One-Minute NMR: E-Seminar Protocols
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1 One-Minute NMR: E- Seminar Protocols Press *6 to mute (listen) Press #6 to un-mute (ask a question) As a courtesy to others, please mute your phone line while listening
description
One-Minute NMR: E-Seminar Protocols. As a courtesy to others, please mute your phone line while listening. Press *6 to mute (listen) Press #6 to un-mute (ask a question). One-Minute NMR 2007 Demo Tour. University of Buffalo: Buffalo, NY; January 8 - PowerPoint PPT Presentation
Transcript of One-Minute NMR: E-Seminar Protocols
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One-Minute NMR: E-Seminar Protocols
Press *6 to mute (listen)
Press #6 to un-mute (ask a question)
As a courtesy to others, please mute
your phone line while listening
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One-Minute NMR2007 Demo Tour
• University of Buffalo: Buffalo, NY; January 8• TriMR Regional Meeting: Research Triangle Park, NC; Feb 15-16• Southwest Regional Demonstration, Kalypsys San Diego; March 27• ENC: Daytona Beach, FL; April 22 – 26• Schedule a live demo in your area! Call Protasis for details.
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One-Minute NMRWinter 2006-07
12th International Symposium on Marine ProductsQueenstown, New Zealand, February 2007
58 Speakers and Many Poster Presentations- Sponsors Included Protasis Corporation -
Sessions:
Discovery• Kirk Gustafson, National Cancer Institute, Frederick, MD
•“Exploring the inherent chemical diversity of marine invertebrates: New compounds from familiar sources”
EnvironmentGenome
Development• Barbara Potts, Neureus, San Diego, CA
• “Marine microbe derived anti-cancer agents in Phase I clinical trials”
New Frontiers• William Fenical, Scripps Institute, San Diego, CA
•“Marine natural products: Where we’ve been and where we’re going”
Integrating NMR into Modern Laboratory WorkflowThe Wellplate and Microvial as Efficient Transport Media Among
Automated Analytical Methods
Professor John BluntUniversity of CanterburyChristchurch, New Zealand
Dr. David DetlefsenNovatia LLCMonmouth Station, NJ USA
Dr. Mike FreyJEOL, Peabody, MA USA
Mark O’Neil-Johnson Sequoia SciencesSt. Louis, MO USA
Data and Application Examples Courtesy of:
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HPLC FractCollect
DADELSD
VacuumCentrifuge
Mass Spec
NMR
Bioassay
Wellplate-Centric WorkflowAn Example from the University of Canterbury
E9,E10,E11
G4
1.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 26.0-200
0
200
400
600
800
1,000
1,200
1,400
1,600
1,800
2,000 CAP PROBE #28 F4470 Int_Chan_1mV
min
Flow: 1.000 ml/min
water: 0.0 %
acetonitrile: 10.0 %
75.0
MeOH: 0.0 %
HPLC with ELSD detectionof 600 g extract of
unidentified endophytic fungus
250 L/well
500 MHz8 g in 6 L CD3ODPRESAT 1.5 min
Recognisable features: 5 CH3 groups, of which 1 methoxyl,3 singlet CH3-C, 1 doublet CH3-C; 1 aldehyde
only 1 hit
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MicroFlow NMR Literaturewww.microNMR.com
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Your MicroFlow NMR Product Sourcewww.protasis.com
