MICROCHEM SILLIKER PVT.LTD.

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MICROCHEM SILLIKER PVT.LTD. TEST REPORT REPORT NO.: 171815312 REPORTDATE: 19/06/2017 Customer Name Samanvay Seeds Pvt. Ltd Address 140,Bhopal Chourasa, Dewas,Madhya Pradessh-455001 Sample(s) Drawn by The Laboratory No Date of Sample Received 09/06/2017 Date of Starting Analysis 15/06/2017 Date of Com pletion 17/06/2017 Sample Description Organic Soyabean Seeds Sample Details Nature:Solid, Qty:610gms, Stamped/Sealed:No, Packing:Plastic Pack PARAMETER NAME RESULT UNIT LOQ METHOD Oil Content 18.36 % - GAFTA 2014 (3.0) Total Ash 5.60 % - GAFTA 2014 (12.0) Protein (N x 6.25) 39.42 % - GAFTA 2014 (4.1) Moisture 8.17 % - GAFTA 2014 (2.1) Damaged grains 0.03 % -- MC/SOP/CHE/03 2,4-D Sum of 2,4-D and its esters expressed BLQ mg/kg 0.01 MC/SOP/INS/ll based on as 2,4-0) NRCG-EURL-SRM-VERSION7.1 Nov 2013 Aldrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC 2007.01 Aldrin, dieldrin (the limits apply to aldrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC and dieldrin singly or in any combination 2007.01 and are expressed as dieldrin) Allethrin and Bioallethrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC 2007.01 HCH (Sum of Isomers, except the gamma BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC Isomers) 2007.01 alpha- HCH BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC 2007.01 beta- HCH BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC 2007.01 lindane (gamma -HCH) BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC 2007.01 _ .. 111111111111I11 171815312 006654 Microchem Silliker Pvt. ltd. MicroChem House, A-Sl3, TTCIndustrial Area, MID(' Mahape,NaviMumbai 400 701.India ·Tel. +91-22-39469700 Fax: +91-22-39469701 CIN . U24233MH2007PTC170S36 www.microchem.co.in

Transcript of MICROCHEM SILLIKER PVT.LTD.

MICROCHEMSILLIKER PVT.LTD.

TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

Customer Name Samanvay Seeds Pvt. Ltd

Address 140,Bhopal Chou rasa, Dewas,Madhya Pradessh-455001

Sample(s) Drawn by The Laboratory No

Date of Sample Received 09/06/2017

Date of Starting Analysis 15/06/2017

Date of Completion 17/06/2017

Sample Description Organic Soyabean Seeds

Sample Details Nature:Solid, Qty:610gms, Stamped/Sealed:No,Packing:Plastic Pack

PARAMETER NAME RESULT UNIT LOQ METHOD

Oil Content 18.36 % - GAFTA 2014 (3.0)Total Ash 5.60 % - GAFTA 2014 (12.0)Protein (N x 6.25) 39.42 % - GAFTA 2014 (4.1)Moisture 8.17 % - GAFTA 2014 (2.1)Damaged grains 0.03 % -- MC/SOP/CHE/032,4-D Sum of 2,4-D and its esters expressed BLQ mg/kg 0.01 MC/SOP/INS/ll based onas 2,4-0) NRCG-EURL-SRM-VERSION7.1

Nov 2013Aldrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Aldrin, dieldrin (the limits apply to aldrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACand dieldrin singly or in any combination 2007.01and are expressed as dieldrin)Allethrin and Bioallethrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01HCH (Sum of Isomers, except the gamma BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACIsomers) 2007.01alpha- HCH BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01beta- HCH BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01lindane (gamma -HCH) BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC

2007.01 _ ..

111111111111I11171815312

006654Microchem Silliker Pvt. ltd.MicroChem House, A-Sl3, TTC Industrial Area, MID('Mahape,NaviMumbai 400 701. India·Tel. +91-22-39469700 Fax: +91-22-39469701

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MICROCHEMSILLIKER PVT.LTD.

TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT lOQ METHOD

delta- HCH BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Bifenthrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Captafol BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Captan BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Carbaryl BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Carbofuran (Sum of Carbo fur an and BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC3-Hydroxy Carbofuran epxressed as 2007.01carbofu ran)Carbosulfan BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC

2007.01

Carboxin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Chlordane (residue to be measured as cis BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACplus trans chlordane) 2007.01

Chlorfenopyr BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Chlorothalonil BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Chlorpyrifos BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Chlorpyrifos Methyl BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

cis-chlordane BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cis-Permethrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cyfluthrin BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC2007.01

Cyfluthrin 1 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cyfluthrin 2 BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC2007.01

Cyfluthrin 3 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cyfluthrin 4 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cypermethrin (sum of isomers) (fat soluble BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACresidue) 2007.01Cypermethrin 1 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Cypermethrin 2 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Cypermethrin 3 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01

1IIIIInlllilim171815312

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006655Microchem Silliker Pvt. Ltd.MicraChem House, A-S13, TTC Industrial Area, MIDCMahape,NaviMumbai 400 701. India-r-r. +91-22-39469700 Fax: +91-22-39469701

MICROCHEMSILLIKER PVT.LTD.

TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Cypermethrin 4 BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

D.D.T. (The limits apply to D.D.T., 0.0.0. ant BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACD.D.E. singly or in any combination) 2007.01

Deltamethrin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Dichlorvos (content of BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACdi-chloroacetaldehyde (D.C.A.) be reported 2007.01where possible)

Dicofol BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Dieldrin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Endosulfan A BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Endosulfan B BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Endosulfan-Sulphate BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Endosulphan (residues are measured and BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACreported as total of endosulfan A and Band 2007.01endosu Ifan-su Iphate)

Endrin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Ethofenprox (Etofenprox) BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenpropathrin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenvalerate (any ratio of constituent BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACisomers (RR,SS,as & sR) including 2007.01esfenvalerateFenvalerate and Esefenvalerate (Sum of Rs BLQ mglkg 0.01 MC/sOP/INs/34 based on AOAC& sR isomers) 2007.01Fipronil BLQ mglkg 0.005 MC/sOP/INs/34 based on AOAC

2007.01Fipronil (Sum of fipronil + Sulfone BLQ mglkg 0.005 MC/sOP/INs/34 based on AOACmetabolite (MB46136) Expressed as 2007.01fipronil)Fipronil sulfone BLQ mglkg 0.005 MC/sOP/INs/34 based on AOAC

2007.01Heptachlor BLQ mglkg 0.01 MC/sOP/INs/34 based on AOAC

2007.01Heptachlor (combined residues of BLQ mglkg 0.01 MC/sOP/INs/34 based on AOACheptachlor and its epoxide to be 2007.01determined and expressed as Heptachlor)Heptachlor epoxide BLQ mglkg 0.01 MC/sOP/INs/34 based on AOAC

2007.01Hexaconazole BLQ mglkg 0.01 MC/sOP/INs/34 based on AOAC

2007.01

1IIIIIR.II~llllnll171815312 Page 3 of 13

006656Microchem Silliker Pvt. Ltd.MicroChem House, A-513, TTC Industrial Area, MIDC.Mahape,Navi Mumbai 400 701. India-rer.: +91-22-39469700 Fax: +91-22-39469701 www.microchem.co.in

MICROCHEMSILLIKER PVT.LTD.

TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Iprodione BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Lambda-cyhalothrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Parathion Ethyl BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Permethrin (Sum of Isomers) BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Propanil BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

tau-Fluvalinate BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

trans-chlordane BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Transfluthrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

trans-Permithrin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

3,4-dichloroaniline BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

3-hyd roxy-ca rbofu ran BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

4-bromo-2-chlorophenol (metabolite of BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACProfenophos) 2007.01

Abamectin (Sum of avermectin Bl a, BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACavermectin B1b and delta 8,9 isomer of 2007.01avermectin Bla)Acephate BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01

Acetamiprid BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Alachlor BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Atrazine BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Azoxystrobin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Benalaxyl including other mixtures of BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACconstituent isomers including Benalaxyl-M 2007.01(sum of isomers)Bendiocarb BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Benfuracarb BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Benomyl BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Benomyl (See carbendazim) BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01 ........_

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CIN U24233MH2007PTCl70S36www.microchem.co.in

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TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Bifenazate BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Bitertanol BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Buprofezin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Butachlor BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Carbendazim BLQ mglkg 0.Q1 MC/SOP/INS/34 based on AOAC2007.01

Carbendazim (including Benomyl) BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Carbofuran BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Chlorantraniliprole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Chlorfenvinphos BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Clothianidin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cyantraniliprole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cyazofamid BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Cymoxanil BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Dazomet (Methylisothiocyanate resulting BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACfrom the use of dazomet and metam) 2007.01Demeton-S-methylsulfone BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Diazinon BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Difenoconazole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Difenthiuron BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Diflubenzuron BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Dimethoate BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Dimethoate (Including Omethoate) BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Dimethomorph BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Dinotefuran* BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Diuron BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01----:;r,...-- •. ~-- ...~.

111111111:11111111171815312 Page 5 of 13

006658Microchem Silliker Pvt. Ltd.MicroChem House, A-Sl3, TTC Industrial Area, MIDC,Mahape,NaviMumbai 400 701. India

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TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT lOQ METHOD

Diuron (Diuron including all components BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACcontaininf 3,4 dicloroaniline moiety 2007.01expressed as 3,4 dichloroaniline)

Dodine BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Edifenphos BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Emamectin Benzoate BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Ethion BLQ mglkg om MC/SOP/INS/34 based on AOAC2007.01

Etoxazole* BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Etrimfos BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Famoxadone BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenamidone BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenarimol BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenazaquin BLQ mglkg om MC/SOP/INS/34 based on AOAC2007.01

Fenitrothion BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenobucarb BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenpyroximate BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenthion BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fenthion (sum of fenthion, its oxygen BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACanalogue and their sulphoxides and 2007.01sulphones expressed as fenthion)Fenthion-sulfone BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Fenthion-sulphoxide BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Flonicamid* BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Flonicamid (sum of fionicamid, TNFG and BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACTNFA)* 2007.01Flubendiamide BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Flufenacet BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Flufenoxuron BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01

1IIIIIgOIIIIIIIII171815312 Page 6 of 13

006659Microchem Silliker Pvt. Ltd.MicroChem House, A-Sl3, TTC Industrial Area, MIDC,Mahape,NaviMumbai 400 701. India·Tel .. +91-22-39469700 Fax: +91-22-39469701

Email

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MICROCHEMSILLIKER PVT.LTD.

TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Flufenzine* BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fluopicolide* BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fluopyram* BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Flusilazole BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Fluxapyroxad* BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Forchlorfenuron (CPPU) BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Hexythiazox BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

lrnldacloprld BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Indoxacarb (Sum of Rand S Isomers) BLQ mgfkg 0.D1 MC/SOP/INS/34 based on AOAC2007.01

lodosulfuron Methyl Sodium/lodosulfuron BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC-methyl (Iodosulfuron - methyl) Including 2007.01salts, expressed as idosulfuron - methyl

Iprobenphos BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Iprovalicarb BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Isoprothiolane BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Isoproturon BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Kresoxim Methyl BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

linuron BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Lufenuron BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Malaoxon BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Malathion BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Malathion (Malathion to be determined BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOACand expressed as combined residues of 2007.01malathion and malaoxon)Mandipropamid BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Metalaxyl BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Methamido-phos (A metabolite of BLQ mgfkg 0.01 MC/SOP/INS/34 based on AOACAcephate) 2007.01

IIIIIIIIIIIIIIII!RI171815312

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TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Methomyl BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Methomyl and Thiodicarb (Sum of BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACmethomyl and thiodicarb expressed as 2007.01methomyl)Metolachlor and S-metolachlor BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC(metolachlor including other mixtures of 2007.01constituent isomers includingS-metolachlor (sum of isomers)Metrafenone* BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01

Metribuzin BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC2007.01

Milbemectin (sum of milbemycin A4 and BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOACmilbemycin A3, expressed as milbemectin) 2007.01

Milbemycin A3 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Milbemycin A4 BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Monocrotophos BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Myclobutanil BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC2007.01

Novaluron BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Omethoate BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Omethoate (refer to Dimethoate) BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Oxadiazon BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Oxyca rboxi n BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Oxydemeton- methyl BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Oxydemeton- methyl (Sum of oxydemeton BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACmethyl and demeton-s-smethylsulfone 2007.01expressed as oxydemeton methylOxyfluorfen BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Paclobutrazol BLQ mg/kg 0.Q1 MC/SOP/INS/34 based on AOAC

2007.01Parathion methyl BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Parathion methyl (combined residues of BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACparathion methyl and its oxygen analogue 2007.01to be determined and expressed asparathion methyl)

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TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Paraxon methyl BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Penconazole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Pencycuron BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Pendimethalin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Phenthoate BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Phorate BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Phorate (sum of Phorate, its oxygen BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACanalogue and their sulphoxides and 2007.01sulphones, expressed as phorate)Phorate sulfone BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Phorate sulphoxide BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Phosalone BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Phosphamidon residues (expressed as the BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACsum of phosphamidon and its desethyl 2007.01derivative)Pirimiphos Methyl BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Profenophos BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Propamocarb (sum of prpamocarb and its BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACsalt expressed as propamocarb)* 2007.01Propargite BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Propetamphos BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Propiconazole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Propoxur BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Pyraclostrobin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Pyridaben* BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Pyriproxyfen BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Quinalphos BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Simazine BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01

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TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Spinosad (Sum of Spinosyn A + D) BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Spinosyn A BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Spinosyn D BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Spirodiclofen* BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Spiromesifen BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Tebuconazole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Temephos BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Tetraconazole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Thiochloprid BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Thiamethoxam (sum of thiamethoxam and BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACclotianidin expreesed as thiamethoxam) 2007.01Thiobencarb (Benthiocarb) BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Thiocyclam* BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Thiodicarb BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Thiodicarb (See Methomyl) BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Thiometon (Residues determined as BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACthiometon its sulfoxide and sulphone 2007.01expressed as thiometon)Thiophanate-Methyl BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Triadimefon BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Triadimefon (sum oftriadimefon and BLQ mglkg 0.01 MC/SOP/INS/34 based on AOACtriadimenol) 2007.01Triadimenol BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Triazophos BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Trich lorfon BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Tricyclazole BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Tridemorph BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01Trifloxystrobin BLQ mglkg 0.01 MC/SOP/INS/34 based on AOAC

2007.01

III~ 11111111111111~II !IIIIIEI ~III171815312 Page 10 of 13

006663Microchem Silliker Pvt. Ltd.MicroChem House, A-513, TTC Industrial Area, MIDC,Mahape,NaviMumbai 400 701. India

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TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Trifluralin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

6-Benzyl adenine A BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Ametoctradin* BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Azadirachtin BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOAC2007.01

Diquat BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Homobrassinolide BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

TNFA* BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

TNFG* BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Alfa Nephthyl Acetic Acid (A.N.A) BLQ mg/kg 0.01 MC/SOP/INS/11 based onNRCG-EURL-SRM-VERSION7.1Nov 2013

4-CPA (4 Chlorophenoxy acetic acid) BLQ mg/kg 0.01 MC/SOP/INS/11 based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Cartap hydrochloride BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Chlormequatcloride (CCC) BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Dithianon BLQ mg/kg 0.01 MC/SOP/INS/11 based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Ethephon BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Fosetyl-A1 (Sum fosetyl + Phophorus acid BLQ mg/kg 0.01 MC/SOP/INS/11 based onand their salts, expressed as fosetyl) NRCG-EURL-SRM-VERSION7.1

Nov 2013Mepiquat BLQ mg/kg 0.01 MC/SOP/INS/ll based on

NRCG-EURL-SRM-VERSION7.1Nov 2013

Nereistoxin* BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

/~;~.~"1IIIIIIIIIIa I1I1I11I~III11111~III

171815312

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MICROCHEMSILLIKER PVT.LTD.

TEST REPORT

REPORTNO.: 171815312 REPORTDATE: 19/06/2017

PARAMETER NAME RESULT UNIT LOQ METHOD

Paraquat BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Uracil BLQ mg/kg 0.01 MC/SOP/INS/ll based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Glufosinate- Ammonium (Sum of BLQ mg/kg 0.01 MC/SOP/INS/41 based onglufosinate, its salts, MPP and NAG NRCG-EURL-SRM-VERSION7.1expressed as glufosinate equivalent) Nov 2013

Glufosinate-ammonium BLQ mg/kg 0.01 MC/SOP/INS/41 based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Glyphosate BLQ mg/kg 0.01 MC/SOP/INS/41 based onNRCG-EURL-SRM-VERSION7.1Nov 2013

MPP BLQ mg/kg 0.01 MC/SOP/INS/41 based onNRCG-EURL-SRM-VERSION7.1Nov 2013

NAG BLQ mg/kg 0.01 MC/SOP/INS/41 based onNRCG-EURL-SRM-VERSION7.1Nov 2013

Dinocap (Sum of dinocap isomers and their BLQ mg/kg 0.01 MC/SOP/INS/14 based oncorresponding phenols expressed as NRCG-EURL-SRM-VERSION7.1dinocap) and methydinocap Nov 2013Meptyldinocap (sum of 2,4 DNOPCand 2,4 BLQ mg/kg 0.01 MC/SOP/INS/34 based on AOACDNOP expressed as meptyldinocap) 2007.01

Dithiocarbamates (the residue tolerance BLQ mg/kg 0.05 MC/SOP/INS/12 based onlimit are determined and expressed as NRCG-EURL-SRM-VERSION7.1mg/CS2/kg and refer separately to the Nov 2013residues arising from any or each group ofdithiocarbamates.Hydrogen Cyanamide (Cyanamide including BLQ mg/kg 0.01 Alalytical Letters Vol 37, No 9 1981salts expressed as cyanamide) -1989,2004Lead (as Pb) BLQ mg/kg 0.01 MC/SOP/INS/21 based on EPA

200.2 & 6020 & AOAC 2013.06Cadmium (as Cd) BLQ mg/kg 0.01 MC/SOP/INS/21 based on EPA

200.2 & 6020 & AOAC 2013.06-=--

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IIIIIIIIIIIIIII!II171815312

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REPORTNO.: 171815312 REPORTDATE: 19/06/2017

TEST REPORT

Remark: BLQ - Below Limit of Quantification

••••••.•..•.• END •••••••••••••

Authorized Signatory

Narasimhachari ChiralaDGM - Lab Operations

Note:I.Test results relate to the submitted sample(s) only.2. Test report shall not be reproduced except in full, without written approval of the laboratory.3. Laboratory is not responsible for the authenticity of photocopied test report.4. The test items will not be retained for perishable products and 1months in the caseof non-perishable samplesunless otherwise agreed with the customer or as required by the applicable regulation.

5. The tests marked with (0) are not accredited by NABL.6.The tests marked with (#) are OutSource.7.The Report no. with suffix R- RevisedReport.8.This is a computer generated report and does not require manual signature.

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IIIIIIIIIIIII171815312 Page 13 of 13

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