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Transcript of Norquay Technology Inc. Moving forward, in Fine & Specialty Chemicals P.O. Box 468 Chester, PA 19016...
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Norquay Technology Inc.
Moving forward, in
Fine & Specialty ChemicalsP.O. Box 468Chester, PA 19016 USA
phone: +1(610) 874-4330fax: +1(610) 874-3575
www.NorquayTech.com
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www.NorquayTech.com 2
today’s discussion
Overview Custom Synthesis Seven (7) Day Guarantee Equipment Product Lines
Contact Information
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www.NorquayTech.com 3
Roach’s Shipyard, old Chester Harbor, 1859-1885
Chester Waterfront ca 1875
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1927-1961
www.NorquayTech.com 4
The
Chester plant
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www.NorquayTech.com5
Norquay TechnologyChester plant
1927-1961
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6
Norquay Overview
Founded 1987: Philadelphia, PA Focus
Niche MarketsHigh Value-added $15.00 - $42,000/kgKilo-Lab: 10 grams to 20 kgLow Volume 50 kg to 85+tpyCommercial Scale 100-1,500 gal
Products Sales Custom Synthesis: 50% Product Line: 50% Export: 30%:
Europe, South America, Japan & Asia
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7
Seamless Scale-up
Laboratory, Kilo-lab,
Pilot PlantCommercial Quantities
Compound pricing studies, Economic Model
Confidentiality Agreements
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8
Equipment
Kilo Lab: ( 5-12-22-30-50 liter)
Plant Reactors: jacketed, condensers & instrumentation Hastelloy –C-276:20-100-350 gal 316 Stainless Steel: 500-1,500 gal Glass Lined: 100-500-750-1,000 gal
Vacuum Distillation: 50 liter to 100-500-1,500 gal <1.0 torr 10 – 25 theoretical plates
Filter-Drying: air & moisture sensitive
Drying: shelf, double-cone & rotary (316 s/s)
Utilities: -78° to 170o C (future to 220o C)
Analytical: HPLC, GC, NMR, UV, L-a-b color, Karl Fischer, etc.
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Formal Response “Yes” or “No” within Seven (7) Days
9
NORQUAY: Seven (7) Day Guarantee
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Project Defined, unequivocally
Chemical Name, CAS Number
Scope Volume, Timing, Stage GATE Process
How is Success measured? (Step 3)
Outline Open IssuesTSCA LVE or REACh for Europe
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Customer Clarifying Questions Key Parameters, measure of SUCCESS Analytical Methods- Need development?Alignment between customer “ Use Test” & QC Methods
TimingQuote to first lab sample <?>Qualification (3 lots?)Steps to commercial scale?
10
NORQUAY: Seven (7) Day Guarantee
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NQ: Product Lines
؏ Substituted Benzophenones ؏ Phenylhydrazines & Indoles ؏ Cyanoacetates ؏ Heterocycles ؏ Metallocenes, cp-ligands ؏ HPLC/Process Surfactants: Sulfonates ؏ Chlorendate Esters
To Contents
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Benzophenonesbenzophenone CAS #
1 . 2,4- Dihydroxy benzophenone 131-56-62 . 2,2',4,4'- Tetrahydroxy benzophenone 131-55-53 . 2- Hydroxy -4-allyloxy benzophenone 2549-87-34 . 2- Hydroxy -4-methoxy benzophenone 131-57-75 . 2- Hydroxy -4-methoxy benzophenone -5-sulfonic Acid 4065-45-66 . 2,2'- Dihydroxy -4,4'-dimethoxy benzophenone 131-54-47 . 2,2'- Dihydroxy -4-methoxy benzophenone 131-53-38 . 2,2'- Dihydroxy -4,4'-dimethoxy benzophenone -5,5'-disulfonic Acid Na Salt 76656-36-5
2,2'4,4'- Tetrahydroxy benzophenone2,2'- Dihydroxy -4,4'-dimethoxy benzophenone
bis (2,4- Dihydroxy phenyl) methanonebis (2- Hydroxy-4-methoxyphenyl) methanone
13 . 2- Hydroxy -4-octyloxy benzophenone 1843-05-614 . 4,4'- Difluoro benzophenone 345-92-615 . 4,4'- Dimethoxy benzophenone 90-96-016 . 4,4'- Dimethyl benzophenone 611-97-217 . 2,4- Dimethyl benzophenone 1140-14-318 . 4- Fluoro benzophenone 345-83-519 . 4- Morpholino benzophenone 24758-49-4
sulfonic acid
9
9
.
.
substituents
1341-54-4
1341-54-4
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Benzophenones
O
OOH
OH
OOH
OH
OH
OH
OOH
O
CH2
OOH
O
OH
OCH3 CH3
OOH
OCH3
OOH
O
OH
CH3
OOH
OCH3
SO3H
O OH
OC8H17
O
F F
O
CH3 CH3
O
O OCH3 CH3
OCH3
CH3
O
F
O
N
O
OOH
O
OH
OCH3 CH3
SO3-Na
+SO3
-Na
+
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O OH
OCH3
SO3H
O OH
OCH3
O OH
OH
PRODUCT OVERVIEW
Primary Use Solubility UV Spectrum (g Product / 100ml Solvent) (30°C)
Helisorb-1 (Benzophenone-1) 2,4-Dihydroxybenzophenone • Cosmetics Water: Insoluble Bath Preparations Methanol: 32.0 Shampoos Ethanol: 32.0 Blushes Nail Polish / Enamel • Paints • Plastics WAVELENGTH λ max: 292/330nm
Helisorb-3 (Benzophenone-3) 2-Hydroxy-4-methoxybenzophenone
• Cosmetics Bath Preparations Water: Insoluble Colognes / Perfumes Methanol: 6.0 Sunscreens Ethanol: 6.0 • Paints • Plastics WAVELENGTH λ max: 285/320nm
Helisorb-4 (Benzophenone-4) 2-Hydroxy-4-methoxybenzophenone- 5-sulfonic acid • Cosmetics Water: 28.0 Bath Preparations Methanol: 40.0 Fragrances, Cologne Ethanol: 35.0 Hair Care Blushes Skin Care • Paints • Plastics WAVELENGTH λ max: 285/320nm
UV-C UV-B UV-A
80%
20%
UV-C UV-B UV-A
40%
20%
UV-C UV-B UV-A
20%
% T
RA
NS
MIT
TA
NC
E
100%
40%
0% 240 260 280 300 320 340 360 380 400
% T
RA
NS
MIT
TA
NC
E
100%
80%
60%
0% 240 260 280 300 320 340 360 380 400
% T
RA
NS
MIT
TA
NC
E
100%
80%
60%
40%
240 260 280 300 320 340 360 380 400
10mg/l 20mg/l 40mg/l
60%
0%
Helisorb-11 (2,2’-Dihydroxy-4,4’-dimethoxybenzophenone)
(Benzophenone-6)
• Cosmetics Water: Insoluble Nail Polish Methanol: <1.0 Nail Enamels Ethanol: <1.0• Plastics• Films
Helisorb-11DS (2,2’-Dihydroxy-4,4’-dimethoxybenzophenone-
(Benzophenone-9) 5,5’-disulfonic acid sodium salt)
Bath Preparations Water: 5.0 Hair Cosmetics Methanol: 2.0 Shampoos Ethanol: 1.0 Skin Products
Helisorb-10 (2,2’,4,4’-Tetrahydroxybenzophenone)
(Benzophenone-2)
• Cosmetics Water: .10 Toilet Water Methanol: 50.0 Fragrances Ethanol: 40.0 Perfumes Shampoos Skin Products• Plastics / Paints
OOH
OH
OH
OH
OOH
O
OH
OCH3 CH3
OOH
O
OH
OCH3 CH3
SO3-Na
+SO3
-Na
+
To Contents
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www.NorquayTech.com 15
Phenylhydrazines
CH3
NHNH2
ClH
F
NHNH2
ClH
NHNH2
F
ClH
NH
NH2
Br
ClH
Cl
NHNH2
ClH
NHNH2
Cl
ClH
NHNH2
Cl
Cl
ClH
NHNH2
CH3
ClH
NHNH2
CH3
ClHNH
NH2
CH3
ClH
Br
NHNH2
ClH
O
NH
NH2
CH3
ClH
CH3
NH NH2
CH3
ClH
N
NH2ClH
To Contents
Phenyl hydrazine CAS #
1 . 2- Bromo phenyl hydrazine HCl 50709-33-6
2 . 4- Bromo phenyl hydrazine HCl 41931-18-4
3 . 2- Chloro phenyl hydrazine HCl 41052-75-9
4 . 4- Chloro phenyl hydrazine HCl 1073-70-7
5 . 2,4- Di chloro phenyl hydrazine HCl 5446-18-4
6 . 3,5- Di chloro phenyl hydrazine HCl 63352-99-8
7 . 3,4- Di methyl phenyl hydrazine HCl 60481-51-8
8 . 1,1- Di phenyl hydrazine HCl 530-47-2
9 . 2- Ethyl phenyl hydrazine HCl 19398-06-2
10 . 2- Fluoro phenyl hydrazine HCl 2924-15-4
11 . 4- Fluoro phenyl hydrazine HCl 823-85-8
12 . 4- Methoxy phenyl hydrazine HCl 19501-58-7
13 . 2- Tolyl hydrazine HCl 635-26-7
14 . 3- Tolyl hydrazine HCl 637-04-7
15 . 4- Tolyl hydrazine HCl 637-60-5
Substitution
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Specialty Cyanoacetates
for: Specialty Adhesives Medical devices Disposable Components
NCO-R
O
NCO
O
CH3
NCO
O
CH3
NCO
O
CH3
NCO
O
CH3
NCO
O
CH3
CH3
NCO
O
CH3
CH3
NCO
O
CH3
CH3
NCO
OCH3
CH3
NCO
O
OCH3
NCO
O
CH3
CH3
O-CH3
NCO
OO CH3
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Specialty Cyanoacetates
cyanoacetate CAS1 . n- Propyl cyanoacetate 14447-15-52 . n- Hexyl cyanoacetate 13361-53-03 . n- Octyl cyanoacetate 15666-97-44 . n- Decyl cyanoacetate 17686-43-05 . Isopropyl cyanoacetate 13361-30-36 . Isobutyl cyanoacetate 13361-31-47 . Isoamyl cyanoacetate 60180-49-68 . 2- Octyl cyanoacetate 52688-08-19 . "2- Methoxyethyl" cyanoacetate 10258-54-5
10 . "2- Methoxyisopropyl" cyanoacetate 32804-79-811 . "2- Ethoxyethyl" cyanoacetate 32804-77-6
substituent
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18
Heterocycles
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www.NorquayTech.com 19
Heterocycles
N
N
OH
N
H3C-O O
O
O-CH3H3C-O
N
O
SH
O
H3C-O
H3C-OO
O-CH3
O-CH3
NH
NH
O
N
NH
OH
S
NH
CH3
CH3
S
NH
CH3
F
To Contents
CAS # Chemical Name2 . 5,6-dimethoxy indanone 2107-69-9 5,6-dimethoxyindanone3 . 2,5-Dimethyl benzothiazole 95-26-1 2,5-Dimethylbenzothiazole4 . 5-Fluoro-2-methyl benzothiazole 399-75-7 5-Fluoro-2-methylbenzothiazole1 . 2- Benzoxazole thiol 2382-96-9 2-Benzoxazolethiol5 . 2-Hydroxy benzimidazole 615-16-7 2-Hydroxybenzimidazole6 . 3,6-Dimethoxy xanthone 1214-24-0 3,6-Dimethoxyxanthone7 . 6-Hydroxy quinoline 580-16-15 6-Hydroxyquinoline8 . 6-Methoxy quinoline 5263-87-6 6-Methoxyquinoline9 . Julolidine 479-59-4 Julolidine
Chemical Name
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etallocenes, Ligands
metallocene CAS #1 . 5-Hexene-2-one 109-49-92 . Vinyl cyclohexane 695-12-53 . 1,4-Bis(1-hydroxycyclopentyl) butadiyne 104766-62-34 . t-Butyl cyclopentadiene 41539-65-55 . Diphenyl fulvene 2175-90-86 . 1,2,3,4-Tetramethyl cyclopentadiene 4249-10-97 . 1,2,3,4,5-Pentamethyl cyclopentadiene 4045-44-78 . Ferrocene tech 102-54-59 . Acetyl ferrocene 1271-55-2
10 . Vinyl ferrocene 1271-51-811 . 1,1-Bis(diphenyl phosphino) ferrocene 12150-46-812 . 1,1-Bis(diphenyl phosphino) ferrocene Pd (II) dichloride 72287-26-413 . Pentamethyl cyclopentadiene titanium trimethoxide 123927-75-314 . Pentamethyl cyclopentadiene titanium trichloride 12129-06-515 . 1-dimethyl- 2,3,4,5-Tetramethyl cyclopentadiene silyl t-butylamine 125542-04-316 . 2,3,4,5-Tetramethylcyclopentadienyldimethylsilyl-t-butylamido titanium dichloride 135072-61-6
Ligand
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CAS # Chemical Name109-49-9 5-Hexene-2-one695-12-5 Vinylcyclohexane
104766-62-3 1,4-Bis(1-hydroxycyclopentyl) butadiyne41539-65-5 t-Butylcyclopentadiene2175-90-8 Diphenylfulvene 4249-10-9 1,2,3,4-Tetramethylcyclopentadiene4045-44-7 1,2,3,4,5-Pentamethylcyclopentadiene102-54-5 Ferrocene (Technical Grade)
1271-55-2 Acetylferrocene1271-51-8 Vinylferrocene12150-46-8 1,1-Bis(diphenylphosphine) ferrocene72287-26-4 1,1-Bis(diphenylphosphine) ferrocene Palladium chloride
123927-75-3 Pentamethylcyclopentadiene titanium trimethoxide12129-06-5 Pentamethylcyclopentadiene titanium trichloride
125542-04-3 2,3,4,5-Tetramethylcyclopentadiene-1-dimethylsilyl-t-butylamine135072-61-6 2,3,4,5-Tetramethylcyclopentadienyldimethylsilyl-t-butylamido titanium dichloride
www.NorquayTech.com 21
etallocenes, Ligands
CH3
CH3
CH3
CH3
CH3
CH3 CH3
Si
CH3
CH3
NHCH3
CH3
CH3
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22
Alkyl Sulfonates
HPLC: high purity Reagent Grade Industrial surfactants Dial-In properties
From C-2 to C-16Salts; Na, K, Li etc
Alkyl sulfonic acidsSodium <25 – 50 ppm
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Alkyl Sulfonates (& their free acids)
SO3Na • H2Oor
CH3(CH2)7SO3Na • H2O
SO3Na
or
CH3(CH2)15SO3Na
CH3 (CH2)3 SO3Na
SO3Na
or
1-Butane sulfonic acid sodium salt
1-Hexadecane sulfonic acid sodium salt
1-Octane sulfonic acid sodium salt monohydrate
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Tentative Specifciations Appearance slightly yellow transparent liquid
Color (APHA): max 700 Acid value (mg KOH/g): < 0.1Assay: Develop GC method PropertiesSpecific gravity (20°C): 1.380 - 1.400 g/ccEster value (mg KOH/g): 223 (no limit)Refractive Index (25°C): 1.512 (no limit)
Chlorendate- DBC
ClCl
Cl
Cl
Cl
ClO-nBu
O
O
O-nBu
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Chlorendate- DEC, DBC, DEHC
ClCl
Cl
Cl
Cl
Cl
O
O
O
O
CH3
CH3
ClCl
Cl
Cl
Cl
ClO-nBu
O
O
O-nBu
ClCl
Cl
Cl
Cl
Cl
O
O
O
O
CH3
CH3
CH3
CH3
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Contact Us
Business DevelopmentRobert W. Heldt PresidentTel +1(610) 874-4330Fax +1(610) 874-3575 [email protected]
Sales & MarketingJohn C. Wetzel, Ph.D.Director of Sales & MarketingTel +1(610) 874-4330Cell +1(803) [email protected]
For more information contact:
cell +1(610) 945-8676
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