Page 88 of 88 - eGram...10306235004 LHA-21/2-4 WI MOD DRO MT 2 PASI-M WI MOD GRO RTP 2 PASI-M EPA...

#=CL#

May 27, 2015

LIMS USE: FR - JERRY MULLIN

LIMS OBJECT ID: 10306235

10306235

Project:

Pace Project No.:

RE:

Mr. Jerry MullinLandmark Environmental2042 West 98th StreetBloomington, MN 55431

HC-15-002 CSAH-53

Dear Mr. Mullin:

Enclosed are the analytical results for sample(s) received by the laboratory on May 13, 2015. Theresults relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Jessica Patterson

[email protected]

Project Manager

Enclosures

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.

1700 Elm Street - Suite 200

Minneapolis, MN 55414

(612)607-1700

Page 1 of 58

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414A2LA Certification #: 2926.01Alaska Certification #: UST-078Alaska Certification #MN00064Alabama Certification #40770Arizona Certification #: AZ-0014Arkansas Certification #: 88-0680California Certification #: 01155CAColorado Certification #PaceConnecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-LFlorida/NELAP Certification #: E87605Guam Certification #:14-008rGeorgia Certification #: 959Georgia EPD #: PaceIdaho Certification #: MN00064Hawaii Certification #MN00064Illinois Certification #: 200011Indiana Certification#C-MN-01Iowa Certification #: 368Kansas Certification #: E-10167Kentucky Dept of Envi. Protection - DW #90062Kentucky Dept of Envi. Protection - WW #:90062Louisiana DEQ Certification #: 3086Louisiana DHH #: LA140001Maine Certification #: 2013011Maryland Certification #: 322Michigan DEPH Certification #: 9909

Minnesota Certification #: 027-053-137Mississippi Certification #: PaceMontana Certification #: MT0092Nevada Certification #: MN_00064Nebraska Certification #: PaceNew Jersey Certification #: MN-002New York Certification #: 11647North Carolina Certification #: 530North Carolina State Public Health #: 27700North Dakota Certification #: R-036Ohio EPA #: 4150Ohio VAP Certification #: CL101Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001Pennsylvania Certification #: 68-00563Puerto Rico CertificationSaipan (CNMI) #:MP0003South Carolina #:74003001Texas Certification #: T104704192Tennessee Certification #: 02818Utah Certification #: MN000642013-4Virginia DGS Certification #: 251Virginia/VELAP Certification #: PaceWashington Certification #: C486West Virginia Certification #: 382West Virginia DHHR #:9952CWisconsin Certification #: 999407970

Green Bay Certification IDs1241 Bellevue Street, Green Bay, WI 54302Florida/NELAP Certification #: E87948Illinois Certification #: 200050Kentucky Certification #: 82Louisiana Certification #: 04168Minnesota Certification #: 055-999-334

North Dakota Certification #: R-150South Carolina Certification #: 83006001Texas Certification #: T104704529-14-1US Dept of Agriculture #: S-76505Wisconsin Certification #: 405132750







(612)607-1700

Page 2 of 58

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Lab ID Sample ID Matrix Date Collected Date Received

10306235001 LGP-18/3-5 Solid 05/12/15 00:00 05/13/15 14:34

10306235002 LGP-19/4-6 Solid 05/12/15 00:00 05/13/15 14:34

10306235003 LHA-20/5-7 Solid 05/12/15 00:00 05/13/15 14:34

10306235004 LHA-21/2-4 Solid 05/12/15 00:00 05/13/15 14:34

10306235005 LGP-22/4-6 Solid 05/12/15 00:00 05/13/15 14:34

10306235006 LGP-23/6-8 Solid 05/12/15 00:00 05/13/15 14:34

10306235007 LGP-23/17-20 Water 05/12/15 00:00 05/13/15 14:34

10306235008 LGP-24/3-5 Solid 05/12/15 00:00 05/13/15 14:34

10306235009 LGP-25/1-3 Solid 05/12/15 00:00 05/13/15 14:34

10306235010 LGP-25/15-20 Water 05/12/15 00:00 05/13/15 14:34







(612)607-1700

Page 3 of 58

#=SA#

SAMPLE ANALYTE COUNT

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Lab ID Sample ID Method

Analytes

Reported LaboratoryAnalysts

10306235001 LGP-18/3-5 EPA 6010C 7 PASI-MIP

EPA 7471B 1 PASI-MLMW

ASTM D2974 1 PASI-MJDL

EPA 8270D by SIM 19 PASI-MAS1

10306235002 LGP-19/4-6 WI MOD DRO 2 PASI-MMT

WI MOD GRO 2 PASI-MRTP

EPA 6010C 7 PASI-MIP




EPA 8260B 70 PASI-MLPM

10306235003 LHA-20/5-7 EPA 6010C 7 PASI-MIP




10306235004 LHA-21/2-4 WI MOD DRO 2 PASI-MMT





















10306235007 LGP-23/17-20 WI MOD DRO 2 PASI-MJRH







(612)607-1700

Page 4 of 58

#=SA#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Analytes

Reported LaboratoryAnalysts

WI MOD GRO 1 PASI-GPMS

EPA 8260B 70 PASI-MAJC

10306235008 LGP-24/3-5 EPA 6010C 7 PASI-MIP











10306235010 LGP-25/15-20 WI MOD DRO 2 PASI-MJRH

WI MOD GRO 1 PASI-GPMS

EPA 8260B 70 PASI-MAJC







(612)607-1700

Page 5 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Sample: LGP-18/3-5 Lab ID: 10306235001 Collected: 05/12/15 00:00 Received: 05/13/15 14:34 Matrix: Solid

Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.

Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit

Analytical Method: EPA 6010C Preparation Method: EPA 30506010C MET ICP

Arsenic ND mg/kg 05/20/15 00:50 7440-38-205/18/15 04:460.95 1

Barium 83.7 mg/kg 05/20/15 00:50 7440-39-305/18/15 04:460.47 1

Cadmium 0.29 mg/kg 05/20/15 00:50 7440-43-905/18/15 04:460.14 1

Chromium 9.1 mg/kg 05/20/15 00:50 7440-47-305/18/15 04:460.47 1

Lead 5.3 mg/kg 05/20/15 00:50 7439-92-105/18/15 04:460.47 1

Selenium ND mg/kg 05/20/15 00:50 7782-49-205/18/15 04:460.95 1

Silver ND mg/kg 05/20/15 00:50 7440-22-405/18/15 04:460.47 1

Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471B Mercury

Mercury 0.022 mg/kg 05/18/15 19:29 7439-97-605/17/15 15:180.021 1

Analytical Method: ASTM D2974Dry Weight

Percent Moisture 13.0 % 05/19/15 09:040.10 1

Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35508270D MSSV PAH by SIM

Acenaphthene ND mg/kg 05/20/15 06:07 83-32-905/15/15 22:170.011 1

Acenaphthylene ND mg/kg 05/20/15 06:07 208-96-805/15/15 22:170.011 1

Anthracene ND mg/kg 05/20/15 06:07 120-12-705/15/15 22:170.011 1

Benzo(a)anthracene ND mg/kg 05/20/15 06:07 56-55-305/15/15 22:170.011 1

Benzo(a)pyrene ND mg/kg 05/20/15 06:07 50-32-805/15/15 22:170.011 1

Benzo(b)fluoranthene ND mg/kg 05/20/15 06:07 205-99-205/15/15 22:170.011 1

Benzo(g,h,i)perylene ND mg/kg 05/20/15 06:07 191-24-205/15/15 22:170.011 1

Benzo(k)fluoranthene ND mg/kg 05/20/15 06:07 207-08-905/15/15 22:170.011 1

Chrysene ND mg/kg 05/20/15 06:07 218-01-905/15/15 22:170.011 1

Dibenz(a,h)anthracene ND mg/kg 05/20/15 06:07 53-70-305/15/15 22:170.011 1

Fluoranthene ND mg/kg 05/20/15 06:07 206-44-005/15/15 22:170.011 1

Fluorene ND mg/kg 05/20/15 06:07 86-73-705/15/15 22:170.011 1

Indeno(1,2,3-cd)pyrene ND mg/kg 05/20/15 06:07 193-39-505/15/15 22:170.011 1

Naphthalene ND mg/kg 05/20/15 06:07 91-20-305/15/15 22:170.011 1

Phenanthrene ND mg/kg 05/20/15 06:07 85-01-805/15/15 22:170.011 1

Pyrene ND mg/kg 05/20/15 06:07 129-00-005/15/15 22:170.011 1

Total BaP Eq. MN 2006sh. ND=0 ND mg/kg 05/20/15 06:0705/15/15 22:170.011 1

Surrogates2-Fluorobiphenyl (S) 70 %. 05/20/15 06:07 321-60-805/15/15 22:1755-125 1

p-Terphenyl-d14 (S) 77 %. 05/20/15 06:07 1718-51-005/15/15 22:1730-150 1



without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 12:27 PM




(612)607-1700

Page 6 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53




Analytical Method: WI MOD DRO Preparation Method: WI MOD DROWIDRO GCS Silica Gel

WDRO C10-C28 45.3 mg/kg 05/19/15 10:20 T605/15/15 13:275.8 1

Surrogatesn-Triacontane (S) 312 %. 05/19/15 10:20 638-68-6 S505/15/15 13:2730-143 1

Analytical Method: WI MOD GRO Preparation Method: EPA 5030 Medium SoilWIGRO GCV

Gasoline Range Organics ND mg/kg 05/18/15 16:3905/15/15 14:5911.6 1

Surrogatesa,a,a-Trifluorotoluene (S) 116 %. 05/18/15 16:39 98-08-805/15/15 14:5980-150 1


Arsenic 1.2 mg/kg 05/20/15 00:55 7440-38-205/18/15 04:460.96 1

Barium 50.5 mg/kg 05/20/15 00:55 7440-39-305/18/15 04:460.48 1

Cadmium 0.22 mg/kg 05/20/15 00:55 7440-43-905/18/15 04:460.14 1

Chromium 6.5 mg/kg 05/20/15 00:55 7440-47-305/18/15 04:460.48 1

Lead 6.7 mg/kg 05/20/15 00:55 7439-92-105/18/15 04:460.48 1

Selenium ND mg/kg 05/20/15 00:55 7782-49-205/18/15 04:460.96 1

Silver ND mg/kg 05/20/15 00:55 7440-22-405/18/15 04:460.48 1


Mercury ND mg/kg 05/18/15 19:31 7439-97-605/17/15 15:180.020 1




Acenaphthene 0.058 mg/kg 05/20/15 06:28 83-32-905/15/15 22:170.011 1

Acenaphthylene 0.078 mg/kg 05/20/15 06:28 208-96-805/15/15 22:170.011 1

Anthracene 0.24 mg/kg 05/20/15 06:28 120-12-705/15/15 22:170.011 1

Benzo(a)anthracene 0.86 mg/kg 05/20/15 17:13 56-55-305/15/15 22:170.11 10

Benzo(a)pyrene 1.1 mg/kg 05/20/15 17:13 50-32-805/15/15 22:170.11 10

Benzo(b)fluoranthene 1.3 mg/kg 05/20/15 17:13 205-99-205/15/15 22:170.11 10

Benzo(g,h,i)perylene 0.62 mg/kg 05/20/15 17:13 191-24-205/15/15 22:170.11 10

Benzo(k)fluoranthene 0.53 mg/kg 05/20/15 17:13 207-08-905/15/15 22:170.11 10

Chrysene 0.88 mg/kg 05/20/15 17:13 218-01-905/15/15 22:170.11 10

Dibenz(a,h)anthracene 0.17 mg/kg 05/20/15 06:28 53-70-305/15/15 22:170.011 1

Fluoranthene 1.8 mg/kg 05/20/15 17:13 206-44-005/15/15 22:170.11 10

Fluorene 0.043 mg/kg 05/20/15 06:28 86-73-705/15/15 22:170.011 1

Indeno(1,2,3-cd)pyrene 0.56 mg/kg 05/20/15 17:13 193-39-505/15/15 22:170.11 10


Phenanthrene 0.58 mg/kg 05/20/15 17:13 85-01-805/15/15 22:170.11 10

Pyrene 1.6 mg/kg 05/20/15 17:13 129-00-005/15/15 22:170.11 10

Total BaP Eq. MN 2006sh. ND=0 1.5 mg/kg 05/20/15 17:1305/15/15 22:170.11 10


p-Terphenyl-d14 (S) 71 %. 05/20/15 06:28 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 7 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53




Analytical Method: EPA 8260B Preparation Method: EPA 5035/5030B8260B MSV 5030 Med Level

Acetone ND mg/kg 05/19/15 21:27 67-64-105/18/15 16:311.1 1

Allyl chloride ND mg/kg 05/19/15 21:27 107-05-105/18/15 16:310.23 1

Benzene ND mg/kg 05/19/15 21:27 71-43-205/18/15 16:310.023 1

Bromobenzene ND mg/kg 05/19/15 21:27 108-86-105/18/15 16:310.057 1

Bromochloromethane ND mg/kg 05/19/15 21:27 74-97-505/18/15 16:310.057 1

Bromodichloromethane ND mg/kg 05/19/15 21:27 75-27-405/18/15 16:310.057 1

Bromoform ND mg/kg 05/19/15 21:27 75-25-205/18/15 16:310.23 1

Bromomethane ND mg/kg 05/19/15 21:27 74-83-905/18/15 16:310.57 1

2-Butanone (MEK) ND mg/kg 05/19/15 21:27 78-93-305/18/15 16:310.29 1

n-Butylbenzene ND mg/kg 05/19/15 21:27 104-51-805/18/15 16:310.057 1

sec-Butylbenzene ND mg/kg 05/19/15 21:27 135-98-805/18/15 16:310.057 1

tert-Butylbenzene ND mg/kg 05/19/15 21:27 98-06-605/18/15 16:310.057 1

Carbon tetrachloride ND mg/kg 05/19/15 21:27 56-23-505/18/15 16:310.23 1

Chlorobenzene ND mg/kg 05/19/15 21:27 108-90-705/18/15 16:310.057 1

Chloroethane ND mg/kg 05/19/15 21:27 75-00-305/18/15 16:310.57 1

Chloroform ND mg/kg 05/19/15 21:27 67-66-305/18/15 16:310.057 1

Chloromethane ND mg/kg 05/19/15 21:27 74-87-305/18/15 16:310.23 1

2-Chlorotoluene ND mg/kg 05/19/15 21:27 95-49-805/18/15 16:310.057 1


1,2-Dibromo-3-chloropropane ND mg/kg 05/19/15 21:27 96-12-805/18/15 16:310.57 1

Dibromochloromethane ND mg/kg 05/19/15 21:27 124-48-105/18/15 16:310.057 1

1,2-Dibromoethane (EDB) ND mg/kg 05/19/15 21:27 106-93-405/18/15 16:310.057 1

Dibromomethane ND mg/kg 05/19/15 21:27 74-95-305/18/15 16:310.23 1

1,2-Dichlorobenzene ND mg/kg 05/19/15 21:27 95-50-105/18/15 16:310.057 1



Dichlorodifluoromethane ND mg/kg 05/19/15 21:27 75-71-805/18/15 16:310.23 1

1,1-Dichloroethane ND mg/kg 05/19/15 21:27 75-34-305/18/15 16:310.057 1


1,1-Dichloroethene ND mg/kg 05/19/15 21:27 75-35-405/18/15 16:310.057 1

cis-1,2-Dichloroethene ND mg/kg 05/19/15 21:27 156-59-205/18/15 16:310.057 1

trans-1,2-Dichloroethene ND mg/kg 05/19/15 21:27 156-60-5 L205/18/15 16:310.057 1

Dichlorofluoromethane ND mg/kg 05/19/15 21:27 75-43-405/18/15 16:310.57 1

1,2-Dichloropropane ND mg/kg 05/19/15 21:27 78-87-505/18/15 16:310.057 1



1,1-Dichloropropene ND mg/kg 05/19/15 21:27 563-58-605/18/15 16:310.057 1

cis-1,3-Dichloropropene ND mg/kg 05/19/15 21:27 10061-01-505/18/15 16:310.057 1

trans-1,3-Dichloropropene ND mg/kg 05/19/15 21:27 10061-02-605/18/15 16:310.057 1

Diethyl ether (Ethyl ether) ND mg/kg 05/19/15 21:27 60-29-705/18/15 16:310.23 1

Ethylbenzene ND mg/kg 05/19/15 21:27 100-41-405/18/15 16:310.057 1

Hexachloro-1,3-butadiene ND mg/kg 05/19/15 21:27 87-68-305/18/15 16:310.29 1

Isopropylbenzene (Cumene) ND mg/kg 05/19/15 21:27 98-82-805/18/15 16:310.057 1

p-Isopropyltoluene ND mg/kg 05/19/15 21:27 99-87-605/18/15 16:310.057 1

Methylene Chloride ND mg/kg 05/19/15 21:27 75-09-205/18/15 16:310.23 1

4-Methyl-2-pentanone (MIBK) ND mg/kg 05/19/15 21:27 108-10-105/18/15 16:310.29 1







(612)607-1700

Page 8 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





Methyl-tert-butyl ether ND mg/kg 05/19/15 21:27 1634-04-405/18/15 16:310.057 1


n-Propylbenzene ND mg/kg 05/19/15 21:27 103-65-105/18/15 16:310.057 1

Styrene ND mg/kg 05/19/15 21:27 100-42-505/18/15 16:310.057 1

1,1,1,2-Tetrachloroethane ND mg/kg 05/19/15 21:27 630-20-605/18/15 16:310.057 1


Tetrachloroethene ND mg/kg 05/19/15 21:27 127-18-405/18/15 16:310.057 1

Tetrahydrofuran ND mg/kg 05/19/15 21:27 109-99-905/18/15 16:312.3 1

Toluene ND mg/kg 05/19/15 21:27 108-88-305/18/15 16:310.057 1

1,2,3-Trichlorobenzene ND mg/kg 05/19/15 21:27 87-61-605/18/15 16:310.23 1


1,1,1-Trichloroethane ND mg/kg 05/19/15 21:27 71-55-605/18/15 16:310.057 1


Trichloroethene ND mg/kg 05/19/15 21:27 79-01-605/18/15 16:310.057 1

Trichlorofluoromethane ND mg/kg 05/19/15 21:27 75-69-405/18/15 16:310.23 1

1,2,3-Trichloropropane ND mg/kg 05/19/15 21:27 96-18-405/18/15 16:310.23 1

1,1,2-Trichlorotrifluoroethane ND mg/kg 05/19/15 21:27 76-13-1 L205/18/15 16:310.23 1

1,2,4-Trimethylbenzene ND mg/kg 05/19/15 21:27 95-63-605/18/15 16:310.057 1


Vinyl chloride ND mg/kg 05/19/15 21:27 75-01-405/18/15 16:310.023 1

Xylene (Total) ND mg/kg 05/19/15 21:27 1330-20-705/18/15 16:310.17 1

Surrogates1,2-Dichloroethane-d4 (S) 102 %. 05/19/15 21:27 17060-07-005/18/15 16:3155-150 1

Toluene-d8 (S) 101 %. 05/19/15 21:27 2037-26-505/18/15 16:3161-125 1

4-Bromofluorobenzene (S) 102 %. 05/19/15 21:27 460-00-405/18/15 16:3154-131 1







(612)607-1700

Page 9 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Sample: LHA-20/5-7 Lab ID: 10306235003 Collected: 05/12/15 00:00 Received: 05/13/15 14:34 Matrix: Solid




Arsenic 1.3 mg/kg 05/20/15 01:00 7440-38-205/18/15 04:461.0 1

Barium 45.5 mg/kg 05/20/15 01:00 7440-39-305/18/15 04:460.51 1

Cadmium 0.22 mg/kg 05/20/15 01:00 7440-43-905/18/15 04:460.15 1

Chromium 5.5 mg/kg 05/20/15 01:00 7440-47-305/18/15 04:460.51 1

Lead 5.2 mg/kg 05/20/15 01:00 7439-92-105/18/15 04:460.51 1

Selenium ND mg/kg 05/20/15 01:00 7782-49-205/18/15 04:461.0 1

Silver ND mg/kg 05/20/15 01:00 7440-22-405/18/15 04:460.51 1


Mercury ND mg/kg 05/18/15 19:33 7439-97-605/17/15 15:180.019 1












Chrysene 0.026 mg/kg 05/20/15 06:49 218-01-905/15/15 22:170.011 1



Fluorene ND mg/kg 05/20/15 06:49 86-73-705/15/15 22:170.011 1




Pyrene 0.041 mg/kg 05/20/15 06:49 129-00-005/15/15 22:170.011 1



p-Terphenyl-d14 (S) 76 %. 05/20/15 06:49 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 10 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





WDRO C10-C28 15.3 mg/kg 05/19/15 10:35 T605/15/15 13:275.2 1

Surrogatesn-Triacontane (S) 72 %. 05/19/15 10:35 638-68-605/15/15 13:2730-143 1





Arsenic 1.6 mg/kg 05/20/15 01:05 7440-38-205/18/15 04:461.0 1

Barium 57.5 mg/kg 05/20/15 01:05 7440-39-305/18/15 04:460.50 1

Cadmium 0.24 mg/kg 05/20/15 01:05 7440-43-905/18/15 04:460.15 1

Chromium 7.7 mg/kg 05/20/15 01:05 7440-47-305/18/15 04:460.50 1

Lead 13.6 mg/kg 05/20/15 01:05 7439-92-105/18/15 04:460.50 1

Selenium ND mg/kg 05/20/15 01:05 7782-49-205/18/15 04:461.0 1

Silver ND mg/kg 05/20/15 01:05 7440-22-405/18/15 04:460.50 1


Mercury ND mg/kg 05/18/15 19:36 7439-97-605/17/15 15:180.022 1






Anthracene 0.019 mg/kg 05/20/15 17:55 120-12-705/15/15 22:170.011 1






Chrysene 0.016 mg/kg 05/20/15 17:55 218-01-905/15/15 22:170.011 1



Fluorene ND mg/kg 05/20/15 17:55 86-73-705/15/15 22:170.011 1




Pyrene 0.017 mg/kg 05/20/15 17:55 129-00-005/15/15 22:170.011 1



p-Terphenyl-d14 (S) 72 %. 05/20/15 17:55 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 11 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





Acetone ND mg/kg 05/19/15 21:48 67-64-105/18/15 16:311.2 1


Benzene ND mg/kg 05/19/15 21:48 71-43-205/18/15 16:310.023 1









































p-Isopropyltoluene 0.061 mg/kg 05/19/15 21:48 99-87-605/18/15 16:310.058 1









(612)607-1700

Page 12 of 58

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ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53








Styrene ND mg/kg 05/19/15 21:48 100-42-505/18/15 16:310.058 1





Toluene ND mg/kg 05/19/15 21:48 108-88-305/18/15 16:310.058 1














Toluene-d8 (S) 101 %. 05/19/15 21:48 2037-26-505/18/15 16:3161-125 1








(612)607-1700

Page 13 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





WDRO C10-C28 ND mg/kg 05/19/15 10:4305/15/15 13:276.0 1






Arsenic ND mg/kg 05/20/15 01:10 7440-38-205/18/15 04:460.93 1

Barium 55.2 mg/kg 05/20/15 01:10 7440-39-305/18/15 04:460.47 1

Cadmium 0.26 mg/kg 05/20/15 01:10 7440-43-905/18/15 04:460.14 1

Chromium 6.8 mg/kg 05/20/15 01:10 7440-47-305/18/15 04:460.47 1

Lead 4.8 mg/kg 05/20/15 01:10 7439-92-105/18/15 04:460.47 1

Selenium ND mg/kg 05/20/15 01:10 7782-49-205/18/15 04:460.93 1

Silver ND mg/kg 05/20/15 01:10 7440-22-405/18/15 04:460.47 1


Mercury ND mg/kg 05/18/15 19:39 7439-97-605/17/15 15:180.020 1












Chrysene ND mg/kg 05/20/15 15:27 218-01-905/15/15 22:170.012 1



Fluorene ND mg/kg 05/20/15 15:27 86-73-705/15/15 22:170.012 1




Pyrene ND mg/kg 05/20/15 15:27 129-00-005/15/15 22:170.012 1



p-Terphenyl-d14 (S) 73 %. 05/20/15 15:27 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 14 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





Acetone ND mg/kg 05/19/15 19:26 67-64-105/18/15 16:311.2 1


Benzene ND mg/kg 05/19/15 19:26 71-43-205/18/15 16:310.023 1


















































(612)607-1700

Page 15 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53








Styrene ND mg/kg 05/19/15 19:26 100-42-505/18/15 16:310.058 1





Toluene ND mg/kg 05/19/15 19:26 108-88-305/18/15 16:310.058 1














Toluene-d8 (S) 98 %. 05/19/15 19:26 2037-26-505/18/15 16:3161-125 1








(612)607-1700

Page 16 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





WDRO C10-C28 ND mg/kg 05/19/15 10:5105/15/15 13:275.9 1






Arsenic 2.4 mg/kg 05/20/15 01:15 7440-38-205/18/15 04:460.81 1

Barium 46.9 mg/kg 05/20/15 01:15 7440-39-305/18/15 04:460.40 1

Cadmium 0.22 mg/kg 05/20/15 01:15 7440-43-905/18/15 04:460.12 1

Chromium 7.0 mg/kg 05/20/15 01:15 7440-47-305/18/15 04:460.40 1

Lead 3.3 mg/kg 05/20/15 01:15 7439-92-105/18/15 04:460.40 1

Selenium ND mg/kg 05/20/15 01:15 7782-49-205/18/15 04:460.81 1

Silver ND mg/kg 05/20/15 01:15 7440-22-405/18/15 04:460.40 1


Mercury ND mg/kg 05/18/15 19:41 7439-97-605/17/15 15:180.020 1












Chrysene ND mg/kg 05/20/15 15:48 218-01-905/15/15 22:170.011 1



Fluorene ND mg/kg 05/20/15 15:48 86-73-705/15/15 22:170.011 1




Pyrene ND mg/kg 05/20/15 15:48 129-00-005/15/15 22:170.011 1



p-Terphenyl-d14 (S) 73 %. 05/20/15 15:48 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 17 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





Acetone ND mg/kg 05/19/15 19:46 67-64-105/18/15 16:311.1 1


Benzene ND mg/kg 05/19/15 19:46 71-43-205/18/15 16:310.023 1


















































(612)607-1700

Page 18 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53








Styrene ND mg/kg 05/19/15 19:46 100-42-505/18/15 16:310.057 1





Toluene ND mg/kg 05/19/15 19:46 108-88-305/18/15 16:310.057 1














Toluene-d8 (S) 101 %. 05/19/15 19:46 2037-26-505/18/15 16:3161-125 1








(612)607-1700

Page 19 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Sample: LGP-23/17-20 Lab ID: 10306235007 Collected: 05/12/15 00:00 Received: 05/13/15 14:34 Matrix: Water



WDRO C10-C28 ND mg/L 05/17/15 17:4005/15/15 13:230.14 1

Surrogatesn-Triacontane (S) 95 %. 05/17/15 17:40 638-68-6 P405/15/15 13:2362-125 1

Analytical Method: WI MOD GROWIGRO GCV

Gasoline Range Organics ND ug/L 05/23/15 00:2750.0 1

Analytical Method: EPA 8260B8260B VOC

Acetone ND ug/L 05/15/15 19:16 67-64-120.0 1

Allyl chloride ND ug/L 05/15/15 19:16 107-05-14.0 1

Benzene ND ug/L 05/15/15 19:16 71-43-21.0 1

Bromobenzene ND ug/L 05/15/15 19:16 108-86-11.0 1

Bromochloromethane ND ug/L 05/15/15 19:16 74-97-51.0 1

Bromodichloromethane ND ug/L 05/15/15 19:16 75-27-41.0 1

Bromoform ND ug/L 05/15/15 19:16 75-25-24.0 1

Bromomethane ND ug/L 05/15/15 19:16 74-83-94.0 1

2-Butanone (MEK) ND ug/L 05/15/15 19:16 78-93-35.0 1

n-Butylbenzene ND ug/L 05/15/15 19:16 104-51-81.0 1

sec-Butylbenzene ND ug/L 05/15/15 19:16 135-98-81.0 1

tert-Butylbenzene ND ug/L 05/15/15 19:16 98-06-61.0 1

Carbon tetrachloride ND ug/L 05/15/15 19:16 56-23-51.0 1

Chlorobenzene ND ug/L 05/15/15 19:16 108-90-71.0 1

Chloroethane ND ug/L 05/15/15 19:16 75-00-31.0 1

Chloroform ND ug/L 05/15/15 19:16 67-66-31.0 1

Chloromethane ND ug/L 05/15/15 19:16 74-87-34.0 1

2-Chlorotoluene ND ug/L 05/15/15 19:16 95-49-81.0 1


1,2-Dibromo-3-chloropropane ND ug/L 05/15/15 19:16 96-12-84.0 1

Dibromochloromethane ND ug/L 05/15/15 19:16 124-48-11.0 1

1,2-Dibromoethane (EDB) ND ug/L 05/15/15 19:16 106-93-41.0 1

Dibromomethane ND ug/L 05/15/15 19:16 74-95-34.0 1

1,2-Dichlorobenzene ND ug/L 05/15/15 19:16 95-50-11.0 1



Dichlorodifluoromethane ND ug/L 05/15/15 19:16 75-71-81.0 1

1,1-Dichloroethane ND ug/L 05/15/15 19:16 75-34-31.0 1


1,1-Dichloroethene ND ug/L 05/15/15 19:16 75-35-41.0 1

cis-1,2-Dichloroethene ND ug/L 05/15/15 19:16 156-59-21.0 1

trans-1,2-Dichloroethene ND ug/L 05/15/15 19:16 156-60-51.0 1

Dichlorofluoromethane ND ug/L 05/15/15 19:16 75-43-41.0 1

1,2-Dichloropropane ND ug/L 05/15/15 19:16 78-87-54.0 1



1,1-Dichloropropene ND ug/L 05/15/15 19:16 563-58-61.0 1

cis-1,3-Dichloropropene ND ug/L 05/15/15 19:16 10061-01-54.0 1







(612)607-1700

Page 20 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53




trans-1,3-Dichloropropene ND ug/L 05/15/15 19:16 10061-02-64.0 1

Diethyl ether (Ethyl ether) ND ug/L 05/15/15 19:16 60-29-74.0 1

Ethylbenzene ND ug/L 05/15/15 19:16 100-41-41.0 1

Hexachloro-1,3-butadiene ND ug/L 05/15/15 19:16 87-68-31.0 1

Isopropylbenzene (Cumene) ND ug/L 05/15/15 19:16 98-82-81.0 1

p-Isopropyltoluene ND ug/L 05/15/15 19:16 99-87-61.0 1

Methylene Chloride ND ug/L 05/15/15 19:16 75-09-24.0 1

4-Methyl-2-pentanone (MIBK) ND ug/L 05/15/15 19:16 108-10-15.0 1

Methyl-tert-butyl ether ND ug/L 05/15/15 19:16 1634-04-41.0 1

Naphthalene ND ug/L 05/15/15 19:16 91-20-34.0 1

n-Propylbenzene ND ug/L 05/15/15 19:16 103-65-11.0 1

Styrene ND ug/L 05/15/15 19:16 100-42-51.0 1

1,1,1,2-Tetrachloroethane ND ug/L 05/15/15 19:16 630-20-61.0 1


Tetrachloroethene ND ug/L 05/15/15 19:16 127-18-41.0 1

Tetrahydrofuran ND ug/L 05/15/15 19:16 109-99-910.0 1

Toluene ND ug/L 05/15/15 19:16 108-88-31.0 1

1,2,3-Trichlorobenzene ND ug/L 05/15/15 19:16 87-61-61.0 1


1,1,1-Trichloroethane ND ug/L 05/15/15 19:16 71-55-61.0 1


Trichloroethene ND ug/L 05/15/15 19:16 79-01-60.40 1

Trichlorofluoromethane ND ug/L 05/15/15 19:16 75-69-41.0 1

1,2,3-Trichloropropane ND ug/L 05/15/15 19:16 96-18-44.0 1

1,1,2-Trichlorotrifluoroethane ND ug/L 05/15/15 19:16 76-13-11.0 1

1,2,4-Trimethylbenzene ND ug/L 05/15/15 19:16 95-63-61.0 1


Vinyl chloride ND ug/L 05/15/15 19:16 75-01-40.40 1

Xylene (Total) ND ug/L 05/15/15 19:16 1330-20-73.0 1

Surrogates1,2-Dichloroethane-d4 (S) 94 %. 05/15/15 19:16 17060-07-075-125 1

Toluene-d8 (S) 100 %. 05/15/15 19:16 2037-26-575-125 1

4-Bromofluorobenzene (S) 98 %. 05/15/15 19:16 460-00-475-125 1







(612)607-1700

Page 21 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





Arsenic 1.7 mg/kg 05/20/15 01:20 7440-38-205/18/15 04:461.1 1

Barium 67.0 mg/kg 05/20/15 01:20 7440-39-305/18/15 04:460.54 1

Cadmium 0.33 mg/kg 05/20/15 01:20 7440-43-905/18/15 04:460.16 1

Chromium 7.5 mg/kg 05/20/15 01:20 7440-47-305/18/15 04:460.54 1

Lead 19.8 mg/kg 05/20/15 01:20 7439-92-105/18/15 04:460.54 1

Selenium ND mg/kg 05/20/15 01:20 7782-49-205/18/15 04:461.1 1

Silver ND mg/kg 05/20/15 01:20 7440-22-405/18/15 04:460.54 1


Mercury ND mg/kg 05/18/15 19:43 7439-97-605/17/15 15:180.022 1






Anthracene 0.081 mg/kg 05/20/15 16:09 120-12-705/15/15 22:170.058 5






Chrysene 0.39 mg/kg 05/20/15 16:09 218-01-905/15/15 22:170.058 5



Fluorene ND mg/kg 05/20/15 16:09 86-73-705/15/15 22:170.058 5




Pyrene 0.67 mg/kg 05/20/15 16:09 129-00-005/15/15 22:170.058 5


Surrogates2-Fluorobiphenyl (S) 66 %. 05/20/15 16:09 321-60-8 D405/15/15 22:1755-125 5

p-Terphenyl-d14 (S) 73 %. 05/20/15 16:09 1718-51-005/15/15 22:1730-150 5







(612)607-1700

Page 22 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





WDRO C10-C28 9.6 mg/kg 05/19/15 10:28 T605/15/15 13:275.5 1






Arsenic 1.4 mg/kg 05/20/15 01:25 7440-38-205/18/15 04:460.88 1

Barium 48.7 mg/kg 05/20/15 01:25 7440-39-305/18/15 04:460.44 1

Cadmium 0.22 mg/kg 05/20/15 01:25 7440-43-905/18/15 04:460.13 1

Chromium 7.1 mg/kg 05/20/15 01:25 7440-47-305/18/15 04:460.44 1

Lead 12.9 mg/kg 05/20/15 01:25 7439-92-105/18/15 04:460.44 1

Selenium ND mg/kg 05/20/15 01:25 7782-49-205/18/15 04:460.88 1

Silver ND mg/kg 05/20/15 01:25 7440-22-405/18/15 04:460.44 1


Mercury 0.019 mg/kg 05/18/15 19:45 7439-97-605/17/15 15:180.018 1






Anthracene 0.022 mg/kg 05/20/15 18:16 120-12-705/15/15 22:170.011 1






Chrysene 0.12 mg/kg 05/20/15 18:16 218-01-905/15/15 22:170.011 1



Fluorene ND mg/kg 05/20/15 18:16 86-73-705/15/15 22:170.011 1




Pyrene 0.17 mg/kg 05/20/15 18:16 129-00-005/15/15 22:170.011 1



p-Terphenyl-d14 (S) 65 %. 05/20/15 18:16 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 23 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53





Acetone ND mg/kg 05/19/15 22:08 67-64-105/18/15 16:311.1 1


Benzene ND mg/kg 05/19/15 22:08 71-43-205/18/15 16:310.022 1


















































(612)607-1700

Page 24 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53








Styrene ND mg/kg 05/19/15 22:08 100-42-505/18/15 16:310.054 1





Toluene ND mg/kg 05/19/15 22:08 108-88-305/18/15 16:310.054 1














Toluene-d8 (S) 102 %. 05/19/15 22:08 2037-26-505/18/15 16:3161-125 1








(612)607-1700

Page 25 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53




WDRO C10-C28 ND mg/L 05/17/15 17:3205/15/15 13:230.13 1



Gasoline Range Organics ND ug/L 05/23/15 00:5350.0 1


Acetone ND ug/L 05/15/15 19:30 67-64-120.0 1


Benzene ND ug/L 05/15/15 19:30 71-43-21.0 1




Bromoform ND ug/L 05/15/15 19:30 75-25-24.0 1






































(612)607-1700

Page 26 of 58

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53















Styrene ND ug/L 05/15/15 19:30 100-42-51.0 1





Toluene ND ug/L 05/15/15 19:30 108-88-31.0 1














Toluene-d8 (S) 98 %. 05/15/15 19:30 2037-26-575-125 1








(612)607-1700

Page 27 of 58

#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

GCV/13744

EPA 5030 Medium Soil

WI MOD GRO

WIGRO Solid GCV

Associated Lab Samples: 10306235002, 10306235004, 10306235005, 10306235006, 10306235009

Parameter Units

Blank

Result

Reporting

Limit Qualifiers

METHOD BLANK: 1966977


Matrix: Solid

Analyzed

Gasoline Range Organics mg/kg ND 10.0 05/18/15 11:05

a,a,a-Trifluorotoluene (S) %. 117 80-150 05/18/15 11:05

Parameter Units

LCS

Result

% Rec

Limits Qualifiers% RecConc.

1966978LABORATORY CONTROL SAMPLE & LCSD:

LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1966979

Gasoline Range Organics mg/kg 44.950 90 80-1208944.7 0 20

a,a,a-Trifluorotoluene (S) %. 129 80-150127

Parameter Units

MS

Result

% Rec


1966980MATRIX SPIKE SAMPLE:

MSSpike

Result

10305711001

Gasoline Range Organics mg/kg 47.056.6 83 80-120ND


Parameter Units

Dup

Result

Max

RPD QualifiersRPDResult

10305711002

1966981SAMPLE DUPLICATE:

Gasoline Range Organics mg/kg ND 20ND

a,a,a-Trifluorotoluene (S) %. 113 1115







(612)607-1700

Page 28 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


GCV/14422

WI MOD GRO

WI MOD GRO

WIGRO GCV Water

Associated Lab Samples: 10306235007, 10306235010

Parameter Units

Blank

Result

Reporting

Limit Qualifiers


Associated Lab Samples:

Matrix: Water

Analyzed

Gasoline Range Organics ug/L ND 50.0 05/22/15 21:27

Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1163078

Gasoline Range Organics ug/L 195200 97 80-120102205 5 20







(612)607-1700

Page 29 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MERP/13552

EPA 7471B

EPA 7471B

7471B Mercury Solids

Associated Lab Samples: 10306235001, 10306235002, 10306235003, 10306235004, 10306235005, 10306235006, 10306235008,10306235009

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Mercury mg/kg ND 0.019 05/18/15 19:07

Parameter Units

LCS

Result

% Rec


1966050LABORATORY CONTROL SAMPLE:

LCSSpike

Mercury mg/kg 0.49.48 101 80-120

Parameter Units

MS

Result

% Rec

Limits Qual% RecConc.

1966051MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpike

Result

10306204001

1966052

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Mercury mg/kg .55 98 75-125100 10 20.48ND 0.54 0.49







(612)607-1700

Page 30 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54373

EPA 3050

EPA 6010C

6010C Solids


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Arsenic mg/kg ND 0.89 05/19/15 23:48

Barium mg/kg ND 0.45 05/19/15 23:48

Cadmium mg/kg ND 0.13 05/19/15 23:48

Chromium mg/kg ND 0.45 05/19/15 23:48

Lead mg/kg ND 0.45 05/19/15 23:48

Selenium mg/kg ND 0.89 05/19/15 23:48

Silver mg/kg ND 0.45 05/19/15 23:48

Parameter Units

LCS

Result

% Rec



LCSSpike

Arsenic mg/kg 45.248.5 93 80-120

Barium mg/kg 46.948.5 97 80-120

Cadmium mg/kg 44.448.5 91 80-120

Chromium mg/kg 46.748.5 96 80-120

Lead mg/kg 44.748.5 92 80-120

Selenium mg/kg 44.048.5 91 80-120

Silver mg/kg 22.324.3 92 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

10306204001

1965107

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Arsenic mg/kg 45 97 75-125100 1 2044.21.9 45.5 46.2

Barium mg/kg 45 104 75-125122 9 2044.230.1 77.0 84.3

Cadmium mg/kg 45 95 75-12596 0 2044.20.16 42.7 42.5

Chromium mg/kg 45 97 75-12599 0 2044.25.6 49.3 49.2

Lead mg/kg 45 88 75-12594 4 2044.23.6 43.4 45.0

Selenium mg/kg 45 91 75-12595 3 2044.2ND 40.8 42.2

Silver mg/kg 22.5 96 75-12597 1 2022.2ND 21.7 21.4







(612)607-1700

Page 31 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54526

ASTM D2974

ASTM D2974

Dry Weight/Percent Moisture

Associated Lab Samples: 10306235001, 10306235002, 10306235003, 10306235004

Parameter Units

Dup

Result

Max


10305246003


Percent Moisture % 0.93 0 300.93

Parameter Units

Dup

Result

Max


10306235003









(612)607-1700

Page 32 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54527

ASTM D2974

ASTM D2974



Parameter Units

Dup

Result

Max


10305312001



Parameter Units

Dup

Result

Max


10306609002









(612)607-1700

Page 33 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MSV/31467

EPA 5035/5030B

EPA 8260B

8260B MSV 5030 Med Level


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

1,1,1,2-Tetrachloroethane mg/kg ND 0.050 05/19/15 17:45

1,1,1-Trichloroethane mg/kg ND 0.050 05/19/15 17:45



1,1,2-Trichlorotrifluoroethane mg/kg ND 0.20 05/19/15 17:45

1,1-Dichloroethane mg/kg ND 0.050 05/19/15 17:45

1,1-Dichloroethene mg/kg ND 0.050 05/19/15 17:45

1,1-Dichloropropene mg/kg ND 0.050 05/19/15 17:45

1,2,3-Trichlorobenzene mg/kg ND 0.20 05/19/15 17:45

1,2,3-Trichloropropane mg/kg ND 0.20 05/19/15 17:45


1,2,4-Trimethylbenzene mg/kg ND 0.050 05/19/15 17:45

1,2-Dibromo-3-chloropropane mg/kg ND 0.50 05/19/15 17:45

1,2-Dibromoethane (EDB) mg/kg ND 0.050 05/19/15 17:45

1,2-Dichlorobenzene mg/kg ND 0.050 05/19/15 17:45


1,2-Dichloropropane mg/kg ND 0.050 05/19/15 17:45






2-Butanone (MEK) mg/kg ND 0.25 05/19/15 17:45

2-Chlorotoluene mg/kg ND 0.050 05/19/15 17:45


4-Methyl-2-pentanone (MIBK) mg/kg ND 0.25 05/19/15 17:45

Acetone mg/kg ND 1.0 05/19/15 17:45

Allyl chloride mg/kg ND 0.20 05/19/15 17:45

Benzene mg/kg ND 0.020 05/19/15 17:45

Bromobenzene mg/kg ND 0.050 05/19/15 17:45

Bromochloromethane mg/kg ND 0.050 05/19/15 17:45

Bromodichloromethane mg/kg ND 0.050 05/19/15 17:45

Bromoform mg/kg ND 0.20 05/19/15 17:45

Bromomethane mg/kg ND 0.50 05/19/15 17:45

Carbon tetrachloride mg/kg ND 0.20 05/19/15 17:45

Chlorobenzene mg/kg ND 0.050 05/19/15 17:45

Chloroethane mg/kg ND 0.50 05/19/15 17:45

Chloroform mg/kg ND 0.050 05/19/15 17:45

Chloromethane mg/kg ND 0.20 05/19/15 17:45

cis-1,2-Dichloroethene mg/kg ND 0.050 05/19/15 17:45

cis-1,3-Dichloropropene mg/kg ND 0.050 05/19/15 17:45







(612)607-1700

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#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Dibromochloromethane mg/kg ND 0.050 05/19/15 17:45

Dibromomethane mg/kg ND 0.20 05/19/15 17:45

Dichlorodifluoromethane mg/kg ND 0.20 05/19/15 17:45

Dichlorofluoromethane mg/kg ND 0.50 05/19/15 17:45

Diethyl ether (Ethyl ether) mg/kg ND 0.20 05/19/15 17:45

Ethylbenzene mg/kg ND 0.050 05/19/15 17:45

Hexachloro-1,3-butadiene mg/kg ND 0.25 05/19/15 17:45

Isopropylbenzene (Cumene) mg/kg ND 0.050 05/19/15 17:45

Methyl-tert-butyl ether mg/kg ND 0.050 05/19/15 17:45

Methylene Chloride mg/kg ND 0.20 05/19/15 17:45

n-Butylbenzene mg/kg ND 0.050 05/19/15 17:45

n-Propylbenzene mg/kg ND 0.050 05/19/15 17:45

Naphthalene mg/kg ND 0.20 05/19/15 17:45

p-Isopropyltoluene mg/kg ND 0.050 05/19/15 17:45

sec-Butylbenzene mg/kg ND 0.050 05/19/15 17:45

Styrene mg/kg ND 0.050 05/19/15 17:45

tert-Butylbenzene mg/kg ND 0.050 05/19/15 17:45

Tetrachloroethene mg/kg ND 0.050 05/19/15 17:45

Tetrahydrofuran mg/kg ND 2.0 05/19/15 17:45

Toluene mg/kg ND 0.050 05/19/15 17:45

trans-1,2-Dichloroethene mg/kg ND 0.050 05/19/15 17:45

trans-1,3-Dichloropropene mg/kg ND 0.050 05/19/15 17:45

Trichloroethene mg/kg ND 0.050 05/19/15 17:45

Trichlorofluoromethane mg/kg ND 0.20 05/19/15 17:45

Vinyl chloride mg/kg ND 0.020 05/19/15 17:45

Xylene (Total) mg/kg ND 0.15 05/19/15 17:45

1,2-Dichloroethane-d4 (S) %. 101 55-150 05/19/15 17:45

4-Bromofluorobenzene (S) %. 107 54-131 05/19/15 17:45

Toluene-d8 (S) %. 105 61-125 05/19/15 17:45

Parameter Units

LCS

Result

% Rec



LCSSpike

1,1,1,2-Tetrachloroethane mg/kg 0.961 96 75-125

1,1,1-Trichloroethane mg/kg 0.851 85 66-125



1,1,2-Trichlorotrifluoroethane mg/kg 0.53 L01 53 55-125

1,1-Dichloroethane mg/kg 0.841 84 67-125

1,1-Dichloroethene mg/kg 0.711 71 62-125

1,1-Dichloropropene mg/kg 0.691 69 65-125

1,2,3-Trichlorobenzene mg/kg 0.921 92 58-132

1,2,3-Trichloropropane mg/kg 1.01 101 71-125








(612)607-1700

Page 35 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

LCS

Result

% Rec



LCSSpike

1,2,4-Trimethylbenzene mg/kg 0.881 88 74-125

1,2-Dibromo-3-chloropropane mg/kg 2.52.5 100 55-142

1,2-Dibromoethane (EDB) mg/kg 0.891 89 75-125

1,2-Dichlorobenzene mg/kg 0.901 90 75-125


1,2-Dichloropropane mg/kg 0.931 93 74-125






2-Butanone (MEK) mg/kg 3.65 71 39-136

2-Chlorotoluene mg/kg 0.881 88 73-125


4-Methyl-2-pentanone (MIBK) mg/kg 4.55 90 55-132

Acetone mg/kg 5.85 116 55-131

Allyl chloride mg/kg 0.711 71 53-125

Benzene mg/kg 0.861 86 69-125

Bromobenzene mg/kg 0.941 94 75-125

Bromochloromethane mg/kg 0.781 78 75-125

Bromodichloromethane mg/kg 0.971 97 75-125

Bromoform mg/kg 0.951 95 71-125

Bromomethane mg/kg 0.821 82 42-150

Carbon tetrachloride mg/kg 0.751 75 62-125

Chlorobenzene mg/kg 0.931 93 75-125

Chloroethane mg/kg 0.961 96 41-150

Chloroform mg/kg 0.961 96 72-125

Chloromethane mg/kg 1.01 103 50-125

cis-1,2-Dichloroethene mg/kg 0.841 84 73-125

cis-1,3-Dichloropropene mg/kg 1.01 100 74-125

Dibromochloromethane mg/kg 1.01 105 75-125

Dibromomethane mg/kg 0.831 83 75-125

Dichlorodifluoromethane mg/kg 0.591 59 30-125

Dichlorofluoromethane mg/kg 0.941 94 30-150

Diethyl ether (Ethyl ether) mg/kg 0.701 70 58-125

Ethylbenzene mg/kg 0.911 91 72-125

Hexachloro-1,3-butadiene mg/kg 0.671 67 59-138

Isopropylbenzene (Cumene) mg/kg 0.811 81 72-125

Methyl-tert-butyl ether mg/kg 0.901 90 72-125

Methylene Chloride mg/kg 0.781 78 71-125

n-Butylbenzene mg/kg 0.881 88 65-125

n-Propylbenzene mg/kg 0.951 95 71-125

Naphthalene mg/kg 0.881 88 55-139

p-Isopropyltoluene mg/kg 0.851 85 69-125

sec-Butylbenzene mg/kg 0.831 83 68-125

Styrene mg/kg 0.901 90 75-125

tert-Butylbenzene mg/kg 0.921 92 70-125







(612)607-1700

Page 36 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

LCS

Result

% Rec



LCSSpike

Tetrachloroethene mg/kg 0.751 75 69-125

Tetrahydrofuran mg/kg 12.010 120 62-129

Toluene mg/kg 0.891 89 72-125

trans-1,2-Dichloroethene mg/kg 0.67 L01 67 68-125

trans-1,3-Dichloropropene mg/kg 0.971 97 74-125

Trichloroethene mg/kg 0.911 91 72-125

Trichlorofluoromethane mg/kg 0.851 85 30-150

Vinyl chloride mg/kg 0.971 97 53-125

Xylene (Total) mg/kg 2.73 88 74-125

1,2-Dichloroethane-d4 (S) %. 96 55-150

4-Bromofluorobenzene (S) %. 104 54-131

Toluene-d8 (S) %. 100 61-125

Parameter Units

MS

Result

% Rec



MSSpike

Result

10306235005

1,1,1,2-Tetrachloroethane mg/kg 1.11.2 97 62-150ND

1,1,1-Trichloroethane mg/kg 1.01.2 86 58-150ND



1,1,2-Trichlorotrifluoroethane mg/kg 1.01.2 87 45-150ND

1,1-Dichloroethane mg/kg 1.01.2 88 56-150ND

1,1-Dichloroethene mg/kg 0.771.2 66 48-150ND

1,1-Dichloropropene mg/kg 0.781.2 67 58-150ND

1,2,3-Trichlorobenzene mg/kg 1.21.2 107 55-150ND

1,2,3-Trichloropropane mg/kg 1.21.2 103 57-148ND


1,2,4-Trimethylbenzene mg/kg 1.11.2 96 64-150ND

1,2-Dibromo-3-chloropropane mg/kg 3.32.9 113 40-150ND

1,2-Dibromoethane (EDB) mg/kg 1.21.2 99 62-147ND

1,2-Dichlorobenzene mg/kg 1.21.2 102 73-133ND


1,2-Dichloropropane mg/kg 1.11.2 93 69-127ND






2-Butanone (MEK) mg/kg 4.75.9 81 49-145ND

2-Chlorotoluene mg/kg 1.11.2 98 68-129ND


4-Methyl-2-pentanone (MIBK) mg/kg 5.65.9 96 60-150ND

Acetone mg/kg 5.55.9 94 65-135ND

Allyl chloride mg/kg 0.811.2 69 55-126ND

Benzene mg/kg 0.991.2 85 63-126ND







(612)607-1700

Page 37 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

MS

Result

% Rec



MSSpike

Result

10306235005

Bromobenzene mg/kg 1.11.2 97 68-133ND

Bromochloromethane mg/kg 0.921.2 79 66-130ND

Bromodichloromethane mg/kg 1.21.2 99 68-129ND

Bromoform mg/kg 1.21.2 100 63-135ND

Bromomethane mg/kg 1.41.2 120 30-150ND

Carbon tetrachloride mg/kg 0.891.2 76 56-140ND

Chlorobenzene mg/kg 1.11.2 93 69-130ND

Chloroethane mg/kg 1.21.2 105 46-150ND

Chloroform mg/kg 1.21.2 99 70-127ND

Chloromethane mg/kg 1.11.2 95 51-125ND

cis-1,2-Dichloroethene mg/kg 0.991.2 84 68-125ND

cis-1,3-Dichloropropene mg/kg 1.11.2 93 67-126ND

Dibromochloromethane mg/kg 1.21.2 103 66-135ND

Dibromomethane mg/kg 1.11.2 95 68-132ND

Dichlorodifluoromethane mg/kg 1.21.2 103 30-138ND

Dichlorofluoromethane mg/kg 1.11.2 92 30-150ND

Diethyl ether (Ethyl ether) mg/kg 0.881.2 76 56-135ND

Ethylbenzene mg/kg 1.11.2 91 69-126ND

Hexachloro-1,3-butadiene mg/kg 1.21.2 102 50-150ND

Isopropylbenzene (Cumene) mg/kg 1.01.2 89 65-135ND

Methyl-tert-butyl ether mg/kg 1.11.2 96 66-129ND

Methylene Chloride mg/kg 0.871.2 74 64-125ND

n-Butylbenzene mg/kg 1.21.2 103 62-141ND

n-Propylbenzene mg/kg 1.21.2 105 65-135ND

Naphthalene mg/kg 1.21.2 106 62-150ND

p-Isopropyltoluene mg/kg 1.21.2 104 62-139ND

sec-Butylbenzene mg/kg 1.11.2 95 64-137ND

Styrene mg/kg 1.01.2 88 70-132ND

tert-Butylbenzene mg/kg 1.21.2 102 65-136ND

Tetrachloroethene mg/kg 0.901.2 77 61-142ND

Tetrahydrofuran mg/kg 11.411.7 98 68-138ND

Toluene mg/kg 1.01.2 88 66-128ND

trans-1,2-Dichloroethene mg/kg 0.831.2 71 63-129ND

trans-1,3-Dichloropropene mg/kg 1.21.2 100 67-132ND

Trichloroethene mg/kg 1.01.2 88 52-150ND

Trichlorofluoromethane mg/kg 1.21.2 105 39-150ND

Vinyl chloride mg/kg 1.11.2 93 50-125ND

Xylene (Total) mg/kg 3.13.5 90 70-130ND



Toluene-d8 (S) %. 104 61-125







(612)607-1700

Page 38 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

Dup

Result

Max


10306235006


1,1,1,2-Tetrachloroethane mg/kg ND 30ND

1,1,1-Trichloroethane mg/kg ND 30ND



1,1,2-Trichlorotrifluoroethane mg/kg ND 30ND

1,1-Dichloroethane mg/kg ND 30ND

1,1-Dichloroethene mg/kg ND 30ND

1,1-Dichloropropene mg/kg ND 30ND

1,2,3-Trichlorobenzene mg/kg ND 30ND

1,2,3-Trichloropropane mg/kg ND 30ND


1,2,4-Trimethylbenzene mg/kg ND 30ND

1,2-Dibromo-3-chloropropane mg/kg ND 30ND

1,2-Dibromoethane (EDB) mg/kg ND 30ND

1,2-Dichlorobenzene mg/kg ND 30ND


1,2-Dichloropropane mg/kg ND 30ND






2-Butanone (MEK) mg/kg ND 30ND

2-Chlorotoluene mg/kg ND 30ND


4-Methyl-2-pentanone (MIBK) mg/kg ND 30ND

Acetone mg/kg ND 30ND

Allyl chloride mg/kg ND 30ND

Benzene mg/kg ND 30ND

Bromobenzene mg/kg ND 30ND

Bromochloromethane mg/kg ND 30ND

Bromodichloromethane mg/kg ND 30ND

Bromoform mg/kg ND 30ND

Bromomethane mg/kg ND 30ND

Carbon tetrachloride mg/kg ND 30ND

Chlorobenzene mg/kg ND 30ND

Chloroethane mg/kg ND 30ND

Chloroform mg/kg .018J 30ND

Chloromethane mg/kg ND 30ND

cis-1,2-Dichloroethene mg/kg ND 30ND

cis-1,3-Dichloropropene mg/kg ND 30ND

Dibromochloromethane mg/kg ND 30ND

Dibromomethane mg/kg ND 30ND

Dichlorodifluoromethane mg/kg ND 30ND

Dichlorofluoromethane mg/kg ND 30ND

Diethyl ether (Ethyl ether) mg/kg ND 30ND

Ethylbenzene mg/kg ND 30ND







(612)607-1700

Page 39 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

Dup

Result

Max


10306235006


Hexachloro-1,3-butadiene mg/kg ND 30ND

Isopropylbenzene (Cumene) mg/kg ND 30ND

Methyl-tert-butyl ether mg/kg ND 30ND

Methylene Chloride mg/kg ND 30ND

n-Butylbenzene mg/kg ND 30ND

n-Propylbenzene mg/kg ND 30ND

Naphthalene mg/kg ND 30ND

p-Isopropyltoluene mg/kg ND 30ND

sec-Butylbenzene mg/kg ND 30ND

Styrene mg/kg ND 30ND

tert-Butylbenzene mg/kg ND 30ND

Tetrachloroethene mg/kg ND 30ND

Tetrahydrofuran mg/kg ND 30ND

Toluene mg/kg ND 30ND

trans-1,2-Dichloroethene mg/kg ND 30ND

trans-1,3-Dichloropropene mg/kg ND 30ND

Trichloroethene mg/kg ND 30ND

Trichlorofluoromethane mg/kg ND 30ND

Vinyl chloride mg/kg ND 30ND

Xylene (Total) mg/kg ND 30ND

1,2-Dichloroethane-d4 (S) %. 103 3105

4-Bromofluorobenzene (S) %. 103 2104

Toluene-d8 (S) %. 99 3101







(612)607-1700

Page 40 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MSV/31440

EPA 8260B

EPA 8260B

8260B MSV 465 W


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/15/15 13:30

1,1,1-Trichloroethane ug/L ND 1.0 05/15/15 13:30



1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 05/15/15 13:30

1,1-Dichloroethane ug/L ND 1.0 05/15/15 13:30

1,1-Dichloroethene ug/L ND 1.0 05/15/15 13:30

1,1-Dichloropropene ug/L ND 1.0 05/15/15 13:30

1,2,3-Trichlorobenzene ug/L ND 1.0 05/15/15 13:30

1,2,3-Trichloropropane ug/L ND 4.0 05/15/15 13:30


1,2,4-Trimethylbenzene ug/L ND 1.0 05/15/15 13:30

1,2-Dibromo-3-chloropropane ug/L ND 4.0 05/15/15 13:30

1,2-Dibromoethane (EDB) ug/L ND 1.0 05/15/15 13:30

1,2-Dichlorobenzene ug/L ND 1.0 05/15/15 13:30


1,2-Dichloropropane ug/L ND 4.0 05/15/15 13:30






2-Butanone (MEK) ug/L ND 5.0 05/15/15 13:30

2-Chlorotoluene ug/L ND 1.0 05/15/15 13:30


4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 05/15/15 13:30

Acetone ug/L ND 20.0 05/15/15 13:30

Allyl chloride ug/L ND 4.0 05/15/15 13:30

Benzene ug/L ND 1.0 05/15/15 13:30

Bromobenzene ug/L ND 1.0 05/15/15 13:30

Bromochloromethane ug/L ND 1.0 05/15/15 13:30

Bromodichloromethane ug/L ND 1.0 05/15/15 13:30

Bromoform ug/L ND 4.0 05/15/15 13:30

Bromomethane ug/L ND 4.0 05/15/15 13:30

Carbon tetrachloride ug/L ND 1.0 05/15/15 13:30

Chlorobenzene ug/L ND 1.0 05/15/15 13:30

Chloroethane ug/L ND 1.0 05/15/15 13:30

Chloroform ug/L ND 1.0 05/15/15 13:30

Chloromethane ug/L ND 4.0 05/15/15 13:30

cis-1,2-Dichloroethene ug/L ND 1.0 05/15/15 13:30

cis-1,3-Dichloropropene ug/L ND 4.0 05/15/15 13:30







(612)607-1700

Page 41 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Dibromochloromethane ug/L ND 1.0 05/15/15 13:30

Dibromomethane ug/L ND 4.0 05/15/15 13:30

Dichlorodifluoromethane ug/L ND 1.0 05/15/15 13:30

Dichlorofluoromethane ug/L ND 1.0 05/15/15 13:30

Diethyl ether (Ethyl ether) ug/L ND 4.0 05/15/15 13:30

Ethylbenzene ug/L ND 1.0 05/15/15 13:30

Hexachloro-1,3-butadiene ug/L ND 1.0 05/15/15 13:30

Isopropylbenzene (Cumene) ug/L ND 1.0 05/15/15 13:30

Methyl-tert-butyl ether ug/L ND 1.0 05/15/15 13:30

Methylene Chloride ug/L ND 4.0 05/15/15 13:30

n-Butylbenzene ug/L ND 1.0 05/15/15 13:30

n-Propylbenzene ug/L ND 1.0 05/15/15 13:30

Naphthalene ug/L ND 4.0 05/15/15 13:30

p-Isopropyltoluene ug/L ND 1.0 05/15/15 13:30

sec-Butylbenzene ug/L ND 1.0 05/15/15 13:30

Styrene ug/L ND 1.0 05/15/15 13:30

tert-Butylbenzene ug/L ND 1.0 05/15/15 13:30

Tetrachloroethene ug/L ND 1.0 05/15/15 13:30

Tetrahydrofuran ug/L ND 10.0 05/15/15 13:30

Toluene ug/L ND 1.0 05/15/15 13:30

trans-1,2-Dichloroethene ug/L ND 1.0 05/15/15 13:30

trans-1,3-Dichloropropene ug/L ND 4.0 05/15/15 13:30

Trichloroethene ug/L ND 0.40 05/15/15 13:30

Trichlorofluoromethane ug/L ND 1.0 05/15/15 13:30

Vinyl chloride ug/L ND 0.40 05/15/15 13:30

Xylene (Total) ug/L ND 3.0 05/15/15 13:30



Toluene-d8 (S) %. 101 75-125 05/15/15 13:30

Parameter Units

LCS

Result

% Rec



LCSSpike

1,1,1,2-Tetrachloroethane ug/L 19.620 98 75-125

1,1,1-Trichloroethane ug/L 19.220 96 75-125



1,1,2-Trichlorotrifluoroethane ug/L 17.620 88 60-135

1,1-Dichloroethane ug/L 18.920 95 69-125

1,1-Dichloroethene ug/L 19.220 96 68-125

1,1-Dichloropropene ug/L 20.020 100 74-125

1,2,3-Trichlorobenzene ug/L 18.920 94 69-136

1,2,3-Trichloropropane ug/L 20.420 102 75-125








(612)607-1700

Page 42 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

LCS

Result

% Rec



LCSSpike

1,2,4-Trimethylbenzene ug/L 19.220 96 75-125

1,2-Dibromo-3-chloropropane ug/L 47.550 95 65-145

1,2-Dibromoethane (EDB) ug/L 20.920 104 75-125

1,2-Dichlorobenzene ug/L 18.920 94 75-125


1,2-Dichloropropane ug/L 18.920 95 75-125






2-Butanone (MEK) ug/L 96.8100 97 63-130

2-Chlorotoluene ug/L 19.420 97 72-125


4-Methyl-2-pentanone (MIBK) ug/L 105100 105 71-126

Acetone ug/L 106100 106 69-131

Allyl chloride ug/L 19.520 98 67-125

Benzene ug/L 19.520 97 71-125

Bromobenzene ug/L 19.820 99 75-125

Bromochloromethane ug/L 19.120 96 75-125

Bromodichloromethane ug/L 19.120 95 75-125

Bromoform ug/L 17.520 87 70-125

Bromomethane ug/L 20.520 102 30-150

Carbon tetrachloride ug/L 18.020 90 75-126

Chlorobenzene ug/L 19.820 99 75-125

Chloroethane ug/L 18.420 92 65-134

Chloroform ug/L 17.920 90 75-125

Chloromethane ug/L 21.620 108 39-150

cis-1,2-Dichloroethene ug/L 19.120 95 72-125

cis-1,3-Dichloropropene ug/L 19.120 95 75-125

Dibromochloromethane ug/L 18.220 91 75-125

Dibromomethane ug/L 19.820 99 75-125

Dichlorodifluoromethane ug/L 16.320 81 50-134

Dichlorofluoromethane ug/L 20.020 100 69-125

Diethyl ether (Ethyl ether) ug/L 19.020 95 72-125

Ethylbenzene ug/L 19.320 97 75-125

Hexachloro-1,3-butadiene ug/L 18.720 94 70-138

Isopropylbenzene (Cumene) ug/L 19.920 100 75-125

Methyl-tert-butyl ether ug/L 19.720 98 73-125

Methylene Chloride ug/L 18.520 93 73-125

n-Butylbenzene ug/L 20.020 100 72-133

n-Propylbenzene ug/L 19.920 99 72-126

Naphthalene ug/L 19.320 97 70-127

p-Isopropyltoluene ug/L 20.220 101 72-132

sec-Butylbenzene ug/L 20.120 101 73-132

Styrene ug/L 20.820 104 75-125

tert-Butylbenzene ug/L 19.820 99 73-128







(612)607-1700

Page 43 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

LCS

Result

% Rec



LCSSpike

Tetrachloroethene ug/L 21.220 106 74-125

Tetrahydrofuran ug/L 209200 104 62-133

Toluene ug/L 20.220 101 74-125

trans-1,2-Dichloroethene ug/L 19.820 99 69-125

trans-1,3-Dichloropropene ug/L 20.120 100 75-125

Trichloroethene ug/L 20.520 103 75-125

Trichlorofluoromethane ug/L 19.320 96 74-127

Vinyl chloride ug/L 20.220 101 66-132

Xylene (Total) ug/L 59.660 99 75-125



Toluene-d8 (S) %. 101 75-125

Parameter Units

MS

Result

% Rec



MSSpike

Result

10306158005

1,1,1,2-Tetrachloroethane ug/L 19.920 100 70-138ND

1,1,1-Trichloroethane ug/L 20.720 104 55-150ND

1,1,2,2-Tetrachloroethane ug/L 20.020 100 64-140ND

1,1,2-Trichloroethane ug/L 20.120 101 67-137ND

1,1,2-Trichlorotrifluoroethane ug/L 22.520 113 51-150ND

1,1-Dichloroethane ug/L 20.120 101 49-150ND

1,1-Dichloroethene ug/L 21.720 108 40-150ND

1,1-Dichloropropene ug/L 22.120 110 50-150ND

1,2,3-Trichlorobenzene ug/L 18.320 91 59-148ND

1,2,3-Trichloropropane ug/L 19.720 99 65-141ND

1,2,4-Trichlorobenzene ug/L 18.920 94 61-140ND

1,2,4-Trimethylbenzene ug/L 19.820 99 58-141ND

1,2-Dibromo-3-chloropropane ug/L 43.050 86 53-150ND

1,2-Dibromoethane (EDB) ug/L 20.620 103 65-137ND

1,2-Dichlorobenzene ug/L 19.520 97 66-133ND

1,2-Dichloroethane ug/L 18.920 94 54-138ND

1,2-Dichloropropane ug/L 19.520 98 62-138ND

1,3,5-Trimethylbenzene ug/L 20.320 102 58-140ND





2-Butanone (MEK) ug/L 91.3100 91 51-147ND

2-Chlorotoluene ug/L 20.120 100 58-147ND

4-Chlorotoluene ug/L 19.820 99 64-138ND

4-Methyl-2-pentanone (MIBK) ug/L 97.5100 97 59-143ND

Acetone ug/L 116100 116 63-147ND

Allyl chloride ug/L 20.620 103 45-150ND

Benzene ug/L 20.520 102 53-139ND







(612)607-1700

Page 44 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

MS

Result

% Rec



MSSpike

Result

10306158005

Bromobenzene ug/L 20.220 101 66-136ND

Bromochloromethane ug/L 20.620 103 64-136ND

Bromodichloromethane ug/L 19.520 98 66-138ND

Bromoform ug/L 16.820 84 59-136ND

Bromomethane ug/L 20.320 102 30-150ND

Carbon tetrachloride ug/L 20.020 100 56-150ND

Chlorobenzene ug/L 20.520 102 65-133ND

Chloroethane ug/L 17.620 88 48-150ND

Chloroform ug/L 18.120 90 57-145ND

Chloromethane ug/L 22.920 114 30-150ND

cis-1,2-Dichloroethene ug/L 20.120 100 49-150ND

cis-1,3-Dichloropropene ug/L 19.320 96 64-130ND

Dibromochloromethane ug/L 18.620 93 68-138ND

Dibromomethane ug/L 20.120 100 67-134ND

Dichlorodifluoromethane ug/L 18.720 94 45-150ND

Dichlorofluoromethane ug/L 19.420 97 54-150ND

Diethyl ether (Ethyl ether) ug/L 19.720 99 50-145ND

Ethylbenzene ug/L 20.320 102 55-139ND

Hexachloro-1,3-butadiene ug/L 20.220 101 49-150ND

Isopropylbenzene (Cumene) ug/L 20.820 104 64-142ND

Methyl-tert-butyl ether ug/L 20.420 102 62-129ND

Methylene Chloride ug/L 19.720 98 57-132ND

n-Butylbenzene ug/L 20.520 103 55-150ND

n-Propylbenzene ug/L 20.820 104 59-142ND

Naphthalene ug/L 18.920 95 51-150ND

p-Isopropyltoluene ug/L 21.120 106 60-149ND

sec-Butylbenzene ug/L 21.120 105 60-150ND

Styrene ug/L 21.520 108 68-134ND

tert-Butylbenzene ug/L 20.820 104 62-146ND

Tetrachloroethene ug/L 22.720 113 50-150ND

Tetrahydrofuran ug/L 243200 122 59-145ND

Toluene ug/L 20.720 103 52-148ND

trans-1,2-Dichloroethene ug/L 22.220 111 45-150ND

trans-1,3-Dichloropropene ug/L 19.320 97 68-132ND

Trichloroethene ug/L 21.820 109 52-150ND

Trichlorofluoromethane ug/L 20.820 104 55-150ND

Vinyl chloride ug/L 21.320 106 43-150ND

Xylene (Total) ug/L 62.560 104 54-144ND



Toluene-d8 (S) %. 101 75-125







(612)607-1700

Page 45 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

Dup

Result

Max


10306158006


1,1,1,2-Tetrachloroethane ug/L ND 30ND

1,1,1-Trichloroethane ug/L ND 30ND

1,1,2,2-Tetrachloroethane ug/L ND 30ND

1,1,2-Trichloroethane ug/L ND 30ND

1,1,2-Trichlorotrifluoroethane ug/L ND 30ND

1,1-Dichloroethane ug/L ND 30ND

1,1-Dichloroethene ug/L ND 30ND

1,1-Dichloropropene ug/L ND 30ND

1,2,3-Trichlorobenzene ug/L .85J 30ND

1,2,3-Trichloropropane ug/L ND 30ND

1,2,4-Trichlorobenzene ug/L .68J 30ND

1,2,4-Trimethylbenzene ug/L ND 30ND

1,2-Dibromo-3-chloropropane ug/L ND 30ND

1,2-Dibromoethane (EDB) ug/L ND 30ND

1,2-Dichlorobenzene ug/L .27J 30ND

1,2-Dichloroethane ug/L ND 30ND

1,2-Dichloropropane ug/L ND 30ND

1,3,5-Trimethylbenzene ug/L ND 30ND

1,3-Dichlorobenzene ug/L ND 30ND


1,4-Dichlorobenzene ug/L ND 30ND


2-Butanone (MEK) ug/L ND 30ND

2-Chlorotoluene ug/L ND 30ND

4-Chlorotoluene ug/L .22J 30ND

4-Methyl-2-pentanone (MIBK) ug/L ND 30ND

Acetone ug/L ND 30ND

Allyl chloride ug/L ND 30ND

Benzene ug/L ND 30ND

Bromobenzene ug/L ND 30ND

Bromochloromethane ug/L ND 30ND

Bromodichloromethane ug/L ND 30ND

Bromoform ug/L ND 30ND

Bromomethane ug/L ND 30ND

Carbon tetrachloride ug/L ND 30ND

Chlorobenzene ug/L ND 30ND

Chloroethane ug/L ND 30ND

Chloroform ug/L ND 30ND

Chloromethane ug/L ND 30ND

cis-1,2-Dichloroethene ug/L ND 30ND

cis-1,3-Dichloropropene ug/L ND 30ND

Dibromochloromethane ug/L ND 30ND

Dibromomethane ug/L ND 30ND

Dichlorodifluoromethane ug/L ND 30ND

Dichlorofluoromethane ug/L ND 30ND

Diethyl ether (Ethyl ether) ug/L ND 30ND

Ethylbenzene ug/L ND 30ND







(612)607-1700

Page 46 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

Dup

Result

Max


10306158006


Hexachloro-1,3-butadiene ug/L .85J 30ND

Isopropylbenzene (Cumene) ug/L ND 30ND

Methyl-tert-butyl ether ug/L ND 30ND

Methylene Chloride ug/L ND 30ND

n-Butylbenzene ug/L .59J 30ND

n-Propylbenzene ug/L ND 30ND

Naphthalene ug/L ND 30ND

p-Isopropyltoluene ug/L ND 30ND

sec-Butylbenzene ug/L ND 30ND

Styrene ug/L ND 30ND

tert-Butylbenzene ug/L ND 30ND

Tetrachloroethene ug/L ND 30ND

Tetrahydrofuran ug/L ND 30ND

Toluene ug/L ND 30ND

trans-1,2-Dichloroethene ug/L ND 30ND

trans-1,3-Dichloropropene ug/L ND 30ND

Trichloroethene ug/L ND 30ND

Trichlorofluoromethane ug/L ND 30ND

Vinyl chloride ug/L ND 30ND

Xylene (Total) ug/L ND 30ND



Toluene-d8 (S) %. 100 2101







(612)607-1700

Page 47 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/29195

EPA 3550

EPA 8270D by SIM

8270D Solid PAH by SIM MSSV


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Acenaphthene mg/kg ND 0.010 05/20/15 02:38

Acenaphthylene mg/kg ND 0.010 05/20/15 02:38

Anthracene mg/kg ND 0.010 05/20/15 02:38

Benzo(a)anthracene mg/kg ND 0.010 05/20/15 02:38

Benzo(a)pyrene mg/kg ND 0.010 05/20/15 02:38

Benzo(b)fluoranthene mg/kg ND 0.010 05/20/15 02:38

Benzo(g,h,i)perylene mg/kg ND 0.010 05/20/15 02:38

Benzo(k)fluoranthene mg/kg ND 0.010 05/20/15 02:38

Chrysene mg/kg ND 0.010 05/20/15 02:38

Dibenz(a,h)anthracene mg/kg ND 0.010 05/20/15 02:38

Fluoranthene mg/kg ND 0.010 05/20/15 02:38

Fluorene mg/kg ND 0.010 05/20/15 02:38

Indeno(1,2,3-cd)pyrene mg/kg ND 0.010 05/20/15 02:38


Phenanthrene mg/kg ND 0.010 05/20/15 02:38

Pyrene mg/kg ND 0.010 05/20/15 02:38

2-Fluorobiphenyl (S) %. 78 55-125 05/20/15 02:38

p-Terphenyl-d14 (S) %. 96 30-150 05/20/15 02:38

Parameter Units

LCS

Result

% Rec



LCSSpike

Acenaphthene mg/kg 0.025.033 76 53-125

Acenaphthylene mg/kg 0.026.033 77 53-125

Anthracene mg/kg 0.029.033 86 61-125

Benzo(a)anthracene mg/kg 0.029.033 88 62-125

Benzo(a)pyrene mg/kg 0.032.033 97 64-125

Benzo(b)fluoranthene mg/kg 0.030.033 91 66-125

Benzo(g,h,i)perylene mg/kg 0.031.033 93 59-125

Benzo(k)fluoranthene mg/kg 0.034.033 101 61-125

Chrysene mg/kg 0.029.033 87 63-125

Dibenz(a,h)anthracene mg/kg 0.032.033 97 59-125

Fluoranthene mg/kg 0.030.033 89 64-125

Fluorene mg/kg 0.027.033 82 57-125

Indeno(1,2,3-cd)pyrene mg/kg 0.031.033 93 58-125

Naphthalene mg/kg 0.024.033 72 52-125

Phenanthrene mg/kg 0.025.033 74 60-125

Pyrene mg/kg 0.031.033 93 63-125







(612)607-1700

Page 48 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Parameter Units

LCS

Result

% Rec



LCSSpike

2-Fluorobiphenyl (S) %. 79 55-125

p-Terphenyl-d14 (S) %. 95 30-150

Parameter Units

MS

Result

% Rec



MSSpike

Result

10306204001

1967336

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Acenaphthene mg/kg .036 71 39-12563 12 30.036ND 0.026 0.023

Acenaphthylene mg/kg .036 68 30-15059 14 30.036ND 0.025 0.022

Anthracene mg/kg .036 80 30-15077 4 30.036ND 0.029 0.028

Benzo(a)anthracene mg/kg .036 86 30-15099 15 30.036ND 0.031 0.036

Benzo(a)pyrene mg/kg .036 99 30-150111 11 30.036ND 0.036 0.041

Benzo(b)fluoranthene mg/kg .036 95 30-150126 28 30.036ND 0.035 0.046

Benzo(g,h,i)perylene mg/kg .036 97 30-15099 2 30.036ND 0.036 0.036

Benzo(k)fluoranthene mg/kg .036 98 30-15095 3 30.036ND 0.036 0.035

Chrysene mg/kg .036 85 30-150100 17 30.036ND 0.031 0.037

Dibenz(a,h)anthracene mg/kg .036 91 30-15089 2 30.036ND 0.033 0.032

Fluoranthene mg/kg R1.036 90 30-150132 38 30.036ND 0.033 0.048

Fluorene mg/kg .036 78 30-14670 11 30.036ND 0.028 0.025

Indeno(1,2,3-cd)pyrene mg/kg .036 92 30-15095 4 30.036ND 0.034 0.035

Naphthalene mg/kg .036 64 30-13157 12 30.036ND 0.023 0.021

Phenanthrene mg/kg .036 72 30-15092 24 30.036ND 0.026 0.034

Pyrene mg/kg .036 97 30-150131 30 30.036ND 0.035 0.048


p-Terphenyl-d14 (S) %. 83 30-15084







(612)607-1700

Page 49 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/29194

WI MOD DRO

WI MOD DRO

WIDRO Solid GCV


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

WDRO C10-C28 mg/kg ND 10.0 05/19/15 09:57

n-Triacontane (S) %. 91 30-143 05/19/15 09:57

Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1967251

WDRO C10-C28 mg/kg 74.780 93 64-1259374.5 0 20

n-Triacontane (S) %. 96 30-14393







(612)607-1700

Page 50 of 58

#=QC#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/29188

WI MOD DRO

WI MOD DRO

WIDRO GCS w/Cleanup


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

WDRO C10-C28 mg/L ND 0.10 05/17/15 17:17

n-Triacontane (S) %. 72 62-125 05/17/15 17:17

Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1967126

WDRO C10-C28 mg/L 2.02 98 54-125931.9 5 20

n-Triacontane (S) %. 104 62-12597







(612)607-1700

Page 51 of 58

#=QL#

QUALIFIERS

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.

ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - Green BayPASI-G

Pace Analytical Services - MinneapolisPASI-M

ANALYTE QUALIFIERS

Sample was diluted due to the presence of high levels of target analytes.D4

Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0

Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results may be biased low.L2

Sample field preservation does not meet EPA or method recommendations for this analysis.P4

RPD value was outside control limits.R1

Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5

High boiling point hydrocarbons are present in the sample.T6







(612)607-1700

Page 52 of 58

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53

Lab ID Sample ID QC Batch Method QC Batch Analytical Method

Analytical

Batch

10306235002 OEXT/29194 GCSV/15720LGP-19/4-6 WI MOD DRO WI MOD DRO

10306235004 OEXT/29194 GCSV/15720LHA-21/2-4 WI MOD DRO WI MOD DRO






10306235002 GCV/13744 GCV/13747LGP-19/4-6 EPA 5030 Medium Soil WI MOD GRO

10306235004 GCV/13744 GCV/13747LHA-21/2-4 EPA 5030 Medium Soil WI MOD GRO




10306235007 GCV/14422LGP-23/17-20 WI MOD GRO

10306235010 GCV/14422LGP-25/15-20 WI MOD GRO

10306235001 MPRP/54373 ICP/23806LGP-18/3-5 EPA 3050 EPA 6010C


10306235003 MPRP/54373 ICP/23806LHA-20/5-7 EPA 3050 EPA 6010C

10306235004 MPRP/54373 ICP/23806LHA-21/2-4 EPA 3050 EPA 6010C





10306235001 MERP/13552 MERC/15762LGP-18/3-5 EPA 7471B EPA 7471B


10306235003 MERP/13552 MERC/15762LHA-20/5-7 EPA 7471B EPA 7471B

10306235004 MERP/13552 MERC/15762LHA-21/2-4 EPA 7471B EPA 7471B





10306235001 MPRP/54526LGP-18/3-5 ASTM D2974

10306235002 MPRP/54526LGP-19/4-6 ASTM D2974

10306235003 MPRP/54526LHA-20/5-7 ASTM D2974

10306235004 MPRP/54526LHA-21/2-4 ASTM D2974

10306235005 MPRP/54527LGP-22/4-6 ASTM D2974

10306235006 MPRP/54527LGP-23/6-8 ASTM D2974

10306235008 MPRP/54527LGP-24/3-5 ASTM D2974

10306235009 MPRP/54527LGP-25/1-3 ASTM D2974

10306235001 OEXT/29195 MSSV/12351LGP-18/3-5 EPA 3550 EPA 8270D by SIM


10306235003 OEXT/29195 MSSV/12351LHA-20/5-7 EPA 3550 EPA 8270D by SIM

10306235004 OEXT/29195 MSSV/12351LHA-21/2-4 EPA 3550 EPA 8270D by SIM










(612)607-1700

Page 53 of 58

#=CR#


Pace Project No.:

Project:

10306235

HC-15-002 CSAH-53


Analytical

Batch


10306235002 MSV/31467 MSV/31499LGP-19/4-6 EPA 5035/5030B EPA 8260B

10306235004 MSV/31467 MSV/31499LHA-21/2-4 EPA 5035/5030B EPA 8260B




10306235007 MSV/31440LGP-23/17-20 EPA 8260B

10306235010 MSV/31440LGP-25/15-20 EPA 8260B







(612)607-1700

Page 54 of 58

#=CL#

May 21, 2015



10306204

Project:

Pace Project No.:

RE:


HC-15-002 CHAH-53

Dear Mr. Mullin:



Sincerely,

Carol Davy for

[email protected]

Project Manager

Jessica Patterson

Enclosures







(612)607-1700

Page 1 of 18

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53









(612)607-1700

Page 2 of 18

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


10306204001 LGP-26/6-8 Solid 05/13/15 00:00 05/13/15 14:35

10306204002 LGP-27/1-3 Solid 05/13/15 00:00 05/13/15 14:35

10306204003 LGP-28/2-4 Solid 05/13/15 00:00 05/13/15 14:35

10306204004 LGP-29/2-4 Solid 05/13/15 00:00 05/13/15 14:35

10306204005 LGP-30/1-3 Solid 05/13/15 00:00 05/13/15 14:35







(612)607-1700

Page 3 of 18

#=SA#


Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


Analytes

ReportedAnalysts

10306204001 LGP-26/6-8 EPA 6010C 7IP

EPA 7471B 1LMW

ASTM D2974 1JDL

EPA 8270D by SIM 19AS1

10306204002 LGP-27/1-3 EPA 6010C 7IP

EPA 7471B 1LMW

ASTM D2974 1JDL


10306204003 LGP-28/2-4 EPA 6010C 7IP

EPA 7471B 1LMW

ASTM D2974 1JDL


10306204004 LGP-29/2-4 EPA 6010C 7IP

EPA 7471B 1LMW

ASTM D2974 1JDL


10306204005 LGP-30/1-3 EPA 6010C 7IP

EPA 7471B 1LMW

ASTM D2974 1JDL








(612)607-1700

Page 4 of 18

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53





Arsenic 1.9 mg/kg 05/19/15 23:56 7440-38-205/18/15 04:460.90 1

Barium 30.1 mg/kg 05/19/15 23:56 7440-39-305/18/15 04:460.45 1

Cadmium 0.16 mg/kg 05/19/15 23:56 7440-43-905/18/15 04:460.13 1

Chromium 5.6 mg/kg 05/19/15 23:56 7440-47-305/18/15 04:460.45 1

Lead 3.6 mg/kg 05/19/15 23:56 7439-92-105/18/15 04:460.45 1

Selenium ND mg/kg 05/19/15 23:56 7782-49-205/18/15 04:460.90 1

Silver ND mg/kg 05/19/15 23:56 7440-22-405/18/15 04:460.45 1


Mercury ND mg/kg 05/18/15 19:11 7439-97-605/17/15 15:180.021 1












Chrysene ND mg/kg 05/20/15 03:19 218-01-905/15/15 22:170.011 1


Fluoranthene ND mg/kg 05/20/15 03:19 206-44-0 R105/15/15 22:170.011 1

Fluorene ND mg/kg 05/20/15 03:19 86-73-705/15/15 22:170.011 1




Pyrene ND mg/kg 05/20/15 03:19 129-00-005/15/15 22:170.011 1



p-Terphenyl-d14 (S) 83 %. 05/20/15 03:19 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 5 of 18

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53





Arsenic 3.0 mg/kg 05/20/15 00:22 7440-38-205/18/15 04:460.94 1

Barium 65.9 mg/kg 05/20/15 00:22 7440-39-305/18/15 04:460.47 1

Cadmium 0.23 mg/kg 05/20/15 00:22 7440-43-905/18/15 04:460.14 1

Chromium 9.4 mg/kg 05/20/15 00:22 7440-47-305/18/15 04:460.47 1

Lead 6.7 mg/kg 05/20/15 00:22 7439-92-105/18/15 04:460.47 1

Selenium ND mg/kg 05/20/15 00:22 7782-49-205/18/15 04:460.94 1

Silver ND mg/kg 05/20/15 00:22 7440-22-405/18/15 04:460.47 1


Mercury ND mg/kg 05/18/15 19:17 7439-97-605/17/15 15:180.022 1












Chrysene 0.065 mg/kg 05/20/15 04:22 218-01-905/15/15 22:170.012 1



Fluorene ND mg/kg 05/20/15 04:22 86-73-705/15/15 22:170.012 1




Pyrene 0.12 mg/kg 05/20/15 04:22 129-00-005/15/15 22:170.012 1



p-Terphenyl-d14 (S) 80 %. 05/20/15 04:22 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 6 of 18

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53





Arsenic 2.1 mg/kg 05/20/15 00:27 7440-38-205/18/15 04:461.0 1

Barium 74.8 mg/kg 05/20/15 00:27 7440-39-305/18/15 04:460.52 1

Cadmium 0.22 mg/kg 05/20/15 00:27 7440-43-905/18/15 04:460.16 1

Chromium 12.0 mg/kg 05/20/15 00:27 7440-47-305/18/15 04:460.52 1

Lead 9.4 mg/kg 05/20/15 00:27 7439-92-105/18/15 04:460.52 1

Selenium ND mg/kg 05/20/15 00:27 7782-49-205/18/15 04:461.0 1

Silver ND mg/kg 05/20/15 00:27 7440-22-405/18/15 04:460.52 1


Mercury 0.022 mg/kg 05/18/15 19:19 7439-97-605/17/15 15:180.019 1












Chrysene 0.020 mg/kg 05/20/15 17:34 218-01-905/15/15 22:170.011 1



Fluorene ND mg/kg 05/20/15 17:34 86-73-705/15/15 22:170.011 1




Pyrene 0.027 mg/kg 05/20/15 17:34 129-00-005/15/15 22:170.011 1



p-Terphenyl-d14 (S) 86 %. 05/20/15 17:34 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 7 of 18

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53





Arsenic 2.3 mg/kg 05/20/15 11:00 7440-38-205/18/15 04:462.2 2

Barium 85.9 mg/kg 05/20/15 11:00 7440-39-305/18/15 04:461.1 2

Cadmium ND mg/kg 05/20/15 11:00 7440-43-905/18/15 04:460.33 2

Chromium 13.3 mg/kg 05/20/15 11:00 7440-47-305/18/15 04:461.1 2

Lead 8.8 mg/kg 05/20/15 11:00 7439-92-105/18/15 04:461.1 2

Selenium ND mg/kg 05/20/15 11:00 7782-49-205/18/15 04:462.2 2

Silver ND mg/kg 05/20/15 11:00 7440-22-405/18/15 04:461.1 2


Mercury 0.023 mg/kg 05/18/15 19:21 7439-97-605/17/15 15:180.023 1












Chrysene ND mg/kg 05/20/15 05:04 218-01-905/15/15 22:170.012 1



Fluorene ND mg/kg 05/20/15 05:04 86-73-705/15/15 22:170.012 1




Pyrene ND mg/kg 05/20/15 05:04 129-00-005/15/15 22:170.012 1



p-Terphenyl-d14 (S) 88 %. 05/20/15 05:04 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 8 of 18

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53





Arsenic ND mg/kg 05/20/15 00:45 7440-38-205/18/15 04:460.85 1

Barium 40.0 mg/kg 05/20/15 00:45 7440-39-305/18/15 04:460.43 1

Cadmium ND mg/kg 05/20/15 00:45 7440-43-905/18/15 04:460.13 1

Chromium 6.0 mg/kg 05/20/15 00:45 7440-47-305/18/15 04:460.43 1

Lead 4.4 mg/kg 05/20/15 00:45 7439-92-105/18/15 04:460.43 1

Selenium ND mg/kg 05/20/15 00:45 7782-49-205/18/15 04:460.85 1

Silver ND mg/kg 05/20/15 00:45 7440-22-405/18/15 04:460.43 1


Mercury ND mg/kg 05/18/15 19:27 7439-97-605/17/15 15:180.022 1












Chrysene ND mg/kg 05/20/15 05:25 218-01-905/15/15 22:170.011 1



Fluorene ND mg/kg 05/20/15 05:25 86-73-705/15/15 22:170.011 1




Pyrene ND mg/kg 05/20/15 05:25 129-00-005/15/15 22:170.011 1



p-Terphenyl-d14 (S) 82 %. 05/20/15 05:25 1718-51-005/15/15 22:1730-150 1







(612)607-1700

Page 9 of 18

#=QC#


Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MERP/13552

EPA 7471B

EPA 7471B



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Mercury mg/kg ND 0.019 05/18/15 19:07

Parameter Units

LCS

Result

% Rec



LCSSpike

Mercury mg/kg 0.49.48 101 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

10306204001

1966052

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Mercury mg/kg .55 98 75-125100 10 20.48ND 0.54 0.49







(612)607-1700

Page 10 of 18

#=QC#


Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54373

EPA 3050

EPA 6010C

6010C Solids


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Arsenic mg/kg ND 0.89 05/19/15 23:48

Barium mg/kg ND 0.45 05/19/15 23:48

Cadmium mg/kg ND 0.13 05/19/15 23:48

Chromium mg/kg ND 0.45 05/19/15 23:48

Lead mg/kg ND 0.45 05/19/15 23:48

Selenium mg/kg ND 0.89 05/19/15 23:48

Silver mg/kg ND 0.45 05/19/15 23:48

Parameter Units

LCS

Result

% Rec



LCSSpike

Arsenic mg/kg 45.248.5 93 80-120

Barium mg/kg 46.948.5 97 80-120

Cadmium mg/kg 44.448.5 91 80-120

Chromium mg/kg 46.748.5 96 80-120

Lead mg/kg 44.748.5 92 80-120

Selenium mg/kg 44.048.5 91 80-120

Silver mg/kg 22.324.3 92 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

10306204001

1965107

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Arsenic mg/kg 45 97 75-125100 1 2044.21.9 45.5 46.2

Barium mg/kg 45 104 75-125122 9 2044.230.1 77.0 84.3

Cadmium mg/kg 45 95 75-12596 0 2044.20.16 42.7 42.5

Chromium mg/kg 45 97 75-12599 0 2044.25.6 49.3 49.2

Lead mg/kg 45 88 75-12594 4 2044.23.6 43.4 45.0

Selenium mg/kg 45 91 75-12595 3 2044.2ND 40.8 42.2

Silver mg/kg 22.5 96 75-12597 1 2022.2ND 21.7 21.4







(612)607-1700

Page 11 of 18

#=QC#


Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54526

ASTM D2974

ASTM D2974



Parameter Units

Dup

Result

Max


10305246003



Parameter Units

Dup

Result

Max


10306235003









(612)607-1700

Page 12 of 18

#=QC#


Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


QC Batch:

QC Batch Method:

Analysis Method:


OEXT/29195

EPA 3550

EPA 8270D by SIM



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed









Chrysene mg/kg ND 0.010 05/20/15 02:38



Fluorene mg/kg ND 0.010 05/20/15 02:38




Pyrene mg/kg ND 0.010 05/20/15 02:38


p-Terphenyl-d14 (S) %. 96 30-150 05/20/15 02:38

Parameter Units

LCS

Result

% Rec



LCSSpike



Anthracene mg/kg 0.029.033 86 61-125






Chrysene mg/kg 0.029.033 87 63-125



Fluorene mg/kg 0.027.033 82 57-125




Pyrene mg/kg 0.031.033 93 63-125


p-Terphenyl-d14 (S) %. 95 30-150







(612)607-1700

Page 13 of 18

#=QC#


Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


Parameter Units

MS

Result

% Rec



MSSpike

Result

10306204001

1967336

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.









Chrysene mg/kg .036 85 30-150100 17 30.036ND 0.031 0.037


Fluoranthene mg/kg R1.036 90 30-150132 38 30.036ND 0.033 0.048

Fluorene mg/kg .036 78 30-14670 11 30.036ND 0.028 0.025




Pyrene mg/kg .036 97 30-150131 30 30.036ND 0.035 0.048


p-Terphenyl-d14 (S) %. 83 30-15084







(612)607-1700

Page 14 of 18

#=QL#

QUALIFIERS

Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53

DEFINITIONS







S - Surrogate













ANALYTE QUALIFIERS

RPD value was outside control limits.R1







(612)607-1700

Page 15 of 18

#=CR#


Pace Project No.:

Project:

10306204

HC-15-002 CHAH-53


Analytical

Batch











10306204001 MPRP/54526LGP-26/6-8 ASTM D2974

10306204002 MPRP/54526LGP-27/1-3 ASTM D2974

10306204003 MPRP/54526LGP-28/2-4 ASTM D2974

10306204004 MPRP/54526LGP-29/2-4 ASTM D2974

10306204005 MPRP/54526LGP-30/1-3 ASTM D2974












(612)607-1700

Page 16 of 18

#=CL#

July 01, 2015



10307337

Project:

Pace Project No.:

RE:


HC-15-002 CSAH-53 REV

Dear Mr. Mullin:



Sincerely,

Chris Bremer for

[email protected]

Project Manager

Jessica Patterson

Enclosures







(612)607-1700

Page 1 of 73

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

10307337










(612)607-1700

Page 2 of 73

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10307337



10307337001 LPG-31/1-3 Solid 05/19/15 00:00 05/21/15 08:35

10307337002 LPG-32/2-4 Solid 05/19/15 00:00 05/21/15 08:35

10307337003 LPG-33/2-4 Solid 05/19/15 00:00 05/21/15 08:35

10307337004 LPG-34/2-4 Solid 05/19/15 00:00 05/21/15 08:35

10307337005 LPG-35/6-8 Solid 05/19/15 00:00 05/21/15 08:35

10307337006 LPG-36/10-12 Solid 05/19/15 00:00 05/21/15 08:35

10307337007 LPG-36/18-20 Solid 05/19/15 00:00 05/21/15 08:35

10307337008 LPG-37/2-4 Solid 05/19/15 00:00 05/21/15 08:35

10307337009 LPG-38/4-6 Solid 05/19/15 00:00 05/21/15 08:35

10307337010 LPG-39/1-3 Solid 05/20/15 00:00 05/21/15 08:35

10307337011 LPG-40/2-4 Solid 05/20/15 00:00 05/21/15 08:35

10307337012 LPG-41/2-4 Solid 05/20/15 00:00 05/21/15 08:35

10307337013 LPG-41/19-22 Water 05/20/15 00:00 05/21/15 08:35

10307337014 LPG-42/1-3 Solid 05/20/15 00:00 05/21/15 08:35

10307337015 LPG-43/4-6 Solid 05/20/15 00:00 05/21/15 08:35

10307337016 LPG-44/5-7 Solid 05/20/15 00:00 05/21/15 08:35

10307337017 LPG-44/19-22 Water 05/20/15 00:00 05/21/15 08:35

10307337018 LPG-45/8-10 Solid 05/20/15 00:00 05/21/15 08:35

10307337019 LPG-45/12-20 Water 05/20/15 00:00 05/21/15 08:35

10307337020 TRIP BLANK Water 05/21/15 08:35







(612)607-1700

Page 3 of 73

#=SA#


Pace Project No.:

Project:

10307337



Analytes

ReportedAnalysts

10307337001 LPG-31/1-3 EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL

EPA 8270D by SIM 19LT

10307337002 LPG-32/2-4 EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL


10307337003 LPG-33/2-4 EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL


10307337004 LPG-34/2-4 EPA 6010C 1DM

EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL


10307337005 LPG-35/6-8 WI MOD DRO 2JRH

WI MOD GRO 2AEJ

EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL


EPA 8260B 70AMT

10307337006 LPG-36/10-12 WI MOD DRO 2JRH

WI MOD GRO 2RTP

ASTM D2974 1JDL

EPA 8260B 70AMT

10307337007 LPG-36/18-20 WI MOD DRO 2JRH

WI MOD GRO 2RTP

ASTM D2974 1JDL

EPA 8260B 70AMT

10307337008 LPG-37/2-4 EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL


10307337009 LPG-38/4-6 EPA 6010C 7DM







(612)607-1700

Page 4 of 73

#=SA#


Pace Project No.:

Project:

10307337



Analytes

ReportedAnalysts

EPA 7471B 1DM

ASTM D2974 1JDL


10307337010 LPG-39/1-3 EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL


10307337011 LPG-40/2-4 EPA 6010C 7DM

EPA 7471B 1DM

ASTM D2974 1JDL


10307337012 LPG-41/2-4 EPA 6010C 7DM, WBS

EPA 7471B 1DM

ASTM D2974 1JDL


10307337013 LPG-41/19-22 WI MOD DRO 2MT

WI MOD GRO 6LPM

EPA 8260B 70AJC

10307337014 LPG-42/1-3 EPA 6010C 7DM, WBS

EPA 7471B 1DM

ASTM D2974 1JDL


10307337015 LPG-43/4-6 EPA 6010C 7DM, WBS

EPA 7471B 1DM

ASTM D2974 1JDL


10307337016 LPG-44/5-7 WI MOD DRO 2JRH

WI MOD GRO 2RTP

ASTM D2974 1JDL

EPA 8260B 70LPM

10307337017 LPG-44/19-22 WI MOD DRO 2MT

WI MOD GRO 6LPM

EPA 8260B 70AJC

10307337018 LPG-45/8-10 WI MOD DRO 2JRH

WI MOD GRO 2RTP

EPA 6010C 7DM

EPA 7471B 1DM







(612)607-1700

Page 5 of 73

#=SA#


Pace Project No.:

Project:

10307337



Analytes

ReportedAnalysts

ASTM D2974 1JDL


EPA 8260B 70LPM

10307337019 LPG-45/12-20 WI MOD DRO 2MT

WI MOD GRO 6LPM

EPA 8260B 70AJC

10307337020 TRIP BLANK EPA 8260B 70AJC







(612)607-1700

Page 6 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337


Sample: LPG-31/1-3 Lab ID: 10307337001 Collected: 05/19/15 00:00 Received: 05/21/15 08:35 Matrix: Solid




Arsenic 3.3 mg/kg 05/29/15 22:37 7440-38-205/29/15 10:351.2 1

Barium 69.2 mg/kg 05/29/15 22:37 7440-39-305/29/15 10:350.60 1

Cadmium ND mg/kg 05/29/15 22:37 7440-43-905/29/15 10:350.18 1

Chromium 10.3 mg/kg 05/29/15 22:37 7440-47-305/29/15 10:350.60 1

Lead 6.1 mg/kg 05/29/15 22:37 7439-92-105/29/15 10:350.60 1

Selenium ND mg/kg 05/29/15 22:37 7782-49-205/29/15 10:351.2 1

Silver ND mg/kg 05/29/15 22:37 7440-22-405/29/15 10:350.60 1


Mercury ND mg/kg 05/29/15 15:01 7439-97-605/29/15 08:010.023 1












Chrysene ND mg/kg 05/29/15 01:55 218-01-905/27/15 23:330.013 1



Fluorene ND mg/kg 05/29/15 01:55 86-73-705/27/15 23:330.013 1




Pyrene 0.016 mg/kg 05/29/15 01:55 129-00-005/27/15 23:330.013 1



p-Terphenyl-d14 (S) 71 %. 05/29/15 01:55 1718-51-005/27/15 23:3330-150 1



without the written consent of Pace Analytical Services, Inc..Date: 07/01/2015 11:38 AM




(612)607-1700

Page 7 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic 2.1 mg/kg 05/29/15 22:57 7440-38-205/29/15 10:351.1 1

Barium 24.7 mg/kg 05/29/15 22:57 7440-39-305/29/15 10:350.53 1

Cadmium ND mg/kg 05/29/15 22:57 7440-43-905/29/15 10:350.16 1

Chromium 7.1 mg/kg 05/29/15 22:57 7440-47-305/29/15 10:350.53 1

Lead 2.3 mg/kg 05/29/15 22:57 7439-92-105/29/15 10:350.53 1

Selenium ND mg/kg 05/29/15 22:57 7782-49-205/29/15 10:351.1 1

Silver ND mg/kg 05/29/15 22:57 7440-22-405/29/15 10:350.53 1


Mercury ND mg/kg 05/29/15 15:07 7439-97-605/29/15 08:010.021 1












Chrysene ND mg/kg 05/29/15 02:17 218-01-905/27/15 23:330.011 1



Fluorene ND mg/kg 05/29/15 02:17 86-73-705/27/15 23:330.011 1




Pyrene ND mg/kg 05/29/15 02:17 129-00-005/27/15 23:330.011 1



p-Terphenyl-d14 (S) 78 %. 05/29/15 02:17 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 8 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic 1.8 mg/kg 05/29/15 23:00 7440-38-205/29/15 10:351.1 1

Barium 16.5 mg/kg 05/29/15 23:00 7440-39-305/29/15 10:350.55 1

Cadmium ND mg/kg 05/29/15 23:00 7440-43-905/29/15 10:350.16 1

Chromium 6.4 mg/kg 05/29/15 23:00 7440-47-305/29/15 10:350.55 1

Lead 2.3 mg/kg 05/29/15 23:00 7439-92-105/29/15 10:350.55 1

Selenium ND mg/kg 05/29/15 23:00 7782-49-205/29/15 10:351.1 1

Silver ND mg/kg 05/29/15 23:00 7440-22-405/29/15 10:350.55 1


Mercury ND mg/kg 05/29/15 15:09 7439-97-605/29/15 08:010.021 1












Chrysene ND mg/kg 05/29/15 02:38 218-01-905/27/15 23:330.011 1



Fluorene ND mg/kg 05/29/15 02:38 86-73-705/27/15 23:330.011 1




Pyrene ND mg/kg 05/29/15 02:38 129-00-005/27/15 23:330.011 1



p-Terphenyl-d14 (S) 79 %. 05/29/15 02:38 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 9 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337





Analytical Method: EPA 6010C Preparation Method: EPA 3010

Leachate Method/Date: EPA 1311; 06/25/15 12:03 Initial pH: 8.4; Final pH: 1.73

6010C MET ICP, TCLP

Lead ND mg/L 06/25/15 23:07 7439-92-106/25/15 14:100.050 1


Arsenic 1.8 mg/kg 05/29/15 23:03 7440-38-205/29/15 10:351.1 1

Barium 11.9 mg/kg 05/29/15 23:03 7440-39-305/29/15 10:350.56 1

Cadmium ND mg/kg 05/29/15 23:03 7440-43-905/29/15 10:350.17 1

Chromium 4.9 mg/kg 05/29/15 23:03 7440-47-305/29/15 10:350.56 1

Lead 3700 mg/kg 05/29/15 23:03 7439-92-105/29/15 10:350.56 1

Selenium ND mg/kg 05/29/15 23:03 7782-49-205/29/15 10:351.1 1

Silver ND mg/kg 05/29/15 23:03 7440-22-405/29/15 10:350.56 1


Mercury ND mg/kg 05/29/15 15:11 7439-97-605/29/15 08:010.023 1






Anthracene 0.014 mg/kg 05/28/15 22:19 120-12-705/27/15 23:330.012 1






Chrysene 0.058 mg/kg 05/28/15 22:19 218-01-905/27/15 23:330.012 1



Fluorene ND mg/kg 05/28/15 22:19 86-73-705/27/15 23:330.012 1




Pyrene 0.073 mg/kg 05/28/15 22:19 129-00-005/27/15 23:330.012 1



p-Terphenyl-d14 (S) 79 %. 05/28/15 22:19 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 10 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






WDRO C10-C28 13.5 mg/kg 05/29/15 10:35 T605/28/15 17:105.1 1






Arsenic 3.5 mg/kg 05/29/15 23:06 7440-38-205/29/15 10:351.2 1

Barium 91.6 mg/kg 05/29/15 23:06 7440-39-305/29/15 10:350.62 1

Cadmium 0.21 mg/kg 05/29/15 23:06 7440-43-905/29/15 10:350.19 1

Chromium 9.6 mg/kg 05/29/15 23:06 7440-47-305/29/15 10:350.62 1

Lead 17.9 mg/kg 05/29/15 23:06 7439-92-105/29/15 10:350.62 1

Selenium ND mg/kg 05/29/15 23:06 7782-49-205/29/15 10:351.2 1

Silver ND mg/kg 05/29/15 23:06 7440-22-405/29/15 10:350.62 1


Mercury 0.035 mg/kg 05/29/15 15:13 7439-97-605/29/15 08:010.023 1




Acenaphthene 0.015 mg/kg 05/28/15 22:40 83-32-905/27/15 23:330.013 1


Anthracene 0.11 mg/kg 05/28/15 22:40 120-12-705/27/15 23:330.013 1






Chrysene 0.53 mg/kg 05/29/15 10:06 218-01-905/27/15 23:330.066 5



Fluorene 0.027 mg/kg 05/28/15 22:40 86-73-705/27/15 23:330.013 1




Pyrene 0.86 mg/kg 05/29/15 10:06 129-00-005/27/15 23:330.066 5



p-Terphenyl-d14 (S) 63 %. 05/28/15 22:40 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 11 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Acetone ND mg/kg 05/29/15 16:28 67-64-105/29/15 10:181.3 1


Benzene ND mg/kg 05/29/15 16:28 71-43-205/29/15 10:180.026 1





























trans-1,2-Dichloroethene ND mg/kg 05/29/15 16:28 156-60-505/29/15 10:180.064 1





















(612)607-1700

Page 12 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337









Styrene ND mg/kg 05/29/15 16:28 100-42-505/29/15 10:180.064 1





Toluene ND mg/kg 05/29/15 16:28 108-88-305/29/15 10:180.064 1








1,1,2-Trichlorotrifluoroethane ND mg/kg 05/29/15 16:28 76-13-105/29/15 10:180.26 1






Toluene-d8 (S) 99 %. 05/29/15 16:28 2037-26-505/29/15 10:1861-125 1








(612)607-1700

Page 13 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






WDRO C10-C28 92.9 mg/kg 05/29/15 12:0005/28/15 17:107.7 2



Gasoline Range Organics 521 mg/kg 05/29/15 09:5705/27/15 15:5923.5 2

Surrogatesa,a,a-Trifluorotoluene (S) 34 %. 05/29/15 09:57 98-08-8 S205/27/15 15:5980-150 2




Acetone ND mg/kg 05/29/15 16:46 67-64-105/29/15 10:181.1 1


Benzene ND mg/kg 05/29/15 16:46 71-43-205/29/15 10:180.023 1








sec-Butylbenzene 0.87 mg/kg 05/29/15 16:46 135-98-805/29/15 10:180.056 1





























(612)607-1700

Page 14 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337













Ethylbenzene 2.1 mg/kg 05/29/15 16:46 100-41-405/29/15 10:180.056 1


Isopropylbenzene (Cumene) 0.86 mg/kg 05/29/15 16:46 98-82-805/29/15 10:180.056 1





Naphthalene 6.2 mg/kg 05/29/15 16:46 91-20-305/29/15 10:180.23 1

n-Propylbenzene 2.4 mg/kg 05/29/15 16:46 103-65-105/29/15 10:180.056 1

Styrene ND mg/kg 05/29/15 16:46 100-42-505/29/15 10:180.056 1





Toluene 0.18 mg/kg 05/29/15 16:46 108-88-305/29/15 10:180.056 1









1,2,4-Trimethylbenzene 28.0 mg/kg 06/01/15 22:35 95-63-605/29/15 10:180.56 10

1,3,5-Trimethylbenzene 10.8 mg/kg 05/29/15 16:46 108-67-805/29/15 10:180.056 1


Xylene (Total) 23.2 mg/kg 05/29/15 16:46 1330-20-705/29/15 10:180.17 1


Toluene-d8 (S) 112 %. 05/29/15 16:46 2037-26-505/29/15 10:1861-125 1








(612)607-1700

Page 15 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






WDRO C10-C28 ND mg/kg 05/29/15 11:0605/28/15 17:106.7 1








Acetone ND mg/kg 05/31/15 22:47 67-64-105/29/15 10:181.2 1


Benzene ND mg/kg 05/31/15 22:47 71-43-205/29/15 10:180.023 1





































(612)607-1700

Page 16 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






















Styrene ND mg/kg 05/31/15 22:47 100-42-505/29/15 10:180.059 1





Toluene ND mg/kg 05/31/15 22:47 108-88-305/29/15 10:180.059 1














Toluene-d8 (S) 65 %. 05/31/15 22:47 2037-26-505/29/15 10:1861-125 1








(612)607-1700

Page 17 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic 2.7 mg/kg 05/29/15 23:09 7440-38-205/29/15 10:350.99 1

Barium 62.2 mg/kg 05/29/15 23:09 7440-39-305/29/15 10:350.50 1

Cadmium ND mg/kg 05/29/15 23:09 7440-43-905/29/15 10:350.15 1

Chromium 8.4 mg/kg 05/29/15 23:09 7440-47-305/29/15 10:350.50 1

Lead 5.4 mg/kg 05/29/15 23:09 7439-92-105/29/15 10:350.50 1

Selenium ND mg/kg 05/29/15 23:09 7782-49-205/29/15 10:350.99 1

Silver ND mg/kg 05/29/15 23:09 7440-22-405/29/15 10:350.50 1


Mercury ND mg/kg 05/29/15 15:20 7439-97-605/29/15 08:010.020 1






Anthracene 0.015 mg/kg 05/29/15 08:40 120-12-705/27/15 23:330.011 1






Chrysene 0.042 mg/kg 05/29/15 08:40 218-01-905/27/15 23:330.011 1



Fluorene ND mg/kg 05/29/15 08:40 86-73-705/27/15 23:330.011 1




Pyrene 0.073 mg/kg 05/29/15 08:40 129-00-005/27/15 23:330.011 1



p-Terphenyl-d14 (S) 73 %. 05/29/15 08:40 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 18 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic 1.3 mg/kg 05/29/15 23:12 7440-38-205/29/15 10:351.0 1

Barium 32.3 mg/kg 05/29/15 23:12 7440-39-305/29/15 10:350.51 1

Cadmium ND mg/kg 05/29/15 23:12 7440-43-905/29/15 10:350.15 1

Chromium 4.9 mg/kg 05/29/15 23:12 7440-47-305/29/15 10:350.51 1

Lead 2.7 mg/kg 05/29/15 23:12 7439-92-105/29/15 10:350.51 1

Selenium ND mg/kg 05/29/15 23:12 7782-49-205/29/15 10:351.0 1

Silver ND mg/kg 05/29/15 23:12 7440-22-405/29/15 10:350.51 1


Mercury ND mg/kg 05/29/15 15:22 7439-97-605/29/15 08:010.022 1












Chrysene 0.021 mg/kg 05/29/15 00:28 218-01-905/27/15 23:330.011 1



Fluorene ND mg/kg 05/29/15 00:28 86-73-705/27/15 23:330.011 1




Pyrene 0.040 mg/kg 05/29/15 00:28 129-00-005/27/15 23:330.011 1



p-Terphenyl-d14 (S) 72 %. 05/29/15 00:28 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 19 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic 2.0 mg/kg 05/29/15 23:15 7440-38-205/29/15 10:350.95 1

Barium 25.8 mg/kg 05/29/15 23:15 7440-39-305/29/15 10:350.48 1

Cadmium ND mg/kg 05/29/15 23:15 7440-43-905/29/15 10:350.14 1

Chromium 6.3 mg/kg 05/29/15 23:15 7440-47-305/29/15 10:350.48 1

Lead 2.9 mg/kg 05/29/15 23:15 7439-92-105/29/15 10:350.48 1

Selenium ND mg/kg 05/29/15 23:15 7782-49-205/29/15 10:350.95 1

Silver ND mg/kg 05/29/15 23:15 7440-22-405/29/15 10:350.48 1


Mercury ND mg/kg 05/29/15 15:24 7439-97-605/29/15 08:010.021 1






Anthracene 0.077 mg/kg 05/29/15 09:01 120-12-705/27/15 23:330.011 1






Chrysene 0.14 mg/kg 05/29/15 09:01 218-01-905/27/15 23:330.011 1



Fluorene ND mg/kg 05/29/15 09:01 86-73-705/27/15 23:330.011 1




Pyrene 0.17 mg/kg 05/29/15 09:01 129-00-005/27/15 23:330.011 1



p-Terphenyl-d14 (S) 85 %. 05/29/15 09:01 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 20 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic 2.5 mg/kg 05/29/15 23:18 7440-38-205/29/15 10:351.0 1

Barium 20.1 mg/kg 05/29/15 23:18 7440-39-305/29/15 10:350.51 1

Cadmium ND mg/kg 05/29/15 23:18 7440-43-905/29/15 10:350.15 1

Chromium 4.4 mg/kg 05/29/15 23:18 7440-47-305/29/15 10:350.51 1

Lead 2.2 mg/kg 05/29/15 23:18 7439-92-105/29/15 10:350.51 1

Selenium ND mg/kg 05/29/15 23:18 7782-49-205/29/15 10:351.0 1

Silver ND mg/kg 05/29/15 23:18 7440-22-405/29/15 10:350.51 1


Mercury ND mg/kg 05/29/15 15:26 7439-97-605/29/15 08:010.019 1












Chrysene ND mg/kg 05/28/15 23:45 218-01-905/27/15 23:330.010 1



Fluorene ND mg/kg 05/28/15 23:45 86-73-705/27/15 23:330.010 1




Pyrene ND mg/kg 05/28/15 23:45 129-00-005/27/15 23:330.010 1



p-Terphenyl-d14 (S) 82 %. 05/28/15 23:45 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 21 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic ND mg/kg 05/30/15 10:23 7440-38-205/29/15 10:355.1 5

Barium 35.4 mg/kg 05/29/15 23:21 7440-39-305/29/15 10:350.51 1

Cadmium ND mg/kg 05/29/15 23:21 7440-43-905/29/15 10:350.15 1

Chromium 4.6 mg/kg 05/29/15 23:21 7440-47-305/29/15 10:350.51 1

Lead 1.8 mg/kg 05/29/15 23:21 7439-92-105/29/15 10:350.51 1

Selenium ND mg/kg 05/30/15 10:23 7782-49-205/29/15 10:355.1 5

Silver ND mg/kg 05/29/15 23:21 7440-22-405/29/15 10:350.51 1


Mercury ND mg/kg 05/29/15 15:28 7439-97-605/29/15 08:010.021 1












Chrysene ND mg/kg 05/29/15 09:23 218-01-905/27/15 23:330.010 1



Fluorene ND mg/kg 05/29/15 09:23 86-73-705/27/15 23:330.010 1




Pyrene ND mg/kg 05/29/15 09:23 129-00-005/27/15 23:330.010 1



p-Terphenyl-d14 (S) 73 %. 05/29/15 09:23 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 22 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337


Sample: LPG-41/19-22 Lab ID: 10307337013 Collected: 05/20/15 00:00 Received: 05/21/15 08:35 Matrix: Water



WDRO C10-C28 ND mg/L 05/28/15 12:2805/27/15 23:580.11 1



Benzene ND ug/L 05/26/15 22:36 71-43-21.0 1


Gasoline Range Organics ND ug/L 05/26/15 22:36100 1

Toluene ND ug/L 05/26/15 22:36 108-88-31.0 1


Surrogatesa,a,a-Trifluorotoluene (S) 101 %. 05/26/15 22:36 98-08-880-150 1


Acetone ND ug/L 05/26/15 02:54 67-64-120.0 1


Benzene ND ug/L 05/26/15 02:54 71-43-21.0 1




Bromoform ND ug/L 05/26/15 02:54 75-25-24.0 1

































(612)607-1700

Page 23 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337





















Styrene ND ug/L 05/26/15 02:54 100-42-51.0 1



Tetrachloroethene 2.8 ug/L 05/26/15 02:54 127-18-41.0 1


Toluene ND ug/L 05/26/15 02:54 108-88-31.0 1














Toluene-d8 (S) 102 %. 05/26/15 02:54 2037-26-575-125 1








(612)607-1700

Page 24 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic ND mg/kg 05/30/15 10:26 7440-38-205/29/15 10:355.3 5

Barium 36.9 mg/kg 05/29/15 23:24 7440-39-305/29/15 10:350.53 1

Cadmium ND mg/kg 05/29/15 23:24 7440-43-905/29/15 10:350.16 1

Chromium 6.3 mg/kg 05/29/15 23:24 7440-47-305/29/15 10:350.53 1

Lead 9.6 mg/kg 05/29/15 23:24 7439-92-105/29/15 10:350.53 1

Selenium ND mg/kg 05/30/15 10:26 7782-49-205/29/15 10:355.3 5

Silver ND mg/kg 05/29/15 23:24 7440-22-405/29/15 10:350.53 1


Mercury ND mg/kg 05/29/15 15:30 7439-97-605/29/15 08:010.020 1












Chrysene 0.020 mg/kg 05/29/15 09:45 218-01-905/27/15 23:330.011 1



Fluorene ND mg/kg 05/29/15 09:45 86-73-705/27/15 23:330.011 1




Pyrene 0.033 mg/kg 05/29/15 09:45 129-00-005/27/15 23:330.011 1



p-Terphenyl-d14 (S) 72 %. 05/29/15 09:45 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 25 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Arsenic ND mg/kg 05/30/15 10:29 7440-38-205/29/15 10:355.0 5

Barium 24.0 mg/kg 05/29/15 23:33 7440-39-305/29/15 10:350.50 1

Cadmium ND mg/kg 05/29/15 23:33 7440-43-905/29/15 10:350.15 1

Chromium 5.1 mg/kg 05/29/15 23:33 7440-47-305/29/15 10:350.50 1

Lead 1.8 mg/kg 05/29/15 23:33 7439-92-105/29/15 10:350.50 1

Selenium ND mg/kg 05/30/15 10:29 7782-49-205/29/15 10:355.0 5

Silver ND mg/kg 05/29/15 23:33 7440-22-405/29/15 10:350.50 1


Mercury ND mg/kg 05/29/15 15:32 7439-97-605/29/15 08:010.020 1












Chrysene ND mg/kg 05/29/15 01:12 218-01-905/27/15 23:330.010 1



Fluorene ND mg/kg 05/29/15 01:12 86-73-705/27/15 23:330.010 1




Pyrene ND mg/kg 05/29/15 01:12 129-00-005/27/15 23:330.010 1



p-Terphenyl-d14 (S) 84 %. 05/29/15 01:12 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 26 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






WDRO C10-C28 ND mg/kg 05/29/15 10:4305/28/15 17:105.1 1








Acetone ND mg/kg 06/01/15 19:37 67-64-106/01/15 09:531.2 1


Benzene ND mg/kg 06/01/15 19:37 71-43-206/01/15 09:530.025 1





































(612)607-1700

Page 27 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






















Styrene ND mg/kg 06/01/15 19:37 100-42-506/01/15 09:530.062 1



Tetrachloroethene 0.15 mg/kg 06/01/15 19:37 127-18-406/01/15 09:530.062 1


Toluene ND mg/kg 06/01/15 19:37 108-88-306/01/15 09:530.062 1














Toluene-d8 (S) 102 %. 06/01/15 19:37 2037-26-506/01/15 09:5361-125 1








(612)607-1700

Page 28 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337





WDRO C10-C28 ND mg/L 05/28/15 12:3505/27/15 23:580.11 1



Benzene ND ug/L 05/26/15 22:59 71-43-21.0 1



Toluene ND ug/L 05/26/15 22:59 108-88-31.0 1


Surrogatesa,a,a-Trifluorotoluene (S) 99 %. 05/26/15 22:59 98-08-880-150 1


Acetone ND ug/L 05/26/15 03:08 67-64-120.0 1


Benzene ND ug/L 05/26/15 03:08 71-43-21.0 1




Bromoform ND ug/L 05/26/15 03:08 75-25-24.0 1

































(612)607-1700

Page 29 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337





















Styrene ND ug/L 05/26/15 03:08 100-42-51.0 1



Tetrachloroethene 9.9 ug/L 05/26/15 03:08 127-18-41.0 1


Toluene ND ug/L 05/26/15 03:08 108-88-31.0 1














Toluene-d8 (S) 101 %. 05/26/15 03:08 2037-26-575-125 1








(612)607-1700

Page 30 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






WDRO C10-C28 ND mg/kg 05/29/15 11:1405/28/15 17:103.9 1






Arsenic 1.3 mg/kg 05/29/15 23:36 7440-38-205/29/15 10:350.95 1

Barium 11.9 mg/kg 05/29/15 23:36 7440-39-305/29/15 10:350.47 1

Cadmium ND mg/kg 05/29/15 23:36 7440-43-905/29/15 10:350.14 1

Chromium 4.7 mg/kg 05/29/15 23:36 7440-47-305/29/15 10:350.47 1

Lead 1.4 mg/kg 05/29/15 23:36 7439-92-105/29/15 10:350.47 1

Selenium ND mg/kg 05/29/15 23:36 7782-49-205/29/15 10:350.95 1

Silver ND mg/kg 05/29/15 23:36 7440-22-405/29/15 10:350.47 1


Mercury ND mg/kg 05/29/15 15:34 7439-97-605/29/15 08:010.020 1












Chrysene ND mg/kg 05/29/15 01:33 218-01-905/27/15 23:330.010 1



Fluorene ND mg/kg 05/29/15 01:33 86-73-705/27/15 23:330.010 1




Pyrene ND mg/kg 05/29/15 01:33 129-00-005/27/15 23:330.010 1



p-Terphenyl-d14 (S) 80 %. 05/29/15 01:33 1718-51-005/27/15 23:3330-150 1







(612)607-1700

Page 31 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337






Acetone ND mg/kg 06/01/15 19:57 67-64-106/01/15 09:531.1 1


Benzene ND mg/kg 06/01/15 19:57 71-43-206/01/15 09:530.021 1


















































(612)607-1700

Page 32 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337









Styrene ND mg/kg 06/01/15 19:57 100-42-506/01/15 09:530.053 1





Toluene ND mg/kg 06/01/15 19:57 108-88-306/01/15 09:530.053 1














Toluene-d8 (S) 105 %. 06/01/15 19:57 2037-26-506/01/15 09:5361-125 1








(612)607-1700

Page 33 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337





WDRO C10-C28 ND mg/L 05/28/15 12:4205/27/15 23:580.11 1



Benzene ND ug/L 05/26/15 23:23 71-43-21.0 1



Toluene ND ug/L 05/26/15 23:23 108-88-31.0 1


Surrogatesa,a,a-Trifluorotoluene (S) 102 %. 05/26/15 23:23 98-08-8 pH80-150 1


Acetone ND ug/L 05/26/15 03:23 67-64-120.0 1


Benzene ND ug/L 05/26/15 03:23 71-43-21.0 1




Bromoform ND ug/L 05/26/15 03:23 75-25-24.0 1

































(612)607-1700

Page 34 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337





















Styrene ND ug/L 05/26/15 03:23 100-42-51.0 1





Toluene ND ug/L 05/26/15 03:23 108-88-31.0 1














Toluene-d8 (S) 105 %. 05/26/15 03:23 2037-26-575-125 1








(612)607-1700

Page 35 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337


Sample: TRIP BLANK Lab ID: 10307337020 Collected: Received: 05/21/15 08:35 Matrix: Water



Acetone ND ug/L 05/26/15 00:43 67-64-120.0 1


Benzene ND ug/L 05/26/15 00:43 71-43-21.0 1




Bromoform ND ug/L 05/26/15 00:43 75-25-24.0 1















































(612)607-1700

Page 36 of 73

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10307337


Sample: TRIP BLANK Lab ID: 10307337020 Collected: Received: 05/21/15 08:35 Matrix: Water





Styrene ND ug/L 05/26/15 00:43 100-42-51.0 1





Toluene ND ug/L 05/26/15 00:43 108-88-31.0 1














Toluene-d8 (S) 100 %. 05/26/15 00:43 2037-26-575-125 1








(612)607-1700

Page 37 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


GCV/13777

EPA 5030 Medium Soil

WI MOD GRO

WIGRO Solid GCV


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Gasoline Range Organics mg/kg ND 10.0 05/28/15 16:48


Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1975916

Gasoline Range Organics mg/kg 44.250 88 80-1208844.0 1 20


Parameter Units

MS

Result

% Rec



MSSpike

Result

10307659001

Gasoline Range Organics mg/kg 41.4 C0,M053.4 67 80-120ND


Parameter Units

Dup

Result

Max


10307659002


Gasoline Range Organics mg/kg 5.1J 20ND

a,a,a-Trifluorotoluene (S) %. 104 0104







(612)607-1700

Page 38 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


GCV/13776

WI MOD GRO

WI MOD GRO

WIGRO GCV Water

Associated Lab Samples: 10307337013, 10307337017, 10307337019

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Benzene ug/L ND 1.0 05/26/15 16:17


Gasoline Range Organics ug/L ND 100 05/26/15 16:17

Toluene ug/L ND 1.0 05/26/15 16:17



Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1975898

Benzene ug/L 99.7100 100 80-1208787.4 13 20

Ethylbenzene ug/L 104100 104 80-1209292.0 12 20

Gasoline Range Organics ug/L 9941000 99 80-12094941 5 20

Toluene ug/L 107100 107 80-1209494.3 12 20

Xylene (Total) ug/L 317300 106 80-12093280 12 20


Parameter Units

MS

Result

% Rec



MSSpike

Result

10306382006

Benzene ug/L 97.9100 98 80-120ND

Ethylbenzene ug/L 104100 104 80-120ND

Gasoline Range Organics ug/L 10101000 99 80-120ND

Toluene ug/L 106100 106 80-120ND

Xylene (Total) ug/L 308300 103 80-120ND








(612)607-1700

Page 39 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MERP/13661

EPA 7471B

EPA 7471B


Associated Lab Samples: 10307337001, 10307337002, 10307337003, 10307337004, 10307337005, 10307337008, 10307337009,10307337010, 10307337011, 10307337012, 10307337014, 10307337015, 10307337018

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Mercury mg/kg ND 0.019 05/29/15 14:57

Parameter Units

LCS

Result

% Rec



LCSSpike

Mercury mg/kg 0.46.45 100 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

10307337001

1976705

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Mercury mg/kg .58 103 75-125102 4 20.56ND 0.62 0.59







(612)607-1700

Page 40 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MPRP/55531

EPA 3010

EPA 6010C

6010C TCLP

Associated Lab Samples: 10307337004

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead mg/L ND 0.050 06/25/15 23:01

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead mg/L ND 0.050 06/25/15 23:49

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead mg/L ND 0.050 06/25/15 23:52

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead mg/L 4.75 93 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

10307337004

2005640

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead mg/L 5 93 75-12593 0 305ND 4.7 4.7







(612)607-1700

Page 41 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54632

EPA 3050

EPA 6010C

6010C Solids


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

Arsenic mg/kg ND 0.98 05/29/15 22:31

Barium mg/kg ND 0.49 05/29/15 22:31

Cadmium mg/kg ND 0.15 05/29/15 22:31

Chromium mg/kg ND 0.49 05/29/15 22:31

Lead mg/kg ND 0.49 05/29/15 22:31

Selenium mg/kg ND 0.98 05/29/15 22:31

Silver mg/kg ND 0.49 05/29/15 22:31

Parameter Units

LCS

Result

% Rec



LCSSpike

Arsenic mg/kg 46.450 93 80-120

Barium mg/kg 50.150 100 80-120

Cadmium mg/kg 47.850 96 80-120

Chromium mg/kg 48.850 98 80-120

Lead mg/kg 48.050 96 80-120

Selenium mg/kg 46.350 93 80-120

Silver mg/kg 23.725 95 80-120

Parameter Units

MS

Result

% Rec



MSSpike

Result

10307337001

1975234

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Arsenic mg/kg 59.2 81 75-12585 3 2058.23.3 51.1 52.6

Barium mg/kg 59.2 96 75-12589 4 2058.269.2 126 121

Cadmium mg/kg 59.2 82 75-12586 3 2058.2ND 48.8 50.3

Chromium mg/kg 59.2 81 75-12588 5 2058.210.3 58.1 61.3

Lead mg/kg 59.2 81 75-12585 3 2058.26.1 54.0 55.4

Selenium mg/kg 59.2 80 75-12584 3 2058.2ND 47.4 49.1

Silver mg/kg 29.5 82 75-12586 3 2029ND 24.3 25.1







(612)607-1700

Page 42 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54713

ASTM D2974

ASTM D2974



Parameter Units

Dup

Result

Max


10307337002



Parameter Units

Dup

Result

Max


10307261002









(612)607-1700

Page 43 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MPRP/54734

ASTM D2974

ASTM D2974


Associated Lab Samples: 10307337003, 10307337004, 10307337005, 10307337006, 10307337007, 10307337008, 10307337009,10307337010, 10307337011, 10307337012, 10307337014, 10307337015, 10307337016, 10307337018

Parameter Units

Dup

Result

Max


10307276001



Parameter Units

Dup

Result

Max


10307382002









(612)607-1700

Page 44 of 73

#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MSV/31586

EPA 5035/5030B

EPA 8260B



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed



























Acetone mg/kg ND 1.0 05/29/15 14:22


Benzene mg/kg ND 0.020 05/29/15 14:22



















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Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed
















Styrene mg/kg ND 0.050 05/29/15 14:22




Toluene mg/kg ND 0.050 05/29/15 14:22









Toluene-d8 (S) %. 98 61-125 05/29/15 14:22

Parameter Units

LCS

Result

% Rec



LCSSpike





1,1,2-Trichlorotrifluoroethane mg/kg 0.831 83 55-125













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Parameter Units

LCS

Result

% Rec



LCSSpike
















Acetone mg/kg 4.25 85 55-131


Benzene mg/kg 0.771 77 69-125
















Dichlorofluoromethane mg/kg 0.861 86 30-150












Styrene mg/kg 0.781 78 75-125








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Parameter Units

LCS

Result

% Rec



LCSSpike



Toluene mg/kg 0.751 75 72-125

trans-1,2-Dichloroethene mg/kg 0.691 69 68-125



Trichlorofluoromethane mg/kg 0.811 81 30-150





Toluene-d8 (S) %. 99 61-125

Parameter Units

MS

Result

% Rec



MSSpike

Result

10307014011



























Acetone mg/kg 4.66.1 76 65-135ND


Benzene mg/kg 1.31.2 104 63-126ND







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Parameter Units

MS

Result

% Rec



MSSpike

Result

10307014011
















Dichlorofluoromethane mg/kg 1.6 CH1.2 130 30-150ND












Styrene mg/kg 1.11.2 90 70-132ND




Toluene mg/kg 1.21.2 96 66-128ND




Trichlorofluoromethane mg/kg 1.4 CH1.2 111 39-150ND





Toluene-d8 (S) %. 103 61-125







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Parameter Units

Dup

Result

Max


10307014012
























2-Butanone (MEK) mg/kg ND 30ND















Chloroform mg/kg ND 30ND

Chloromethane mg/kg ND 30ND















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Parameter Units

Dup

Result

Max


10307014012
























Toluene-d8 (S) %. 96 297







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#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MSV/31613

EPA 5035/5030B

EPA 8260B



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed



























Acetone mg/kg ND 1.0 06/01/15 15:54


Benzene mg/kg ND 0.020 06/01/15 15:54



















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Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed
















Styrene mg/kg ND 0.050 06/01/15 15:54




Toluene mg/kg ND 0.050 06/01/15 15:54









Toluene-d8 (S) %. 103 61-125 06/01/15 15:54

Parameter Units

LCS

Result

% Rec



LCSSpike





1,1,2-Trichlorotrifluoroethane mg/kg 1.21 118 55-125













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Parameter Units

LCS

Result

% Rec



LCSSpike
















Acetone mg/kg 5.75 115 55-131


Benzene mg/kg 1.21 120 69-125
















Dichlorofluoromethane mg/kg 1.2 CH1 118 30-150












Styrene mg/kg 1.11 109 75-125








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Parameter Units

LCS

Result

% Rec



LCSSpike



Toluene mg/kg 1.11 107 72-125

trans-1,2-Dichloroethene mg/kg 1.3 L01 126 68-125



Trichlorofluoromethane mg/kg 1.0 CH1 103 30-150





Toluene-d8 (S) %. 100 61-125

Parameter Units

MS

Result

% Rec



MSSpike

Result

10307379001



























Acetone mg/kg 5.75.4 106 65-135ND


Benzene mg/kg 1.31.1 123 63-126ND







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Parameter Units

MS

Result

% Rec



MSSpike

Result

10307379001
















Dichlorofluoromethane mg/kg 1.3 CH1.1 117 30-150ND












Styrene mg/kg 1.21.1 108 70-132ND




Toluene mg/kg 1.21.1 113 66-128ND




Trichlorofluoromethane mg/kg 1.1 CH1.1 103 39-150ND





Toluene-d8 (S) %. 103 61-125







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Parameter Units

Dup

Result

Max


10307379002
























2-Butanone (MEK) mg/kg .18J 30ND















Chloroform mg/kg .014J 30ND

Chloromethane mg/kg .013J 30ND















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Parameter Units

Dup

Result

Max


10307379002
























Toluene-d8 (S) %. 101 10103







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#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


MSV/31527

EPA 8260B

EPA 8260B

8260B MSV 465 W


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed





1,1,2-Trichlorotrifluoroethane ug/L ND 1.0 05/26/15 00:14


1,1-Dichloroethene ug/L ND 1.0 05/26/15 00:14

1,1-Dichloropropene ug/L ND 1.0 05/26/15 00:14


1,2,3-Trichloropropane ug/L ND 4.0 05/26/15 00:14



1,2-Dibromo-3-chloropropane ug/L ND 10.0 05/26/15 00:14

1,2-Dibromoethane (EDB) ug/L ND 1.0 05/26/15 00:14









2-Butanone (MEK) ug/L ND 5.0 05/26/15 00:14



4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 05/26/15 00:14

Acetone ug/L ND 20.0 05/26/15 00:14

Allyl chloride ug/L ND 4.0 05/26/15 00:14

Benzene ug/L ND 1.0 05/26/15 00:14

Bromobenzene ug/L ND 1.0 05/26/15 00:14

Bromochloromethane ug/L ND 1.0 05/26/15 00:14

Bromodichloromethane ug/L ND 1.0 05/26/15 00:14

Bromoform ug/L ND 4.0 05/26/15 00:14

Bromomethane ug/L ND 10.0 05/26/15 00:14

Carbon tetrachloride ug/L ND 1.0 05/26/15 00:14

Chlorobenzene ug/L ND 1.0 05/26/15 00:14

Chloroethane ug/L ND 1.0 05/26/15 00:14

Chloroform ug/L ND 1.0 05/26/15 00:14

Chloromethane ug/L ND 4.0 05/26/15 00:14

cis-1,2-Dichloroethene ug/L ND 1.0 05/26/15 00:14

cis-1,3-Dichloropropene ug/L ND 4.0 05/26/15 00:14







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Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Dibromochloromethane ug/L ND 1.0 05/26/15 00:14

Dibromomethane ug/L ND 4.0 05/26/15 00:14

Dichlorodifluoromethane ug/L ND 1.0 05/26/15 00:14

Dichlorofluoromethane ug/L ND 1.0 05/26/15 00:14

Diethyl ether (Ethyl ether) ug/L ND 4.0 05/26/15 00:14


Hexachloro-1,3-butadiene ug/L ND 1.0 05/26/15 00:14

Isopropylbenzene (Cumene) ug/L ND 1.0 05/26/15 00:14

Methyl-tert-butyl ether ug/L ND 1.0 05/26/15 00:14

Methylene Chloride ug/L ND 4.0 05/26/15 00:14

n-Butylbenzene ug/L ND 1.0 05/26/15 00:14

n-Propylbenzene ug/L ND 1.0 05/26/15 00:14

Naphthalene ug/L ND 4.0 05/26/15 00:14

p-Isopropyltoluene ug/L ND 1.0 05/26/15 00:14

sec-Butylbenzene ug/L ND 1.0 05/26/15 00:14

Styrene ug/L ND 1.0 05/26/15 00:14

tert-Butylbenzene ug/L ND 1.0 05/26/15 00:14

Tetrachloroethene ug/L ND 1.0 05/26/15 00:14

Tetrahydrofuran ug/L ND 10.0 05/26/15 00:14

Toluene ug/L ND 1.0 05/26/15 00:14

trans-1,2-Dichloroethene ug/L ND 1.0 05/26/15 00:14

trans-1,3-Dichloropropene ug/L ND 4.0 05/26/15 00:14

Trichloroethene ug/L ND 0.40 05/26/15 00:14

Trichlorofluoromethane ug/L ND 1.0 05/26/15 00:14

Vinyl chloride ug/L ND 1.0 05/26/15 00:14




Toluene-d8 (S) %. 102 75-125 05/26/15 00:14

Parameter Units

LCS

Result

% Rec



LCSSpike





1,1,2-Trichlorotrifluoroethane ug/L 14.320 71 60-135


1,1-Dichloroethene ug/L 15.620 78 68-125

1,1-Dichloropropene ug/L 18.020 90 74-125


1,2,3-Trichloropropane ug/L 18.320 91 75-125








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10307337



Parameter Units

LCS

Result

% Rec



LCSSpike


1,2-Dibromo-3-chloropropane ug/L 50.850 102 65-145

1,2-Dibromoethane (EDB) ug/L 18.420 92 75-125









2-Butanone (MEK) ug/L 97.4100 97 63-130



4-Methyl-2-pentanone (MIBK) ug/L 97.3100 97 71-126

Acetone ug/L 102100 102 69-131

Allyl chloride ug/L 19.120 95 67-125

Benzene ug/L 17.020 85 71-125

Bromobenzene ug/L 20.220 101 75-125

Bromochloromethane ug/L 19.220 96 75-125

Bromodichloromethane ug/L 16.820 84 75-125

Bromoform ug/L 19.220 96 70-125

Bromomethane ug/L 12.020 60 30-150

Carbon tetrachloride ug/L 15.620 78 75-126

Chlorobenzene ug/L 20.520 103 75-125

Chloroethane ug/L 17.920 89 65-134

Chloroform ug/L 17.720 89 75-125

Chloromethane ug/L 13.220 66 39-150

cis-1,2-Dichloroethene ug/L 17.720 89 72-125

cis-1,3-Dichloropropene ug/L 17.720 88 75-125

Dibromochloromethane ug/L 20.020 100 75-125

Dibromomethane ug/L 19.420 97 75-125

Dichlorodifluoromethane ug/L 15.420 77 50-134

Dichlorofluoromethane ug/L 16.420 82 69-125

Diethyl ether (Ethyl ether) ug/L 17.320 87 72-125

Ethylbenzene ug/L 17.720 89 75-125

Hexachloro-1,3-butadiene ug/L 19.620 98 70-138

Isopropylbenzene (Cumene) ug/L 18.420 92 75-125

Methyl-tert-butyl ether ug/L 18.420 92 73-125

Methylene Chloride ug/L 19.020 95 73-125

n-Butylbenzene ug/L 17.020 85 72-133

n-Propylbenzene ug/L 18.620 93 72-126

Naphthalene ug/L 23.220 116 70-127

p-Isopropyltoluene ug/L 19.220 96 72-132

sec-Butylbenzene ug/L 19.520 98 73-132

Styrene ug/L 20.420 102 75-125

tert-Butylbenzene ug/L 16.920 84 73-128







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Parameter Units

LCS

Result

% Rec



LCSSpike

Tetrachloroethene ug/L 18.020 90 74-125

Tetrahydrofuran ug/L 219200 109 62-133

Toluene ug/L 18.620 93 74-125

trans-1,2-Dichloroethene ug/L 15.620 78 69-125

trans-1,3-Dichloropropene ug/L 17.220 86 75-125

Trichloroethene ug/L 18.020 90 75-125

Trichlorofluoromethane ug/L 16.420 82 74-127

Vinyl chloride ug/L 16.220 81 66-132

Xylene (Total) ug/L 54.560 91 75-125



Toluene-d8 (S) %. 99 75-125

Parameter Units

MS

Result

% Rec



MSSpike

Result

10306438008

1975163

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

1,1,1,2-Tetrachloroethane ug/L 20 97 70-13894 3 3020ND 19.5 18.8

1,1,1-Trichloroethane ug/L 20 102 55-150105 3 3020ND 20.4 21.0

1,1,2,2-Tetrachloroethane ug/L 20 103 64-140112 9 3020ND 20.6 22.5

1,1,2-Trichloroethane ug/L 20 90 67-13796 6 3020ND 18.1 19.2

1,1,2-Trichlorotrifluoroethane ug/L 20 91 51-15098 8 3020ND 18.1 19.6

1,1-Dichloroethane ug/L 20 103 49-15097 6 3020ND 20.7 19.4

1,1-Dichloroethene ug/L 20 89 40-150104 15 3020ND 17.8 20.7

1,1-Dichloropropene ug/L 20 101 50-15098 3 3020ND 20.1 19.6

1,2,3-Trichlorobenzene ug/L 20 101 59-14898 3 3020ND 20.1 19.6

1,2,3-Trichloropropane ug/L 20 96 65-14190 6 3020ND 19.1 18.0

1,2,4-Trichlorobenzene ug/L 20 100 61-140105 5 3020ND 19.9 21.0

1,2,4-Trimethylbenzene ug/L 20 98 58-141101 3 3020ND 19.6 20.2

1,2-Dibromo-3-chloropropane

ug/L 50 92 53-150103 12 3050ND 45.8 51.5

1,2-Dibromoethane (EDB) ug/L 20 95 65-13791 5 3020ND 19.1 18.2

1,2-Dichlorobenzene ug/L 20 92 66-13397 5 3020ND 18.5 19.5

1,2-Dichloroethane ug/L 20 91 54-13884 8 3020ND 18.2 16.8

1,2-Dichloropropane ug/L 20 106 62-138110 3 3020ND 21.3 21.9

1,3,5-Trimethylbenzene ug/L 20 95 58-14098 3 3020ND 19.0 19.5





2-Butanone (MEK) ug/L 100 90 51-14797 8 30100ND 89.7 97.2

2-Chlorotoluene ug/L 20 96 58-147102 6 3020ND 19.1 20.3

4-Chlorotoluene ug/L 20 102 64-138106 4 3020ND 20.4 21.2

4-Methyl-2-pentanone(MIBK)

ug/L 100 93 59-143102 9 30100ND 92.8 102

Acetone ug/L 100 142 63-147129 9 30100ND 142 129







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Parameter Units

MS

Result

% Rec



MSSpike

Result

10306438008

1975163

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Allyl chloride ug/L 20 95 45-15099 4 3020ND 18.9 19.8

Benzene ug/L 20 94 53-13992 1 3020ND 18.7 18.4

Bromobenzene ug/L 20 105 66-136107 2 3020ND 21.0 21.5

Bromochloromethane ug/L 20 98 64-136107 9 3020ND 19.6 21.5

Bromodichloromethane ug/L 20 86 66-13895 10 3020ND 17.1 18.9

Bromoform ug/L 20 97 59-13699 3 3020ND 19.3 19.9

Bromomethane ug/L 20 61 30-15079 26 3020ND 12.2 15.8

Carbon tetrachloride ug/L 20 98 56-15098 0 3020ND 19.6 19.5

Chlorobenzene ug/L 20 104 65-13396 7 3020ND 20.8 19.3

Chloroethane ug/L 20 97 48-150116 18 3020ND 19.4 23.2

Chloroform ug/L 20 103 57-145104 2 3020ND 20.5 20.9

Chloromethane ug/L 20 78 30-15082 6 3020ND 15.5 16.5

cis-1,2-Dichloroethene ug/L 20 95 49-150100 5 3020ND 19.1 20.1

cis-1,3-Dichloropropene ug/L 20 95 64-13089 6 3020ND 19.0 17.9

Dibromochloromethane ug/L 20 100 68-138109 8 3020ND 20.0 21.7

Dibromomethane ug/L 20 100 67-13494 6 3020ND 20.0 18.8

Dichlorodifluoromethane ug/L 20 93 45-15096 3 3020ND 18.7 19.2

Dichlorofluoromethane ug/L 20 98 54-15093 5 3020ND 19.6 18.7

Diethyl ether (Ethyl ether) ug/L 20 94 50-14593 1 3020ND 18.7 18.6

Ethylbenzene ug/L 20 97 55-139100 3 3020ND 19.5 20.1

Hexachloro-1,3-butadiene ug/L 20 103 49-150115 12 3020ND 20.5 23.1

Isopropylbenzene (Cumene) ug/L 20 98 64-142105 6 3020ND 19.7 21.0

Methyl-tert-butyl ether ug/L 20 93 62-12992 1 3020ND 18.6 18.4

Methylene Chloride ug/L 20 98 57-13291 7 3020ND 19.5 18.2

n-Butylbenzene ug/L 20 100 55-15098 2 3020ND 20.1 19.6

n-Propylbenzene ug/L 20 102 59-142106 4 3020ND 20.4 21.2

Naphthalene ug/L 20 108 51-150113 5 3020ND 21.6 22.6

p-Isopropyltoluene ug/L 20 106 60-149113 6 3020ND 21.3 22.5

sec-Butylbenzene ug/L 20 100 60-150104 4 3020ND 20.0 20.7

Styrene ug/L 20 106 68-134106 1 3020ND 21.1 21.3

tert-Butylbenzene ug/L 20 95 62-146101 7 3020ND 18.9 20.3

Tetrachloroethene ug/L 20 93 50-150101 8 3020ND 18.6 20.1

Tetrahydrofuran ug/L 200 122 59-145114 7 30200ND 244 229

Toluene ug/L 20 99 52-14898 2 3020ND 19.9 19.5

trans-1,2-Dichloroethene ug/L 20 85 45-15090 5 3020ND 17.1 18.1

trans-1,3-Dichloropropene ug/L 20 88 68-13297 10 3020ND 17.6 19.4

Trichloroethene ug/L 20 98 52-150101 4 3020ND 19.5 20.2

Trichlorofluoromethane ug/L 20 87 55-150100 13 3020ND 17.5 19.9

Vinyl chloride ug/L 20 109 43-150117 7 3020ND 21.8 23.4

Xylene (Total) ug/L 60 100 54-144101 1 3060ND 60.2 60.9



Toluene-d8 (S) %. 103 75-12599







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#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


OEXT/29323

EPA 3550

EPA 8270D by SIM



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed









Chrysene mg/kg ND 0.010 05/28/15 18:20



Fluorene mg/kg ND 0.010 05/28/15 18:20




Pyrene mg/kg ND 0.010 05/28/15 18:20


p-Terphenyl-d14 (S) %. 81 30-150 05/28/15 18:20

Parameter Units

LCS

Result

% Rec



LCSSpike



Anthracene mg/kg 0.031.033 92 61-125






Chrysene mg/kg 0.028.033 84 63-125



Fluorene mg/kg 0.029.033 87 57-125




Pyrene mg/kg 0.031.033 93 63-125







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Parameter Units

LCS

Result

% Rec



LCSSpike


p-Terphenyl-d14 (S) %. 80 30-150

Parameter Units

MS

Result

% Rec



MSSpike

Result

10307150001

1977124

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.









Chrysene mg/kg .04 80 30-15076 6 30.04ND 0.032 0.030


Fluoranthene mg/kg .04 93 30-15085 9 30.04ND 0.037 0.034

Fluorene mg/kg .04 87 30-14682 5 30.04ND 0.035 0.033




Pyrene mg/kg .04 92 30-15085 8 30.04ND 0.037 0.034


p-Terphenyl-d14 (S) %. 71 30-15071







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#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


OEXT/29342

WI MOD DRO

WI MOD DRO

WIDRO Solid GCV


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Solid

Analyzed

WDRO C10-C28 mg/kg ND 10.0 05/29/15 09:33

n-Triacontane (S) %. 91 30-143 05/29/15 09:33

Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1978121

WDRO C10-C28 mg/kg 69.080 86 64-1259072.0 4 20








(612)607-1700

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#=QC#


Pace Project No.:

Project:

10307337



QC Batch:

QC Batch Method:

Analysis Method:


OEXT/29307

WI MOD DRO

WI MOD DRO

WIDRO GCS w/Cleanup


Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

WDRO C10-C28 mg/L ND 0.10 05/28/15 12:14

n-Triacontane (S) %. 80 62-125 05/28/15 12:14

Parameter Units

LCS

Result

% Rec



LCSSpike LCSD

% Rec RPD

Max

RPD

LCSD

Result

1976566

WDRO C10-C28 mg/L 1.42 71 54-125771.5 8 20








(612)607-1700

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#=QL#

QUALIFIERS

Pace Project No.:

Project:

10307337


DEFINITIONS







S - Surrogate













WORKORDER QUALIFIERS

WO: 10307337

This report was revised on July 1, 2015 to add TCLP Lead to sample 004.[1]

ANALYTE QUALIFIERS

Result confirmed by second analysis.C0

The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biasedhigh.

CH

Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0

Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0

Sample field preservation does not meet EPA or method recommendations for this analysis.P4

Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from samplere-analysis).

S2

High boiling point hydrocarbons are present in the sample.T6

Post-analysis pH measurement indicates insufficient VOA sample preservation.pH







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#=CR#


Pace Project No.:

Project:

10307337



Analytical

Batch

10307337005 OEXT/29342 GCSV/15797LPG-35/6-8 WI MOD DRO WI MOD DRO








10307337005 GCV/13777 GCV/13785LPG-35/6-8 EPA 5030 Medium Soil WI MOD GRO





10307337013 GCV/13776LPG-41/19-22 WI MOD GRO

10307337017 GCV/13776LPG-44/19-22 WI MOD GRO

10307337019 GCV/13776LPG-45/12-20 WI MOD GRO

10307337004 MPRP/55531 ICP/24329LPG-34/2-4 EPA 3010 EPA 6010C














10307337001 MERP/13661 MERC/15908LPG-31/1-3 EPA 7471B EPA 7471B













10307337001 MPRP/54713LPG-31/1-3 ASTM D2974

10307337002 MPRP/54713LPG-32/2-4 ASTM D2974







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Pace Project No.:

Project:

10307337



Analytical

Batch

10307337003 MPRP/54734LPG-33/2-4 ASTM D2974

10307337004 MPRP/54734LPG-34/2-4 ASTM D2974

10307337005 MPRP/54734LPG-35/6-8 ASTM D2974

10307337006 MPRP/54734LPG-36/10-12 ASTM D2974

10307337007 MPRP/54734LPG-36/18-20 ASTM D2974

10307337008 MPRP/54734LPG-37/2-4 ASTM D2974

10307337009 MPRP/54734LPG-38/4-6 ASTM D2974

10307337010 MPRP/54734LPG-39/1-3 ASTM D2974

10307337011 MPRP/54734LPG-40/2-4 ASTM D2974

10307337012 MPRP/54734LPG-41/2-4 ASTM D2974

10307337014 MPRP/54734LPG-42/1-3 ASTM D2974

10307337015 MPRP/54734LPG-43/4-6 ASTM D2974

10307337016 MPRP/54734LPG-44/5-7 ASTM D2974

10307337018 MPRP/54734LPG-45/8-10 ASTM D2974

10307337001 OEXT/29323 MSSV/12419LPG-31/1-3 EPA 3550 EPA 8270D by SIM













10307337005 MSV/31586 MSV/31600LPG-35/6-8 EPA 5035/5030B EPA 8260B





10307337013 MSV/31527LPG-41/19-22 EPA 8260B

10307337017 MSV/31527LPG-44/19-22 EPA 8260B

10307337019 MSV/31527LPG-45/12-20 EPA 8260B

10307337020 MSV/31527TRIP BLANK EPA 8260B







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