ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton,...

24
Client: I I City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Nl,lillber: 00010503 ontinental Anal!:Jtical Services, Inc. Page: 2 Date Sample Rptd: 01/19/2000 Date Sample Recd: 01/11/2000 Continental File No: 7074 Continental Order No: 60515 Client P.O.: Sample Description: Mulberry Well Date Sampled: 01/10/2000 Time Sampled: 1130 Analysis Trichloroethylene pH Concentration 6.8 7.7 H Date Units μg/L Std Date Analyzed Book/Page 01/14/2000 4194/316 01/11/2000 4358/78 Analysis Trichloroethylene pH Prepared QC Batch Analyst Method(s) NA 1GC1013 JTJ 601/8021B NA 000111-1 AJV 150.l/9040B H - Recommended sample holding time was exceeded. Conclusion of Lab Number: 00010503 Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified. CONTINENTAL ANALYTICAL SERVICES, INC. Cli~;..jf:f: Lab~~~\Jirector 1 804 GLENDALE ROAD SALINA, KANSAS 6740 l -6675 785-827-1 273 800-535-3076 FAX 785-823-7830

Transcript of ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton,...

Page 1: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

Client:

I

I • City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020

Lab Nl,lillber: 00010503

ontinental Anal!:Jtical Services, Inc.

Page: 2

Date Sample Rptd: 01/19/2000 Date Sample Recd: 01/11/2000 Continental File No: 7074 Continental Order No: 60515 Client P.O.:

Sample Description: Mulberry Well Date Sampled: 01/10/2000 Time Sampled: 1130

Analysis

Trichloroethylene pH

Concentration

6.8 7.7 H

Date

Units

µg/L Std

Date Analyzed Book/Page

01/14/2000 4194/316 01/11/2000 4358/78

Analysis

Trichloroethylene pH

Prepared QC Batch Analyst Method(s)

NA 1GC1013 JTJ 601/8021B NA 000111-1 AJV 150.l/9040B

H - Recommended sample holding time was exceeded.

Conclusion of Lab Number: 00010503

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONTINENTAL ANALYTICAL SERVICES, INC.

Cli~;..jf:f: Lab~~~\Jirector

1 804 GLENDALE ROAD • SALINA, KANSAS 6740 l -6675

785-827-1 273 • 800-535-3076 • FAX 785-823-7830

Page 2: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

OPt;RATIONAL CONTROL PARAMETERS

PH DATE UNITS

ALK. ml/I

2

I 1._,_.-. ./ ir"1 . 3 1 /,.::7" '--' t)DD J

4

5

6

8 r

9

10 /2t) C'c!:. /

11

12 V,5c ,OOl1

13

14

15

16

f DO mg/I

CJ

11 / :5'(}, , ,,.,!/!JD /

18

19

22

23

27

2a j,;). rJ OOb ,.

29

30

SET SUS. SOLIDS SETTLEABILITY SOLIDS RAW MIXED LIQUOR MIXED LIQUOR

i ml/I mg/I ml/I

SLLJDGE DISP. (LBS. DRY WT.)

TEMP RAIN 'F. 'C AND

· WEATI-iER

coMMENrs /?.L.::-1/&/?7,/T 4 ~o- O/~t/.3J?CJ (!>TY c.') /:::- (!' A /77 Oc?-J I t) /LY J/ ;< e (!) t...J 1c.-r e I ic:. e. c L-=- P. o Bex / 63/ s CAMD1:=~ro.J t., s o;:Jo

TESTS PERFORMED av TITLE PHONE#

TESTS PERFORMED BY TITLE PHONE#

MO 780-1306 (12-97)

(!)-

E _g :;::: C Q) 0 f:O

... 0

f!.! (!)

ui Q)

Ol '-6

)0)} fJL-e-k' T C:o s,;---:tq

J=J L-J U/IZ ECTtl)lc,

..573,- 3'-le:.- 7;292

DATE

DATE

Page 3: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

j

Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020

Lab Number: 00020738

Continental · Analytical Services, Inc.

Page: 2

. Date Sample Rptd: 02/22/2000 Date Sampl·e Recd: 02/08/2000 Continental File No: 7074 Continental Order No: 61089 Client P.O.:

Sample: pescription: Mulberry Well Date Sampled: 02/07/2000 Time Sampled: 1250

Analysis

Trichloroethylene pH

Concentration

6.0 7.5

Date

Units

µg/L Std

Date Analyzed Book/Page

02/18/2000 4370/113 02/08/2000 4358/101

Analysis

Trichloroethylene pH

Prepared QC Batch Analyst Method(s)

NA 1GC4048 JTJ NA 000208-1 MRM

Conclusion of Lab Number: 00020738 \

601/8021B 150,1/9040B

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated, update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONT~INE&AL@TJ:/CAL Cli d . Baker Techn 1 M ager

SERVICES, INC.

1 804 GLENDALE RCJAD • SALINA, KANSAS 6740 1 ·6675

785-827·1 273 • 8CJCJ·535·3CJ76 • F"AX 795·823·783Cl

KDHE Environmental Laboratory Accreditation No. E-10146

Page 4: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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I I 0!; ~ tt: · 1 l!.( fr' 7 -3. hi. . It'll .\ I O z (\ . ~ r ~v . \ !r ~ ~ \ ~ \J'\ '\. ~ 1. Fill .out one copy of report eacJmonth_ and mail in ~onthly !or each trea~ent facility._fu, · ft . I

1 N ~ ~) 2.. Mail one copy of report to the appropriate DNA regional office as note~ in your permirfind k~ one copy in your files. · th } ~ & ~ 3. . Reports must be signed by whoever performed tests and by an appropriate official. e D

\...:_.. ~ 4. In the weathef column, use the followin!] symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy and 0-overcast. • 9 D (A) ~ ~ 5. Use grab sample for pH, Temp. and 0.0. Use grab samples f9r all operational control test.

,.\\.. ~ "'1 6. Use 24 hr. composite (proportional) samples for 8.0.D. 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard , ' ,. I Methods" or an approved equal for all parameters.

~ ('} ~ 7. Treatment r:>lant flow _measurem~nts may be made on either influent or ~ffluent. Lagoon in_fluent flow measu~ements need he on_ly at the time 1 q, }... \: 9f composite sampling of the influent. All tests must be performed In accordance with NPDES Permit Con. and Operational Control )\f ) ~ Regulation 10 CSR 20-9.010. Review your permit for specific requirements.

~ () 111 8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources. ci "'l ·9. Represe~tative sludge samples should be taken either before entering ·,digesters and/or holding tanks or after removal from digesters or ~ , ~ holding tanks. · U..1 (\J

Page 5: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

I

Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020

Lab Number: 00030568

Continental · Analytical Services. Inc.

Page: 2

Date Sample Rptd: 03/16/2000 Date Sample Recd: 03/07/2000 Continental File No: 7074 Continental Order No: 61694 Client P.O.:

Sample Description: Mulberry Well Date Sampled: 03/06/2000 Time Sampled: 1320

Date Concentration Units Analyzed Book/Page Analysis

Trichloroethylene pH

8.9 7.4

µ.g/L Std

03/08/2000 3890/379 03/07/2000 4486/25

Analysis

Trichloroethylene pH

Date Prepared QC Batch Analyst

NA 1GC2068 JTJ NA 000307-1 MRM

Conclusion of Lab Number: 00030568

Method(s)

601/8021B 150.l/9040B

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONiTINE~T

6AL.1~TICAL

Cli d 0 Baker Tech:h ca] anager

SERVICES, INC.

l 804 GLENDALE ROAD • SALINA, KANSAS 67401-6675

785-827-1273 • 800-535-3076 • FAX 785-823-7830

Page 6: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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~ ~ 1. Fill out one copy of report each month and mail in monlhly for each treatment facility. ~ - :-y ~ ~- t.." 2. Mail one copy of report to the appropriate DNA regional office as not~ in your permit and keep one copy i~our files.

, : ~ 3. -Reports must be signed by whoever performed tests and by an appropriate official.

0 (A t:., ~- 4. In the weather column, use the followin~ symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy and 0-overcast. ~ ~- ~ _ 5. Use grab sample for pH, Temp. and D.O. Use grab samples f9r all operational control test.

r-, ~ , 6. Use 24 hr. composite (proportional) samples for 8.0.D. 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard ,. Methods" or an approved equal for all parameters.

\ . ~ 'l ~ 7. Treatment plant flow measurements may be made on either influent or effluent Lagoon influent flow measurements need he only at the time 'ij {} t, 9f composite sampling of the influent. All tests must be performed in accordance with NPDES Permit Con. and Operational Control' \) tr; Regulation 10 CSR 20-9.01Q. Review your permit for specific requirements. _ _

~ ~ 'i} 8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources. W t! ·9. Representative sludge· samples should be taken either before entering digesters and/or holding tanks or after removal from digesters or ~ holding t~nks. _ ·

iJ

"")

Page 7: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

j

Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020

Lab Number: 00040930

ontinental Anal!:dtical Services. Inc.

Page: 2

Date Sample Rptd: 04/21/2000 Date Sample Recd: 04/11/2000 Continental File No: 7074 Continental Order No: 62483 Client P.O.:

Sample' Description: Mulberry Well Date Sampled: 04/10/2000 Time Sampled: 1248

Date Concentration Units Analyzed Book/Page Analysis

Trichloroethylene pH

7.4 7.5

µg/L Std

04/13/2000 4194/403 04/11/2000 4486/61

Analysis

Trichloroethylene pH

Date Prepared QC Batch Analyst

NA 1GC1103 JTJ NA 000411-1 MDB

Conclusion of Lab Number: 00040930

Method(s)

601/8021B 150.l/9040B

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONTINENTAL ANALYTICAL SERVICES, INC.

Cli ~£)A~~::: Tec~1t~1(:jnager

1 804 GLENDALE ROAD • SALINA, KANSAS 67401 ·6675

785·827·1 273 • 800·535·3076 • FAX 785·823·7830

KDHE Environmental Laboratory Accreditation No. E-1D146

Page 8: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

a irl irl ' r--o () c., . Ci) I\) I\) I\) I\) I\) I\) I\) I\) I\) I\) ~ - ~ ~ ~ ~ ~ ~ ~ ~ ~- 'lk '? en en tv' \J 3: • m _m cit ~ ~ "'- '- 11, \. ~ _... o co m ..._,, m en ~. (i.) N _... o co ex, '"'1 m en ~ tJ N ....a. o co ex, ---.J Ol rn ~ C.tJ N .... ~ .-"'D_

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Fill out one copy j report1~ch month :~d mail in monthly for each treatment facility. 'l "', i Mail one copy of report to the appropriate DNA regiona! office as noted in your permit and keep one copy in your files. · ~

. Reports must be signed by whoever performed tests and by an approp.riate official. ,

In the weather column, use the followin~ symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy and a-overcast. Use grab sample for pH, Temp. and 0.0. Use grab samples for all operational control test.

;;; )> '.D ~z~ :r: 0 Z g:J

Use 24 hr. composite (proportional) samples for 8.0.D., 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard Methods" or an approved equal for all parameters. ·

·1 ~ '-'

~ -~ ~\) 7. Treatment plant flow measurements may be made on either influent or effluent. lagoon influent flow measurements need be only at the time

9f composite sampling of the influent. All tests must be performed in accordance with NPDES Permit Con. and Operational Control Regulation 10 CSR 20-9.010. Review your permit for specific requirements. .

N '1 lll

~ ~si 8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources.

9. Representative sludge samples sh~uld be taken either before entering digesters and/or holding tanks or after removal from digesters or holding tanks.

Page 9: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

-[ontin ntal /

Client: 8ity of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020

· Anal!::Jtical Services. Inc. Page: 2

Date Sample Rptd: 05/12/2000 Date Sample Recd: 05/09/2000 Continental File No: 7074 Continental Order No: 63114 Client P.O.:

Lab Number: 00050756 Sample;Description: Mulberry Well

Date Sampled: 05/08/2000 Time Sampled: 1310

Analysis

Trichloroethylene pH

Concentration

7.9 7.4

Date

Units

µg/L Std

Date Analyzed Book/Page

05/11/2000 4194/436 05/09/2000 4486/85

Analysis

Trichloroethylene pH

Prepared QC Batch Analyst Method(s)

NA 1GC1132 LPL NA 000509-1 MDB

Conclusion of Lab Number: 00050756

601/8021B 150.1/9040B

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONT~INENT&eL ~iLiICAL

Clif J. aker Techn 1 a ager

SERVICES, INC.

1 804 GLENDALE ROAD O SALINA, KANSAS 67401-6675

785-827-1273 • 800-535-3076 • FAX 785-823-7830

KDHE Environmental Laborator!J Accreditation No. E-10146

Page 10: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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~ j '\., ' I •' \ ,I'°\ t!-1, l) N ~ '--\ 1. Fill out one copy of report each month and mail in monthly for each treatment facility. ':-t ~ ( W I'<.... ~ • 2. Mail one copy of report to the appropriate DNA regional office as note~ in your permit and keep one copy in your files.· ......._, ~ r-, 3. . Reports must be signed by whoever performed tests and by an appropriate official.

" \j_) l'. n) 4. In the weather- column, use the followin::i symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy and 0-overcast.

f"· \J t I 5.

~: ~ 'l 6.

I ~i ~ I 7.

Use grab sample for pH, Temp. and D.O. Use grab samples f9r all operational control test.

Use 24 hr. composite (proportional) samples for B.0.0. 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard Methods" or an approved equal for all parameters.

Treatment plant tlow measurements may be made on either influent or effluent. Lagoon influent flow measurements need he only at the time 9f composite sampling of the influent. All tests must be performed in accordance with NPOES Permit Con. and Operational Control Regulation 10 CSR 20-9.010. Review your permit for specific requirements. . . . ~ ~ o\}

~ d (, ~ ~ )1

8. Unusual conditions, significantly affecting operations must be reported immediately to the Department ot Natural Resources.

9. Representative sludge samples should be taken either before entering digesters and/or holding tanks or after removal from digesters or holding tanks. ·

Page 11: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

j ~r[ontinental 06/27/2000

City of Camdenton Attn: Vince Costa P.O. Box .:1,048 Camdenton, MO 65020

Date Received: 06/14/2000 Continental File No.: 7074 Continental Order No.: 63921 Your P.O./Project No.:

Dear Mr. Costa:

Anal!:Jtical Services. Inc.

This laboratory report consisting of 2 pages contains the analytical results for the following samples:

CAS LAB ID#

00060959

SAMPLE DESCRIPTION

Mulberry Well

SAMPLE TYPE

Liquid

DATE SAMPLED

06/13/2000

The following summary provides the date and time sampled, the date and time analyzed, and the total time elapsed for each analysis with an EPA recommended holding time of forty-eight hours or less.

CAS LAB ID# 00060959

ANALYSIS pH

DATE/TIME SAMPLED

06/13/2000 1240

DATE/TIME ANALYZED

06/14/2000 1051

ELAPSED HRS:MIN

22:11

Thank you for choosing Continental for this project. If you have any questions, please contact me at (800)-535-3076.

CONTINENTAL ANALYTICAL SERVICES, INC.

k- 7.' tf}/LL4 Brian T. O'Donnell Project Manager

Page 1

1 804 GLENDALE ROAD • SALINA, KANSAS 6740 1 -6675

785-827-1273 • 800-535-3076 • FAX 785-823-7830

KnI-n= l=nvirnnmont-.=11 I .=1hnrMf-nr1 1 A.rrrorllt-;==rf-inn l\ln r:= .. 1n1L1Fi

Page 12: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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~ ~- 1 ' ._( \ 1. Fill out one copy of report each month and mail in monthly for each treatment facility.

2. Mail one copy of report to the appropriate DNA regional office as note~ in your permit and keep one copy in your files. · \I 3. . Reports must be signed by whoever performed tests and by an appropriate official. 1"1-

4. In the weather- column, use the followin!;) symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy and O-overcast "-

5. Use grab sample for pH, Temp. and 0.0. Use grab samples f;x all operational control test.

6. Use 24 hr. composite (proportional) samples for 8.O.D. 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard Methods" or an approved equal for all parameters.

7. Treatment plant flow measurements may be made on either influent or effluent. Lagoon influent flow measurements need he only at the time of composite sampling of the influent. AU tests must be performed in accordance with NPDES Permit Con. and Operational Control Regulation 10 CSR 20-9.010. Review your permit for specific requirements.

8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources.

9. Representative sludge samples should be taken either before entering'' digesters and/or holding tanks or after removal from digesters or holding tanks.

Page 13: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

[ontin ntal j

Client: City of Camdenton Attn:Vince Costa P.O. Box 1048 Camdenton, MO 65020

Lab Nµmber: 00070825

Anal!dtical Services. Inc. Page: 2

Date Sample Rptd: 07/28/2000 Date Sample Recd: 07/13/2000 Continental File No: 7074 Continental Order No: 64534 Client P.O.:

Sampl~ Description: Mulberry Well Date Sampled: 07/12/2000 Time Sampled: 1330

Analysis

Trichloroethylene pH

Concentration

9.9 7.4

Date

Units

µg/L Std

Date Analyzed Book/Page

07/21/2000 3891/715 07/13/2000 4600/82

Analysis

Trichloroethylene pH

Prepared QC Batch Analyst Method(s)

NA 1GC2203 SPA 601/8021B NA 000713-1 MRM 150.l/9040B

Conclusion of Lab Number: 00070825

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, sw~846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONTIINENT04L ~[;:;:ICAL

Clif J. aker Techn 1 a ager

SERVICES, INC.

1 804 GLENDALE ROAD • SALINA, KANSAS 67401-6675

785-827·1 273 • 800-535-3076 • FAX 785-823-7830

KDHE Environmental Laboratond Accreditation No. E-10146

Page 14: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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Fill out :le copy of report each month and mail in monthly for each treatment facility .

Mail one copy of report to the appropriate DNA regional office as noted in your permit and keep one copy in your files.· . Reports must be signed by whoever performed tests and by an approp'riate official.

In the weather column, use the followin~ symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy and 0-overcast. Use grab sample for pH, Temp. and D.O. Use grab samples f9r all operational control test.

Use 24 hr. composite (proportional) samples for 8.G_D. 5, and Sus_ Solids tests unless NPDES permit indicates otherwise .. Use "Standard

°' ~ "' ·~ r;v- l 7. Treatment plant flow measurements may be made on either influent or effluent. Lagoon influent flow measurements need he only at the time 1 l'.i- I'\. 9f composite sampling of the influent. All tests must be performed in accordance with NPDES Permit Con_ and Operational Control

Methods" or an approved equal for all parameters.

~ 'I\ n\) Regulation 10 CSR 20-9.010. Review your permit for specific requirements. .

t fl. D 8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources_

~ 1J S 9. Representative sludge samples should be taken either before entering digesters and/or holding tanks or alter removal from digesters or 1J\j ~ 'I.: holding tanks.

[~ ~

Cl ~ I)

c)

~ I'

~

~ ~ ~ ~, (' r

Page 15: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

I

ClieBt: City of Camdenton Attn:Vince Costa P.O. Box 1048 Camdenton, MO 65020

Lab Number: 00080865 Sample Description: Mulberry Well

Analysis

Trichloroethylene pH

Analysis

Trichloroethylene pH

Concentration

Conclusion of

8.5 7.3

Date Pre:eared

NA NA

Lab Number:

Units

µg/L Std

Page: 2

Date Sample Rptd: 08/24/2000 Date Sample Recd: 08/10/2000 Continental File No: 7074 Continental Order No: 65149 Client P.O.:

Date Sampled: 08/09/2000 Time Sampled: 1300

Date Analyzed Book/Page

08/19/2000 4650/69 os/10/2000 4600/134

QC Batch Analyst Method(s)

1GC1232 JTJ 601/8021B 000810-1 MRM 150.1/9040B

00080865

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

•~ SERVICES, INC.

1 B04 GLENDALE ROAD • SALINA, KANSAS 6740 1-6675

785-B27-1 273 • BOO-S:35•::3076 • F'AX 7B5•823•7830

KDHE Environmental Laboratory Accreditation No. E-10146

Page 16: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

,:: 0

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~ ~ ~ ~' \ i ~ I~ ~ t ~ ~ } h ~H ~ ~ ~ ~ \;,\ ~. ~ ~ I~ ~ ~ ~ f N ~~~ l. ~ ~ ~ •. • '\ I= • - I \i':., 'v I \."'I, i!_ '\. ~ ' \"

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~ r-;--.__~_ ~- •~ l!}t (>_ f.'j ~ 1~· ~ ,~ ~ ,t'.I~ j ~ ~ ~t. , \ ·" ~ ~ :,- .~ a 1e · ~ '~ I~ 1h- ~: · ~ t I 6 2 · · ~ ~\ I • ' ;, \ '- l ~ I .'c.' f,--( ~ (}, ~ ~ ~,. 1. Fill out one copy of report each month and mail in monthly for each trea\ment facility_ :, ~ ~· fil

V L- 0 2. Mail one copy of report to the appropriate DNR regional office as note~ in your permit and keep one copy in your files.· ~ ~ UJ ~I 3. · Reports must be signed by whoever performed tests and by an appropriate official. ~ "'- ~ ~ 4_ In the weather column, use the followin'.J symbols: R-rain, S-snow, C-clear, lP.C.-partly cloudy and 0-overcast. 6', '-,. '-1 5. Use grab sample for pH, Temp. and.0.0. Use grab samples for all operational control test.

., ~ 6. Use 24 hr. composite (proportional) samples for 8-0.D. 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard ti-. "- Methods" or an approved equal for all parameters.

~ ''tl Q '\J 7. Treatment plant flow measurements may be made on either influent or effluent. Lagoon influent flow measurements need he only at the time f\J ~ ~ 9f composite sampling of the influent. All tests must be performed in accordance with NPOES Permit Con. and Operational Control ~ ~ '::--1 Regulation 10 CSR 20-9.010. Review your permit for specific requirements. .

c;j O :H 8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources.

~ ·9. Representative sludge samples should be taken either before entering dlgesters and/or holding tanks or after removal from digesters or holding tanks.

0

~ m

Page 17: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

Continental j

· Anal!:Jtical Services. Inc.

Client: icity of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020

Lab Number: 00090810 Sampl~ Description: Mulberry Well

Analysis

Trichloroethylene pH

Analysis

Trichloroethylene pH

Concentration

7.6 7.7

Date Prepared

NA NA

Units

µg/L Std

Page: 2

Date Sample Rptd: 09/15/2000 Date Sample Recd: 09/12/2000 Continental File No: 7074 Continental Order No: 65785 Client P.O.:

Date Sampled: 09/11/2000 Time Sampled: 1310

Date Analyzed Book/Page

09/14/2000 4650/93 09/12/2000 4600/192

QC Batch

1GC1257 000912-1

Analyst

JTJ KLT

Method(s)

601/8021B SM 4500H+B/9040B

Conclusion of Lab Number: 00090810

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONTINENTAL ANALYTICAL SERVICES, INC.

Clif~[/ A.t:: Technical~ager

1 804 GLENDALE ROAD • SALINA, KANSAS 67401 ·6675

785·827· 1 273 • 800·535-3076 • FAX 785-823·7830

KDHE Environmental Laboratory Accreditation No. E-10146

Page 18: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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~ Fill out one copy of report each month and mail in monthly for each treatment facility, ~ I 1. ,, 2. Mail one copy of report to the appropriate DNA regional office as noted in your permit and keep one copy in your files.· 'I 3. . Reports must be signed by whoever performed tests and by an approp.riate official.

t

4. In the weather- column, use the followin!;) symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy arid 0-overcast. 5. Use grab sample for pH, Temp. and 0.0. Use grab samples for all operational control test. 6. Use 24 hr. composite (proportional) samples for 8.0.D. 5, and Sus .. Solids tests unless NPDES permit indicates otherwise. Use "Standard

Methods" or an appr.oved equal for all parameters. 7. Treatment plant flow measurements may be made on either influent or effluent. Lagoon influent flow measurements need be only at the time

9f composite sampling of the influent. All tests must be performed in accordance with NPDES Permit Con. and Operational Control Regulation 10 CSR 20-9.010. Review your permit for specific requirements.

8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources. 9. Representative sludge samples should be taken either before entering dlgesters and/or holding tanks or after removal from digesters or

holding tanks .

..

Page 19: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

-- Continental / " Anal!::]tical Services. Inc.

Client: City of Camdenton Attn: Bill Jeffries P.O. Box 1048 Camdenton, MO 65020

Lab Number: 00101180 Sample Description: Mulberry Well

I

Analysis

Trichloroethylene pH

Analysis

Trichloroethylene pH

Concentration

Conclusion of

6.9 7.4

Date Pre2ared

NA NA

Lab Number:

Units

µg/L

Page: 2

Date Sample Rptd: 10/20/2000 Date Sample Recd: 10/11/2000 Continental File No: 7074 Continental Order No: 66464 Client P.O.:

Date Sampled: 10/10/2000 Time Sampled: 1245

Date Analyzed Book/Page

10/20/2000 4650/143 standard units 10/11/2000 4683/46

QC Batch Analyst Method (s)

1GC1293 JTJ 601/8021B 001011-1 MRM SM 4500H+B/9040B

00101180

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

~ObNENT~t~

~J. Baker Technical Manager

SERVICES, INC.

l 804 GLENDALE ROAD • SALINA, KANSAS 6740 l ·6675

785·827·1273 • 800·535·3076 • FAX 785·823·7830

KDHE Environmental Laboratory Accreditation No. E-10146

Page 20: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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~~~ ;az ~ ~ ~ ~ 1. Fill out one copy of report each month and mail in monthly for each treatment facility.

<· \ ~ . 2. Mail one copy of report to the appropriate DNA regional office as note~ in your permit and keep one copy in your files. · ~ ~ • 3. . Reports must be signed by wh_oever performed tests and by an appropriate official.

~ ~"' ~ 4. In the weather column, use the followin~ symbols: A-rain, S-snow, C-clear, P.C.-partly cloudy and 0-overcast. 11 \0 \ 'O 5. Use grab sample for pH, Temp. and D.O. Use grab samples for all operational control test.

~ ~ 6. Use 24 hr. composite (proportional) samples for 8.0.D. 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard Methods" or an approved equal for all parameters. ~ ~ 7. T raatment plant flow _measuremems may be made on either Influent or effluent. Lagoon Influent flow measurements need be o~ty at the time

\~ \. f'l- <;>f composite sampling of the influent. All tests must be performed m accordance with NPDES Permit Con. and Operational Control V\) f' \' Regulation 10 CSR 20-9.010. Review your permit for specific requirements. .

~ 8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources.

9. Representative sludge samples should be taken either before entering digesters and/or holding tanks or after removal from digesters or holding tanks.

Page 21: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

j Continental · Anal!:dtical Services, Inc.

I

Client: City of Camdenton Attn: Bill Jeffries P.O. Box 1048 Camdenton, MO 65020

LcJ.b Number: 00110507

Page: 2

Date Sample Rptd: 11/14/2000 Date Sample Recd: 11/07/2000 Continental File No: 7074 Continental Order No: 67045 Client P.O.:

Sample Description: Mulberry Well Date Sampled: 11/06/2000 Time Sampled: 1230

Analysis

Trichloroethylene pH

Concentration

9.4 7.3

Date

Units

µg/L std. units

Date Analyzed Book/Page

11/09/2000 4742/7 11/07/2000 4683/90

Analysis

Trichloroethylene pH

Prepared QC Batch Analyst Method(s)

NA 1GC2314 JTJ 601/8021B NA 001107-1 JRT SM 4500H+B/9040B

Conclusion of Lab Number: 00110507

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONT~~AiL, 11YTICAL

Cliff~d p. Baker Technical\ nager

\

SERVICES, INC.

1 804 GLENDALE ROAD • SALINA, KANSAS 67401-6675

785-827- l 273 • 800-53 5-3076 • F"AX 785-823-7830

KnHF FnvirnnmPntr1I I r1hnrr1tnn, ArrrPrlitr1tlnn !\In F-1n14Fi

Page 22: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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1. Fill out one copy of report each month and mail in monthly tor each treatment facility.

2. Mail one copy of report to the appropriate DNR regional ollice as noted in your permit and keep one copy in your files.·

3. . Reports must be signed by whoever performed tests and by an approp.riate official.

4. In the weathel' column, use the followin'.1 symbols: A-rain, S-snow, C-c!ear, P.C.-partly cloudy and 0-overcast.

5. Use grab sample for pH, Temp. and 0.0. Use grab samples for all operational control test.

I .:(:• ~I \.

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6. Use 24 hr. composite (proportional) samples for B.0.0. 5, and Sus. Solids tests unless NPDES permit indicates otherwise. Use "Standard Methods" or an approved equal for all parameters.

7. Treatment plant tlow measurements may be made on either influent or effluent. Lagoon influent flow measurements need be only at the time 9f composite sampling of the influent. All tests must be performed in accordance with NPDES Permit Con. and Operational Control Regulation 10 CSR 20-9.010. Review your permit for specific requirements.

8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources.

9. Representative sludge samples should be taken either before entering digesters and/or holding tanks or after removal from digesters or holding tanks.

,, ~ ~ ~ ~ 11) ~ >~ r< C \: \:'r-­'f...' \':

Page 23: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

j

Client: City of Camdenton Attn: Bill Jeffries P.O. Box 1048 Camdenton, MO 65020

Lab Number: 00121628

I Anal!::jtical Services. Inc.

Page: 2

Date Sample Rptd: 12/26/2000 Date Sample Recd: 12/20/2000 Continental File No: 7074 Continental Order No: 67936 Client P.O.:

Sample: Description: Mulberry Well Date Sampled: 12/18/2000 Time Sampled: 1216

Analysis

Trichloroethylene pH

Concentration

8.2 7.6 H

Date

Units

µ,g/L std. units

Date Analyzed Book/Page

12/21/2000 4650/213 12/20/2000 4683/162

Analysis

Trichloroethylene pH

Prepared QC Batch Analyst Method(s)

NA 1GC1356 JTJ 601/8021B NA 001220-1 MRM SM 4500H+B/9040B

H - Regulatory holding time for this analysis was exceeded.

Conclusion of Lab Number: 00121628

Laboratory analyses were performed on samples utilizing procedures published in Title 40 of the Code of Federal Regulations, Parts 136 or 141, or in EPA Publication, SW-846, 3rd edition, September, 1986 and the latest promulgated update. ND(), where noted, indicates none detected with the reporting limit in parentheses. Samples will be retained for thirty days unless otherwise notified.

CONT~Tt~L 1A%TICAL

Cliffcf#d_JJ. Baker Technical M ager

SERVICES, INC.

l 804 GLENDALE ROAD • SALINA, KANSAS 6740 l ·6675

785-827· l 273 • 800·535-3076 • FAX 785·823·7830

KDHE Environmental Laborator!d Accreditation No. E-10146

Page 24: ontinental - dnr.mo.gov · j Client: City of Camdenton Attn: Vince Costa P.O. Box 1048 Camdenton, MO 65020 Lab Number: 00020738 Continental · Analytical Services, Inc.

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i. Fill out one copy of report each month and mail in monthly for each treatment facility. 2. Mail one copy of report to the appropriate DNA regional office as noted in your permit and keep one copy in your files_·

3. -Reports must be signed by whoever performed tests and by an approp.riate official. 4. In the weather column. use the followin'.J symbols: A-rain, S-snow, C-clear, P.C.-partfy cloudy and 0-overcast. 5. Use grab sample for pH, Temp. and 0.0. Use grab samples tor all operational control test. 6. Use 24 hr. composite (proportional) samples for B.0.0. 5, and Sus_ Solids tests unless NPDES permit indicates otherwise. Use "Standard

Methods" or an approved equal for all parameters. 7. Treatment plant flow measurements may be made on either influent or effluent. Lagoon influent flow measurements need be only at the time

91 composite sampling of the influent. All tests- must be performed in accordance with NPDES Permit Con. and Operational Control Regulation i 0 CSR 20-9.01 0'. Review your permit for specific requirements.

8. Unusual conditions, significantly affecting operations must be reported immediately to the Department of Natural Resources. 9. Representative sludge samples should be taken either before entering digesters and/or holding tanks or after removal from digesters or

holding tanks .

..

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