N/A 4131 SW 47th AVENUE SUITE 1408 Certiﬁcate …

This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation

Jorge SegredoLab Director

State License # n/aISO Accreditation # 97164 ___________________

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01/16/2020

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4131 SW 47th AVENUE SUITE 1408

Kaycha Labs200mg froggies

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Certificateof Analysis

SAMPLE:DA00109009-002Harvest/Lot ID: cono1913

Seed to Sale #n/aBatch Date :N/A

Batch#: cono1913Sample Size Received: 56 gram

Ordered : 01/08/20Sampled : 01/08/20

Completed: 01/16/20 Expires: 01/16/21Sampling Method: SOP Client Method

Jan 16, 2020 | Green Roads5150 SW 48TH WAY DAVIEFL, USA 33314

PASSED of 5

PRODUCT IMAGE SAFETY RESULTS MISC.

PesticidesPASSED

Heavy MetalsPASSED

MicrobialsPASSED

MycotoxinsPASSED

ResidualsSolventsPASSED

FilthNOT TESTED

Water ActivityNOT TESTED

MoistureNOT TESTED

TerpenesTESTED

CANNABINOID RESULTS

Total THC

0.000%THC/Container :0.00 mg

Total CBD

0.334%CBD/Container :187.04mg

Total Cannabinoids

0.334%

CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD THCA D9-THC

ND ND ND ND ND ND ND ND 0.334 % ND ND

ND ND ND ND ND ND ND ND3.340mg/g ND ND

0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.001 0.0001

Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :1224 3.0883g NA NA

Analysis Method -SOP.T.40.020, SOP.T.30.050Analytical Batch -DA009266POT Instrument Used : DA-LC-003 Batch Date : 01/09/20

Reagent Dilution Consums. ID

123019.R09 40 76124-662070219.R15 SFN-BX-1025010920.R05 849C4-849AK010920.R04 840C6-840HFull spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method:SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1mg/L).




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Certificate of Analysis PASSED

Green Roads

5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email: [email protected]

Sample : DA00109009-002Harvest/LOT ID: cono1913

Batch# : cono1913Sampled : 01/08/20Ordered : 01/08/20

Sample Size received : 56 gramCompleted : 01/16/20 Expires : 01/16/21Sample Method : SOP Client Method

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Terpenes TESTED

Terpenes LOD TEST RESULT (%)

ALPHA-CEDRENE 0.007 NDALPHA-HUMULENE 0.007 NDALPHA-PINENE 0.007 NDALPHA-TERPINENE 0.007 NDBETA-MYRCENE 0.007 NDBETA-PINENE 0.007 NDBORNEOL 0.013 NDCAMPHENE 0.007 NDCAMPHOR 0.013 NDCARYOPHYLLENE OXIDE 0.007 NDCEDROL 0.007 NDALPHA-BISABOLOL 0.007 NDISOPULEGOL 0.007 NDCIS-NEROLIDOL 0.007 ND3-CARENE 0.007 NDFENCHYL ALCOHOL 0.007 NDHEXAHYDROTHYMOL 0.007 NDEUCALYPTOL 0.007 NDISOBORNEOL 0.007 NDFARNESENE 0.007 NDFENCHONE 0.007 NDGAMMA-TERPINENE 0.007 NDGERANIOL 0.007 NDGERANYL ACETATE 0.007 NDGUAIOL 0.007 NDLIMONENE 0.007 NDLINALOOL 0.007 NDNEROL 0.007 NDOCIMENE 0.007 NDALPHA-PHELLANDRENE 0.007 NDPULEGONE 0.007 NDSABINENE 0.007 NDSABINENE HYDRATE 0.007 ND

Terpenes LOD TEST RESULT(%)

TERPINEOL 0.007 ND

TERPINOLENE 0.007 ND

BETA-CARYOPHYLLENE 0.007 ND

TRANS-NEROLIDOL 0.007 ND

VALENCENE 0.007 ND

Terpenes TESTED

Analyzed by Weight Extraction date Extracted By1118 0.9710g 01/09/20 1118

Analysis Method -SOP.T.40.090Analytical Batch -DA009267TERInstrument Used : Liquid Injection GCMS QP2020 (E-SHI-128)Batch Date : 01/09/20


052119.04 10 76124-662280630187

Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.

Total 0




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Pesticides PASSED

Pesticides LOD Action Level Units ResultCHLORDANE 0.005 0.1 ppm NDCAPTAN 0.05 3 ppm NDBOSCALID 0.01 3 PPM NDDIMETHOATE 0.01 0.1 ppm NDAZOXYSTROBIN 0.01 3 ppm NDABAMECTIN B1A 0.02 0.3 ppm NDCIS-PERMETHRIN 0.05 1 ppm NDSPINETORAM 0.01 3 PPM NDACEPHATE 0.001 3 ppm NDFENOXYCARB 0.01 0.1 ppm NDDIMETHOMORPH 0.005 3 ppm NDBIFENAZATE 0.01 3 ppm NDETHOPROPHOS 0.01 0.1 ppm NDACEQUINOCYL 0.01 2 ppm NDACETAMIPRID 0.01 3 ppm NDETOFENPROX 0.01 0.1 ppm NDBIFENTHRIN 0.01 0.5 ppm NDALDICARB 0.02 0.1 ppm NDETOXAZOLE 0.01 1.5 ppm NDFENPYROXIMATE 0.01 2 ppm NDFIPRONIL 0.02 0.1 ppm NDFENHEXAMID 0.01 3 ppm NDCARBARYL 0.01 0.5 ppm NDCARBOFURAN 0.01 0.1 ppm NDFLONICAMID 0.01 2 ppm NDFLUDIOXONIL 0.01 3 ppm NDCHLORFENAPYR 0.01 0.1 ppm NDCHLORANTRANILIPROLE 0.01 3 ppm NDHEXYTHIAZOX 0.01 2 ppm NDCHLORPYRIFOS 0.01 0.1 ppm NDIMAZALIL 0.01 0.1 ppm NDMALATHION 0.01 2 ppm NDCLOFENTEZINE 0.01 0.5 ppm NDDAMINOZIDE 0.02 0.1 ppm NDIMIDACLOPRID 0.01 3 ppm NDMETALAXYL 0.01 3 ppm NDDICHLORVOS 0.05 0.1 ppm NDMETHIOCARB 0.01 0.1 ppm NDCOUMAPHOS 0.005 0.1 ppm ND

Pesticides LOD Action Level Units ResultMETHOMYL 0.01 0.1 ppm NDKRESOXIM-METHYL 0.01 1 ppm NDDIAZANON 0.01 0.2 ppm NDCYPERMETHRIN 0.01 1 ppm NDMEVINPHOS 0.01 0.1 ppm NDMYCLOBUTANIL 0.01 3 ppm NDNALED 0.01 0.5 ppm NDOXAMYL 0.01 0.5 ppm NDPACLOBUTRAZOL 0.01 0.1 ppm NDTRANS-PERMETHRIN 0.05 1 ppm NDPHOSMET 0.01 0.2 ppm NDPIPERONYL BUTOXIDE 0.01 3 ppm NDPRALLETHRIN 0.05 0.4 ppm NDPROPICONAZOLE 0.01 1 ppm NDPROPOXUR 0.01 0.1 ppm NDPYRETHRIN I 0.01 1 ppm NDPYRIDABEN 0.01 3 ppm NDSPINOSAD (SPINOSYN A) 0.01 3 ppm NDSPINOSAD (SPINOSYN D) 0.01 3 ppm NDSPIROMESIFEN 0.01 3 ppm NDSPIROTETRAMAT 0.02 3 ppm NDSPIROXAMINE 0.01 0.1 ppm NDTEBUCONAZOLE 0.01 1 ppm NDTHIACLOPRID 0.01 0.1 ppm NDTHIAMETHOXAM 0.01 1 ppm NDTRIFLOXYSTROBIN 0.01 3 ppm ND

Pesticides PASSED

Analyzed by Weight Extraction date Extracted By585 0.9803g NA NA

Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch - DA009277PESInstrument Used : LCMS E-SHI-039Batch Date : 01/09/20

Reagent Dilution Consums. ID101519.04 180711010220.R05010220.R06

SOP.T.30.065, SOP.T.40.065




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Residual Solvents PASSED

SOLVENT LOD ACTIONLEVEL(PPM)

PASS/FAIL RESULT

PROPANE 120 2100 PASS ND

BUTANES (N-BUTANE) 96 2000 PASS ND

ETHYLENE OXIDE 0.6 5 PASS ND

METHANOL 22.5 250 PASS ND

ETHANOL 90 5000 PASS ND

PENTANES (N-PENTANE) 67.5 750 PASS ND

ETHYL ETHER 45 500 PASS ND

ACETONE 67.5 750 PASS ND

2-PROPANOL 45 500 PASS ND

ACETONITRILE 5.4 60 PASS ND

DICHLOROMETHANE 11.25 125 PASS ND

N-HEXANE 4.5 250 PASS ND

ETHYL ACETATE 36 400 PASS ND

BENZENE 0.09 1 PASS ND

HEPTANE 45 500 PASS ND

TOLUENE 13.5 150 PASS ND

CHLOROFORM 0.18 2 PASS ND

1,2-DICHLOROETHANE 0.18 2 PASS ND

TRICHLOROETHYLENE 2.25 25 PASS ND

1,1-DICHLOROETHENE 1 8 PASS ND

TOTAL XYLENES 13.5 150 PASS ND

Residual Solvents PASSED


Analysis Method -SOP.T.40.032Analytical Batch -DA009287SOLInstrument Used : Headspace GCMSBatch Date : 01/09/20


1 00268767161040-124152436

Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 34 Residual solvents.(Method: SOP.T.30.042 Residual Solvents Analysis via GC-MS).




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Mycotoxins PASSED

Analyte LOD Result Action Level(PPM)

AFLATOXIN G2 0.002 NDAFLATOXIN G1 0.002 NDAFLATOXIN B2 0.002 NDAFLATOXIN B1 0.002 NDOCHRATOXIN A+ 0.002 ND 0.02TOTAL AFLATOXINS 0.02 ND 0.02

Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA009278Instrument Used : LCMS E-SHI-039Batch Date : 01/09/20

Analyzed by Weight Extraction date Extracted By585 1g NA NA

Microbials PASSED

Analyte LOD ResultASPERGILLUS_FLAVUS 10000 not present in 1 gram.ASPERGILLUS_FUMIGATUS 10000 not present in 1 gram.ASPERGILLUS_NIGER 10000 not present in 1 gram.ASPERGILLUS_TERREUS 10000 not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP 10000 not present in 1 gram.SALMONELLA_SPECIFIC_GENE 10000 not present in 1 gram.TOTAL_YEAST_AND_MOLD 100 not present in 1 gram.

Analysis Method -SOP.T.40.043Analytical Batch -DA009268MICInstrument Used : PathogenDX PCR_Array ScannerBatch Date : 01/09/20

Analyzed by Weight Extraction date Extracted By513 1g NA NA

Heavy Metals PASSED


010220.R09 50010820.R01010620.R02121319.R05010320.R03010220.R04111319.01

Metal LOD Result Action Level(PPM)

ARSENIC 0.01 ND 1.5CADMIUM 0.01 ND 0.5LEAD 0.01 ND 0.5MERCURY 0.01 ND 3


Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA009259HEAInstrument Used : ICPMS-2030Batch Date : 01/09/20

Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.

N/A 4131 SW 47th AVENUE SUITE 1408 Certiﬁcate …

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