OUTLINE

Pre-CAS TECO, Incheon, 17.11.09*Persistent Toxic Substances (PTS) in ambient air of Russian Arctic

Alexey Konoplev

Centre for Environmental Chemistry (CEC)SPA Typhoon of Roshydromet, Obninsk, RUSSIA

Pre-CAS TECO, Incheon, 17.11.09

OUTLINEWhat are PTS and why in the Arctic?International Treaties in the field of PTS and the environment.Monitoring of POPs in ambient air of Russian Arctic.Long-term mercury monitoring in atmosphere of Russian Arctic.Perspectives for hydrometeorological observatory in Tiksi.

Pre-CAS TECO, Incheon, 17.11.09*


IntroductionOccurrence and behavior of pollutants in the Arctic is governed by both the Arctic climatic conditions and pollutants properties.The issue of the Arctic pollution was brought to the forefront when high levels of PTS were detected among the indigenous peoples of the North.With no PTS production and application by the indigenous peoples, they often become affected by pollutants originating from industrially developed regions of the world.Pre-CAS TECO, Incheon, 17.11.09*


International agreements on the environmental pollution with PTSA series of international agreements and conventions provide for regular monitoring of PTS in the environment at the global and national levels and, first of all, in the Arctic .The most important of them are the Stockholm Convention on POPs, Convention on Long-Range Transboundary Air Pollution, agreements of the Arctic Council and its working groups (AMAP and ACAP).Pre-CAS TECO, Incheon, 17.11.09*


Pre-CAS TECO, Incheon, 17.11.09Attributes of PTSHigh toxicity;Persistence in the environment;Semi-volatility and ability to be transported over long distances;Ability for bioconcentration and accumulation;Global occurrence in the environmental media and biota.

PTS = POPs + Some Heavy Metals (Hg, Pb)*


The pattern of the atmospheric circulation, river and sea currents and low air temperatures are conducive to transport and accumulation of semi-volatile PTS in the Arctic. Due to the low solubility in water and high solubility in fats PTS tend to accumulate in the Arctic food chains that are rich in fats. In turn, animals of higher trophic levels form the basis of the traditional diet of the indigenous peoples of the Arctic. As a result, some of the Arctic indigenous communities are among the population groups that are worst exposed to PTS in the world.Pre-CAS TECO, Incheon, 17.11.09Transport and accumulation of POPs in the Arctic*


Pre-CAS TECO, Incheon, 17.11.09*POPs and Hg air monitoring at Russian Arctic sitesDunay: - POPs 1993 1994 Amderma: - POPs 1999 - 2001; - Hg 2001 presentValkarkay (Chukchi): - POPs 2002-2003; 2008-2009


Pre-CAS TECO, Incheon, 17.11.09*Objectives of POPs air monitoringTo measure the concentrations of POPs in the atmosphere of Russian Arctic. This provides the opportunity to make comparative analysis of POPs in the ambient air for different areas of the Arctic and the basis for modelling of their atmospheric transport.The data allow to assess the efficacy of international Conventions such as Stockholm Convention on POPs and Convention on transboundary air pollution.


Monitoring POPs and mercury on global Arctic GAW stationsCanada - Alert (GAW);USA- Point Barrow (GAW)Norway- Ny Alesund (GAW)Finland - Pallas (GAW)Pre-CAS TECO, Incheon, 17.11.09 *


Pre-CAS TECO, Incheon, 17.11.09*The list of determined compounds includes 154 individual substances:46 OCP and their metabolites (chlorobenzenes, DDT, mirex, Toxaphenes, ldrin, dieldrin, endrin, heptachlor, chlordane etc.);88 PCB congeners;20 PAH.


*Methods and materialsInternationally approved protocols of sampling and analysis are used. Weekly samples are collected by means of a high volume sampler. Samples are shipped to the laboratory, extracted and after clean-up analysed using gas chromatography-mass-spectrometry detection (GC-MS).

Pre-CAS TECO, Incheon, 17.11.09*Air POPs monitoring: Summary In general atmospheric concentrations of most OCP at Russian Arctic are similar to other Arctic sites.Concentrations of a number POPs especially PCBs, DDX and PAH at Valkarkay (Chukchi) are elevated as compared with global Arctic. This conclusion is confirmed by the data on human milk and blood.


Pre-CAS TECO, Incheon, 17.11.09*Results of PCB monitoring in ambient airThe tri substituted PCBs dominate in homologues profile for Amderma and five substituted PCB dominate in profile for Valkarkai.


*Air POPs monitoring: SummaryLong-range transport was a key factor for OCPs and their metabolites and determined the atmospheric levels of those chemicals in Russian Arctic.During winter atmospheric pollution by PCBs was also determined by long-range transport while in summer it was caused mainly by volatilization of these chemicals from the underlying surface, rather than by their long-range transport.

1

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-26.8982257119

-27.1857378365

-26.0856757821

-27.3749035948

-27.284871493

-29.761386566

-27.9483250707

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-28.7899116067

-28.4597465288

-29.3140089851

-27.9593602369

-27.1287359686

-27.4339153422

1/T

lnP

PCB 138 (summer)

T

SamplingSampling

DateDate

P OnOff

RA-99-14-PC-17.33/28/994/5/99

RA-99-15-PC-15.14/5/994/12/99

RA-99-16-PC-18.84/12/994/19/99

RA-99-17-PC-7.34/19/994/26/99

RA-99-18-PC-16.54/28/995/3/99

RA-99-19-PC-12.55/3/995/10/99

RA-99-20-PC-9.45/10/995/17/99

RA-99-21-PC-4.85/17/995/24/99

RA-99-22-PC-3.15/24/995/31/99

RA-99-23-PC-0.25/31/996/7/99

RA-99-24-PC-0.96/7/996/14/99

RA-99-25-PC16/14/996/21/99

RA-99-27-PC5.76/28/997/5/99

RA-99-28-PC4.67/5/997/12/99

RA-99-30-PC7.37/19/997/26/99

RA-99-31-PC9.07/26/998/2/99

RA-99-32-PC7.28/2/998/9/99

RA-99-33-PC9.18/9/998/16/99

RA-99-34-PC2.68/16/998/23/99

RA-99-35-PC2.18/23/998/30/99

RA-99-36-PC4.98/30/999/6/99

RA-99-37-PC1.69/6/999/13/99

RA-99-38-PC5.49/13/999/20/99

RA-99-39-PC0.19/20/999/27/99

RA-99-40-PC5.19/27/9910/4/99

RA-99-42-PC-1.710/11/9910/18/99

RA-99-43-PC-6.010/18/9910/25/99

RA-99-44-PC-2.810/25/9911/1/99

RA-99-45-PC-10.611/1/9911/8/99

RA-99-46-PC-6.211/8/9911/15/99

RA-99-47-PC-15.511/15/9911/22/99

RA-99-48-PC-1311/22/9911/29/99

RA-99-49-PC-6.911/29/9912/6/99

RA-99-50-PC-10.512/6/9912/13/99

RA-99-51-PC-4.712/13/9912/20/99

RA-99-52-PC-11.812/20/9912/27/99

RA-00-04-PC-15.31/17/001/24/00

RA-00-08-PC-12.92/14/002/21/00

RA-00-12-PC-11.73/13/003/20/00

RA-00-13-PC-9.33/20/003/27/00

RA-00-14-PC-17.03/27/004/3/00

RA-00-15-PC-10.14/3/004/10/00

RA-00-16-PC-4.64/10/004/17/00

RA-00-17-PC-5.54/17/004/24/00

RA-00-18-PC-10.94/24/005/1/00

RA-00-19-PC-8.75/1/005/8/00

RA-00-20-PC-6.95/8/005/15/00

RA-00-24-PC0.46/5/006/12/00

RA-00-28-PC4.57/3/007/10/00

RA-00-46-PC-211/6/0011/13/00

RA-00-47-PC-10.711/13/0011/20/00

RA-00-48-PC-8.311/20/0011/27/00

RA-00-49-PC-21.611/27/0012/4/00

RA-00-50-PC-12.612/4/0012/11/00

RA-00-51-PC-13.412/11/0012/18/00

RA-00-52-PC-20.612/18/0012/25/00

RA-01-01-PC-15.91/1/011/8/01

RA-01-02-PC-15.61/8/011/15/01

RA-01-06-PC-15.22/5/012/12/01

RA-01-07-PC-21.32/12/012/19/01

RA-01-08-PC-28.82/19/012/26/01

RA-01-09-PC-292/26/013/5/01

RA-01-11-PC-20.63/12/013/19/01

RA-01-12-PC-203/19/013/26/01

RA-01-13-PC-22.83/26/014/2/01

P,ng

PCB/OC for NCP. File Name:OC1OC2OC3OC4OC5OC6OC7OC8OC9OC10OC11OC12OC13OC14OC15OC16OC17OC18OC19OC20OC21OC22OC23OC24OC25OC26OC27OC28OC29OC30OC31OC32OC33OC34OC35OC36OC37OC38OC39OC40OC41OC47OC48OC49OC50OC51OC52OC53OC54OC55OC56OC57OC58OC59OC60OC61OC62OC63OC64OC65OC66OC67OC68OC69OC70OC71OC72OC73OC74OC75OC76OC77OC78OC79OC80OC81OC82OC83OC84OC85OC86OC87OC88OC89OC90OC91OC92OC93OC94OC95OC96OC97OC98OC99OC100OC101OC102OC103OC104OC105OC106OC107OC108OC109OC110OC111OC112OC113OC114OC115OC116OC117OC118OC119OC120OC121OC122OC123OC124OC125OC126OC127OC128OC129OC130OC131OC132OC133OC134

1,2,4,5-tetrachlorobenzene1,2,3,4-tetrachlorobenzenepentachlorobenzenehexachlorobenzenealpha-hexachlorocyclohexanebeta-hexachlorocyclohexanegama-hexachlorocyclohexanecomponent of technical chlordaneheptachloroctachlorostyrenecomponent of technical chlordanecomponent of technical chlordaneheptachloro compound in technical chlordaneheptachloro compound in technical chlordanecomponent of technical chlordaneintermediate metabolite of chlordanephotoheptachloroxychlordanetrans-chlordanecis-chlordanetrans-nonachlorcis-nonachlorheptachlor epoxidedieldrin1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethylene1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane1,1-dichloro-2,2-bis(p-chlorophenyl)ethane1,1,1-trichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane1,1,1-trichloro-2,2-bis(p-chlorophenyl)ethanemirexphotomirexpentachloroanisoleendosulfanmethoxychlortrichloroveratroltetrachloroveratrolendrintrifluralintoxaphene-2toxaphene-3242,2'/2,62,42,3'PCB8/52,2',62,2',52,2',42,3,6/2,3',62,2',3/2,4',2,3',52,3',42,4',52,4,4'2',3,42,3,4'2,2',3,62,2',3,6'2,2',5,5'2,2',4,5'2,2',4,4'2,2',4,52,2',3,5'2,2',3,4'2,2',3,4/2,32,3,4',62,2',3,3'2,4,4',52,3',4',5/2'2,3',4,4'2,2',3,5',62,3,3',4'/2,2,2',3,4',62,2',3,3',6/2,2',4,5,5'2,2',4,4',52,2',3,3',52,2',3',4,52,2',3,3',4,2,2',3,4,4'2,2',3,3',6,2,3,3',4',62,2',3,3',42,2',3,5,5',PCB144/1352,2',3,4',5'2,3',4,4',52,2',3,3',5,2,3,4,4',52,2',3,3',4,2,2',3,4',5,2,2',4,4',5,2,2',3,3',4,2,3,3',4,4'2,2',3,4,5,52,2',3,3',5,2,2',3,4,4',2,2',3,3',4,2,2',3,4,4',2,3,3',4,4',2,2',3,3',5,2,2',3,3',4,2,2',3,4',5,2,2',3,4,4',2,2',3,3',4,2,2',3,4,5,52,2',3,3',4,2,2',3,3',4'2,2',3,3',4,2,3,3',4,4',PCB201/1572,2',3,3',4,2,2',3,4,4',2,3,3',4',5,2,3,3',4,4',2,2',3,3',4,2,2',3,3',4,2,2',3,3',4,2,2',3,3',4,PCB196/2032,3,3',4,4',2,2',3,3',4,2,2',3,3',4,2,2',3,3',4,2,3,3',4,4',2,2',3,3',4,2,2',3,3',4,

Sample ID1245TCB1234TCBP5CBZHCBZa-HCHb-HCHg-hch"C"HEPTACLROCSTYRC1AC1B/U6C2/U-5C3C5U3U1OXYCHLORT-CHLORC-CHLORDT-NONAC-NONAHEPT EPOXDIELDop-DDEpp-DDEop-DDDpp-DDDop-DDTpp-DDTMIREXPH.MIREXPCAENDOSULFANMEOCL3CL-VER4CL-VERENDRINTRIFLUTOX_f1TOX_f2CB1CB3CB4/10CB7CB6CB8/5CB19CB18CB17CB24/27CB16/32CB26CB25CB31CB28CB33CB22CB45CB46CB52CB49CB47CB48CB44CB42CB41/71CB64CB40CB74CB70/76CB66CB95CB56/60CB91CB84/89CB101CB99CB83CB97CB87CB85CB136CB110CB82CB151CB144/135CB149CB118CB134CB114CB131CB146CB153CB132CB105CB141CB179CB137CB130/176CB138CB158CB178/129CB175CB187CB183CB128CB185CB174CB177CB171CB156CB201/157CB172/197CB180CB193CB191CB200CB170CB198CB199CB196/203CB189CB195CB207CB194CB205CB206CB209

ngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngng

smplidTCB1245TCB1234P5CBHCBA_HCHB_HCHG_HCHCHEPTCHLOCSTYRC1AC1B_U6C2_U5C3C5U3U1OXYCHLRT_CHLORC_CHLORT_NONAC_NONAHEPTEPODIELDOP_DDEPP_DDEOP_DDDPP_DDDOP_DDTPP_DDTMIREXPHOTMIRPCAA_ENDOSMETHOXYclver3CLVER4ENDRINTRIFLUTOX_2TOX_3P001P003P004_AP007P006p008_aP019P018P017P024_AP016_AP026P025P031P028P033P022P045P046P052P049P047P048P044P042P041_CP064P040P074P070_AP066P095P056_CP091P084_AP101P099P083P097P087P085P136P110P082P151P144_AP149P118P134P114P131P146P153P132P105P141P179P137P130_BP138P158P178_AP175P187P183P128P185P174P177P171P156P201_AP172_AP180P193P191P200P170P198P199P196_AP189P195P207P194P205P206P209

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

Formulas

RA-99-14-PC50.68675.30447.797271.44299.6730.00020.9210.0000.0000.2310.0000.0000.0000.0000.0000.0000.0000.5180.8601.3191.0940.0000.8173.0870.3011.5240.0000.0002.0411.3670.0000.0007.5015.8240.0000.0004.3821.3070.0000.0000.0000.0000.0000.0000.6284.13614.0165.30516.1506.3980.0002.0911.0320.4564.7484.8722.6591.3290.0000.0005.1972.1921.7190.9983.0870.1420.5610.6830.0001.7043.4760.00010.3651.2530.0000.4324.5272.4260.0000.8951.6620.0000.3052.1140.0000.4040.0001.2351.8570.5210.0000.0000.0001.4320.2120.2400.1250.0000.0000.0001.0530.0841.8810.0000.1220.0000.0000.0000.0000.0000.0000.0000.0000.0000.1750.0000.0000.0000.1070.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-15-PC20.45433.25052.575342.194134.8250.00027.8090.0000.0001.9980.0000.0000.0000.0000.0000.0000.0000.9881.1861.7351.7210.0522.1032.4350.5761.5110.0000.0002.0100.8400.0000.0006.57014.0350.0000.0006.6760.0000.0000.0000.0000.0000.0000.0000.60910.21915.1478.90826.96813.5460.0003.6080.0000.3796.71810.3243.2191.5940.0000.0004.9142.7091.2152.0443.0211.6440.0000.0000.0001.5335.1880.00010.8040.0000.0000.6065.5162.1110.0001.0202.4800.0000.0003.1350.0000.0000.0002.1223.2040.0000.0000.0000.0003.1761.0530.7720.1540.0000.0000.0002.9520.1770.0000.0000.0000.0000.1010.0000.0000.0000.0000.0000.0000.0000.3860.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-16-PC43.30653.46925.08183.13013.7650.0004.8360.0000.0000.2470.0000.0000.0000.0000.0000.0000.0000.2230.1980.3710.3850.0000.4311.4480.0470.6170.0000.0000.4830.3410.0000.0672.2992.7430.0000.0000.6430.0000.0000.0000.0000.0000.0000.0000.0001.6028.0594.7036.7352.8900.0001.1960.8532.2751.6624.8242.4120.9490.0000.0001.8270.6501.0650.0001.9700.5920.0000.3650.0000.4661.3610.0002.7100.0000.0000.2441.5260.9740.0000.2641.0720.0000.0001.8140.0000.0000.0001.1281.8420.0000.0000.0000.0002.0290.7990.7100.2000.0000.0000.0002.4350.1090.0000.0000.0000.0000.1090.0000.0000.0000.0000.0000.0000.0000.4620.0000.0000.0000.0850.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-17-PC26.06339.72131.136256.06452.2061.56732.4730.0840.2770.3020.0000.0000.0000.0000.0000.0000.0001.0351.3622.4922.8830.0002.8114.3560.6972.7940.0000.1104.4032.1510.0000.0006.98121.6240.0002.2612.5530.0000.0000.5840.0000.0000.0001.7280.75710.14116.9806.30314.7478.5180.0002.9860.5060.3308.3808.5523.8731.2050.0000.0004.2692.1342.7370.2834.0740.6540.7121.2460.0002.5337.1640.00015.5303.6370.5001.20710.3254.1160.0002.4534.2510.0000.7906.5280.2691.4650.0005.4777.2570.5010.0000.0000.5884.8191.7521.8500.8420.0000.0000.4004.5120.5371.0320.5120.5960.4930.3750.0000.2670.0000.0000.1460.0000.0000.6020.1850.0000.0000.2470.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-18-PC34.66498.77777.765122.87531.0703.71714.6331.0010.1370.1500.0960.0000.0830.0000.2540.0000.0000.6530.7801.7191.1740.2701.6932.4751.1280.6270.1461.5801.1000.8670.0000.0008.98610.2050.0000.0001.2370.0000.0000.9930.1390.0000.0001.0304.3614.3227.8702.0907.2013.7170.0001.7440.2590.2483.2391.8371.4631.1200.0000.1540.9550.6330.5780.0001.0120.4420.4700.4001.2700.0001.0150.0001.3950.1100.2250.1671.2050.6420.0000.2810.3340.0000.0000.7380.0000.1290.0000.3840.4880.0000.0000.0000.0000.9670.0000.0000.0000.1740.0000.0000.2570.0270.0000.0000.0810.0000.0000.0450.3180.0890.0000.1720.1290.0000.0510.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-19-PC2.0931.32124.043194.330111.2901.16675.8731.0520.0800.4350.2050.0250.6990.0000.0510.1910.2531.9931.6026.2253.4780.2094.4324.0940.9971.1780.1320.0002.5831.7950.0000.00026.80165.8990.0000.0002.5940.2950.0007.2166.5750.0000.0000.5810.1632.17311.8573.52116.2172.5960.0002.0850.8580.3107.6263.8543.0000.9950.0000.0002.6241.1850.4730.0002.4900.5040.6421.3241.0611.1863.0200.00064.6260.9311.2370.8236.0161.5390.0001.0721.9570.0000.3413.8980.0000.4080.0002.0093.1820.0000.0000.0000.0001.9860.5250.5250.1010.0000.0000.0001.0860.1370.0000.0000.0000.0000.0990.0000.0000.0000.0000.7270.0000.0000.0750.0000.0000.0000.0370.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-20-PC7.59332.68669.587237.197121.7930.91972.9780.4760.0000.3690.1430.0120.6480.0000.2900.1220.2431.6691.1943.1173.5570.1924.2854.1951.0301.2180.1350.4471.8702.0560.0000.00023.75957.0290.0000.0001.7230.0000.0006.0194.4790.0000.0001.1550.1435.57514.7112.21213.5773.7330.0002.2080.9640.3967.2533.6051.9811.2680.0000.0001.4970.7340.5890.0002.0480.4990.8441.3970.6520.7672.5490.0005.6750.5610.7310.7685.4241.8460.0000.9451.3300.0000.3393.7440.1790.4620.0001.7173.0860.0000.0000.0000.1122.3630.4780.4780.0800.1390.0000.0001.3340.1640.0000.0000.1800.0000.0900.0000.2380.0000.0000.3440.0000.0000.0880.0000.0000.0000.0430.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-21-PC8.17124.68639.453350.865195.1961.019111.2203.2360.0005.0000.0000.0000.5530.0000.2260.0000.3282.3151.8434.1144.4230.2605.7166.1691.2394.5250.0000.2444.4953.8980.0000.00016.06383.8240.0000.0007.4330.0150.0008.6155.0170.0000.0003.1691.6377.50020.7250.00020.6354.9730.1332.3040.0000.12210.8973.5601.1240.3200.0000.1892.2800.7140.8631.4072.8350.0000.0000.6100.0001.3493.4300.0009.9491.7611.9930.4004.6732.5210.0001.2631.7240.0000.4763.2180.2590.6690.0001.9743.2540.1590.0000.0000.3101.7891.1930.5190.1820.0620.0000.1701.4730.1640.1560.0000.2080.0000.1100.0270.0930.0260.2490.0000.0200.0000.0670.0000.0000.0000.0750.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

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RA-99-34-PC2.8347.4587.876151.89231.7771.0774.7450.4710.0000.7320.0000.0810.0330.0000.0000.0000.0500.6660.1800.7520.8000.0683.3703.6370.2911.7940.0000.1291.3090.8760.0000.0004.60816.7000.0000.00010.4200.6250.0002.9936.9440.0000.0000.0000.0006.7615.4280.0004.1081.0810.0001.6600.0000.1808.3931.6440.7060.5960.0850.0002.4461.3780.4360.6611.2090.1600.1590.4810.0000.8451.3740.0002.6400.1970.6270.1001.3080.9630.0000.5340.6400.0000.0001.5530.0000.1200.0000.6311.0570.0000.0000.0000.0000.7080.2530.2530.0000.0250.0000.0670.5860.0000.0000.0000.0000.0000.0500.0000.0000.0000.0000.0000.0000.0000.0600.0000.0000.0000.0940.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-35-PC4.48411.39913.505227.302124.3710.77415.6300.0490.0000.9610.0000.3300.1320.0000.0000.0000.3392.1791.0752.1281.6650.2272.6852.7640.8922.6180.0000.4122.4902.4490.0000.00011.60513.8160.0000.00015.9870.6290.0003.6235.0100.0000.0000.0001.13011.94115.9410.0007.5732.6720.0002.3830.5640.08711.2262.7151.5000.6200.1310.0003.6001.8260.8760.9672.1470.3970.0000.6640.0000.9182.3170.0004.0800.5270.4470.2002.6271.3770.0000.6331.0730.0000.1042.5830.0000.2110.0001.3721.7080.0510.0000.0000.0931.2130.5910.5910.1510.1140.0000.2001.1960.1450.0620.0000.4580.0000.0900.0000.3010.0000.1840.0000.1850.1000.1170.0000.0000.0000.1030.0000.0000.0000.0590.0000.0000.0000.0000.0000.000

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RA-00-46-PC6.40226.07056.436320.081129.8850.00087.7760.3500.3191.6800.0000.0000.2500.0000.0000.0000.4041.3181.1261.9551.4980.0002.6455.4071.58016.9560.5600.4766.48010.5210.0000.00023.38421.0750.0000.00026.9520.2480.0005.2961.2880.0000.0001.0210.00016.10920.7460.00025.1909.1810.0005.1250.8800.84212.3846.0224.3791.2690.5710.0007.6342.7650.9400.5252.0550.4860.4261.2580.3890.8613.0890.0005.0290.3020.3380.1213.3111.1850.0000.6871.2190.1580.1581.6290.1580.4900.0001.3031.8750.0000.0430.0440.4471.2650.3330.4020.2420.1070.0000.2801.3710.1110.1720.0000.1330.0940.1350.0250.0860.0670.0540.0000.0560.0080.1530.0150.0140.0180.0710.0000.0170.0190.0650.0000.0000.0500.0000.0300.042

RA-00-47-PC20.541113.120115.268317.760175.0480.00072.7370.6060.2721.4930.0000.0000.3190.0000.0440.0550.0720.8740.4591.3420.9270.0001.9965.7251.73210.3820.4820.1082.2541.7710.0000.00034.40719.2010.0000.00033.0160.3000.0001.9720.2210.0000.0000.0000.0008.82910.6031.78627.6348.2500.0004.6180.5420.6097.1115.8024.2501.5290.6960.3145.9671.9401.0630.0242.0450.4550.3320.7970.2581.0123.3430.0004.8670.3860.2870.1043.6611.5230.0000.9181.3690.1670.1671.9180.1410.3540.1371.1462.0310.0000.0000.0000.2241.1180.3080.5130.1660.0410.0000.0891.2060.1190.0960.0000.0740.0550.1210.0000.0490.0160.0400.0000.0000.0000.0850.0000.0000.0000.0250.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-00-48-PC5.71119.03839.030258.624162.8851.03267.4760.7380.2871.7300.0000.0600.2230.0000.0350.0000.3482.1531.8113.3602.5650.0003.4014.4181.59516.1760.0000.3624.1946.8840.1520.00036.76825.9060.0000.00026.5950.1210.0004.7875.1850.0000.0000.0000.00017.62913.9040.00019.16710.7780.5802.8651.0040.84710.5065.5763.6011.3140.5710.0005.5110.3700.2130.0932.7060.5450.2640.7170.3100.6782.5980.0004.1300.2040.3860.0002.9791.0280.0000.7561.1190.1310.1311.5570.0740.5470.1611.6611.9920.0000.0000.5850.6012.5890.9010.5710.2920.1110.0110.1421.5780.1370.1610.0000.1650.1370.1110.0260.1220.0700.0620.0000.0710.0000.2960.0300.0160.0000.0990.0000.0000.0190.0510.0000.0000.0560.0000.0660.084

RA-00-49-PC54.83090.80445.182123.30828.5790.2006.0560.1500.1280.2210.0000.0000.0000.0000.0000.0000.2580.0950.5110.4310.0800.0000.7650.2790.0921.9770.0000.0000.2490.0630.0000.0003.5111.1550.0000.0002.5950.0250.0000.2840.3400.0000.0001.4000.6324.3449.5230.84310.6862.0430.3721.8940.2310.3381.5662.2691.4070.4390.0000.0001.0270.4960.3200.0000.5050.3420.0000.0740.0000.2880.5000.0000.8410.2660.0610.0000.5840.2230.0000.0000.1390.0000.0000.3350.0000.0000.0000.1840.5630.0000.0000.0000.0620.4890.4600.4400.0820.0000.0000.0000.7210.0510.0000.0000.0660.0620.0280.0000.0670.0360.0000.0000.0000.0000.0740.0000.0000.0000.0420.0000.0000.0000.0300.0000.0000.0000.0000.0000.000

RA-00-50-PC85.41065.259117.998398.881165.8650.00061.0640.7850.6202.0920.0000.0000.1870.0000.0000.0000.0002.0831.3992.6592.5960.0003.3913.4041.63110.0000.1520.2303.5442.7540.0000.00038.85123.5570.0000.00034.6170.0840.0008.4110.6870.0000.0001.2022.38421.62143.2597.79022.7655.5050.0003.4450.4540.55512.0235.6673.6520.6820.0000.1453.6392.0830.3930.1392.4160.8350.4091.3530.0000.5422.2990.0004.1610.9220.6100.0003.1411.0340.0000.6981.0591.0341.0331.5550.0000.4490.0571.5412.3980.0000.0000.0000.3551.5950.5170.4230.2760.1080.0000.3601.5230.1320.1200.0000.2010.1380.1280.0000.1060.0490.1200.0000.0000.0000.2130.0210.0000.0000.0540.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-00-51-PC75.24189.351107.512232.425125.7950.91997.6950.5490.7881.0650.0000.0000.3370.0000.0000.0000.0000.9411.2741.5961.2710.0003.0303.6881.3679.6070.0000.0592.5361.0300.0000.00029.6528.8430.0000.00024.9000.4460.0003.7750.2850.0000.0004.1460.79717.11718.7573.45039.88924.0490.0007.0350.4130.5867.8585.5595.6011.9620.4140.0004.0891.5291.9690.0592.3300.3360.1250.4661.1940.7753.2400.0005.4291.2350.5610.7764.3771.8800.0000.9741.3950.3420.3422.6860.3040.6110.1671.4753.2300.0870.1090.1110.4791.8090.5390.8290.2700.0630.0000.1721.9230.1490.0670.0000.1590.1180.1460.0040.1250.0700.1500.0000.0000.0000.1170.0000.0000.0000.0350.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-00-52-PC50.776238.444132.569220.843167.3080.92338.4330.6590.3231.3660.0000.0000.0000.0000.0590.0000.2370.7830.7990.8090.5240.0001.3584.8191.0898.2670.0000.1232.4813.4060.0000.00044.0115.9770.0000.00035.5270.1840.0001.1740.3240.0000.0000.0000.25410.4309.6390.78226.5058.4840.7544.1000.6420.7525.5785.1633.6231.5240.5890.0004.2651.2401.0570.0001.5050.6280.2270.7630.0980.7192.5390.0003.4070.2080.4400.0002.5771.1380.0000.6510.9900.0860.0861.3440.0500.2910.1120.9551.6290.0000.0000.0900.3151.0550.2540.3910.1300.0440.0000.0920.9020.0980.0420.0000.0700.0570.0760.0000.0470.0350.0000.0000.0000.0000.1160.0000.0000.0000.0070.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-01-01-PC46.241134.186169.284485.84695.2540.000155.7081.0891.7913.9690.0000.0000.1090.0000.0210.0000.1631.7761.7882.7251.8100.0005.5546.0893.13335.7420.2390.3145.5223.8470.0000.00060.73622.6790.0000.00029.0740.2360.0005.0221.3890.0000.0005.2662.19219.33829.5674.41447.41424.3930.39515.7381.5621.16015.37214.52010.0113.8911.2610.0668.7754.8762.5860.8514.4521.8220.4851.9730.7861.4815.7430.0007.8541.6631.4670.2636.6282.9110.0001.8902.6520.3370.3373.7630.3240.6240.4322.0065.0170.1030.1980.1960.5472.2810.7111.3330.2360.1140.0000.3662.6960.2840.0840.0140.1420.1050.3350.0000.0500.0480.1450.0000.0000.0000.1360.0000.0000.0000.0320.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-01-02-PC52.411203.908146.796256.624194.5622.42934.3430.9010.6602.0110.0000.0000.1910.0000.1170.0000.0000.7041.1411.2111.2020.0001.3823.0171.87012.3611.1312.5887.3323.9420.0000.00028.8558.0740.0000.00030.2870.1680.0003.7810.9060.0000.0008.6921.88012.29424.5762.29026.6447.0070.0007.8930.6060.4727.3276.3054.1731.9700.0000.0735.2501.3241.1130.1132.1751.1500.2920.9970.2960.7122.5790.0003.7170.3430.5190.0003.4931.4220.0000.8211.2170.1860.1861.7280.1040.3440.1111.1302.1650.0000.0000.0000.2971.2250.4200.4620.1710.0560.0000.2131.2490.0950.0460.0000.1190.0760.1060.0000.0640.0260.0570.0000.0000.0000.1460.0000.0000.0000.0430.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-01-06-PC10.29780.240117.612221.055131.6070.00034.3130.6540.2392.4550.4790.0000.2770.0000.0000.0000.1470.9271.1822.3591.0730.0001.6292.4981.56815.3700.3920.0003.1880.9460.0000.00029.84211.4490.0000.00025.5140.1720.0004.2992.7600.0000.0000.0000.37215.75013.5580.80220.8485.2970.0003.0100.4551.2866.2294.4463.2061.2690.0000.0004.2251.5250.6210.1152.0720.4130.2620.8670.0520.6102.2580.0003.4650.2930.1260.1003.1491.4500.2940.5430.7940.1510.1511.4710.1530.4290.0001.2491.9520.1470.1500.0000.1411.0790.3080.2560.2190.0280.0000.1131.1600.0960.0380.0000.1050.1220.0480.0000.1330.0620.0000.0000.0000.0190.1190.0000.0000.0000.1070.0000.0410.0000.0000.0000.0000.0000.0000.0000.000

RA-01-07-PC101.657197.150123.333189.720138.2430.00017.8500.7530.2730.9940.0000.0000.0000.0000.0000.0000.5060.2330.3000.6890.4220.0005.7481.0080.87511.2240.0000.0002.2480.4880.0000.00024.1682.3460.0000.0006.0900.2600.0001.2260.1820.0000.0002.9420.30411.96912.2182.17515.9754.0970.3933.5330.7190.4083.7143.3572.0031.0650.2830.0003.1360.6190.5310.0861.8540.8300.1190.5510.0000.3341.2270.0001.7880.1670.1690.0001.5800.5540.0000.2290.1470.0670.0670.7230.0000.1510.0000.4570.8910.1050.0980.0000.0000.5080.1840.1140.0770.0000.0000.0390.5170.0310.0000.0000.0470.0270.0130.0000.0560.0810.0490.0000.0000.0000.0650.0000.0000.0000.0440.0000.0000.0000.0840.0000.0000.0000.0000.0000.000

RA-01-08-PC128.796186.871109.791161.62390.5790.0006.8010.4760.1890.4210.0000.0000.0000.0000.0000.0000.0000.0360.0200.0800.0000.0050.3120.6240.2973.1040.1890.0000.7840.2380.0000.00014.5200.1970.0000.0003.1640.1100.0000.0000.0000.0000.0001.3010.0005.8539.8580.84312.5542.3850.0002.6070.3890.1502.8682.7811.4430.6920.2020.0001.5530.7750.5240.1070.6660.1010.0370.2150.0000.1260.2320.0000.5250.0580.0870.0000.3130.2980.0840.0000.0000.0000.0000.1250.0000.0000.0000.0790.2780.0000.0000.0000.0000.3630.0780.0610.0470.0000.0000.0000.1590.0320.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0430.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-01-09-PC7.98399.95086.12487.635146.5070.00054.0931.2350.0000.2230.0000.0190.0800.0000.0000.0000.2371.2971.0922.2740.5950.0001.4332.4271.63031.6730.1710.00015.6084.5320.0000.00036.8718.4810.0000.00034.1860.0570.0000.8221.1880.0000.0000.5340.0004.2419.9640.27913.3235.4991.6944.8930.0280.1001.4387.2784.3401.3130.1090.0002.6701.2630.1430.0000.2530.1160.1110.3110.0000.4742.1360.0002.8820.1580.3590.0972.6400.9140.0000.3500.4540.1070.1071.2600.3460.0000.0000.5801.4950.2490.1490.0000.1500.7670.3770.3020.0770.0000.0000.0520.5920.0430.0000.0000.0200.0520.0530.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-01-11-PC53.835180.169121.862246.664105.8110.00013.7621.4230.0000.6200.0000.0000.4200.0000.0000.0000.2330.4030.4461.0490.5410.0001.1490.8560.7923.7350.0000.0001.2310.6640.0000.00016.7567.5790.0000.0009.4521.3370.0002.6521.0830.0000.0000.0000.3885.85711.7741.02720.7223.5690.0003.0560.1600.2983.5394.1671.3440.9490.0000.2432.8561.6530.2570.1091.6530.2370.2020.4960.0000.3751.3790.0002.1380.1610.2370.0872.1110.8860.0000.3690.6370.1080.1081.0720.0760.2340.0000.6541.3590.0860.0000.0000.1050.6830.2190.2360.0970.0000.0000.0370.6400.0350.0000.0000.0390.0300.0420.0000.0620.0760.0000.0000.0000.0000.0460.0000.0000.0000.0280.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-01-12-PC33.839181.243151.512235.11990.4330.48613.0590.9110.0000.6670.0000.0000.1070.0000.0000.0000.4250.5350.5931.2430.9080.0001.3231.3850.8623.7530.0510.0001.3690.5400.0000.00014.56611.2390.0000.0007.3040.0000.0004.8200.9010.0000.0001.4400.5873.68810.9350.63222.3054.3990.0004.0380.2710.3634.1976.1832.5611.6490.7070.0704.1772.0350.4230.1171.8790.3170.4880.8860.0280.5842.2190.0003.3710.0000.3330.1882.9831.1960.0730.5570.8360.2540.2541.6140.0970.2970.0000.9231.7280.1350.0000.0000.0570.8900.3350.1600.1400.0000.0000.0940.9000.0680.0000.0000.0640.0420.0670.0000.0250.0320.0320.0000.0000.0000.0750.0000.0000.0000.0590.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-01-13-PC28.637164.27497.633168.10493.7450.39311.5890.6650.0000.8590.0000.0000.0000.0000.0000.0000.0000.5630.4751.0240.4760.0000.8430.5450.1521.5530.0000.0000.2200.3000.0000.00011.2228.6880.0000.0002.0260.0000.0001.4401.1930.0000.0000.0610.0000.5832.7640.6897.6431.5120.0001.0960.1290.1921.2551.5770.8400.5750.1070.0001.7530.6940.2180.1210.8050.1230.1000.2800.0580.1490.7010.0001.2390.1340.1130.0000.9420.4140.0000.1230.2930.0000.0000.5420.0000.1560.0000.4090.6210.0230.0000.0000.0000.7810.1150.0700.0550.0000.0000.0000.3970.0000.0000.0000.0230.0000.0000.0000.0400.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-99-18-P19.49315.6041.4600.8140.0750.0000.5910.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0450.0670.0000.0000.0000.5490.0000.1630.0000.0000.0000.0870.0000.0000.2400.1240.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0001.1902.0630.0000.0000.0000.0000.0000.4871.1170.4411.1920.5480.0000.0000.0000.3570.1900.0000.0000.3810.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.2090.0000.0000.4310.0000.0000.0000.0000.4880.0000.0000.0000.0000.6070.0000.0000.0000.0000.0000.0000.7490.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.1860.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-99-22-P16.22613.7081.4760.9480.1400.0960.6960.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.4900.0000.1750.0000.0000.0000.0000.0000.0000.4470.0670.0000.0000.0340.0000.0000.0000.0000.0000.0000.0000.0000.9552.2160.0000.5130.0000.0000.0000.0001.0420.0001.2340.7270.1860.0000.0000.4140.1890.4340.0000.3440.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.2670.0000.0000.3020.0000.0000.0000.2650.3430.0000.0000.0000.0000.5360.0000.0000.0000.0000.0000.0000.6580.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.1460.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-00-10-P10.3300.3770.0680.3701.0260.0520.6760.1610.0360.0000.0000.0000.3160.0000.0000.0000.0000.0000.0000.0810.0000.0000.0000.5190.0000.6720.0000.0000.1660.5420.0000.0001.0880.1560.0000.1130.0280.0090.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0400.0000.0000.0000.3480.0000.0000.0000.0000.2260.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-00-14-P10.1870.2400.2020.8150.7270.0000.4950.0000.0910.0000.0000.0000.1880.0000.0000.0000.0000.0000.0000.0420.0000.0000.0000.4810.0000.2920.0000.1540.1530.1260.0000.0001.5970.2210.0000.0100.0960.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.1780.0000.0000.0000.0000.1650.0000.2990.2840.0000.0000.0000.4330.2170.0000.0000.4390.0000.0000.2840.0000.0000.1330.0000.0000.0000.0000.0000.0000.0450.0000.0000.2220.9390.0000.1110.0000.0000.0000.0000.0000.0000.0640.0000.0000.0880.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.2000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-00-18-P10.3440.4690.0390.2212.3960.0231.0430.0000.1020.0000.0000.0000.4690.0000.0000.0000.0000.0000.0000.0280.0000.0000.0000.6930.1611.1350.0000.0000.2300.5570.0000.0002.0550.1200.0000.0000.0000.0350.0000.0000.0000.0000.0000.0000.0000.0000.3840.0000.0000.0000.0000.0000.0000.0000.0000.0000.6810.0000.0000.0000.0000.0950.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.4330.1970.0000.2980.0000.0000.0000.0000.0000.0000.0000.1150.2080.1070.0000.3930.2120.0000.1000.0000.0000.0000.0000.1280.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-00-22-P10.2610.8630.1830.6911.7790.0630.6830.0000.1780.0000.0000.0000.3660.0000.0000.0000.0000.0000.0650.1000.0000.0000.0000.6030.1121.2410.0000.0000.4690.8360.0000.0000.4700.1760.0000.0000.0200.2280.0000.0000.0000.0000.0000.2260.0000.0000.5730.0000.0000.0000.0000.0980.0000.1280.0000.1550.1410.0670.0000.0000.0000.0000.0000.0000.1510.0000.0000.0640.0000.0000.0000.0000.0000.0000.0000.0000.0000.0960.0000.0000.0000.9030.0000.1510.0000.0000.0000.0000.0000.0000.4360.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-averagetotal2.8075.2100.5710.6431.0240.0390.6970.0270.0680.0000.0000.0000.2230.0000.0000.0000.0000.0000.0180.0530.0000.0000.0000.5560.0460.6130.0000.0260.1700.3580.0000.0000.9830.1440.0000.0210.0300.0450.0000.0000.0000.0000.0000.0380.0000.3580.8730.0000.1150.0000.0000.0230.0810.4090.0730.5380.3970.0420.0000.0000.2380.1150.0720.0000.2190.0000.0000.0580.0000.0000.0220.0000.0000.0000.0000.0000.0000.0230.0000.0000.1160.3070.0000.1660.0000.0000.0000.0440.1390.0000.1560.0330.0000.2550.0000.0000.0000.0000.0000.0000.2340.0190.0350.0180.0000.0660.0350.0000.0170.0000.0000.0000.0000.0210.0550.0330.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RB-average20000.2810.4870.1230.5241.4820.0350.7240.0400.1020.0000.0000.0000.3350.0000.0000.0000.0000.0000.0160.0620.0000.0000.0000.5740.0680.8350.0000.0390.2540.5150.0000.0001.3030.1680.0000.0310.0360.0680.0000.0000.0000.0000.0000.0560.0000.0000.2390.0000.0440.0000.0000.0340.0000.0730.0000.2010.2770.0170.0000.0000.1650.0780.0000.0000.1480.0000.0000.0870.0000.0000.0330.0000.0000.0000.0000.0000.0000.0350.0000.0000.0550.4600.0000.0660.0000.0000.0000.0000.0000.0000.2330.0490.0000.0970.0000.0000.0000.0000.0000.0000.0000.0290.0520.0270.0000.0980.0530.0000.0250.0000.0000.0000.0000.0320.0000.0500.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

Column, Description1: Station Letter2: A-Active, B=Field Blank L=Lab Blank D=Duplicate Q=Lab QC3: dash4-5 : year6 : dash7-8: Week number9: dash10-11: F1=Filter 1, P1=Puff 1, P1=Puff 2(12-13 are used to identify repeats ...)12: R=Repeat, blank=main 13: Repeat number

Notes:If Lab QC, describe method in lab textual comment field

14-18 1999 18 1999

19-22 1999 22 1999

23 99 . -

2000 - 8 10 2000

12-14 2000 14 2000

15-18 2000 18 2000

19-28 2000 22 2000

46 2000 - 2000

51 1999 lnP 1/, -

P-2Blank,ng

PCB/OC for NCP. File Name:SampleTotalMain SampleOC1OC2OC3OC4OC5OC6OC7OC8OC9OC10OC11OC12OC13OC14OC15OC16OC17OC18OC19OC20OC21OC22OC23OC24OC25OC26OC27OC28OC29OC30OC31OC32OC33OC34OC35OC36OC37OC38OC39OC40OC41OC47OC48OC49OC50OC51OC52OC53OC54OC55OC56OC57OC58OC59OC60OC61OC62OC63OC64OC65OC66OC67OC68OC69OC70OC71OC72OC73OC74OC75OC76OC77OC78OC79OC80OC81OC82OC83OC84OC85OC86OC87OC88OC89OC90OC91OC92OC93OC94OC95OC96OC97OC98OC99OC100OC101OC102OC103OC104OC105OC106OC107OC108OC109OC110OC111OC112OC113OC114OC115OC116OC117OC118OC119OC120OC121OC122OC123OC124OC125OC126OC127OC128OC129OC130OC131OC132OC133OC134

VolumeExtractExtract1,2,4,5-tetrachlorobenzene1,2,3,4-tetrachlorobenzenepentachlorobenzenehexachlorobenzenealpha-hexachlorocyclohexanebeta-hexachlorocyclohexanegama-hexachlorocyclohexanecomponent of technical chlordaneheptachloroctachlorostyrenecomponent of technical chlordanecomponent of technical chlordaneheptachloro compound in technical chlordaneheptachloro compound in technical chlordanecomponent of technical chlordaneintermediate metabolite of chlordanephotoheptachloroxychlordanetrans-chlordanecis-chlordanetrans-nonachlorcis-nonachlorheptachlor epoxidedieldrin1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethylene1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane1,1-dichloro-2,2-bis(p-chlorophenyl)ethane1,1,1-trichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane1,1,1-trichloro-2,2-bis(p-chlorophenyl)ethanemirexphotomirexpentachloroanisoleendosulfanmethoxychlortrichloroveratroltetrachloroveratrolendrintrifluralintoxaphene-2toxaphene-3242,2'/2,62,42,3'PCB8/52,2',62,2',52,2',42,3,6/2,3',62,2',3/2,4',2,3',52,3',42,4',52,4,4'2',3,42,3,4'2,2',3,62,2',3,6'2,2',5,5'2,2',4,5'2,2',4,4'2,2',4,52,2',3,5'2,2',3,4'2,2',3,4/2,32,3,4',62,2',3,3'2,4,4',52,3',4',5/2'2,3',4,4'2,2',3,5',62,3,3',4'/2,2,2',3,4',62,2',3,3',6/2,2',4,5,5'2,2',4,4',52,2',3,3',52,2',3',4,52,2',3,3',4,2,2',3,4,4'2,2',3,3',6,2,3,3',4',62,2',3,3',42,2',3,5,5',PCB144/1352,2',3,4',5'2,3',4,4',52,2',3,3',5,2,3,4,4',52,2',3,3',4,2,2',3,4',5,2,2',4,4',5,2,2',3,3',4,2,3,3',4,4'2,2',3,4,5,52,2',3,3',5,2,2',3,4,4',2,2',3,3',4,2,2',3,4,4',2,3,3',4,4',2,2',3,3',5,2,2',3,3',4,2,2',3,4',5,2,2',3,4,4',2,2',3,3',4,2,2',3,4,5,52,2',3,3',4,2,2',3,3',4'2,2',3,3',4,2,3,3',4,4',PCB201/1572,2',3,3',4,2,2',3,4,4',2,3,3',4',5,2,3,3',4,4',2,2',3,3',4,2,2',3,3',4,2,2',3,3',4,2,2',3,3',4,PCB196/2032,3,3',4,4',2,2',3,3',4,2,2',3,3',4,2,2',3,3',4,2,3,3',4,4',2,2',3,3',4,2,2',3,3',4,

Sample IDWeightWeight1245TCB1234TCBP5CBZHCBZa-HCHb-HCHg-hch"C"HEPTACLROCSTYRC1AC1B/U6C2/U-5C3C5U3U1OXYCHLORT-CHLORC-CHLORDT-NONAC-NONAHEPT EPOXDIELDop-DDEpp-DDEop-DDDpp-DDDop-DDTpp-DDTMIREXPH.MIREXPCAENDOSULFANMEOCL3CL-VER4CL-VERENDRINTRIFLUTOX_f1TOX_f2CB1CB3CB4/10CB7CB6CB8/5CB19CB18CB17CB24/27CB16/32CB26CB25CB31CB28CB33CB22CB45CB46CB52CB49CB47CB48CB44CB42CB41/71CB64CB40CB74CB70/76CB66CB95CB56/60CB91CB84/89CB101CB99CB83CB97CB87CB85CB136CB110CB82CB151CB144/135CB149CB118CB134CB114CB131CB146CB153CB132CB105CB141CB179CB137CB130/176CB138CB158CB178/129CB175CB187CB183CB128CB185CB174CB177CB171CB156CB201/157CB172/197CB180CB193CB191CB200CB170CB198CB199CB196/203CB189CB195CB207CB194CB205CB206CB209

m3ggngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngngng

smpliddummydummydummyTCB1245TCB1234P5CBHCBA_HCHB_HCHG_HCHCHEPTCHLOCSTYRC1AC1B_U6C2_U5C3C5U3U1OXYCHLRT_CHLORC_CHLORT_NONAC_NONAHEPTEPODIELDOP_DDEPP_DDEOP_DDDPP_DDDOP_DDTPP_DDTMIREXPHOTMIRPCAA_ENDOSMETHOXYclver3CLVER4ENDRINTRIFLUTOX_2TOX_3P001P003P004_AP007P006p008_aP019P018P017P024_AP016_AP026P025P031P028P033P022P045P046P052P049P047P048P044P042P041_CP064P040P074P070_AP066P095P056_CP091P084_AP101P099P083P097P087P085P136P110P082P151P144_AP149P118P134P114P131P146P153P132P105P141P179P137P130_BP138P158P178_AP175P187P183P128P185P174P177P171P156P201_AP172_AP180P193P191P200P170P198P199P196_AP189P195P207P194P205P206P209

XXXXXXXXXXXxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

Formulas

RA-99-14-PC1496629.6014.6431.70044.09644.877269.81499.5220.00019.7390.0000.0000.2310.0000.0000.0000.0000.0000.0000.0000.5180.7711.1841.0940.0000.8171.9890.3011.1980.0000.0002.0411.1920.0000.0007.0215.5750.0000.0004.3821.3070.0000.0000.0000.0000.0000.0000.6281.7569.8905.30516.1506.3980.0002.0910.058-1.7783.8672.4881.5641.3290.0000.0004.4831.8131.7190.9982.3260.1420.5610.6830.0001.7043.4760.00010.3651.2530.0000.4324.5272.4260.0000.8951.2440.0000.3051.2510.0000.4040.0001.2350.8800.5210.0000.0000.0000.2190.2120.2400.1250.0000.0000.000-0.4450.0841.8810.0000.1220.0000.0000.0000.0000.0000.0000.0000.0000.000-0.1970.0000.0000.0000.1070.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-15-PC1319730.9315.421.4672.04249.655340.566134.6750.00026.6280.0000.0001.9980.0000.0000.0000.0000.0000.0000.0000.9881.0971.6001.7210.0522.1031.3370.5761.1840.0000.0002.0100.6660.0000.0006.09013.7860.0000.0006.6760.0000.0000.0000.0000.0000.0000.0000.6097.83911.0208.90826.96813.5460.0003.608-0.975-1.8545.8367.9412.1241.5940.0000.0004.2002.3301.2152.0442.2601.6440.0000.0000.0001.5335.1880.00010.8040.0000.0000.6065.5162.1110.0001.0202.0620.0000.0002.2720.0000.0000.0002.1222.2280.0000.0000.0000.0001.9631.0530.7720.1540.0000.0000.0001.4550.1770.0000.0000.0000.0000.1010.0000.0000.0000.0000.0000.0000.0000.0140.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-16-PC421328.6914.3824.32022.26122.16181.50213.6140.0003.6550.0000.0000.2470.0000.0000.0000.0000.0000.0000.0000.2230.1090.2360.3850.0000.4310.3500.0470.2900.0000.0000.4830.1660.0000.0671.8192.4940.0000.0000.6430.0000.0000.0000.0000.0000.0000.0000.000-0.7783.9324.7036.7352.8900.0001.196-0.1220.0410.7802.4401.3170.9490.0000.0001.1130.2711.0650.0001.2080.5920.0000.3650.0000.4661.3610.0002.7100.0000.0000.2441.5260.9740.0000.2640.6540.0000.0000.9510.0000.0000.0001.1280.8650.0000.0000.0000.0000.8160.7990.7100.2000.0000.0000.0000.9380.1090.0000.0000.0000.0000.1090.0000.0000.0000.0000.0000.0000.0000.0890.0000.0000.0000.0850.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-17-PC1163626.1413.157.0768.51328.216254.43652.0561.56731.2910.0840.2770.3020.0000.0000.0000.0000.0000.0000.0001.0351.2732.3572.8830.0002.8113.2580.6972.4670.0000.1104.4031.9760.0000.0006.50221.3750.0002.2612.5530.0000.0000.5840.0000.0000.0001.7280.7577.76112.8536.30314.7478.5180.0002.986-0.469-1.9047.4996.1682.7781.2050.0000.0003.5551.7552.7370.2833.3130.6540.7121.2460.0002.5337.1640.00015.5303.6370.5001.20710.3254.1160.0002.4533.8330.0000.7905.6650.2691.4650.0005.4776.2800.5010.0000.0000.5883.6061.7521.8500.8420.0000.0000.4003.0150.5371.0320.5120.5960.4930.3750.0000.2670.0000.0000.1460.0000.0000.2300.1850.0000.0000.2470.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-18-PC651426.5013.2515.67767.56974.845121.24830.9193.71713.4511.0010.1370.1500.0960.0000.0830.0000.2540.0000.0000.6530.6911.5841.1740.2701.6931.3771.1280.3000.1461.5801.1000.6920.0000.0008.5069.9560.0000.0001.2370.0000.0000.9930.1390.0000.0001.0304.3611.9413.7432.0907.2013.7170.0001.744-0.716-1.9862.358-0.5460.3681.1200.0000.1540.2410.2530.5780.0000.2510.4420.4700.4001.2700.0001.0150.0001.3950.1100.2250.1671.2050.6420.0000.281-0.0830.0000.000-0.1240.0000.1290.0000.384-0.4890.0000.0000.0000.000-0.2470.0000.0000.0000.1740.0000.000-1.2400.0270.0000.0000.0810.0000.0000.0450.3180.0890.0000.1720.1290.000-0.3210.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-19-PC1337725.6012.67-10.360-26.09521.091192.434111.0110.97474.4811.0520.0800.4350.2050.0250.6990.0000.0510.1910.2531.9931.6026.2253.4780.2094.4323.1140.9970.8280.1320.0002.5831.7950.0000.00025.90765.7640.0000.0002.5260.2950.0007.2166.5750.0000.0000.5810.1630.2637.4243.52115.1912.5960.0002.0850.858-1.7737.6261.3851.5460.6230.0000.0001.7960.807-0.3950.0001.8020.5040.6421.3241.0611.1863.0200.00064.6260.9311.2370.8236.0161.5390.0001.0721.4230.0000.3413.2940.0000.4080.0001.4782.4960.0000.0000.0000.0000.9140.5250.5250.1010.0000.0000.000-0.2300.1370.0000.0000.0000.0000.0990.0000.0000.0000.0000.7270.0000.000-0.2160.0000.0000.0000.0370.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-20-PC1295425.4112.74-4.8605.27066.636235.300121.5130.72771.5850.4760.0000.3690.1430.0120.6480.0000.2900.1220.2431.6691.1943.1173.5570.1924.2853.2151.0300.8690.1350.4471.8702.0560.0000.00022.86656.8950.0000.0001.6550.0000.0006.0194.4790.0000.0001.1550.1433.66510.2782.21212.5513.7330.0002.2080.964-1.6877.2531.1360.5260.8960.0000.0000.6680.355-0.2800.0001.3600.4990.8441.3970.6520.7672.5490.0005.6750.5610.7310.7685.4241.8460.0000.9450.7960.0000.3393.1400.1790.4620.0001.1872.4010.0000.0000.0000.1121.2910.4780.4780.0800.1390.0000.0000.0180.1640.0000.0000.1800.0000.0900.0000.2380.0000.0000.3440.0000.000-0.2030.0000.0000.0000.0430.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-21-PC1283027.8113.81-4.281-2.73036.502348.968194.9160.827109.8283.2360.0005.0000.0000.0000.5530.0000.2260.0000.3282.3151.8434.1144.4230.2605.7165.1891.2394.1760.0000.2444.4953.8980.0000.00015.17083.6900.0000.0007.3650.0150.0008.6155.0170.0000.0003.1691.6375.59016.2920.00019.6094.9730.1332.3040.000-1.96210.8971.091-0.330-0.0520.0000.1891.4510.335-0.0051.4072.1470.0000.0000.6100.0001.3493.4300.0009.9491.7611.9930.4004.6732.5210.0001.2631.1900.0000.4762.6140.2590.6690.0001.4432.5680.1590.0000.0000.3100.7171.1930.5190.1820.0620.0000.1700.1570.1640.1560.0000.2080.0000.1100.0270.0930.0260.2490.0000.0200.000-0.2250.0000.0000.0000.0750.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-22-PC1300128.4714.32-5.790-5.19424.027347.734186.6400.748108.0892.6110.0005.0000.0000.0000.2890.0000.3190.0000.2622.2061.3014.0714.0580.3256.1364.6691.0063.4020.0001.3434.1554.2870.0000.00013.55554.8661.1730.00010.2640.1850.0007.4466.8080.0000.0000.2981.1563.2688.9150.88212.5013.3650.1211.6870.000-1.9238.5920.7060.4610.4280.0000.0001.5710.8190.0431.2921.0030.0000.0001.0390.0001.4002.2770.0007.4071.3541.5680.3003.2351.9080.0000.6370.7320.0000.2821.8410.1920.4940.2521.1431.9220.0000.0000.0000.2660.5481.1970.4940.1520.0600.0680.1800.0470.1730.0240.0000.1170.0000.0890.0000.1520.0000.0800.0000.0000.000-0.2120.0000.0000.0000.0760.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-23-PC1320030.5015.20-0.2788.48011.388268.074150.0261.15467.9591.159-0.1360.1790.0000.129-0.1880.0000.0000.0000.2111.8380.9962.8713.6900.4325.3773.8990.8693.1680.0000.5155.0955.0380.0000.00014.03224.5940.000-0.04111.854-0.0910.0006.5666.5610.0000.0001.0480.3475.43310.3091.64514.8302.8160.6421.611-0.162-0.6045.4441.5281.4640.7910.1800.0001.1390.5470.4280.4720.5660.0000.0000.1520.0000.6021.8990.0005.5260.4820.9150.1692.4961.5840.0960.5560.849-0.6140.1593.7150.0000.3320.1941.3071.8000.133-0.177-0.0660.1510.7130.8120.4880.1600.0530.0960.1920.8890.1310.001-0.0080.202-0.0470.0670.0220.0610.1130.3440.0000.016-0.043-0.004-0.0570.0000.0000.1010.0000.0140.0170.0120.0000.0000.0000.0000.0000.000

RA-99-24-PC1317927.3213.563.8536.06522.746167.784125.1212.38844.2050.603-0.1360.0000.0000.000-0.1480.0000.2910.1000.2231.8580.8312.6162.4260.1015.1262.9080.5250.4740.0351.3692.4913.5340.0000.00014.11714.9660.000-0.0412.8060.1960.0006.7349.9630.0000.0003.0390.2687.07314.8582.2338.2955.4670.0002.8250.473-0.8177.2111.5972.0651.3430.0000.0001.6191.4551.1110.0002.4230.4870.9210.8290.0000.0002.7150.0004.1310.3330.5200.8145.3482.3120.0000.8731.277-0.6140.2953.0700.3450.4420.0001.4642.5310.000-0.311-0.0660.5132.6550.8250.8250.1200.0990.0000.0001.0210.148-0.069-0.0360.000-0.1310.0930.0000.1380.0000.0000.4820.000-0.0430.088-0.0670.0000.0000.0990.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

RA-99-25-PC1312533.6316.77-0.0382.73013.010269.592160.3430.31568.5532.080-0.1363.5000.0000.0000.0260.0000.1100.0000.2452.3041.0643.4062.8610.3963.6952.8191.0462.6320.0000.3223.8125.3520.0000.00015.83618.1530.000-0.04120.022-0.0830.0004.8635.6940.0000.0000.3140.6287.81513.2980.9009.2905.7180.5342.552-0.162-0.73210.1522.6721.0240.5110.3920.0001.9890.9700.4880.7921.6080.4140.0000.4430.0001.5262.4260.0006.8860.6021.1430.4003.9061.8740.0000.7670.992-0.6140.1012.0720.2110.4720.0001.7682.3620.039-0.311-0.0660.1541.2321.0240.7440.1380.0420.1310.1100.8510.064-0.017-0.0360.167-0.0710.0670.000-0.0020.0510.2370.0000.054-0.043-0.018-0.0670.0000.0000.0830.0000.0770.0000.0000.0000.0000.0000.0000.0000.000

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