New Agilent Molecular Spectroscopy Solutions for your Analytical

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Steve Bouffard, PhD Agilent Technologies Product Specialist Molecular Spectroscopy New Agilent Molecular Spectroscopy Solutions for your Analytical Laboratory

Transcript of New Agilent Molecular Spectroscopy Solutions for your Analytical

Steve Bouffard, PhD Agilent Technologies Product Specialist Molecular Spectroscopy

New Agilent Molecular Spectroscopy Solutions for your Analytical Laboratory

Agilent Molecular Spectroscopy Portfolio

UV-Vis 8453

Fluorescence Cary Eclipse

UV-Vis Cary 60

UV-Vis-NIR Cary 4000 Cary 5000 Cary 6000i

FTIR, Microscopy & Imaging Cary 640 Cary 660 Cary 680 Cary 680

Cary 610 Cary 620

UV-Vis Cary 100 Cary 300

Dedicated FTIR 5500

Portable FTIR 4500

4100 Exoscan 4100 Flex Scan FTIR

Cary 630

Agilent UV/Vis/NIR Spectrophotometer Portfolio

Cary 300 UV/Vis

Cary 4000 UV/Vis

8453 UV/Vis

Cary 100 UV/Vis Cary 60 UV/Vis

Cary 5000 UV/Vis/NIR Cary 6000i UV/Vis/NIR

Cary 60 UV/Vis Spectrophotometer • Unique Xenon lamp technology

– Fast data collection (80 pts/sec or up to 24000 nm/min)

– Small volume samples – Fiber optics (>50% coupling efficiency) – Room light immunity

• Measure with open sample compartment

– Lamps flashes only while sampling • Eliminates photo-degradation • Long lamp lifetime

• Double Beam Design • Covers range from 190 -1100 nm • 1.5 nm spectral bandwidth • Linear to 4 Abs • Economical price

Application focus • Chemicals QA/QC • Biotech • Academic

Agilent 8453 UV/Vis System • Unique Diode Array Spectrometer

• Scans entire spectrum simultaneously • Full Spectrum Kinetics (0.1 sec)

•Small Footprint

•Room light immunity

•ChemStation Software

•(Almost) No moving parts!!

•Popular in Pharma Environment

•Covers the range from 190 – 1100 nm

•1.5 nm spectral bandwidth

•Linear to almost 3 Abs

•Fast, Simple, Reliable

Application focus • Pharma • Biotech • Academic

Cary 100 and 300 UV/Vis Systems

Proven Cary design… • Superior photometric range and

accuracy • True Double Beam (PMT Detector) • Wide range of accessories

– Diffuse Reflectance Accessories • Research grade instrument • 0.2 to 4 nm variable SBW

• Variable in 0.1 nm intervals

• 190 – 900 nm scan range • Excellent stray light rejection

– Cary 100 linear to 4 Abs – Cary 300 linear to 5 Abs

• Pre-monochromator

Application focus • Materials testing • Academic research • Biotech research • Thermal Denaturation Studies

Cary 4000, 5000, and 6000i UV/Vis/NIR Systems

Ultra High Performance Systems • Double beam • Double Monochromator • Unsurpassed photometric range and

accuracy • High Resolution: as low as 0.01 nm • Wavelength range into the NIR • Unsurpassed stray light rejection • Linear up to 8 Abs • Accessories, Accessories, Accessories

– Diffuse Reflectance – Specular Reflectance

Application focus •Optical Components •Solar Cells •Semiconductors •Thin films •Anti-reflective Coatings •Nanocomposites

Cary Eclipse Fluorescence Spectrometer

The Power of Xenon… • Unique Xe flashlamp technology

• Measure small volume samples

• Fiber optics, Temp. Control

• Room light immunity: unique,

patented technology

• Eliminate photo-degradation

• Long lamp lifetime

Application focus • Biochemical applications • Academia

Moving On to Agilent

FTIR Systems

FTIR Portfolio Positioning Analyzers to Mobile Measurements

Portable Analyzer • Chemicals, Petrochem • Fixed sampling interface

with method-driven software

• Customers needing remote capabilities but still doing specific applications eg. oil in wind turbines

Out-of-lab • Materials testing, Chemicals • Interchangeable sampling

accessories • Customers that require

flexibility to take the instrument to the sample, where the sample cannot be easily ‘prepared’ for traditional lab-based FTIR measurements

4500 Series FTIR

4100 Exoscan

Dedicated Analyzer • Chem/Petrochem • Sealed unit with fixed

sampling interface with method-driven software

• Customers wanting to do measurements in a ‘non-lab’ environment and measuring samples based on standard or in-house methods, eg. measuring Biodiesel or Oil Analysis

Out-of-lab • Materials testing, Chemicals • Customers needing added

flexibility getting to ‘hard-to-reach’ areas where the hand-held Exoscan cannot

4200 Flexscan

5500 Series FTIR

FTIR Portfolio Positioning In-lab…from routine to research

Routine-Research • Materials/Polymers,

Chemicals, Biotech, Academic research

• Customers needing more than MidIR or DTGS capabilities

• Customers who want to expand their capabilities in the future

Research • Materials/Polymers,

Chemicals, Biotech, Academic research

• Customers needing superior optical performance

• Customers wanting to perform high-end experiments: PEM-IRRAS, PAS, us and ns TRS

660 FTIR

670/680 FTIR

Routine • Chemicals,

Pharma/Biotech, Academic teaching

• Customers doing routine FTIR measurements in the MidIR spectral region

• Customers whose budget is <$20K

• Majority of 640 FTIR customers will fit the profile for a 630 FTIR

Research • Materials/Polymers,

Chemicals, Biotech, Academic research

• Customers needing to measure <10um in area

• Customers wanting to do imaging, primarily looking at small defects within a larger sample.

610/620 FTIR

630 FTIR

The New Agilent Cary 630 FTIR System

• The World’s Smallest FTIR!

• Match the accessory with the application

• Purpose driven software to give results not data

INTUITIVE: Sampling Flexibility Solving problems through innovation…

630 Engine DialPath TumblIR

Diamond ATR Diffuse Reflectance Transmission

INNOVATIVE: Revolutionary technology for Liquids Analysis using the “DialPath”

Pathlength (μm) Typical Conc. Range 30 Neat - 0.1% 50 50% - 500 ppm 100 20% - 100 ppm 200 10 % - 50 ppm

TRADITIONAL APPROACH

INTUITIVE: A better approach to software… Method Driven and Guided Sampling

Software guides the user through the selected method.

Also recognizes the correct sampling interface to guide proper sampling techniques and

cleaning.

INTUITIVE: A better approach to software… Visual Results

Library results are shown with the hit list and can be

overlaid or stacked

Quant results can be programmed for critical action levels with color coded queues

(red, green, yellow)

Agilent Molecular Spectroscopy Portfolio

UV-Vis 8453

Fluorescence Cary Eclipse

UV-Vis Cary 60

UV-Vis-NIR Cary 4000 Cary 5000 Cary 6000i

FTIR, Microscopy & Imaging Cary 640 Cary 660 Cary 680 Cary 680

Cary 610 Cary 620

UV-Vis Cary 100 Cary 300

Dedicated FTIR 5500

Portable FTIR 4500

4100 Exoscan 4100 Flex Scan FTIR

Cary 630