Pacheco_CV_Feb2017

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Carlos Pacheco

Address: 14 Chemistry Building Office: 814-863-1182 Pennsylvania State University/University Park Cell: 609-240-5957

Department of Chemistry E-mail: [email protected] State College, PA 16802 E-mail: [email protected]

Webpage (work): http://sites.psu.edu/nmrlaboratorypsu/;

Webpages (personal): www.linkedin.com/in/carlospacheco08540; http://cpacheco223.com/.

ResearcherID: A-2324-2015 ORCID ID: orcid.org/0000-0002-5607-5517

Table of Contents Education...................................................................................................................................................................1

Professional Experience ..............................................................................................................................................2

Publications................................................................................................................................................................2

Conference Proceedings .............................................................................................................................................5

Presentations .............................................................................................................................................................5

Service, Projects, Miscellaneous ..................................................................................................................................7

Technical Communications..........................................................................................................................................9

Courses, Training: Presentations................................................................................................................................ 11

Graduate Research, Undergraduate internship........................................................................................................... 12

Meetings: Participation ........................................................................................................................................... 13

Professional Visits..................................................................................................................................................... 16

Courses: Participation ............................................................................................................................................... 16

Participation in Theses Committees, Editorial Boards, Committees .............................................................................. 18

Participation and Affiliation in Scientific Societies, Professional Associations, Synergistic Activities, Consultancies ......... 19

Awards .................................................................................................................................................................... 19

Knowledge of Languages ........................................................................................................................................... 19

Education

Ph.D. in Chemistry, Nuclear Magnetic Resonance, Department of Chemistry, University of

Rhode Island, Rhode Island, USA, 1993-1996, supervision of Prof. Daniel D. Traficante.

mailto:[email protected]

mailto:[email protected]

http://sites.psu.edu/nmrlaboratorypsu/

http://www.linkedin.com/in/carlospacheco08540

http://cpacheco223.com/

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M.S. in Chemical Engineering, Thermodynamics, Graduate Studies in Engineering (COPPE), Federal University of Rio de Janeiro, Rio de Janeiro, Brazil, 1983-1986, supervision of Prof. Angela

M. C. Uller. B.Sc. in Chemical Engineering, School of Chemistry, Federal University of Rio de Janeiro, Rio

de Janeiro, Brazil, 1979-1983.

Professional Experience 2014-present: NMR Spectroscopist at Pennsylvania State University/Chemistry, State College, PA. 2012-2013: NMR Laboratory Manager at University of Connecticut/Chemistry, Storrs, CT. 2000-2011: NMR Laboratory Manager at Princeton University/Chemistry, Princeton, NJ.

1997-1999: Manager of the Nuclear Magnetic Resonance (NMR) Laboratory of the Chemistry Department, PETROBRAS R&D Center, Rio de Janeiro, Brazil.

1993-1996: Ph.D. studies at the University of Rhode Island, RI. 1990-1992: Manager of the Spectroscopy Laboratory (FTIR and UV-VIS) of the Chemistry Department, PETROBRAS R&D Center, Rio de Janeiro, Brazil. 1986-1990: Manager of the Spectrometry Laboratory (FTIR, UV-VIS, NMR) of the Chemistry Department, PETROBRAS R&D Center, Rio de Janeiro, Brazil. 1984-1984: Lecturer of “Organic Processes in Chemical Engineering”, Department of Chemistry, Military Institute of Engineering, Rio de Janeiro, Brazil.

Note: Courses, conferences, publications, and lectures whose titles were originally in Portuguese and translated into

English are indicated with (P).

Publications Ph.D. Dissertation

“The Use of Inverse Detected NMR for the Analyses of Diesel Oil Extracts” University of Rhode Island, Kingston, Rhode Island, USA, 1996. Advisor: Prof. Daniel D. Traficante.

Book Chapters

Morgado Jr., E.; Pacheco, C., and Menezes, S. M. C. “NMR Studies of Colloidal Oxides” Book

Chapter in Surfaces of Nanoparticles and Porous Materials, Series Surfactant Science Series, v78, Eds. Schwarz, J. A., and Contescu, C. I. Marcel Dekker editor, NY, USA, 1999. ISBN: 0-8247-1933-

6.

Pacheco, C., Teixeira, M. A. G.; Faria, F.; Cardoso, R.; and Gonçalves, M. L. Book Chapter “Chemical Characterization of Asphaltenes and Paraffin Waxes”, In Asphaltenes and Waxes. Their

Study and Control for Crude Oil Production, International Symposium on Colloid Chemistry in Oil Production (by Taylor and Francis Group and ISCOP ´99, best papers of the 1999 Symposium).

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Articles Silverberg, L. J.; Pacheco, C.; Lagalante, A.; Tierney, J.; Bachert, J.; Bayliff, J. A.; Cali, A. S.; Chen,

L.; Cooper, A. D.; Minehan, M. J.; et al. Synthesis and Spectroscopic Properties of a Series of Novel 2-Aryl-3-Phenyl-2,3-Dihydro-4H-1,3-Benzothiazin-4-Ones. ARKIVOC 2016, (vi), 122–143.

DOI: http://dx.doi.org/10.3998/ark.5550190.p009.875. Wilfong, WC; Kail, BW; Jones, CW; Pacheco, C.; Gray, ML “Spectroscopic Investigation of the

Mechanisms Responsible for the Superior Stability of Hybrid Class 1/Class 2 CO2 Sorbents: A New Class 4 Category”, ACS Applied Materials & Interfaces 2016. Articles ASAP. DOI: 10.1021/acsami.6b02062.

Van Buiten, C.B.; Pacheco, C.; Hatzakis, H.; Elias, RJ “Influence of molecular structure on interactions between tea polyphenols and an immunodominant gluten peptide”, in preparation.

Contro, J.; Pacheco, C.; Nery, JG et al. “Spectroscopic characterization of Vanadosilicates synthesized with 2,6-dimethylpiperidines as structure directing agents”, in preparation.

Curtis, F.; Pacheco, C.; Brown, N. et al. “The Effects of Temperature on Eucalyptus Hardwood Lignin”, in preparation.

Sariola, V.; Pena-Francesch, A.; Jung, H.; Çetinkaya, M.; Pacheco, C.; Sitti, M.; Demirel, M. C. Sci

Rep 2015, 5, 13482. Dey, K.; Pong, F.; Breffke, J.; Pavlick, R.; Hatzakis, E.; Pacheco, C.; Sen, A. Angewandte Chemie

Int Ed Engl 2015, 55 (3), 1113.

Silverberg, L.; Pacheco, C.; Lagalante, A.; Cannon, K.; Bachert, J.; Xie, Y.; Baker, L.; Bayliff, A. Int J Chem 2015, 7 (2).

Pinkerton, N. M.; Gindy, M. E.; Calero-DdelC, V. L.; Wolfson, T.; Pagels, R. F.; Adler, D.; Gao, D.; Li, S.; Wang, R.; Zevon, M.; Yao, N.; Pacheco, C.; Therien, M. J.; Rinaldi, C.; Sinko, P. J.;

Prud’homme, R. K. Adv Healthc Mater 2015, 4 (9), 1376. Samanamu, C.R., Pacheco, C., Angeles-Boza, A. et al. “Homogeneous Catalysis of the

Electrochemical Reduction of CO2 by Re (I) Complexes. Role of the Pyridine Ligands”, submitted to Inorganic Chemistry, 2014.

LaFountain, A.M., Pacheco, C., Prum, R. O. et al. “Nuclear magnetic resonance analysis of carotenoids from the burgundy plumage of the Pompadour Cotinga (Xipholena punicea)”,

Archives of Biochemistry and Biophysics 359(2013),133-141.

Pacheco, C., Sebastião, R.C.O., Braga, J., Virtuoso, L. S., Vello, K., da Silva, L. H.M. “Ion-Polymer

Interaction Analysis: an Inversion of NMR Spin Echo Experimental Data”, Brazilian Journal of Physics 40(2010)423-428.

Pacheco, C., Xu, S., Simmons, G. C., Mahadevan T. S., Scherer, G. W., Garofalini, S. H. “Transport of Water in Small Pores”, Langmuir 25(2009)5084-5090.

Pacheco, C., Fu, L., Prud'homme, R.K. "Translational and Rotational Diffusion of Globular Proteins in Concentrated Polymer Networks." Soft Materials 7(2009)213-231.

Pacheco, C., Deshmukh, A. P., Hay, M., Myneni, S. “Structural environment of carboxyl groups

in natural organic molecules from terrestrial systems. Part 2: 2D NMR spectroscopy” Geochimica et Cosmochimica Acta, 71(2007)3533-3544.

Sebastião, R. C.O., Pacheco, C., Braga J.P., Piló-Veloso, D. “Diffusion Coefficient Distribution from NMR-DOSY Experiments Using Hopfield Neural Network” J Mag. Res., 182(2006)22-28.

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Guo, X., Biehl, R., Pacheco, C., Monkenbusch, M., Richter, D., FU, L., Lin Fu, Prud’homme, R.K. “Diffusion of Protein in Polymer Solutions: A Comparison between Neutron Spin-Echo

Spectroscopy and NMR Measurements Methods” Polymer Preprints, 45(2004)788. Axt, M.; Costa, V. E. U.; Pacheco, C., “The Assignment of Complex 1H and 13C NMR Spectra of

Polycyclic Alcohols by Combination of LIS Methodology and Simple Sequences as APT, COSY and HETCOR” Annals of Magnetic Resonance 1(2-3), 93-101 (2002).

Mao, J.; Pacheco, C.; Traficante, D. D., and Rosen, W. “Identification and Characterization of Nitrogen Compounds in Brazilian Diesel Oil by Particle Beam LC-MS and HPLC-UV” Journal of Liquid Chromatography, v.18, n. 5, p. 903 916, 1995.

Pacheco, C., Traficante, D. D., and Rosen, W. “Analysis of Benzoquinolines and Acridines in Brazilian Diesel Oil by Particle Beam LC-MS.” Mao, J.; Fuel, v. 74, n. 6, pp. 880 887, 1995.

Mao, J.; Pacheco, C., Traficante, D. D., and Rosen, W. “Analysis of Neutral Nitrogen Compounds in Diesel Oil by Direct Injection High-Performance Liquid Chromatography-Mass Spectrometry and Ultraviolet Spectrometry Methods” Journal of Chromatography, v. 684, pp. 103 111, 1994.

Mansur, C. R. E, Lucas, E. F., Pacheco, C., and González, G. “Surfactant/Hydrotrope interaction in aqueous systems by 1H and 13C Nuclear Magnetic Resonance” (P), Química Nova, Feb 2001 (24) 1, 47-54.

Pacheco, C., Pelczer, I., Cheatham, S. “19F as a Probe of Differential Concentration” - The NMR Newsletter, July 2000.

Srivastava, Rajendra Mohan; Da Conceicao Pereira, Maria; Hallwass, Fernando; Pacheco, C. “Synthesis and Molecular Orbital Calculations of N, N-Diethyl-3- [3-(Aryl)-1,2,4- Oxadiazol-5-Yl]

Propionamides”, Heterocycles (1999), 51(12), 2961-2967. Veloso, D. P.; Seidl, P.; Menezes, S. M. C.; Guimarães, A. P.; Marsaioli, A. J.; Villar, J. D. F.;

Vugman, N. V.; Costa, V. E.; Pacheco, C., “Parameters and Symbols to be Used in Nuclear Magnetic Resonance” (P) Quimica Nova, 1999 (July), vol.22 no.4, 622-629.

Souza, C.M.G., Pacheco, C., Tavares, M.I. “Evaluation of EVA/PVAc Blends Behavior by 1-D and 2-D Solid State NMR” Journal of Applied Polymer Science, 1999, 73, 221-226.

Pacheco, C., Tavares, M. I., Souza, C. “2D HETCOR Studies of the Miscibility of EVA/PVAc Blends” Poster and Proceedings of 39th Experimental NMR Conference, Pacific Grove, CA, USA,

March of 1998.

Pacheco, C., and Traficante, D. D. “Two New Window Functions for Long Acquisition Times” Journal of Magnetic Resonance, Series A, 120, 116 120, 1996.

Pacheco, C., “Force Detection Magnetic Resonance” Recent Developments and Perspectives of NMR (P), Special Edition, v. 1, pp. 31 36, 1995.

Articles (with extensive participation, acknowledged)

Zhao, Q., Majsztrik, P., Benziger, J. “Diffusion and Interfacial Transport of Water in Nafion”, J. Phys. Chem. B. 115(2011), 2717–2727. Run the NMR diffusion experiments and discussions of the

results. Mentioned in the Acknowledgments. Barnett, M. P., Pelczer, I. "Pulse Sequence Editing by Symbolic Calculation" Journal of Magnetic

Resonance 204 (2010)189-195. Extensive technical consulting for the publication. Published the programs and documentation at Princeton Chemistry’s NMR lab web-page www.princeton.edu/~nmr/useful_links.htm.

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Marzal, R. M. E., Scherer, G. W. “Crystallization of sodium sulfate salts in limestone” Environ Geol 56(2008)605–621. Discussions of the applicable NMR experiments and results. Run the NMR experiments.

Scherer, G. W., Valenza II, J. J., Simmons, G. “New methods to measure liquid permeability in porous materials” Cement and Concrete Research 37(2007)386–397. Run the NMR experiments

and discussions of the results.

Conference Proceedings Pacheco, C., Guo, X., Li L., Fu, L. Prud'homme, R.K. “Protein Diffusion through Polymer

Meshes as Observed by Pulsed-Field Gradient NMR”, 1st International Conference on

Bioinformatics and Biomedical Engineering. Proceedings, (2007)706-708. Pacheco, C., Fu, L., Pethica, B., Prud'homme, R.K. “Translational and Rotational Diffusion of

Globular Protein in Concentrated Polymer Solutions”. Proceedings of the AIChE 2006 Annual Meeting, San Francisco, CA.

Pacheco, C., Fu, L., Prud’homme, Robert K. “Translational and Rotational Diffusion of a Globular Protein in a Condensed Polymer Matrix”, Published at the book of abstracts at the Eastern Analytical Symposium, November 14-17, 2005, Somerset, New Jersey.

Deshmukh, A., Pacheco, C., Myneni, S. “Carboxyl Structures in Humic Substances”, Proceedings of the 230th ACS National Meeting, in Washington, DC, Aug 28th -Sept 1st, 2005.

(a) Silva, Naira M., Menezes, Sonia M.C., Pacheco, C., “Petroleum Distillates Analysis Using DOSY and DECRA Processing”; (b) Pacheco, C., Detlefsen, D. “CapNMR and Z-SPEC Probes:

Comparing Gradient Performance and Diffusion Results”; (c) Seidel, P., Pacheco, C., “Trends in NMR Spectroscopy: An Update” Proceedings at the 10th Nuclear Magnetic Resonance Users

Meeting/3rd Portuguese-Brazilian NMR Meeting/1st Iberoamerican NMR Meeting, May 9-13,

2005, Rio de Janeiro, Brazil.

Presentations

Pacheco, C. “NMR Pathways”, presentation of candidacy to the NMR Director position and the

PennState NMR Facility, Pennsylvania State University/Chemistry, October 10, 2016.

Pacheco, C.; Pong, F. 4th Penn State Bioinorganic Workshop, June 2 – 10, 2016 – Coordinated the demonstration in laboratory of NMR experiments performed in Paramagnetic Proteins.

Pacheco, C. “Overview of the new solid-state 500-MHz NMR System” – Symposium “Celebration of the new solid-state 500-MHz NMR System”, April 22, 2016.

Silverberg, L.J., Tierney, J., Pacheco, C. et al. “Studies on Cyclic Six- and Seven-Membered 2, 3-Diaryl-1, 3-thiaza-4-ones,” National Meeting of the American Chemical Society, Denver, CO, Mar. 2015.

“The Use of Low-Field NMR In The Oil Industry: From the Characterization of Reservoirs to the Determination of Wax Deposition in the Oil Production”, talk at the NJACS/NMR Topical Group

– NJ, May 16, 2000.

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Pacheco, C., and Rodriguez, M. R. “The Use of Low-Field NMR to Characterize a Reservoir of Complex Lithology: an Example from the Sergipe-Alagoas Basin” (P) Oral presentation at the 5th

Seminar of Analytical Chemistry, Petrobras Research Center, Rio de Janeiro, December 1998. Pacheco, C. Marques, R.G.G. “Average Molecular Parameters of Feedstock and Products in Oil

Industry: a 1H and 13C NMR Approach” (P) Poster presentation at the 5th Analytical Chemistry Seminar, Petrobras R&D Center, Rio de Janeiro, December 1998.

Teixeira, M. A. G, Pacheco, C. Marques, R.G.G., Oliveira, L. B. “New Approach for the Determination of the Average Molecular Parameters of Asphaltenes by 1H and 13C NMR” (P) Poster presentation at the 5th Analytical Chemistry Seminar, Petrobras Research Center, Rio de Janeiro, December of 1998.

Pacheco, C., and Rodriguez, M. R. “The Use of Low-Field NMR to Characterize a Reservoir of Complex Lithology: an Example from the Sergipe-Alagoas Basin” (P) Oral presentation at the 5th

Brazilian Journey of Magnetic Resonance, Campinas, SP, Brazil, August of 1998. Pacheco, C., and Traficante, D. D. “Proton Detected Experiments: 2D Heteronuclear Chemical

Shift at Natural Abundance 15N Level of Diesel Oils Extracts” Poster and Proceedings of the 6 th NMR Meeting (P), organized by the Brazilian NMR Users Association -AUREMN, Angra dos

Reis, Rio de Janeiro, 1997. Pacheco, C. R. N and Traficante, D. D. “Two New Window Functions for Long Acquisition

Times” Poster and Proceedings of the 6th NMR Meeting (P), organized by the Brazilian NMR Users Association -AUREMN, Angra dos Reis, Rio de Janeiro, 1997.

Pacheco, C.; Stewart, L., and Traficante, D. D. “New Window Functions for Truncated FIDs and Long Acquisition Times” Poster and Proceedings of 36th Experimental NMR Conference, Boston, USA, March of 1995.

Ficara, M. L. G.; Pereira, R. C. L., and Pacheco, C., “Evaluation of the Methods for Characterization of Nitrogen Compounds in Oils Fractions” (P) Analytical Chemistry Technical

Meeting (P), Rio de Janeiro, 17f, 1988.

Souza, G. L. M.; Menezes, S. M. C. and Pacheco, C., “Characterization of the Coke Formed on

Used and Regenerated Hydrotreatment Catalysts by Solid State 13C NMR” (P) Iberian-American Symposium of Catalysis, 12, Rio de Janeiro, 1990.

Pacheco, C. Melo, D.L. A.; Farias, J. L., and Concha, F. J. M. “Connection of the Varian EM 360 Model NMR Spectrometer to a HP Mini-Computer” (P) Laboratory Seminar, 8, Rio de Janeiro, pp. 26 42, 1987.

Ficara, M. L. G. and Pacheco, C. R.N “Compatibility Studies of the of Vehicle Membranes with Gasoline Using TGA-FTIR” (P) 7th Automotive Engineering Seminar, Sao Paulo, 1993.

Pacheco, C., “NMR Techniques in Two Dimensions” (P), seminar at the Federal University of Rio de Janeiro (UFRJ)/Chemistry, invited speaker for the Departmental Seminar, December 1999.

Pacheco, C., “NMR Techniques in Two Dimensions” (P), seminar at the Federal University of the State of Rio de Janeiro (UFF)/Chemistry, invited speaker for the Departmental Seminar, November 1999.

Pacheco, C., “Inverse Detected NMR: Applications on Natural Abundance N-15”, Department of Chemistry McGill University, Montréal, Canada, invited speaker for Departmental Seminar,

August of 1998. Pacheco, C., “Applications of Low-Field NMR on the Reservoir Characterization: an Example

from the Sergipe-Alagoas Basin” (P), 5th Brazilian Journey of Magnetic Resonance, Campinas, SP, Brazil, August of 1998.

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Pacheco, C., “Two-Dimensional NMR Techniques: Inverse Detection of 13C and 15N Frequencies” (P), seminar at the Federal University of Pernambuco (UFPE)/Chemistry, invited

speaker for the Departmental Seminar, June 1998. Pacheco, C., “Statistics of the Use of the NMR Spectrometers at Petrobras R&D Center” (P),

presented at the 5th Brazilian Journey of Magnetic Resonance, Campinas, SP, Brazil, August 1998.

Pacheco, C., “Two-Dimensional NMR: Theory and Practical Aspects” (P), seminar at the Polymer Institute, Federal University of Rio de Janeiro (UFRJ), invited speaker for the Graduate Seminar, September 1997.

Pacheco, C., “Statistics of the NMR Spectrometers in Brazil: Status in 1997” (P), presented at the 6th Brazilian NMR Meeting, May 1997.

Pacheco, C., “Proton Detection of 13C and 15N Frequencies at Natural Abundance”, (P), 3rd Brazilian Varian Users Meeting, Le Meridien Hotel, Rio de Janeiro, May 1997.

Pacheco, C., “Inverse Detection of 15N in NMR: An Alternative Approach for the Characterization of Nitrogen-Rich Diesel Extracts”, (P), PETROBRAS R&D Center, Departmental lecture on the Doctoral research, March 1997.

“Pacheco, C., The Use of Inverse Detected NMR For The Analyses of Diesel Oil Extracts”, Doctoral Dissertation Oral Examination, December of 1996; Graduate Seminar, Department of Chemistry, University of Rhode Island, USA, November of 1996.

Pacheco, C., “Force Detection Microscopy using NMR”, Graduate Seminar, Department of Chemistry at the University of Rhode Island, USA, April 1995.

Pacheco, C., “TG-FTIR”, (P), 1st National Meeting of FTIR Users, Rio de Janeiro, October 1992.

Service, Projects, Miscellaneous

Project: Organization of the “Penn State’s ssNMR Symposium” to celebrate the installation of the new 500-MHz console at the NMR Facility, April 22, 2016 (http://sites.psu.edu/nmrlaboratorypsu/news-and-events/).

Featured speakers: - Prof. Tatyana Polenova, Department of Chemistry and Biochemistry, University of

Delaware “Magic Angle Spinning NMR: A Versatile Technique for Analysis of Inorganic and Biological Materials”;

- Dr. Bernie O'Hare, Bruker BioSpin “Solid State NMR with Bruker: Materials, fast-MAS, and Beyond”;

- Prof. Karl T. Mueller, Department of Chemistry, PennState University “NMR for the Characterization of Complex Materials: From Plant Cell Walls to Batteries”.

Contacted and gathered sponsors for the event; Divulged it at several places: AMMRL (NMR managers list), NJ ACS North Jersey/NMR

Topical Group list, direct contacted Research Groups that will benefit from this new capability at the NMR Facility, both within Chemistry and at various others Departments

on Campus. Project: “New PennState NMR Facility web page” (http://sites.psu.edu/nmrlaboratorypsu/).

- Planning, Design, Implementation, Maintenance. 2015-current.

Project: “Upgrade of the existing solid-state 500-MHz instrument: from Tecmag/Apollo console to the Bruker’s Avance-III-HD, adding two new probes: one high-resolution MAS probe,

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applicable to semi-solid samples, and one solid-state CPMAS probe, which can operate in double- or triple-resonance mode. The upgrade also comprised the Bruker interface A2B, which

allows the use of existing 500-MHz non-Bruker probes. 2014-2016. - The project involved: 1) Definition of the configuration of the new system. 2) Follow-up of

several phases of the purchase process. 3) Follow closely the installation of the new console in January-March of 2016 with the Bruker engineer. Trained to switch probes between the HR-MAS probe and the SS probe, as well as to NMR Facility’s 3.2-mm SS

probe (using the A2B interface). Invited software tester/reviewer, December 2009: for the ACD/Workbook v.12

(http://www.acdlabs.com/products/adh/nmr/nmr_workbook/). The product is developed by Advanced Chemistry Development, Inc. (www.acdlabs.com).

Invited reviewer, 2009: Magnetic Resonance in Chemistry, John Wiley & Sons, Ltd, for the Special edition on “NMR-Based Mixture Analysis - Metabolomics and Beyond” – Vol. 47 Issue S1, Pages S1 - S173 (December 2009). Publication reviewed: “Determination of metabolite profiles in

tropical wines by 1H NMR spectroscopy and Chemometrics”, Hallwass et al. Project: “Solid-State NMR Proposal – submitted to the MRI Program/NSF”, January 2003.

Grant proposal submitted to MRI program at NSF for a new 400WB Solid-State NMR spectrometer with microimaging capability. The proposal brought together two Departments (Chemistry and Chemical Engineering) from Princeton University, also the Princeton Materials Institute (PMI) and the Center for Molecular and Biomolecular Imaging (CMBI). Ten faculty members contributed to the proposal, encompassing studies such as template-controlled silica polymerization, surface functionalization, and high-temperature membranes employed in fuel cells.

Project: “Chemistry’s NMR Facility Home-Page” (http://www.princeton.edu/~nmr). Planning, Implementation, Maintenance, October 2002.

Princeton University NMR Facility, Note #4: Pacheco, C. “Temperature Calibration Curve Determination on the VARIAN INOVA-400”, November 2002. NMR Lab Report distributed to students, Princeton University.

Princeton University NMR Facility, Note #3: “Pacheco, C. “Long-Range Proton-Carbon Coupling Constants: Accordion Sequences and Determination”, July 2002. NMR Lab Report distributed to

students, Princeton University. Princeton University NMR Facility, Note #2: Pacheco, C. Schuster, I. “1H/19F Double Resonance

Experiments on the INOVA-400”, July 2002. NMR Lab Report distributed to students, Princeton University.

Princeton University NMR Facility, Note #1: Pacheco, C., “ACD 5.0 Software: Evaluation of the Chemical Shift Predictors (1H, 13C, 31P, and 19F) Modules”, April 2002. NMR Lab Report

distributed to students, Princeton University.

Project: “CapNMR Probe for the 600-MHz” with David Detlefsen (Novatia, LLC, Princeton, NJ - http://www.enovatia.com).

Preliminary runs using the CapNMR probe were performed on the 500-MHz to evaluate its performance. In some biochemical systems, protein-ligand binding was investigated. Results of these experiments can be seen at http://www.princeton.edu/~nmr/news.htm, IAP Newsletter, and http://www.princeton.edu/~chemdept/news/index.html).

Pacheco, C., “Solid-State NMR Spectroscopy of Inorganic Materials” Edited by John J. Fitzgerald – Book review published in The NMR Newsletter, September 2001.

Pacheco, C., Manuscript reviewer of t “31P NMR Probes of Chemical Dynamics: Paramagnetic Relaxation Enhancement of the 1H and 31P NMR Resonances of Methylphosphite and

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Methylethylphosphate Anions by Selected Metal Complexes", by Jack S. Summers, Charles G. Hoogstraten, R. David Britt, Karel Base, Barbara Ramsay Shaw, Anthony A. Ribeiro, and Alvin L.

Crumbliss. For Inorganic Chemistry, Edward Solomon, Editor, August 2000. Pacheco, C., “NMR Techniques in Catalysis” Edited by Alexis T. Bell and Alexander Pines. Book

review published in The NMR Newsletter, March 2000.

Project Report Pacheco, C.R.N. and Rodriguez, M. R. “Visit to CHEVRON Research Company and HALLIBURTON-NUMAR Corporation”

Report describing the use low-field NMR by CHEVRON to determine petrophysical properties of formation rocks; at HALLIBURTON, visit to the facilities where the NMR log tool is tested, calibrated, and developed for field applications and, at NUMAR laboratory to see how low-field NMR measurements (relaxometry) on rocks are carried out and how their petrophysical properties are determined. July of 1998.

Pacheco, C., “Pyrrole-Type Nitrogen in Aviation Kerosene by Visible Spectroscopy” (P) Tempo de Análise (Journal of the Chemistry Department of PETROBRAS R&D Center), Rio de Janeiro, v.1, n.1, p.2, 1989.

Pacheco, C. “Determination of the Critical Micelle Concentration of a Bi-functional Polymer

Surfactant by 1H NMR”, (P) Tempo de Análise, Journal of Department of Chemistry of the R&D Center, August of 1998.

Pacheco, C., “Mono-, Di-, and Polyaromatics in Oil Fractions by UV Absorption” (P) Tempo de Análise (Journal of the Chemistry Department of PETROBRAS R&D Center), Rio de Janeiro, v. 2,

n. 1, p. 2, 1990. Webmaster of the Brazilian NMR Users Association (AUREMN), 1998-1999.

Responsible for the Maintenance of the Brazilian NMR Users Discussion List, 1998-1999.

Technical Communications Pacheco, C. Teixeira, M. A. G.; Menezes, S. M. C.; Marques, R.G.G.; Bagueira, R. V. A.

“Determination of the Total Solid Content in Oil as Function of Temperature by Low-Resolution

1H NMR” (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication, December of 1999.

Pacheco, C., “The Molecular Structure Determination of a Glycolipid by NMR” (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication,

December of 1999. Pacheco, C., and Mendes, A. S. “Incorporation of Acyl Chlorides in Partially Hydrolyzed Poly

(vinyl alcohol): Analysis by 1H and 13C NMR” (P), - PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication 147/99, October of 1999.

Pacheco, C. Marques, R.G.G. and Mendes, A. S. “Determination of Bay Region Hydrogen Types in Lubricant Oils by 1H NMR” (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ,

Technical Communication 111/99, July of 1999.

Menezes, S. M. C., Pacheco, C. Faria, F. D., Pereira, R. C. “The Role of the Department of Chemistry of the Research Center on the Problem of the UDS Process Unity at Capuava Refinery” (P), PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication 37/99, February of 1999.

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Pacheco, C., Marques, R.G.G. and Mendes, A. S. “Determination of the Composition of the Copolymers Poly (octadecyl acrylate- methyl acrylate) and Poly (hexadecyl acrylate- methyl

acrylate)” (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication 21/99, January of 1999.

Pacheco, C., Marques, R.G.G. and Mendes, A. S. “Determination of the Position of the Phosphorus atom in the Molecular Structure of Bellasol S40 - a Scale Inhibitor” (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication 20/99, January of 1999.

Braga, C. M. S., Pacheco, C., and Ferreira, A. L. “Determination of Lubrizol LZ 8195CB Content in Gasoline” (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication 256/98, December of 1998.

Lopes, M. I. C., Meilli, C. and Pacheco, C., “Evaluation of Glutaraldehyde-based Commercial

Reagents” (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication 253/98, December of 1998.

Pacheco, C. Martins, C., Carvalho, R. L., Braga, C. M. S., Cintra, R. H., Marques, R.G.G., Mendes, A. S., Silva, F. F., Vieira, R. “Evaluation of the Wax Produced by RLAM Refinery which

received Complaint from Candle Makers” (P) Technical Communication of the Products Division, Rio de Janeiro, RJ, November of 1998.

Pacheco, C. R.N “Determination of the Critical Micelle Concentration (CMC) of C4-(PO)10-(EO)6-OH by 1H NMR”, (P) PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ,

Technical Communication 37/99, October of 1998.

Pacheco, C. Marques, R.G.G., Mendes, A. S. “Determination by 13C NMR of the Composition of Styrene-Butadiene Copolymer with High Styrene Content and Incorporated Acrylic Acid” (P)

PETROBRAS. CENPES. DIQUIM. SEQUOR, Rio de Janeiro, RJ, Technical Communication 149/98, August of 1998.

Cardoso, L.G. C.; Pereira, J. L.; Ficara, M. L. G., and Pacheco, C., “Compatibility of Elastomers with Automotive Gasoline. 1. Status Report” (P) PETROBRAS R&D Center, Rio de Janeiro,

Document #650 15203, 1993. Souza, G. L. M.; Menezes, S. M. C., and Pacheco, C., “Characterization of the Coke Formed on

Used and Regenerated Hydrotreatment Catalysts by Solid State 13C NMR” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #611983, 1990.

Veiga, G. D.; Pacheco, C., and Correia, E. V. “Determination of the Aromatic Content in Diesel Oil by UV-VIS Spectroscopy” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 12981, 1990.

Molina, P. R. S.; Pacheco, C., and Saldanha, W. A. “Validation of the 1H NMR Method to Estimate Aviation Kerosene Breakpoint” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 12811, 1990.

Lopes, M. I. C.; Menezes, S. M. C., and Pacheco, C., “Analytical Support to the Project of Synthesis of Flotation Collector Developed by the Polymer Department” (P) PETROBRAS R&D

Center, Rio de Janeiro, Document #666992, 1990.

Pacheco, C., “Determination of Low Content Asphaltenes in RLAM Refinery Paraffin ‘Micro’ by

UV-VIS” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #627191, 1990. Menezes, S. M. C.; Pacheco, C., and Faria, F. R. D. “Analysis of the Hydraulic Fluid from the

ROV (MRL 10) Condenser” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 14635, 1992.

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Lopes, M. I. C.; Pacheco, C., and Gabardo, I. T. “Chemical Characterization of the Biocide Bulab 6020 Manufactured by Buckman Laboratories” (P) PETROBRAS R&D Center, Rio de Janeiro,

Document # 650 14634, 1992. Lopes, M. I. C.; Pacheco, C., and Louro, E. M. “Evaluation of the Chemical Composition of

Commercial Bactericides” (P) PETROBRAS R&D Center, Rio de Janeiro, Document number 650 14824, 1992.

Silva, A. M. P.; Pacheco, C. R. N. and Ficara, M. L. G. “Chemical Characterization of the Products T MULZ AO2, T MULZ FCO (Thompson Hayward Chem CO), and FONGRANAT RL (Hoechst) Used as Emulsifiers in Agriculture” (P) PETROBRAS R&D Center, Rio de Janeiro, Report of the Department of Products 020/92, 1992.

D’Ornellas, C. V.; Krause, I. M. K. and Pacheco, C., “Evaluation of the Occurrence with Gasoline in a Petrobras Gas Station” (P) PETROBRAS R&D Center, Rio de Janeiro, Document

#650 14299, 1992. Ficara, M. L. G.; Pacheco, C., and Gabardo, I. T. “Chemical Characterization of the Product

‘Isoparaffin’ from UNIPAR” (P) PETROBRAS R&D Center, Rio de Janeiro, Document number 650 14272, 1992.

Pacheco, C., “Correlation Between Aviation Kerosene Breakpoint and the Several Hydrogen Types of Obtained by 1H NMR” (P) Poster and Proceedings of the 6th National Meeting of Analytical Chemistry (P) Department of Chemistry of Sao Paulo State University, Sao Paulo, September of 1991.

Pacheco, C., “Determination of the Degree of Hydrolysis of Polyacrylamide by FTIR” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #776181, 1991.

Molina, P. R. S.; Pacheco, C., and Rocha, M. I. “Evaluation of the Hydrogenation of the Aviation

Kerosene Obtained from Cabiunas Crude Oil at the U 106 of Gabriel Passos Refinery” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 12657, 1990.

Castello Branco, V. A; Pacheco, C., and Louro, E. M. “Characterization of Nitrogen Compounds in Oil Fractions. Part 2- Preliminary Results of the Use of Alumina and Ion Exchange Resins at

the Concentration Step” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 12205, 1989.

Pacheco, C.,; Marques, R. G. G. and Silva, E. M. B. “Use of 1H and 13C NMR for Average Molecular Parameters Determination in Feedstock and Products from the FCC Process” (P) PETROBRAS R&D Center, Rio de Janeiro, Document # 650 12636, 1989.

Molina, P. R. S.; Pacheco, C., and Rehim, H. “Study of the Kerosene/Water Emulsion” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 12606, 1989.

Gabardo, I. T.; Pereira, R. C. L., and Pacheco, C., “PAHs Analysis in Oil-Based Perforation Mud” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 14284, 1988.

Nascimento, C.A.R., Pacheco, C. and Leite, L. F. M. “Evaluation of a Rubber Tube for Airplane Fueling Purposes” (P) PETROBRAS R&D Center, Rio de Janeiro, Document #650 09184, 1986.

Courses, Training: Presentations “Superusers NMR Training”, October 12,14,19, and 21; 2016, NMR Facility/Chemistry.

2-week training on Varian Systems at Petrobras R&D Center, Rio de Janeiro, March 2014.

2-week training on Varian Systems at Petrobras R&D Center, Rio de Janeiro, July 2011.

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Twenty-five new NMR users, annual average, are trained on basic operational aspects of the Varian and Bruker systems at the Princeton NMR Facility (see www.princeton.edu/~nmr), 2000-

2011. “Concepts and Practicalities of NMR in Liquid and Solid State” (P), Petrobras R&D Center, Rio

de Janeiro, July 1-5, 1999. - 12-hour course covering the theoretical and practical aspects of liquid and solid state

NMR.

“NMR: Basic Concepts, One-, and Two-Dimensional” (P), Petrobras R&D Center, Rio de Janeiro, June 14-17, 1999.

- A 24-hour course, divided into 12 hours of theoretical aspects and 12 hours of laboratory demonstration.

“Theoretical and Experimental Aspects of NMR in Two and Higher Dimensions” (P),

Department of Chemistry, Military Institute of Engineers (IME), Rio de Janeiro, March 2-4, 1999. - A 24-hour course, divided into 12 hours of theoretical and practical aspects, 8 hours of

exercises of interpretation of 2D NMR spectra, and 4 hours of laboratory demonstration. Federal University of the State of Rio de Janeiro (UFF), Rio de Janeiro, Brazil: Implementation of

the Inverse Techniques for Detection of 15N and 13C Frequencies at Natural Abundance (P), Department of Chemistry’s 300 MHz-Varian INOVA Spectrometer, 2 days, September 1998

- Parameter optimization for HMQC, HSQC, and HMBC pulse sequences. Establishment of a protocol for 2D 1H-13C and 1H-15N analyses. Federal University of Pernambuco (UFPE),

Pernambuco, Brazil. 2 days, June 1998. - Implementation of the Inverse Techniques for Detection of 15N and 13C Frequencies at

Natural Abundance at the Department of Chemistry’s 300 MHz-Varian UNITY-PLUS Spectrometer.

- Parameter optimization for HMQC and HMBC pulse sequences. Establishment of a protocol for the 2D 1H-13C and 1H-15N analyses.

Graduate Research, Undergraduate internship

“The Use of Inverse Detected NMR for the Analysis of Diesel Oil Extracts”, Doctoral Dissertation. Supervision of Prof. Daniel D. Traficante, Department of Chemistry, University of Rhode Island, Rhode Island, USA, 1993-1996.

“Gas Solubility in Liquids: Studies on Non-Polar Systems”. Supervision of Prof. Angela M. C. Uller, Graduate Studies in Engineering of the Federal University of Rio de Janeiro (COPPE). Research

co-sponsored by PETROBRAS R&D Center, 1985-1986.

“Distillation of Ethanol-Water Mixtures on Packed Bed Column”, supervision of Prof. Angela M.

C. Uller, Graduate Studies in Engineering of the Federal University of Rio de Janeiro (COPPE) and Prof. Neil Ashton, visiting professor of the University of Birmingham, England, 1983-1984.

Scientia Engineering Systems, Prototype and Process Development, consulting company in Chemical Engineering based in Rio de Janeiro, 1981-1983, under supervision of Prof. Afonso Silva

Teles.

http://www.princeton.edu/~nmr

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Meetings: Participation

57th Experimental Nuclear Magnetic Resonance Conference, Wyndham Grand Hotel, Pittsburgh, PA, April 10 - 15, 2016.

EUROPEAN MAGNETIC RESONANCE (EUROMAR), Frankfurt am Main, Germany (in conjunction with the 8th European Federation of EPR Groups Meeting), August 21-25, 2011.

EUROPEAN MAGNETIC RESONANCE (EUROMAR), Florence, Italy, (in conjunction with the 17th ISMAR Conference), July 4-9, 2010.

EUROPEAN MAGNETIC RESONANCE (EUROMAR), Tarragona, Spain (in conjunction with the 6th Ibero-American NMR meeting), July 1-5, 2007

2004 Monthly Meetings of the Northern New Jersey American Chemical Society/ NMR Topical group:

Dr. Craig Milling "Microcoil NMR: Reducing Sample Size, Reducing System Size", September 22; Dr. Dan Norwood, "NMR from the View of a Mass Spectrometrist" June 23; Prof. Arthur Palmer " New Methods and Applications for Studying Protein Motions through Nuclear Spin Relaxation”,

May 18; Prof. Wolfgang Richter “Diffusion Tensor Imaging”, March 10; Prof. Babis Kalodimos “"Unraveling Protein-DNA Recognition Mechanisms: A Combined Structural, Dynamic, Protein Engineering & Thermodynamic Approach", January 22;

7th Brazilian Journey of Magnetic Resonance (P) Rio de Janeiro, RJ, Brazil, July 27-30, 2004.

“Microsample NMR: Protocols, practice, and applications using capillary and capillary flow methods”, February 19, 26; March 4, 11; 2004, Princeton University.


Dr. Hunter Moseley “Automation of the NMR Protein Structure Determination Process for Structural Genomics”, December 9; Workshop on "Structure Elucidation by NMR", October 3:

Prof. Daniel D. Traficante “The Theory and Practice of Applied NMR Spectroscopy”; Dr. R. Thomas Williamson "Identification of Natural Products by NMR"; Prof. Eric Munson "Solid State NMR in Pharmaceutical Applications”; Dr. Linda Lohr “Systematic Identification of Impurit ies in Pharmaceutical Products and Raw Materials”; Dr. Steve Castellino "Identification of Metabolites in Biological Samples"; Dr. Vasilios Marathias "Enantiomeric Identification by NMR"; Dr.David Detlefsen “Computational Aspects of Structure Confirmation”; Prof. Lucio Frydman, Chemical Physics Department, Weizmann Institute of Science, Rehovot, Israel "GONE IN 60 (milli) SECONDS - Some New Developments in Multidimensional NMR", June 17; Dr. Stephan Zech, Ann McDermott, Columbia University, Chemistry Department, "Insight into structure and function of membrane proteins and protein-ligand complexes from Solid-State-NMR spectroscopy", May 21;

Dr. Mari Smith, Johns Hopkins University Medical School, "Broadband Selective Excitation Pulses and the Nuclear Overhauser Effect", March 19.

American Chemical Society, 36th Middle Atlantic Regional Meeting (MARM), hosted by The Trenton Local Section and the Princeton University/Department of Chemistry, Princeton, New

Jersey, June 8-11, 2003. Attended Analytical Chemistry Section only.

44th Experimental NMR Conference, Savannah, GA, March 30-April 4, 2003.

Including attending: a) “Advances in NMR”, Nalorac Symposium, Savannah, GA, March 30, 2003. b) Bruker Users Meeting, March 30, 2003. c) Bruker: Solid State Workshop - Savannah, GA, March

29, 2003, and d) Varian Users Meeting, Savannah, GA, March 29, 2003.

“Applications of Microcoil NMR” Workshop, Princeton University/Chemistry, March 18, 2003.

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Speakers: Dr. Tim Peck - President, MRM; Dr. Mark O’Neil-Johnson, Director, Scientific Development Sequoia Sciences; Dr. Dave Detlefsen, Vice President, Novatia LLC, Princeton.


Dr.Gregory Leo, Johnson & Johnson Pharmaceutical Research and Development “Evaluation of Metabonomics in a Pharmaceutical Drug Discovery Environment", November 20, 2002; Prof. Wolfgang Richter, Princeton University "Fundamentals of Anatomic and Functional Magnetic Resonance Imaging", October 23, 2002; Prof. James Baleja, Tufts University School of Medicine, Department of Biochemistry, "Protein Peptide Interactions by NMR: What are those chemical shift changes telling us?", March 20, 2002; Dr. George B. Crull, Bristol-Myers Squibb, "Linear Prediction: How to, When and When Not to", January 16, 2002.

41st Eastern Analytical Symposium (NMR Session), Somerset, NJ, November 18-21, 2002.

SMASH (Small Molecule NMR Conference) Meeting, Breckenridge, Colorado, September 15-18, 2002.

Attending also the Varian Users Meeting at SMASH on 9/15/2002.

ACD – North American Users’ Meeting, March 7–8, 2002, Princeton, NJ.

Metabolic Engineering Symposium, Lewis-Sigler Institute for Integrative Genomics at Princeton University, NJ, December 7, 2001.

CW-EPR Operation. Practical training, by Dr. Alexei Tyryshkin, Princeton University/Chemistry - EPR Facility, December, 2001.

“Green Chemistry”, Princeton University – Chemistry, lectured by Dr. István Horvath, November 2001.

“Saturation Transfer Difference Experiments: Pulse Sequence and Applications to Protein-Ligand Studies”, Princeton University – Chemistry, lectured by Dr. I. Pelczer, November 2001.

15th Annual CABM Symposium - Structural Genomics in Pharmaceutical Design Symposium, Doral Forrestal at Princeton Hotel, NJ, October 24-25, 2001.

40th Eastern Analytical Symposium (NMR Session), Atlantic City, NJ, October 2, 2001.

“NMR on Metabonomics” Workshop, with John P Shockor, Jeremy K. Nicholson, John C. Lindon,

and Elaine Holmes, Princeton University, NJ, April 27, 2001. 42nd Experimental NMR Conference, Orlando, Florida, March 11-16, 2001.

Nalorac Symposium, Orlando, Florida, March 11, 2001. Varian Users Conference, Orlando, Florida, March 9-10, 2001.


h) Patricia Stone Wilkinson and Frank E. Koehn “LC-NMR and LC-NMR-MS Methods”, December

4, 2001. g) Daniel Barabino “NMR at 900 MHz”, November 15, 2001. f) Thomas Szyperski “Structural Biology in Supercooled Water”, October 17, 2001. e) Jonathan D. Cohen “Imaging the

Brain: A Window on the Mind”, September 19, 2001. d) Workshop "Current Topics in NMR", May 31, 2001 – Speakers: Krish Krishnamurthy “Band Selective Excitation”; Tatyana Polenova “Solid-

State NMR for Structural Studies of Uniformly and Sparsely Isotopically Labeled Proteins”; Jeffrey Peng “NMR Approaches for Lead Generation”; Junfeng Wang “PISA Wheel Image and its

Application in Structural Determination of M2 Protein from Influenza A”; Melissa Lin “LC-NMR & Flow-NMR in Drug Discovery”; Nico Tjandra “Molecular Alignment and its Consequences to

Biomolecular Structure Determination”. c) R. Thomas Williamson, “Application of Emerging NMR Techniques and Technologies to Small Molecule Structure Problems”, April 9, 2001. b) John P

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Shockor "Hyphenated NMR and Pattern Recognition of Biofluids: Predicting Toxicity", February 21, 2001. a) Daniel Wyss “Structures and dynamics of hepatitis C virus NS3 protease and helicase”

and “Alignment of weakly interacting molecules to protein surfaces using simulations of chemical shift perturbations”, January 16, 2001.

42nd Rocky Mountain Conference on Analytical Chemistry, Broomfield, CO, USA – July 30-Aug 2, 2000.

SMASH (Small Molecule NMR Conference) Meeting, Argonne National Laboratory, Chicago, Illinois, July 16-19, 2000.


d) Scott Smith “Automated NMR Spectral Interpretation” – December 2000c) Jasna Fejzo “NMR screening” – October 2000. b) Daniel Traficante “Pulse Field Gradient NMR” – September 2000. a)

Ravinder Reddy “Magnetic Resonance Imaging” – March, 2000. 7th NMR Meeting (P) organized by the Brazilian NMR Users Association -AUREMN, Angra dos

Reis, Rio de Janeiro, May 1999. 5th Seminar of Analytical Chemistry (P) PETROBRAS Research and Development Center, Rio de

Janeiro, December 1998.

5th Brazilian Journey of Magnetic Resonance (P) Campinas, SP, Brazil, August 1998.

“Current Tools for Oil Logging” (P) Seminar, 3 days, Natal, RN, Brazil, July 1998.

39th ENC Asilomar, Pacific Grove, CA, USA, March 1998.

Varian Users Meeting, Palo Alto, CA, USA, March 1998.

Nalorac Symposium, Monterey, CA, USA, March 1998.

6th NMR Meeting (P) organized by the Brazilian NMR Users Association -AUREMN, Angra dos Reis, Rio de Janeiro, May 1997.

3rd National Varian Users Meeting (P) Meridien Hotel, Rio de Janeiro, May 1997.

36th Experimental NMR Conference, Boston, USA, March 1995.

Nalorac Symposium, Boston, USA, March 1995.

2nd Brazilian Journey of Magnetic Resonance (P) organized by the Brazilian NMR Users Association -AUREMN, Rio de Janeiro, August 1992.

1st Meeting of Aviation Kerosene (P) PETROBRAS Human Resources, December of 1991.

6th National Meeting of Analytical Chemistry (P) Department of Chemistry of Sao Paulo State University, Sao Paulo, September of 1991.

3rd NMR Meeting (P) organized by the Brazilian NMR Users Association -AUREMN, Buzios, Rio

de Janeiro, May of 1991.

1st Brazilian Journey of Magnetic Resonance (P) organized by the Brazilian NMR Users Association -AUREMN, Rio de Janeiro, August of 1990.

2nd NMR Meeting (P) organized by the Brazilian NMR Users Association -AUREMN, Angra dos Reis, Rio de Janeiro, May of 1989.

Aviation Kerosene Meeting (P) PETROBRAS Research and Development Center, April of 1989.

30th Experimental NMR Conference, Asilomar, CA, USA, March 1989.

Varian Users Conference - Palo Alto, California, USA, March 1989.

Octane and Cetane Meeting (P) PETROBRAS Human Resources, Friburgo, Rio de Janeiro, April of 1987.

1st NMR Meeting (P) organized by the Brazilian NMR Users Group, Angra dos Reis, Rio de Janeiro, September of 1987.

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Recent Progress in Organic NMR, workshop, Campinas University, Sao Paulo, July of 1986. 9th Meeting of International Society of Magnetic Resonance (ISMAR), Gloria Hotel, Rio de

Janeiro, July of 1986.

Professional Visits

Petrobras R&D Center, Rio de Janeiro, RJ, Brazil, August 2004.

- Discuss and Implement NMR Diffusion Experiments. Re-structure the Program to calculate Average Molecular Parameters in Oils (using Varian’s Magical language).

VARIAN Associates - Palo Alto, CA. 400-MHz NMR spectrometer demonstration, with Dr. Steve Cheatham. June 2000.

Bristol-Meyer-Squibb Research Corp. – Lawrenceville, NJ – One of the managers (Dr. Vikram Roongta) discussed the features of the JEOL models in his laboratory. June 2000.

Bruker Instruments, Inc. - Billerica, MA. 400-MHz NMR spectrometer demonstration, with Dr. Sophie Kazanis – May 2000.

PETROBRAS’ LANDULFO ALVES REFINERY – State of Bahia – Brazil - Discussion of the problem of contamination of the paraffin produced by that refinery that was generating complaints from the candle manufacturers - 1998.

HALLIBURTON-NUMAR Corporation - Houston, TX, USA, 2 days, March 1998. Visit to the facilities where the NMR log tool is tested, calibrated, and developed for field applications. Visit to the NUMAR laboratory that performs low-field NMR measurements (relaxometry) on rocks to determine their petrophysical properties. Contact: Eng. Guillermo Velasquez

CHEVRON Research Company - La Habra, CA, USA, 2 days, March 1998. Discussion with the

Formation and Evaluation Group about the use of low-field NMR for the determination of petrophysical properties of formation rocks. Contact: Dr. Gerald LaTorraca

VARIAN Associates - Florham Park, NJ, USA, 16 hours, 1996. Spectrometer training with Varian’s INOVA model under the supervision of Dr. Bruce Adams.

VARIAN Associates - Palo Alto, CA, USA, 16 hours, 1989. Spectrometer training with Varian’s GEMINI model under the supervision of Dr. James Shoolery.

Courses: Participation Bruker Course of “Service and Maintenance” – April 14-17,2015, in Billerica, MA.

Workshop on CAChe 5.0 – Princeton University, Dec 10, 2002

Dreamweaver MX Intermediate, Princeton University, Nov 27, 2002 Dreamweaver MX Introductory Part I and II - Princeton University, Oct 23-24, 2002

Electron Paramagnetic Resonance Spectroscopy: Applications & Practical Training – CHM510 – Fall/2002 - Princeton University – Chemistry

Biophysical Chemistry II - CHM516 - Spring/2002 - Princeton University – Chemistry Advanced Organic Chemistry - CHM532 - Spring/2002 - Princeton University – Chemistry

“Green Chemistry”, Princeton University – Chemistry, lectured by Dr. István Horvath, November

2001.

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“Saturation Transfer Difference Experiments: Pulse Sequence and Applications to Protein-Ligand Studies”, Princeton University – Chemistry, lectured by Dr. István Pelczer, November 2001.

NMR Section of the “Bio-Physical Chemistry Tools” at Princeton University - Chemistry - , lectured by Dr. István Pelczer, February of 2000.

“Recent Advances in NMR”, University of Sao Carlos, Sao Carlos, 16 hours, Dr. Bruce Adams (Varian, USA), May of 1997.

“NMR of Proteins, Peptides, and Nucleic Acids”, NMR Concepts, Rhode Island, USA, 40 hours, Prof. Lewis Kay (University of Toronto, Canada), Prof. David Wemmer (University of California, USA), and Prof. David Cowburn (Rockefeller University, USA), November of 1994.

“NMR Concepts and Operating Techniques II “, NMR Concepts, Rhode Island, USA, 40 hours, Prof. Daniel D. Traficante (NMR Concepts, USA), Prof. Brian Hunter (Kings College, Canada),

Prof. Thomas C. Farrar (University of Wisconsin, USA), and Dr. Susan Pochapsky (Bruker, USA), November of 1994.

“Electronics”, NMR Concepts, Rhode Island, USA, 80 hours, Prof. Daniel D. Traficante, Dr. Michael McGregor (NMR Concepts, USA), and James Simms (Massachusetts Institute of Technology, USA), March-April, 1994.

“Advanced Two-Dimensional NMR”, NMR Concepts, Rhode Island, USA, 40 hours, Prof. Dieter Ziessow (Technical University of Berlin - Germany) and Prof. Thomas C. Farrar (University of Wisconsin, USA), March of 1994.

“Introduction to Two-Dimensional NMR”, NMR Concepts, Rhode Island, USA, 40 hours, Prof. Daniel D. Traficante, Dr. Michael McGregor (NMR Concepts, USA), and Dr. Charles Rodger

(Sterling Winthrop, Inc.), March of 1994. “NMR Concepts and Operating Techniques”, NMR Concepts, Rhode Island, USA, 40 hours, Prof.

Daniel D. Traficante and Dr. Michael McGregor (NMR Concepts, USA), October of 1993. “Interpretation of One-Dimensional NMR Spectra”, NMR Concepts, Rhode Island, USA, 40

hours, Prof. Daniel D. Traficante and Dr. Michael McGregor (NMR Concepts, USA), April of 1993.

“Two-Dimensional NMR”, PETROBRAS Research and Development Center, 48 hours, Prof. Daniel Traficante (NMR Concepts - USA), August of 1992.

“Composition of Polymers” (P) PETROBRAS Research and Development Center, 20 hours, January of 1991.

“Technical Meeting about Petroleum Treatment” (P) PETROBRAS Human Resources, 40 hours,

December of 1990. “Fundaments of Catalysis” (P) PETROBRAS Research and Development Center, 40 hours,

October of 1990. “Programming in Dialog Plus” (P) PETROBRAS Research and Development Center, 20 hours,

November of 1989.

“Nuclear Magnetic Resonance” (P) PETROBRAS Research and Development Center, 80 hours, November of 1988.

“Nuclear Magnetic Resonance Applied to Polymers”, PETROBRAS Research and Development

Center, 40 hours, Prof. Q. Pham (CNRS- France), September of 1988.

“Recent Developments in NMR” (P) Military Institute of Engineering, Rio de Janeiro, 100 hours, February of 1988.

“Seminar of Chemistry and Computers” (P) Brazilian Chemical Association, 7 hours, December of 1987.

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“8th Laboratory Seminar” (P) Brazilian Petroleum Institute, November of 1987. “DOS” (P) PETROBRAS Research and Development Center, 17 hours, October of 1987.

“Introduction to Nuclear Magnetic Resonance” (P) PETROBRAS Research and Development Center, 24 hours, September of 1987.

“Creativity: A Rational Approach” (P) PETROBRAS Research and Development Center, 32 hours,

August of 1987. “Fourier Transform Infrared Spectroscopy” (P) Perkin-Elmer, Sao Paulo, 8 hours, July of 1987.

“Design of Experiments” (P) PETROBRAS Research and Development Center, 32 hours, March of 1987.

“Statistics Applied to Laboratory” (P) PETROBRAS Research and Development Center, 32 hours, August of 1986.

“Artificial Intelligence” (P) Graduate Studies in Engineering of the Federal University of Rio de Janeiro (COPPE), 34 hours, May of 1986.

“Ultraviolet and Visible Spectroscopy” (P) Hewlett Packard from Brazil, Sao Paulo, 24 hours, April of 1986.

“Recent Developments in Organic NMR” (P) Brazilian Chemical Society, Sao Paulo, July of 1986.

“Overview of Conflict Resolution”, Princeton University, July 2001 Computer programming: FORTRAN, BASIC, and PASCAL.

English Course at Cultura Inglesa, Rio de Janeiro, 7 years, and German Course at Oxford Course

of Languages (P)Rio de Janeiro, 2 years.

Participation in Theses Committees, Editorial Boards, Committees

M.Sc. The thesis of Flávio Santos G. Lima, “Standardization of the Models Employed in the Near Infrared Spectroscopy” (P) co-supervision with Prof. Luiz E. P. Borges, Military Institute of

Engineering, Rio de Janeiro, March of 2000. D.Sc. The thesis of Dellyo Alvares, “Development of New Polyacrylates and Poly (ethylene-vinyl

acetate) to Minimize Paraffin Deposition in Oil Production” (P) Macromolecular Institute of the Federal University of Rio de Janeiro, April of 1999.

D.Sc. The thesis of Monica R. M. P. Aguiar “Study of -Lactam Derivatives by Solid State NMR” (P) Department of Chemistry of the Federal University of Rio de Janeiro, March of 1997.

M.Sc. The thesis of Marcia H. R. Velloso “Generation of DANTE Pulses and Their Application in Selective NMR” (P) Department of Chemistry of the Military Institute of Engineer, Rio de Janeiro, December of 1997.

Annals of Magnetic Resonance, Editorial Board Member, AUREMN – current. Member of the Editorial Board of the Series about Concepts and Applications of NMR, written in

Portuguese. Invited writer for Issue about Signal Processing in NMR. Ad-hoc member of the Editorial Board of the Special Edition on NMR of the Journal of Brazilian

Chemical Society (JBCS) May of 1999.

Member of the Scientific Committee of the 7th Brazilian NMR Users Meeting - May of 1999.

Member of the Scientific Committee of the 5th Brazilian Journey of Magnetic Resonance, August of 1998.10. President of the Scientific Committee which Selected the Best Work Presented at the 5th Brazilian Journey of Magnetic Resonance, Campinas, SP, Brazil, August of 1998.

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Member of the Committee of the Statistics of NMR in Brazil, coordinated by the Brazilian NMR Users Association, Rio de Janeiro, 1997-1999.

Member of the Committee of NMR Nomenclature in Portuguese, organized by the Brazilian NMR Users Association, Rio de Janeiro, 1999-present.

Participation and Affiliation in Scientific Societies, Professional Associations,

Synergistic Activities, Consultancies

Brazilian NMR Users Association –AUREMN: current.

Founder, 1987; Elected Treasurer, 1990-1992.

American Chemical Society (ACS), 1993-1996, 2001-present.

North Jersey Section, American Chemical Society/NMR Topical Group

Chair, 2001; Chair, Treasurer, 2002; Scientific Advisor, 2003, 2004.

Consultant for Bio-Rad Laboratories: Project to develop the 1D processing software ProcessIt NMR package, part of the KnowItAll® Informatics System product line, 2003.

Project: “Donation of Chemistry Journals to Brazilian Universities” – July-December, 2002.

A six-month project aiming at moving 20+ publications from Princeton University - Chemistry - (temporarily stored in the NMR laboratory) to Rio de Janeiro, Brazil (http://www.princeton.edu/~nmr/news.htm, IAP Newsletter, and http://www.princeton.edu/~chemdept/news/index.html).

Consultant for technical aspects of NMR and spectrometer maintenance for Synthon Chiragenics Corporation, Monmouth Junction, NJ, 2001.

Chemists and Chemical Engineers Syndicate (1986-2000), Petrobras Engineer Association (AEPET, 1986-2000), Petroleum Employees Syndicate (SINDIPETRO, 1986-2000).

Awards

At the 10th Brazilian Conference of NMR Users, August 4-8, 2008 - UFF, Niteroi, RJ, Brazil, 20th-year anniversary of AUREMN (Brazilian NMR Users Association): awarded as one of the

founders.

Four-year Scholarship granted by Petrobras S/A to pursue Graduate Studies at the University of Rhode Island, RI, 1993-1996.

Knowledge of Languages

English (reading, speaking, and writing), Spanish (conversational, reading). Portuguese (native language).

http://www.princeton.edu/~nmr/news.htm

http://www.princeton.edu/~chemdept/news/index.html

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Carlos Pacheco

Thursday, February 16, 2017

Pacheco_CV_Feb2017

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Transcript of Pacheco_CV_Feb2017