NPDES Form 2C - Wastewater Discharge Information · 2014-12-12 · Temperature (winter) VALUE VALUE...

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1 Peltier, Hannah From: Ahrendsen, Blake Sent: Friday, December 12, 2014 9:55 AM To: Peltier, Hannah Subject: FW: NPDES Permit Renewal Application - AR0046116 Attachments: WF-06_NPDES_Form_2C_Amendment_121214.pdf; ATT00001..htm; 678528.pdf; ATT00002..htm Importance: High From: Seth Pickens [mailto:[email protected]] Sent: Friday, December 12, 2014 9:49 AM To: Fuller, Kim Cc: Ahrendsen, Blake; Ahrendsen, Blake; Bruce Shackleford; GREG HICKS; [email protected] Subject: Re: NPDES Permit Renewal Application - AR0046116 Importance: High Blake, As requested in Item 3 of the email sent on December 3, 2014, please find attached to this email the updated Section V.A of EPA Form 2C for Outfall 001 for the West Fraser Huttig, AR Facility and the associated lab report test data. As we have now addressed all 4 items from the email below, our application should now be complete. Please let me know if the Department requires any additional information or has any further questions. Cordially, Seth Pickens, B.S., CPSWPPP, CCSI Environmental Scientist Environmental Consulting Operations, Inc Integrating ECOnomy and ECOlogy since 1990 17724 I30 Suite 5A Benton, AR 72019 Office 15013159009 Cell 14795181819 [email protected]

Transcript of NPDES Form 2C - Wastewater Discharge Information · 2014-12-12 · Temperature (winter) VALUE VALUE...

1

Peltier, Hannah

From: Ahrendsen, BlakeSent: Friday, December 12, 2014 9:55 AMTo: Peltier, HannahSubject: FW: NPDES Permit Renewal Application - AR0046116Attachments: WF-06_NPDES_Form_2C_Amendment_121214.pdf; ATT00001..htm; 678528.pdf;

ATT00002..htm

Importance: High

  

From: Seth Pickens [mailto:[email protected]] Sent: Friday, December 12, 2014 9:49 AM To: Fuller, Kim Cc: Ahrendsen, Blake; Ahrendsen, Blake; Bruce Shackleford; GREG HICKS; [email protected] Subject: Re: NPDES Permit Renewal Application - AR0046116 Importance: High Blake, As requested in Item 3 of the email sent on December 3, 2014, please find attached to this email the updated Section V.A of EPA Form 2C for Outfall 001 for the West Fraser Huttig, AR Facility and the associated lab report test data. As we have now addressed all 4 items from the email below, our application should now be complete. Please let me know if the Department requires any additional information or has any further questions. Cordially, Seth Pickens, B.S., CPSWPPP, CCSI Environmental Scientist Environmental Consulting Operations, Inc Integrating ECOnomy and ECOlogy since 1990 17724 I‐30 Suite 5A Benton, AR 72019 Office ‐ 1‐501‐315‐9009 Cell ‐ 1‐479‐518‐1819 [email protected]  

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information on separate sheets (use the same format) instead of completing these pages. SEE INSTRUCTIONS.

EPA I.D. NUMBER (copy from Item 1 of Form 1)

V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) OUTFALL NO.

PART A –You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.

2. EFFLUENT 3. UNITS

(specify if blank) 4. INTAKE (optional)

a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE

(if available) c. LONG TERM AVRG. VALUE

(if available) a. LONG TERM

AVERAGE VALUE

1. POLLUTANT (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF

ANALYSES a. CONCEN-

TRATION b. MASS (1)

CONCENTRATION (2) MASS b. NO. OF

ANALYSES

a. Biochemical Oxygen Demand (BOD) b. Chemical Oxygen Demand (COD) c. Total Organic Carbon (TOC) d. Total Suspended Solids (TSS)

e. Ammonia (as N)

f. Flow VALUE VALUE VALUE

VALUE

g. Temperature (winter)

VALUE VALUE VALUE °C

VALUE

h. Temperature (summer)

VALUE VALUE VALUE °C

VALUE

i. pH MINIMUM MAXIMUM MINIMUM MAXIMUM

STANDARD UNITS PART B – Mark “X” in column 2-a for each pollutant you know or have reason to believe is present. Mark “X” in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either

directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.

2. MARK “X” 3. EFFLUENT 4. UNITS 5. INTAKE (optional)

a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE

(if available) c. LONG TERM AVRG. VALUE

(if available) a. LONG TERM AVERAGE

VALUE 1. POLLUTANT

AND CAS NO.

(if available)

a. BELIEVED PRESENT

b. BELIEVED ABSENT

(1) CONCENTRATION (2) MASS

(1) CONCENTRATION (2) MASS

(1) CONCENTRATION (2) MASS

d. NO. OF ANALYSES

a. CONCEN-TRATION b. MASS

(1) CONCENTRATION (2) MASS

b. NO. OF ANALYSES

a. Bromide (24959-67-9)

b. Chlorine, Total Residual

c. Color

d. Fecal Coliform

e. Fluoride (16984-48-8)

f. Nitrate-Nitrite (as N)

EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT 2. MARK “X” 3. EFFLUENT 4. UNITS 5. INTAKE (optional)

a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE

(if available) c. LONG TERM AVRG. VALUE

(if available) a. LONG TERM

AVERAGE VALUE 1. POLLUTANT

AND CAS NO.

(if available)

a. BELIEVED PRESENT

b. BELIEVED ABSENT

(1) CONCENTRATION (2) MASS

(1) CONCENTRATION (2) MASS

(1) CONCENTRATION (2) MASS

d. NO. OF ANALYSES

a. CONCEN-TRATION b. MASS

(1) CONCENTRATION (2) MASS

b. NO. OF ANALYSES

g. Nitrogen, Total Organic (as N)

h. Oil and Grease i. Phosphorus (as P), Total (7723-14-0)

j. Radioactivity

(1) Alpha, Total

(2) Beta, Total

(3) Radium, Total

(4) Radium 226, Total

k. Sulfate (as SO4) (14808-79-8)

l. Sulfide (as S)

m. Sulfite (as SO3) (14265-45-3)

n. Surfactants

o. Aluminum, Total (7429-90-5)

p. Barium, Total (7440-39-3)

q. Boron, Total (7440-42-8)

r. Cobalt, Total (7440-48-4)

s. Iron, Total (7439-89-6)

t. Magnesium, Total (7439-95-4)

u. Molybdenum, Total (7439-98-7)

v. Manganese, Total (7439-96-5)

w. Tin, Total (7440-31-5)

x. Titanium, Total (7440-32-6)

EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]

Page 1 of 112/10/2014Printed

Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

LELAP-accredited #02008

Account Project

678528WFS2 -L

Report To

West Fraser, Inc.

Greg Hicks

PO Box 384

Huttig, AR 71742

Report

Employee Owned Integrity Caring Continual Improvement

Table of Contents

PagesDescriptionReport Name

This report consists of this Table of Contents and the following pages:

678528_r03_03_ProjectResults_1355090 Ana-Lab Project P:678528 C:WFS2 1355090 Outfall 001 Permit Renewal 2 678528_r10_05_ProjectQC Ana-Lab Project P:678528 C:WFS2 Project Quality Control Groups 4 678528_r99_09_CoC__1_of_1 Ana-Lab CoC WFS2 678528_1_of_1 2

8 Total Pages:

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptTOC Created 10/06/2004 v1.1LDSClient v1.5.50.962

NELAP-accredited #T104704201

Report Page 1 of 9

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2

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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement

Results12/10/2014Printed: Page 1 of 2

Report To

West Fraser, Inc.

Greg Hicks

PO Box 384

Huttig, AR 71742

678528WFS2-LAccount Project

Results

BottleCASFlagsRLUnitsResultsParameter

1355090 Outfall 001 Permit Renewal

12/04/2014 10:30:00M MatthewsCollected by:

12/04/2014Received:

Non-Potable Water Affiliation: West Fraser, Inc.

Prepared: 592828 12/05/2014 09:15:00

EPA 200.7 4.4 12/05/2014 15:29:28LPS QCgroup 592997Analyzed

2.40 mg/L 0.500 7439-95-4Magnesium, Total 05N

Prepared: 592833 12/05/2014 09:30:00

EPA 350.1 2 12/08/2014 10:00:00RSV QCgroup 593136Analyzed

0.111 mg/L 0.020Ammonia Nitrogen 06N

Prepared: 592807 12/10/2014 11:07:06

SM 5210 B-2001 12/10/2014 11:07:06MKC QCgroup 592807Analyzed

8.35 mg/L D2.00 1026-3Biochemical Oxygen Demand (BOD5) 01N

Prepared: 593365 12/09/2014 13:50:33

SM 5310 C-96 12/09/2014 13:50:33ALH QCgroup 593365Analyzed

6.87 mg/L 0.500Total Organic Carbon 03N

The above methods that we used are approved for NPDES reporting as listed in 40 CFR 136 Table 1B or Ana-Lab has specific approval from EPA to use

these methods for NPDES reporting.

Sample Preparation for Sample 1355090

1355090 Outfall 001 Permit Renewal 12/04/2014Received:

Prepared: 592828 12/05/2014 09:15:00

EPA 200.2 2.8 12/05/2014 09:15:00TES QCgroup 592828Analyzed

50/50 mlLiquid Metals Digestion 02N

Prepared: 592833 12/05/2014 09:30:00

EPA 350.2, Rev. 2.0 12/05/2014 09:30:00CDB QCgroup 592833Analyzed

50/50 mlAmmonia Distillation 04N

Prepared: 592807 12/05/2014 07:01:13

SM 5210 B-2001 12/05/2014 07:01:13MKC QCgroup 592807Analyzed

StartedBOD Set StartedN

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.5.50.962 www.ana-lab.com

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

NELAP-accredited #T104704201

Report Page 2 of 9

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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement

Results12/10/2014Printed: Page 2 of 2

Qualifiers:

D - Duplicate RPD was higher than expected

We report results on an 'As Received' or wet basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at Ana-lab's

corporate laboratory that holds the following Federal and State certificates: Texas Department of Health Lead Firm Certificate 2110076, US

Department of Agriculture Soil Import Permit S-37592, Texas Commisson on Environmental Quality Drinking Water Laboratory Certificate

TX219, Texas Commission on Environmental Quality NELAP T104704201, Oklahoma Department of Environmental Quality Drinking

Water Certification Lab ID# D9913, EPA Lab Number TX00063, USEPA Approved Perchlorate Testing Lab, Oklahoma Department of

Environmental Quality Laboratory Certificate 8125, Arkansas Department of Environmental Quality Certification #03-070-0, Louisiana

Department of Environmental Quality Laboratory Certification (NELAP, LELAP) #02008, Louisiana Department of Health and Hospitals

Drinking Water (NELAP) # LA030020, US Department of Energy Approved, State of Kansas Department of Health and Environment

Waste Water and Solid/Hazardous Waste Cert. E-10365. The Accredited column designates accreditation by N -- NELAC, or z -- not

covered under NELAC scope of accreditation.

These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of

Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.

RL is the Reporting Limit (sample specific quantitation limit) and is at or above the Method Detection Limit (MDL). CAS is Chemical

Abstract Service number.

C. H. Whiteside, Ph.D., President

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.5.50.962 www.ana-lab.com

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

NELAP-accredited #T104704201

Report Page 3 of 9

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3

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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]

Quality Control Page 1 of 412/10/2014Printed

Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

LELAP-accredited #02008

Employee Owned Integrity Caring Continual Improvement

WFS2 -LAccount Project

West Fraser, Inc.

Greg Hicks

PO Box 384

Huttig, AR 71742

Report To001

678528

SM 5210 B-2001Non-Potable Water 592807

Blank

FileUnitsMQLMDLReadingPrepSetParameter

Biochemical Oxygen

Demand (BOD5)

592807 0.11 0.200 0.500 mg/L 115028382

Biochemical Oxygen

Demand (BOD5)

592807 0.12 0.200 0.500 mg/L 115028431

Biochemical Oxygen

Demand (BOD5)

592807 0.18 0.200 0.500 mg/L 115028478

Biochemical Oxygen

Demand (BOD5)

592807 -0.04 0.200 0.500 mg/L 115028525

Duplicate

Limit%RPDUnitUnknownResultTypeSampleParameter

Biochemical Oxygen

Demand (BOD5)

1354701 Duplicate 3.97 2.97 mg/L 28.8 20.0

Biochemical Oxygen

Demand (BOD5)

1354743 Duplicate 253 314 mg/L 21.5 20.0

Biochemical Oxygen

Demand (BOD5)

1354766 Duplicate 4.20 4.24 mg/L 0.948 20.0

Biochemical Oxygen

Demand (BOD5)

1354947 Duplicate 35.4 34.2 mg/L 3.45 20.0

Biochemical Oxygen

Demand (BOD5)

1354982 Duplicate 14.0 12.0 mg/L 15.4 20.0

Biochemical Oxygen

Demand (BOD5)

1355016 Duplicate 8.76 8.32 mg/L 5.15 20.0

Biochemical Oxygen

Demand (BOD5)

1355090 Duplicate 32.0 8.35 mg/L 117 20.0

Seed Drop

FileOutUnitsMQLMDLReadingPrepSetParameter

Biochemical Oxygen

Demand (BOD5)

592807 0.957 0.200 0.500 mg/L 115028383

Biochemical Oxygen

Demand (BOD5)

592807 1.03 0.200 0.500 mg/L 115028432

Biochemical Oxygen

Demand (BOD5)

592807 0.980 0.200 0.500 mg/L 115028479

Biochemical Oxygen

Demand (BOD5)

592807 1.02 0.200 0.500 mg/L 115028526

Standard

FileOutLimits%Recover%UnitsKnownReadingSampleParameter

Biochemical Oxygen

Demand (BOD5)

194 198 mg/L 98.0 83.7 - 116 115028384

Biochemical Oxygen

Demand (BOD5)

196 198 mg/L 99.0 83.7 - 116 115028433

Biochemical Oxygen

Demand (BOD5)

192 198 mg/L 97.0 83.7 - 116 115028480

Biochemical Oxygen

Demand (BOD5)

191 198 mg/L 96.5 83.7 - 116 115028527

EPA 350.1 2Non-Potable Water 593136

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

NELAP-accredited #T104704201

Report Page 4 of 9

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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]

Quality Control Page 2 of 412/10/2014Printed

Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

LELAP-accredited #02008

Employee Owned Integrity Caring Continual Improvement

Blank

FileUnitsMQLMDLReadingPrepSetParameter

Ammonia Nitrogen 592833 ND 0.00974 0.020 mg/L 115035005

CCV

FileOutLimits%Recover%UnitsKnownReadingParameter

Ammonia Nitrogen 2.00 2.00 mg/L 100 90.0 - 110 115034983

Ammonia Nitrogen 1.96 2.00 mg/L 98.0 90.0 - 110 115034994

Ammonia Nitrogen 2.03 2.00 mg/L 102 90.0 - 110 115035002

Ammonia Nitrogen 2.00 2.00 mg/L 100 90.0 - 110 115035011

Ammonia Nitrogen 1.98 2.00 mg/L 99.0 90.0 - 110 115035022

Ammonia Nitrogen 1.99 2.00 mg/L 99.5 90.0 - 110 115035029

Ammonia Nitrogen 2.02 2.00 mg/L 101 90.0 - 110 115035037

Ammonia Nitrogen 1.99 2.00 mg/L 99.5 90.0 - 110 115035050

Ammonia Nitrogen 2.00 2.00 mg/L 100 90.0 - 110 115035064

Ammonia Nitrogen 1.97 2.00 mg/L 98.5 90.0 - 110 115035071

Duplicate

Limit%RPDUnitUnknownResultTypeSampleParameter

Ammonia Nitrogen 1354824 Duplicate 0.178 0.181 mg/L 1.67 20.0

Ammonia Nitrogen 1354837 Duplicate 0.265 0.279 mg/L 5.15 20.0

ICV

FileOutLimits%Recover%UnitsKnownReadingParameter

Ammonia Nitrogen 2.17 2.00 mg/L 108 90.0 - 110 115034982

LCS

OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter

Ammonia Nitrogen 592833 2.03 2.00 mg/L 101 90.0 - 110 115035006

LCS Dup

Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter

Ammonia Nitrogen 592833 2.03 2.11 2.00 90.0 - 110 101 106 mg/L 3.86 20.0

Mat. Spike

FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter

Ammonia Nitrogen 1354824 2.45 0.181 2.00 mg/L 113 80.0 - 120 115035010

Ammonia Nitrogen 1354837 2.43 0.279 2.00 mg/L 108 80.0 - 120 115035014

EPA 200.7 4.4Non-Potable Water 592997

Blank

FileUnitsMQLMDLReadingPrepSetParameter

Magnesium, Total 592828 ND 0.0102 0.500 mg/L 115032566

CCV

FileOutLimits%Recover%UnitsKnownReadingParameter

Magnesium, Total 26.4 25.0 mg/L 106 90.0 - 110 115032552

Magnesium, Total 25.8 25.0 mg/L 103 90.0 - 110 115032554

Magnesium, Total 25.2 25.0 mg/L 101 90.0 - 110 115032562

Magnesium, Total 24.6 25.0 mg/L 98.4 90.0 - 110 115032572

Magnesium, Total 24.7 25.0 mg/L 98.8 90.0 - 110 115032576

ICL

FileOutLimits%Recover%UnitsKnownReadingParameter

Magnesium, Total 50.3 50.0 mg/L 101 95.0 - 105 115032547

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

NELAP-accredited #T104704201

Report Page 5 of 9

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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]

Quality Control Page 3 of 412/10/2014Printed

Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

LELAP-accredited #02008

Employee Owned Integrity Caring Continual Improvement

ICV

FileOutLimits%Recover%UnitsKnownReadingParameter

Magnesium, Total 25.5 25.0 mg/L 102 90.0 - 110 115032551

LCS

OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter

Magnesium, Total 592828 4.99 5.00 mg/L 99.7 85.0 - 115 115032567

LCS Dup

Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter

Magnesium, Total 592828 4.99 4.93 5.00 85.0 - 115 99.7 98.5 mg/L 1.21 25.0

MS

Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter

Magnesium, Total 1354973 5.70 0 0.988 5.00 75.0 - 125 94.2 mg/L 25.0

MSD

Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter

Magnesium, Total 1354973 5.70 5.75 0.988 5.00 75.0 - 125 94.2 95.2 mg/L 1.06 25.0

SM 5310 C-96Non-Potable Water 593365

AWRL

FileOutLimits%Recover%UnitsKnownReadingParameter

Total Organic Carbon 2.22 2.00 mg/L 111 75.0 - 125 115040179

Blank

FileUnitsMQLMDLReadingPrepSetParameter

Total Organic Carbon 593365 0.110 0.0618 0.500 mg/L 115040178

Total Organic Carbon 593365 0.101 0.0618 0.500 mg/L 115040211

Total Organic Carbon 593365 0.0959 0.0618 0.500 mg/L 115040235

CCB

FileOutUnitsMQLMDLReadingPrepSetParameter

Total Organic Carbon 593365 0.137 0.0618 0.500 mg/L 115040172

Total Organic Carbon 593365 0.191 0.0618 0.500 mg/L 115040183

Total Organic Carbon 593365 0.148 0.0618 0.500 mg/L 115040188

Total Organic Carbon 593365 0.118 0.0618 0.500 mg/L 115040197

Total Organic Carbon 593365 0.0993 0.0618 0.500 mg/L 115040209

Total Organic Carbon 593365 0.175 0.0618 0.500 mg/L 115040222

Total Organic Carbon 593365 0.139 0.0618 0.500 mg/L 115040233

CCV

FileOutLimits%Recover%UnitsKnownReadingParameter

Total Organic Carbon 10.4 10.0 mg/L 104 90.0 - 110 115040175

Total Organic Carbon 10.2 10.0 mg/L 102 90.0 - 110 115040184

Total Organic Carbon 10.3 10.0 mg/L 103 90.0 - 110 115040189

Total Organic Carbon 10.2 10.0 mg/L 102 90.0 - 110 115040198

Total Organic Carbon 10.3 10.0 mg/L 103 90.0 - 110 115040210

Total Organic Carbon 10.3 10.0 mg/L 103 90.0 - 110 115040223

Total Organic Carbon 10.6 10.0 mg/L 106 90.0 - 110 115040234

Duplicate

Limit%RPDUnitUnknownResultTypeSampleParameter

Total Organic Carbon 1355739 Duplicate 0.0885 0.0969 mg/L 9.06 20.0

Total Organic Carbon 1355739 Duplicate 0.0854 0.0969 mg/L 12.6 20.0

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

NELAP-accredited #T104704201

Report Page 6 of 9

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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]

Quality Control Page 4 of 412/10/2014Printed

Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

LELAP-accredited #02008

Employee Owned Integrity Caring Continual Improvement

ICL

FileOutLimits%Recover%UnitsKnownReadingParameter

Total Organic Carbon 20.7 20.0 mg/L 104 90.0 - 110 115040174

ICV

FileOutLimits%Recover%UnitsKnownReadingParameter

Total Organic Carbon 10.5 10.0 mg/L 105 90.0 - 110 115040176

LCS

OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter

Total Organic Carbon 593365 5.34 5.00 mg/L 107 85.0 - 115 115040177

Total Organic Carbon 593365 5.17 5.00 mg/L 103 85.0 - 115 115040212

Total Organic Carbon 593365 5.41 5.00 mg/L 108 85.0 - 115 115040236

MS

Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter

Total Organic Carbon 1354322 14.3 0 4.28 10.0 70.0 - 130 100 mg/L 20.0

Total Organic Carbon 1354399 14.6 0 4.79 10.0 70.0 - 130 98.1 mg/L 20.0

Total Organic Carbon 1354454 12.0 0 1.89 10.0 70.0 - 130 101 mg/L 20.0

Total Organic Carbon 1354978 11.8 0 1.96 10.0 70.0 - 130 98.4 mg/L 20.0

MSD

Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter

Total Organic Carbon 1354322 14.3 14.1 4.28 10.0 70.0 - 130 100 98.2 mg/L 1.82 20.0

Total Organic Carbon 1354399 14.6 14.6 4.79 10.0 70.0 - 130 98.1 98.1 mg/L 0 20.0

Total Organic Carbon 1354454 12.0 11.7 1.89 10.0 70.0 - 130 101 98.1 mg/L 2.91 20.0

Total Organic Carbon 1354978 11.8 12.0 1.96 10.0 70.0 - 130 98.4 100 mg/L 1.61 20.0

Standard

FileOutLimits%Recover%UnitsKnownReadingSampleParameter

Total Organic Carbon 52.2 50.0 mg/L 104 90.0 - 110 115040173

RPD is Relative Percent Difference: abs(r1-r2) / mean(r1,r2) * 100% Recover% is Recovery Percent: result / known * 100%

Blank - Method Blank; LCS - Laboratory Control Sample; CCV - Continuing Calibration Verification; MS - Matrix Spike; ICV - Initial Calibration

Verification; CCB - Continuing Calibration Blank; AWRL - Ambient Water Reporting Limit

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

NELAP-accredited #T104704201

Report Page 7 of 9

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Report Page 9 of 9

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