)

10 to 500 µg/kgAnilophos 10 to 500 µg/kgChlorimuron-ethyl 10 to 500 µg/kgClodinafop-propargyl 10 to 500 µg/kgClomazone 10 to 500 µg/kgCyhalofop-butyl 10 to 500 µg/kgDiclofop-methyl 10 to 500 µg/kgEthoxysulfuron 10 to 500 µg/kgParaquat NAL/SOP/INS/003


Pretilachlor 10 to 500 µg/kgPyrazosulfuron ethyl 10 to 500 µg/kgSulfosulfuron 10 to 500 µg/kgQuizalofop-ethyl 10 to 500 µg/kgCinosulfuran 10 to 500 µg/kgChlorimuron-ethyl 10 to 500 µg/kgBensulfuron methyl 10 to 500 µg/kgBentazone – sodium 10 to 500 µg/kgMolinate 10 to 500 µg/kgCycloxydim 10 to 500 µg/kgCarpropamid 10 to 500 µg/kgTriflumizole 10 to 500 µg/kgFludioxonil 10 to 500 µg/kgFlutolanil 10 to 500 µg/kgOxadiargyl 10 to 500 µg/kgCyhalothrin 10 to 500 µg/kg1-Naphthylacetic acid 10 to 200 µg/kg2,4-D 10 to 200 µg/kg4-bromo-2-chlorophenol 10 to 200 µg/kg4 Chlorophenoxy acetic acid

10 to 200 µg/kg











6-Benzyl adenine 10 to 200 µg/kgAbamectin 10 to 200 µg/kgAcephate 10 to 200 µg/kgAcetamiprid 10 to 200 µg/kgAlachlor 10 to 200 µg/kgAldrin 10 to 200 µg/kgDieldrin 10 to 200 µg/kgAllethrin/Bioallethrin 10 to 200 µg/kgAmetoctradin NAL/SOP/INS/003


Atrazine 10 to 200 µg/kgAzadirachtin 10 to 200 µg/kgAzoxystrobin 10 to 200 µg/kgBenalaxyl and isomers 10 to 200 µg/kgBendiocarb 10 to 200 µg/kgBenfuracarb 10 to 200 µg/kgBenomyl 10 to 200 µg/kgBifenazate 10 to 200 µg/kgBifenthrin 10 to 200 µg/kgBitertenol 10 to 200 µg/kgBromophos 10 to 200 µg/kgButachlor 10 to 200 µg/kgBuprofezin 10 to 200 µg/kgCaptafol 10 to 200 µg/kgCaptan 10 to 200 µg/kgCarbaryl 10 to 200 µg/kgCarbendazim 10 to 200 µg/kgCarbofuran 10 to 200 µg/kg3-hydroxy-carbofuran 10 to 200 µg/kgCarbosulfan 10 to 200 µg/kgCarboxin 10 to 200 µg/kgCartap hydrochloride 10 to 200 µg/kgChlorantraniliprole 10 to 200 µg/kg











Cis-chlordane 10 to 200 µg/kgtrans-chlordane 10 to 200 µg/kgChlorfenopyr 10 to 200 µg/kgChlorfenvinphos 10 to 200 µg/kgChlormequat chloride (CCC)

10 to 200 µg/kg

Chlorothalonil NAL/SOP/INS/003 (LC-MS MS& GC MSMS)

10 to 200 µg/kgChlorobenzilate 10 to 200 µg/kgChlorpyrifos 10 to 200 µg/kgChlorpyrifos methyl 10 to 200 µg/kgClothianidin 10 to 200 µg/kgCyantraniliprole 10 to 200 µg/kgCyazofamid 10 to 200 µg/kgCyfluthrin 1 10 to 200 µg/kgCyfluthrin 2 10 to 200 µg/kgCyfluthrin 3 10 to 200 µg/kgCyfluthrin 4 10 to 200 µg/kgCymoxanil 10 to 200 µg/kgCypermethrin 1 10 to 200 µg/kgCypermethrin 2 10 to 200 µg/kgCypermethrin 3 10 to 200 µg/kgCypermethrin 4 10 to 200 µg/kgDazomet 10 to 200 µg/kgp,p´-DDT 10 to 200 µg/kgo,p´-DDT 10 to 200 µg/kgp,p´-DDE 10 to 200 µg/kgp,p´-TDE (DDD) 10 to 200 µg/kgDeltamethrin 10 to 200 µg/kgDiafenthiuron 10 to 200 µg/kgDiazinon 10 to 200 µg/kgDichlorvos 10 to 200 µg/kgDicofol 10 to 200 µg/kg











Difenoconazole 10 to 200 µg/kgDiflubenzuron 10 to 200 µg/kgDimethoate 10 to 200 µg/kgOmethoate 10 to 200 µg/kgDimethomorph NAL/SOP/INS/003


Dinocap 10 to 200 µg/kgDinotefuran 10 to 200 µg/kgDiquat 10 to 200 µg/kgDithianon 10 to 200 µg/kgMancozeb 10 to 200 µg/kgManeb 10 to 200 µg/kgPropineb 10 to 200 µg/kgThiram 10 to 200 µg/kgZineb 10 to 200 µg/kgZiram 10 to 200 µg/kgMetiram 10 to 200 µg/kgDiuron 10 to 200 µg/kg3,4-dichloroaniline 10 to 200 µg/kgDodine 10 to 200 µg/kgEdifenphos 10 to 200 µg/kgEmamectin Benzoate 10 to 200 µg/kgalpha-Endosulphan 10 to 200 µg/kgbeta-Endosulphan 10 to 200 µg/kgEndosulphan Sulphate 10 to 200 µg/kgEndrin 10 to 200 µg/kgEthephon 10 to 200 µg/kgEthion 10 to 200 µg/kgEthofenprox (Etofenprox) 10 to 200 µg/kgEtrimfos 10 to 200 µg/kgFamoxadone 10 to 200 µg/kgFenamidone 10 to 200 µg/kgFenarimol 10 to 200 µg/kg











Fenazaquin 10 to 200 µg/kgFenitrothion 10 to 200 µg/kgFenobucarb

NAL/SOP/INS/003 (LC-MS MS& GC MSMS)

10 to 200 µg/kgFenpropathrin 10 to 200 µg/kgFenpyroximate 10 to 200 µg/kgFenthion 10 to 200 µg/kgFenthion-sulfone 10 to 200 µg/kgFenthion-sulphoxide 10 to 200 µg/kgFenvalerate 10 to 200 µg/kgFenvalerate and Esfenvalerate

10 to 200 µg/kg

Fipronil 10 to 200 µg/kgFipronil sulfone 10 to 200 µg/kgFlonicamide 10 to 200 µg/kgTNFG 10 to 200 µg/kgTNFA 10 to 200 µg/kgFlubendiamide 10 to 200 µg/kgFluchloralin 10 to 200 µg/kgFlufenacate 10 to 200 µg/kgFlufenoxuron 10 to 200 µg/kgFlufenzine 10 to 200 µg/kgFlusilazole 10 to 200 µg/kgFluvalinate 10 to 200 µg/kgForchlorfenuron (CPPU) 10 to 200 µg/kgFormothion 10 to 200 µg/kgFosetyl-Al 10 to 200 µg/kgGibberellic acid 10 to 200 µg/kgGlufosinate-ammonium 10 to 200 µg/kgMPP 10 to 200 µg/kgNAG 10 to 200 µg/kgGlyphosate 10 to 200 µg/kgalpha-HCH 10 to 200 µg/kg











beta-HCH


10 to 200 µg/kgGamma-HCH 10 to 200 µg/kgdelta-HCH 10 to 200 µg/kgHexachlorbenzene 10 to 200 µg/kgHeptachlor 10 to 200 µg/kgHeptachlor epoxide 10 to 200 µg/kgHexaconazole 10 to 200 µg/kgHexythiazox 10 to 200 µg/kgHomobrassinolide 10 to 200 µg/kgHydrogen Cyanamide 10 to 200 µg/kgImidacloprid 10 to 200 µg/kgIndoxacarb 10 to 200 µg/kgIodosulfuron-methyl 10 to 200 µg/kgIprobenphos 10 to 200 µg/kgIprodione 10 to 200 µg/kgIprovalicarb 10 to 200 µg/kgIsoprothioline 10 to 200 µg/kgIsoproturon 10 to 200 µg/kgKresoxim methyl 10 to 200 µg/kgLambda-cyhalothrin 10 to 200 µg/kgLinuron 10 to 200 µg/kgLufenuron 10 to 200 µg/kgMalathion 10 to 200 µg/kgMalaoxon 10 to 200 µg/kgMandipropamid 10 to 200 µg/kgMalic Hydrazide 10 to 200 µg/kgMepiquat Chloride 10 to 200 µg/kgMevinphos 10 to 200 µg/kgMetalaxyl 10 to 200 µg/kgMetalaxyl-M 10 to 200 µg/kgMethamidophos NAL/SOP/INS/003


Methomyl 10 to 200 µg/kg











Methyl chloro phenoxy acetic Acid (MPCA)

10 to 200 µg/kg

Thiodicarb 10 to 200 µg/kgMetasulfuron-methyl 10 to 200 µg/kgMethabenzthiazuron 10 to 200 µg/kgMetolachlor 10 to 200 µg/kgMetribuzin 10 to 200 µg/kgMilbemectin A3 10 to 200 µg/kgMilbemectin A4 10 to 200 µg/kgMonocrotophos 10 to 200 µg/kgMyclobutanil 10 to 200 µg/kgNovaluro 10 to 200 µg/kgOxadiazon 10 to 200 µg/kgOxycarboxin 10 to 200 µg/kgOxydemeton- methyl 10 to 200 µg/kgDemeton-S-methylsulfone

10 to 200 µg/kg

Oxyfluorfen 10 to 200 µg/kgPaclobutrazole 10 to 200 µg/kgParaquit dichloride 10 to 200 µg/kgParathion Methyl 10 to 200 µg/kgParaoxon methyl 10 to 200 µg/kgParathion ethyl 10 to 200 µg/kgPenconazole 10 to 200 µg/kgPencycuron 10 to 200 µg/kgPendimethalin 10 to 200 µg/kgcis-Permethrin 10 to 200 µg/kgtrans-Permethrin 10 to 200 µg/kgPhenthoate 10 to 200 µg/kgPhorate NAL/SOP/INS/003


Phorate-sulfone 10 to 200 µg/kgPhorate-sulfoxide 10 to 200 µg/kg











Phosalone 10 to 200 µg/kgPhosphamidon 10 to 200 µg/kgPhosmet 10 to 200 µg/kgPirimiphos-methyl 10 to 200 µg/kgProfenofos 10 to 200 µg/kgPropamocarb 10 to 200 µg/kgPropanil 10 to 200 µg/kgPropagite 10 to 200 µg/kgPropetamphos 10 to 200 µg/kgPropiconazole 10 to 200 µg/kgPropoxur 10 to 200 µg/kgPyraclostrobin 10 to 200 µg/kgPyrethrins –I 10 to 200 µg/kgPyrethrins –II 10 to 200 µg/kgPyridaben 10 to 200 µg/kgPyriproxyfen 10 to 200 µg/kgQuinalphos 10 to 200 µg/kgSimazine 10 to 200 µg/kgSpinosad A 10 to 200 µg/kgSpinosad D 10 to 200 µg/kgSpirodiclofen 10 to 200 µg/kgSpiromesifen 10 to 200 µg/kgSulphur 10 to 200 µg/kgtau- Fluvalinate 10 to 200 µg/kgTebuconazole 10 to 200 µg/kgTemephos 10 to 200 µg/kgTetraconazole 10 to 200 µg/kgThiacloprid NAL/SOP/INS/003


Thiamethoxam 10 to 200 µg/kgThiobencarb 10 to 200 µg/kgThiometon 10 to 200 µg/kgThiophanate-methyl 10 to 200 µg/kg











Transfluthrin 10 to 200 µg/kgTriadimefon 10 to 200 µg/kgTriadimenol 10 to 200 µg/kgTriazophos 10 to 200 µg/kgTrichlorfon 10 to 200 µg/kgTricyclazole 10 to 200 µg/kgTridemorph 10 to 200 µg/kgTrifloxystrobin 10 to 200 µg/kgTrifluralin 10 to 200 µg/kgTriallate 10 to 200 µg/kgUracil 10 to 200 µg/kgVinclozolin 10 to 200 µg/kg

f. Spice & Spice products (Pesticide Residue)

BHC


10 to 500 µg/kgEthion 10 to 500 µg/kgDicofol 10 to 500 µg/kg

Endosulphan 10 to 500 µg/kgp,p´-DDT 10 to 500 µg/kgo,p´-DDT 10 to 500 µg/kgHeptachlor 10 to 500 µg/kgAldrin 10 to 500 µg/kgDieldrin 10 to 500 µg/kgEndrin 10 to 500 µg/kgDiendrin 10 to 500 µg/kgChlorothalonil 10 to 500 µg/kgPhosmet NAL/SOP/INS/003


Chlorpyriphos 10 to 500 µg/kgParathion Methyl 10 to 500 µg/kgPhorate 10 to 500 µg/kgParathion 10 to 500 µg/kgPrimiphos-methyl 10 to 500 µg/kgBifenthrin 10 to 500 µg/kg











Cypermethrin 10 to 500 µg/kgFenvalerate 10 to 500 µg/kgFenitrothion 10 to 500 µg/kgChlorfenvinphos 10 to 500 µg/kgAzinphos ethyl 10 to 500 µg/kgCyhalothrin (includes lambda cyhalothrin)

10 to 500 µg/kg

Cypermethrin 10 to 500 µg/kgCarbaryl 10 to 500 µg/kgCarbofuran 10 to 500 µg/kgMethomyl 10 to 500 µg/kgAldicarb 10 to 500 µg/kgDithiocarbamates Mancozeb, Maneb, Propineb , Metiram, Thiram,Zineb and Ziram collectively estimated as CS2)

10 to 500 µg/kg

Dimethoate 10 to 500 µg/kgEtrimfos 10 to 500 µg/kgQuinalphos 10 to 500 µg/kgMonocrotophos 10 to 500 µg/kgMalathion 10 to 500 µg/kgPhenthoate 10 to 500 µg/kgPhosalone NAL/SOP/INS/003


Profenofos 10 to 500 µg/kgTrichlorfon 10 to 500 µg/kgMethoate 10 to 500 µg/kgAlachlor 10 to 500 µg/kgDithianon 10 to 500 µg/kgFosetyl-Al 10 to 500 µg/kgIprodion 10 to 500 µg/kg











Iprobenphos 10 to 500 µg/kgTriazophos 10 to 500 µg/kg

g. Tea & Coffee Products

Pesticide ResidueEndosulfan


10 to 500 µg/kgAldrin 10 to 500 µg/kgDieldrin 10 to 500 µg/kgo,p’-DDE 10 to 500 µg/kgp,p’-DDE 10 to 500 µg/kgo,p’-DDT 10 to 500 µg/kgp,p’-DDT 10 to 500 µg/kgo,p’-DDD 10 to 500 µg/kgp,p’-DDD 10 to 500 µg/kgDicofol 10 to 500 µg/kgEndrin 10 to 500 µg/kgHeptachlor isomer 10 to 500 µg/kgHexachlor benzene 10 to 500 µg/kgHexachloro cyclo hexane Isomer

10 to 500 µg/kg

Ethion 10 to 500 µg/kgChlorpyrifos 10 to 500 µg/kgCyfluthrin Isomers 10 to 500 µg/kgCypermethrin 1 10 to 500 µg/kgDeltamethrin NAL/SOP/INS/003


Fenitrothion 10 to 500 µg/kgFenvalerate 10 to 500 µg/kgFenpropathrin 10 to 500 µg/kgLambda-cyhalothrin 10 to 500 µg/kgDisulfoton 10 to 500 µg/kgPermethrin 10 to 500 µg/kgLindane 10 to 500 µg/kgPhorate 10 to 500 µg/kgCarbaryl 10 to 500 µg/kg



http://www.fao.org/fao-who-codexalimentarius/standards/pestres/pesticide-detail/en/?p_id=112










Carbofuran 10 to 500 µg/kgCarbosulfan 10 to 500 µg/kgPropineb 10 to 500 µg/kgThiram 10 to 500 µg/kgZiram 10 to 500 µg/kgAldicarb 10 to 500 µg/kgCartap 10 to 500 µg/kgMancozeb 10 to 500 µg/kgEthephon 10 to 500 µg/kgFlufenzine 10 to 500 µg/kgBifenthrin 10 to 500 µg/kgAcephate 10 to 500 µg/kgAzadiractin 10 to 500 µg/kgDimethoate 10 to 500 µg/kgFenazaquin 10 to 500 µg/kgMalathion 10 to 500 µg/kgMonocrotophos 10 to 500 µg/kgOxydemeton-methyl 10 to 500 µg/kgPhosalone 10 to 500 µg/kgProfenofos 10 to 500 µg/kg

Quinalphos NAL/SOP/INS/003 (LC-MS MS& GC MSMS)

10 to 500 µg/kg

Indoxacarb 10 to 500 µg/kgMethidathion 10 to 500 µg/kgHaloxyfop 10 to 500 µg/kg2,4-D 10 to 500 µg/kgAlachlor 10 to 500 µg/kgDiuron 10 to 500 µg/kgGlyphosate 10 to 500 µg/kgOxyflurofen 10 to 500 µg/kgParaquat 10 to 500 µg/kg













Simazine 10 to 500 µg/kgGlufosinate Ammonium 10 to 500 µg/kg Diquat 10 to 500 µg/kgSaflufenacil 10 to 500 µg/kgBitertanol 10 to 500 µg/kgCarbendazim 10 to 500 µg/kgChlorothalonil 10 to 500 µg/kgHexaconazole 10 to 500 µg/kgPropiconazole 10 to 500 µg/kgTebuconazole 10 to 500 µg/kgTridemorph 10 to 500 µg/kgGibberellic acid 10 to 500 µg/kgAzoxystrobin 10 to 500 µg/kgCyproconazole 10 to 500 µg/kgBoscalid 10 to 500 µg/kgFlutriafol 10 to 500 µg/kgPyraclostrobin 10 to 500 µg/kgTriadimefon 10 to 500 µg/kgTriadimenol 10 to 500 µg/kgAcetamiprid NAL/SOP/INS/003


Clothianidin 10 to 500 µg/kgDiazinon 10 to 500 µg/kgDichlorvos 10 to 500 µg/kgDiflubenzuron 10 to 500 µg/kgFlufenoxuron 10 to 500 µg/kgImidacloprid 10 to 500 µg/kgMilbemectin 10 to 500 µg/kgSpiromesifen 10 to 500 µg/kgThiacloprid 10 to 500 µg/kgThiamethoxam 10 to 500 µg/kgTriazophos 10 to 500 µg/kgFlubendamide 10 to 500 µg/kg




















Buprofezin 10 to 500 µg/kgChlorantraniliprole 10 to 500 µg/kgCyantraniliprole 10 to 500 µg/kgSpirodiclofen 10 to 500 µg/kgTerbufos 10 to 500 µg/kgBifenazate 10 to 500 µg/kgEtoxazole 10 to 500 µg/kgHexythiazox 10 to 500 µg/kgPropargite 10 to 500 µg/kgClofentezine 10 to 500 µg/kg

h. Edible Oils & Fats Pesticide Residue Aldrin


10 to 500 µg/kgChlordane 10 to 500 µg/kg Dieldrin 10 to 500 µg/kg Endosulphan alpha 10 to 500 µg/kgEndosulphan Beta 10 to 500 µg/kg Endosulphan Sulphate 10 to 500 µg/kg Heptachlor NAL/SOP/INS/003


HCH-α 10 to 500 µg/kgHCH-ß 10 to 500 µg/kgHCH-γ 10 to 500 µg/kg HCH-delta 10 to 500 µg/kgo,p- DDT 10 to 500 µg/kgo,p-DDD 10 to 500 µg/kgo,p-DDE 10 to 500 µg/kgp,p-DDT 10 to 500 µg/kgp,p-DDD 10 to 500 µg/kgp,p-DDE 10 to 500 µg/kgChlorfenvinphos 10 to 500 µg/kgChlorpyriphos 10 to 500 µg/kgCypermethrin 10 to 500 µg/kgEthion 5 to 200 µg/kg
















Fenitrothion 10 to 500 µg/kgLambda-cyhalothrin 10 to 500 µg/kgPhorate 5 to 200 µg/kgPirimiphos-methyl 10 to 200 µg/kgCarbofuran 5 to 200 µg/kgThiodicarb 10 to 500 µg/kgMetiram 10 to 500 µg/kgFenpropathrin 10 to 500 µg/kgFluvalinate 10 to 500 µg/kgFenthion 5 to 200 µg/kgMonocrotophos 5 to 200 µg/kgPhenthoate 5 to 200 µg/kgPhosalone 5 to 200 µg/kgTriazophos 5 to 200 µg/kgTrichlorfon 5 to 200 µg/kgProfenofos NAL/SOP/INS/003


Acetamiprid 10 to 200 µg/kgImidacloprid 5 to 200 µg/kgNovaluron 5 to 200 µg/kgIndoxacarb 10 to 500 µg/kgSpinosad A 10 to 500 µg/kgThiacloprid 5 to 200 µg/kgFenvalerate 10 to 500 µg/kg2,4-D 10 to 200 µg/kgMetolachlor 10 to 200 µg/kgMetribuzin 5 to 200 µg/kgOxyfluorfen 10 to 200 µg/kgParaquat dichloride 5 to 200 µg/kgPendimethalin 10 to 200 µg/kgClomazone 10 to 500 µg/kgImazethapyr 10 to 500 µg/kgBenomyl 5 to 200 µg/kg











Carbendazim 5 to 200 µg/kgEdifenphos 5 to 200 µg/kg

X HAZARDOUS & RESTRICTED CHEMICALS ROHS (RESTRICTION OF HAZARDOUS SUBSTANCES)

a. Electro Technical Products Plastic, Leather, Rubber, Metals

Cadmium as Cd ASTM E351,IEC 62321 1 to 100 mg/kgLead as Pb ASTM E351,IEC 62321 1 to 1000 mg/kgMercury as Hg IEC 62321 1 to 1000 mg/kgHexavalent Chromium as Cr6+

ASTM D 6492-99,IEC 62321

1 to 1000 mg/kg

b. Paints Cadmium ASTM D 3335– 85a 1 to 1000 mg/kgLead ASTM D 3335– 85a 1 to 1000 mg/kgMercury ISO 7252 1 to 1000 mg/kgHexavalent Chromium as Cr6+

ISO 3856-5 1 to 1000 mg/kg

XI METALS AND ALLOYS

a. Ferrous materials Low Alloy Steel

Carbon IS 228 (Part -1 & 4) 0.03 % to 4.5 % Manganese IS 228 (Part- 2) 0.05 % to 2.0 %Silicon IS 228 (Part- 8),

IS 228 (Part -11)0.10 % to 2.0 %

Sulphur IS 228 (Part- 9) 0.01 % to 0.5 %Phosphorus IS 228 (Part -3) 0.02 % to 0.15 %Chromium IS 228 (Part -6),

IS 12308(Part- 8)0.1 % to 5.0 %

Nickel IS 228 (Part -5) 0.05 % to 5.0 % Molybdenum IS 228 (Part -7)

IS 228 (Part -10)0.1 % to 2.0 %

Copper IS 228 (Part -15) 0.1 % to 1.0 % b. Stainless Steel Carbon IS 228 (Part -1 &4) 0.03 % to 1.5 %

Manganese IS 228 (Part -2) 0.05 % to 10.0 %











Silicon IS 228 (Part -8),IS 228 (Part -11)

0.10 %to 2.0 %

Sulphur IS 228 (Part -9) 0.01 % to 0.05 %Phosphorus IS 228 (Part -3) 0.01 % to 0.10 %Chromium IS 228 (Part -6),

IS 12308 (Part- 8)5.0 % to 30 %

Nickel IS 228 (Part -5) 0.10 % to 22 % Molybdenum IS 228 (Part -7),

IS 228 (Part -10)0.01 % to 4 %

c. Tool Steel Carbon IS 228(Part- 1 &4) 0.3 % to 2.5 % Manganese IS 228 (Part- 2) 0.1 % to 0.6 % Silicon IS 228 (Part -8),

IS 228 (Part-11)0.1 % to 0.6 %

Sulphur IS 228 (Part -9) 0.01 % to 0.05 % Phosphorus IS 228 (Part-3) 0.01 % to 0.05 % Chromium IS 228 (Part -6),

IS 12308 (Part -8)0.5 % to 5 %

Molybdenum IS 228 (Part -7),IS 228 (Part -10)

0.1 % to 10.0 %

d. Carbon Steel Carbon IS 228 (Part-1 &4) 0.02 % to 3.5 % Manganese IS 228 (Part -2) 0.05 % to 10.0 %Silicon IS 228 (Part -8),

IS 228 (Part -11)0.05 %to 3.5 %

Sulphur IS 228 (Part- 9) 0.01 % to 0.3 %Phosphorus IS 228 (Part -3) 0.01 % to 0.15 %Chromium IS 228 (Part- 6),

IS 12308 (Part -8)0.1 % to 3 %

Nickel IS 228 (Part -5) 0.01 % to 5 % Molybdenum IS 228 (Part -7)

IS 228 (Part -10)0.02 % to 4 %

Copper IS 228 (Part-15) 0.01 % to 3 %XII SOLID FUELS











a. Coal and Coke Total moisture IS 1350 (Part -1) 1.00 % to 60.00 %Ash IS 1350 (Part -1) 0.1 to 50 %Volatile matter IS 1350 (Part -1) 0.5 % to 60 %Sulphur IS 1350 (Part- 3) 0.5 % to 2 %Carbon IS 1350 (Part -4/Sec I) 30 % to 90 %Gross calorific value IS 1350 (Part -1) 500 to 10,000 kcal/kgNitrogen content IS 1350 (Part 4/Sec II) 0.50 % to 4.00 %

XIII BUILDING MATERIAL

a. Fly Ash Alumina as Al2O3 IS 1727 0.1 % to 40 %Calcium Oxide as Cao IS 1727 0.1 % to 20 %Potassium as K2O IS 1727 0.5 % to 7.0 %Ferric oxide(Fe2O3) IS 1727 0.1 % to 5 %Available alkali as Na2O IS 4032 0.05 % to 5 %Sulfuric anhydride IS 1727 0.1 % to 5 %











MECHANICAL TESTING

I. PLASTICS AND POLYMERS

1. Container for Packaged Drinking Water / Packaged Natural Mineral Water

Finish & Appearance IS 15410 QualitativeBrimful Capacity IS 2798,Cl. 5 200 ml to 25 lWall Thickness IS 2798,Cl. 4.5 0.050 to 5 mmTransparency IS 15410,Cl. 4.6.2

Annexure A50 % to 100 %

Leakage Test Closure Leakage IS 2798,Cl. 6.1 QualitativeVibration Leakage IS 2798,Cl. 6.2 QualitativeAir Pressure Leakage IS 2798

Cl. 6.3Qualitative

Drop Test IS 2798Cl. 8 QualitativeMigration Test IS 9845 0.1 to 50 mg/dm2

0.1 to 200 mg/l Water Potability Test IS 15410

Cl. 4.6.6 Annexure BQualitative

Design, Shape And Dimension

IS 15410 Qualitative

2. Films for Packaged Drinking Water / Packaged Natural Mineral Water

Description IS 15609 QualitativeOdour IS 15609 QualitativeThickness IS 2508,Annexure 2 0.001 to 1 mmWidth IS 15609 100 to 400 mm Overall Migration IS 9845 0.1 to 60 mg/dm2Tensile Strength IS 2508,Annexure 4 150 to 600 kgf/cm2Elongation At Break IS 2508,Annexure 4 100 % to 1500 % Dart Impact Resistance IS 2508 ,Annexure 6 52 to 250 gf

3. Flexible Pouch for Packaged

Water Potability Test IS 15609,Annexure E QualitativeDrop Test IS 15609 ,Annexure G Qualitative











Drinking Water / Packaged Natural Mineral Water

Ink Adhesion Test For Printed Pouch

IS 15609 ,Annexure H Qualitative

Product Resistance Test For Printed Pouch

IS 15609,Annexure J Qualitative

II. MECHANICAL PROPERTIES OF METALS

1. Ferrous and Non Ferrous Metals

Tensile Strength IS 1608,ASTM-A370 100 to 1000 N/mm2

Yield Strength IS 1608,ASTM-A370 100 to 1000 N/mm2

0.2 Proof Strength IS 1608,ASTM-A370 100 to 1000 N/mm2

% Elongation IS 1608,ASTM-A370 1 % to 75 %% Reduction Area IS 1608,ASTM-A370 5.0 % to 80.0 %Bend Test IS 1559 Qualitative

Mandrel dia. 2 mm to 200 mm

2. Inorganic and Organic Coating

Neutral Salt Spray Testing

IS 9844,ASTM-B117-16 Qualitative

3. Hardness Test Rockwell Hardness Test IS 1586 (Part -2),ISO 6508-1

100 kgf [20 HRB to 100 HRB]150 kgf [ 20 HRC to 70 HRC]15 N [80 HRN to 93 HRN]30 N [59 HRN to 84 HRN]45 N [43 HRN to 75 HRN]

Brinell Hardness Test IS 1500 (Part- 2),ISO 6506-1

500 kgf load/10 mm dia ball [50 to 150]750 kgf load/5 mm dia ball [150 to300] 1000 kgf load/10 mm dia ball [100 to 500]3000 kgf load/10 mm dia











ball [100 to 500]Micro Vickers Hardness Test

IS 1501 (Part -2),ISO 6507-1

HV1 [150 to 1100]HV5 [100 to 1400]HV10 [100 to 1500]HV30 [100 to 1900]

4. Metallic and Oxide Coating On Metal

Coating Thickness ASTM B487-85,ISO 1463 Upto 500 micron



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