Page 1 of 56 - NRC: Home Page · Page 1 of 56 Erin Trent for. Certificates of Analysis and QC...

November 14, 2014 Mr. Gregory Hisel St. Francis Hospital 62 Kibbe Rd Ellington, Connecticut 06029 Re: Total Activity Wipes Work Order: 359240 Dear Mr. Hisel:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for thesample(s) we received on October 16, 2014. This original data report has been prepared and reviewed inaccordance with GEL’s standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needson time every time. We trust that you will find everything in order and to your satisfaction. If you have anyquestions, please do not hesitate to call me at (843) 556-8171, ext. 4443.

Sincerely, PM_SIGN_HERE Lindsay Fabra Project Manager

Purchase Order: 0100320614 Enclosures

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Erin Trent for

Certificates of Analysisand QC Summary

of 56

Reviewed by USER_SIGN_HERE

GEL LABORATORIES LLC2040 Savage Road Charleston SC 29407 − (843) 556−8171 − www.gel.com

Certificate of Analysis Report

STFR001 St. Francis Hospital

Client SDG: 359240 GEL Work Order: 359240

Where the analytical method has been performed under NELAP certification, the analysis has met all of therequirements of the NELAC standard unless qualified on the Certificate of Analysis.

The designation ND, if present, appears in the result column when the analyte concentration is not detected abovethe limit as defined in the ’U’ qualifier above.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLCstandard operating procedures. Please direct any questions to your Project Manager, Lindsay Fabra.

The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a Tracer compound** Analyte is a surrogate compoundU Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

for

of 56

Certificate of Analysis

GEL LABORATORIES LLC2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com

Report Date: November 14, 2014

Rad Liquid Scintillation Analysis

Parameter Result UnitsQualifier Analyst Date Time

14309740841pCi/Filter 10/29/14GXR15.00

DF

Mr. Gregory Hisel Contact:

St. Francis HospitalCompany :62 Kibbe Rd

Ellington, Connecticut 06029

Address :

Total Activity WipesProject:

359240001Filter12-OCT-14 15:0016-OCT-14

S-3-2 STFR00100Project:STFR001Client ID:

Client

+/-1.40

Sample ID:

Receive Date:

Client Sample ID:

Matrix:Collect Date:

Collector:

Batch

2.45

Method

The following Analytical Methods were performed:

1Method Description

1

GL-RAD-A-041Analyst Comments

UTotal ActivityLiquid Scint. Total activity "As Received"

Uncertainty

-0.108

RLMDC

Notes:Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

of 56






14309740857pCi/Filter 10/29/14GXR15.00

DF




Address :


359240002Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.40

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.0531

RLMDC


of 56






14309740913pCi/Filter 10/29/14GXR15.00

DF




Address :


359240003Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.40

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.15

RLMDC


of 56






14309740930pCi/Filter 10/29/14GXR15.00

DF




Address :


359240004Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.39

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.253

RLMDC


of 56






14309740946pCi/Filter 10/29/14GXR15.00

DF




Address :


359240005Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.36

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-1.01

RLMDC


of 56






14309741002pCi/Filter 10/29/14GXR15.00

DF




Address :


359240006Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.39

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.335

RLMDC


of 56






14309741018pCi/Filter 10/29/14GXR15.00

DF




Address :


359240007Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.42

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

0.362

RLMDC


of 56






14309741034pCi/Filter 10/29/14GXR15.00

DF




Address :


359240008Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.40

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.46

Method


1Method Description

1



Uncertainty

-0.185

RLMDC


of 56






14309741050pCi/Filter 10/29/14GXR15.00

DF




Address :


359240009Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.36

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.932

RLMDC


of 56






14309741106pCi/Filter 10/29/14GXR15.00

DF




Address :


359240010Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.41

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

0.123

RLMDC


of 56






14309741123pCi/Filter 10/29/14GXR15.00

DF




Address :


359240011Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.41

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

0.282

RLMDC


of 56






14309741139pCi/Filter 10/29/14GXR15.00

DF




Address :


359240012Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.47

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.46

Method


1Method Description

1



Uncertainty

1.53

RLMDC


of 56






14309741155pCi/Filter 10/29/14GXR15.00

DF




Address :


359240013Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.40

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.0581

RLMDC


of 56






14309741211pCi/Filter 10/29/14GXR15.00

DF




Address :


359240014Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.41

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.46

Method


1Method Description

1



Uncertainty

-0.00992

RLMDC


of 56






14309741227pCi/Filter 10/29/14GXR15.00

DF




Address :


359240015Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.41

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.46

Method


1Method Description

1



Uncertainty

0.0582

RLMDC


of 56






14309741243pCi/Filter 10/29/14GXR15.00

DF




Address :


359240016Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.40

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.46

Method


1Method Description

1



Uncertainty

-0.176

RLMDC


of 56






14309741259pCi/Filter 10/29/14GXR15.00

DF




Address :


359240017Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.38

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.535

RLMDC


of 56






14309741316pCi/Filter 10/29/14GXR15.00

DF




Address :


359240018Filter12-OCT-14 15:0016-OCT-14


Client

+/-1.42

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

0.397

RLMDC


of 56






14309741332pCi/Filter 10/29/14GXR15.00

DF




Address :


359240019Filter12-OCT-14 15:3016-OCT-14


Client

+/-1.36

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.45

Method


1Method Description

1



Uncertainty

-0.797

RLMDC


of 56






14309741348pCi/Filter 10/29/14GXR15.00

DF




Address :


359240020Filter12-OCT-14 15:3016-OCT-14


Client

+/-1.41

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

2.46

Method


1Method Description

1



Uncertainty

0.0296

RLMDC


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14309750401pCi/Filter 10/29/14GXR15.00

DF




Address :


359240021Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.16

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.580

RLMDC


of 56






14309750417pCi/Filter 10/29/14GXR15.00

DF




Address :


359240022Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.14

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

-0.0165

RLMDC


of 56






14309750433pCi/Filter 10/29/14GXR15.00

DF




Address :


359240023Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.13

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

-0.376

RLMDC


of 56






14309750450pCi/Filter 10/29/14GXR15.00

DF




Address :


359240024Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.11

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

-1.11

RLMDC


of 56






14309750506pCi/Filter 10/29/14GXR15.00

DF




Address :


359240025Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.14

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.71

Method


1Method Description

1



Uncertainty

-0.206

RLMDC


of 56






14309750522pCi/Filter 10/29/14GXR15.00

DF




Address :


359240026Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.20

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

2.01

RLMDC


of 56






14309750538pCi/Filter 10/29/14GXR15.00

DF




Address :


359240027Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.16

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.478

RLMDC


of 56






14309750555pCi/Filter 10/29/14GXR15.00

DF




Address :


359240028Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.14

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

-0.169

RLMDC


of 56






14309750611pCi/Filter 10/29/14GXR15.00

DF




Address :


359240029Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.13

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

-0.145

RLMDC


of 56






14309750627pCi/Filter 10/29/14GXR15.00

DF




Address :


359240030Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.14

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.0165

RLMDC


of 56






14309750644pCi/Filter 10/29/14GXR15.00

DF




Address :


359240031Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.18

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

1.52

RLMDC


of 56






14309750700pCi/Filter 10/29/14GXR15.00

DF




Address :


359240032Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.15

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.180

RLMDC


of 56






14309750717pCi/Filter 10/29/14GXR15.00

DF




Address :


359240033Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.14

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.169

RLMDC


of 56






14309750733pCi/Filter 10/29/14GXR15.00

DF




Address :


359240034Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.17

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.890

RLMDC


of 56






14309750749pCi/Filter 10/29/14GXR15.00

DF




Address :


359240035Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.08

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

-2.05

RLMDC


of 56






14309750805pCi/Filter 10/29/14GXR15.00

DF




Address :


359240036Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.13

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

-0.414

RLMDC


of 56






14309750822pCi/Filter 10/29/14GXR15.00

DF




Address :


359240037Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.16

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.812

RLMDC


of 56






14309750838pCi/Filter 10/29/14GXR15.00

DF




Address :


359240038Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.15

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.235

RLMDC


of 56






14309750854pCi/Filter 10/29/14GXR15.00

DF




Address :


359240039Filter12-OCT-14 15:3016-OCT-14


Client

+/-2.15

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.69

Method


1Method Description

1



Uncertainty

0.258

RLMDC


of 56






14309750911pCi/Filter 10/29/14GXR15.00

DF




Address :


359240040Filter12-OCT-14 16:0016-OCT-14


Client

+/-2.17

Sample ID:

Receive Date:

Client Sample ID:


Collector:

Batch

3.70

Method


1Method Description

1



Uncertainty

0.639

RLMDC


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QC Summary

GEL LABORATORIES LLC2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com

Rad Liquid Scintillation1430974

1430975

Batch

Batch

Total Activity

Total Activity

Total Activity

Total Activity

Total Activity

Total Activity

Parmname


St. Francis Hospital62 Kibbe RdEllington, Connecticut

November 14, 2014Report Date:

Units

pCi/Filter

pCi/Filter

pCi/Filter

pCi/Filter

pCi/Filter

pCi/Filter

Anlst Date Time

GXR1

GXR1

10/29/14 14:20

10/29/14 14:36

10/29/14 14:04

10/29/14 09:43

10/29/14 10:00

10/29/14 09:27

QC

84.4

85.2

-0.454

86.6

83.9

0.371

NOM Sample Range

(75%-125%)

(0%-20%)

(75%-125%)

(0%-20%)

Qual

U

U

QC1203196641

QC1203196642

QC1203196640

QC1203196645

QC1203196646

QC1203196644

The Qualifiers in this report are defined as follows:

1.00

3.16

REC%

97.1

98.1

99.6

96.5

86.9

86.9

86.9

86.9

LCS

LCSD

MB

LCS

LCSD

MB

359240Workorder:

**

<

>

BD

FA

H

J

K

L

M

M

N/A

N1

ND

NJ

Analyte is a Tracer compound

Result is less than value reported

Result is greater than value reported

Results are either below the MDC or tracer recovery is low

Failed analysis.

Analytical holding time was exceeded

Value is estimated

Analyte present. Reported value may be biased high. Actual value is expected to be lower.

Analyte present. Reported value may be biased low. Actual value is expected to be higher.

M if above MDC and less than LLD

REMP Result > MDC/CL and < RDL

RPD or %Recovery limits do not apply.

See case narrative

Analyte concentration is not detected above the detection limit

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

+/-3.51

+/-3.53

+/-1.39

+/-3.90

+/-3.86

+/-2.14

RPD%

Uncertainty

Uncertainty

Uncertainty

Uncertainty

Uncertainty

Uncertainty

Notes:

Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Page 1 of 2

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QC Summary

GEL LABORATORIES LLC2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com

Parmname

Page 2 of 2

Units Anlst Date TimeQCNOM Sample RangeQual REC%

359240Workorder:

Q

R

U

UI

UJ

UL

X

Y

^

h

One or more quality control criteria have not been met. Refer to the applicable narrative or DER.

Sample results are rejected

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Gamma Spectroscopy--Uncertain identification

Gamma Spectroscopy--Uncertain identification

Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

Other specific qualifiers were required to properly define the results. Consult case narrative.

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

Preparation or preservation holding time was exceeded

N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater thanfive times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- theRL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of therequirements of the NELAC standard unless qualified on the QC Summary.

RPD%

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Chain of Custody andSupporting

Documentation

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Data Package QualifierDefinitions

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Data Review Qualifier Definitions

Qualifier Explanation

* A quality control analyte recovery is outside of specified acceptance criteria

** Analyte is a surrogate compound

< Result is less than value reported

> Result is greater than value reported

^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL

A The TIC is a suspected aldol-condensation product

B Target analyte was detected in the associated blank

B Metals-Either presence of analyte detected in the associated blank, or

MDL/IDL < sample value < PQL

BD Results are either below the MDC or tracer recovery is low

C Analyte has been confirmed by GC/MS analysis

D Results are reported from a diluted aliquot of the sample

d 5-day BOD-The 2:1 depletion requirement was not met for this sample

E Organics-Concentration of the target analyte exceeds the instrument calibration range

E Metals-%difference of sample and SD is >10%. Sample concentration must meet flagging criteria

H Analytical holding time was exceeded

h Preparation or preservation holding time was exceeded

J Value is estimated

N Metals-The Matrix spike sample recovery is not within specified control limits

N Organics-Presumptive evidence based on mass spectral library search to make a tentative

identification of the analyte (TIC). Quantitation is based on nearest internal standard

response factor

N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration

by 4X or more

ND Analyte concentration is not detected above the reporting limit

UI Gamma Spectroscopy-Uncertain identification

X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

Y QC Samples were not spiked with this compound

Z Paint Filter Test-Particulates passed through the filter, however no free liquids were observed.

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P Organics-The concentrations between the primary and confirmation columns/detectors is >40% difference.

For HPLC, the difference is >70%.

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

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LaboratoryCertifications

of 56

State CertificationAlaska

ArkansasCLIA

California NELAPColorado

ConnecticutDelaware

DoD ELAP/ ISO17025 A2LAFlorida NELAP

Foreign Soils PermitGeorgia

Georgia SDWAHawaii

Idaho ChemistryIdaho Radiochemistry

Illinois NELAPIndiana

Kansas NELAPKentucky

Louisiana NELAPLouisiana SDWA

MarylandMassachusetts

MichiganMississippiNebraskaNevada

New Hampshire NELAPNew Jersey NELAP

New MexicoNew York NELAP

North CarolinaNorth Carolina SDWA

OklahomaPennsylvania NELAPPlant Material Permit

South Carolina ChemistrySouth Carolina GVL

South Carolina RadiochemiTennessee

Texas NELAPUtah NELAP

VermontVirginia NELAP

WashingtonWisconsin

UST−11088−0651

42D090404601151CASC00012PH−0169

SC000122013−102567.01E87156

P330−12−00283, P330−12−00284SC00012

967SC000122013−10

SC00012SC00012200029

C−SC−01E−10332

9012903046 (AI33904)

LA130005270

M−SC0129976

SC000122013−10NE−OS−26−13SC000122014−1

2054SC002

SC0001211501233

457099904

68−00485PDEP−12−00260

101200012361100110120002TN 02934

T104704235−14−9SC000122014−16

VT87156460202

C780−12999887790

List of current GEL Certifications as of 14 November 2014

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