MAX LABORATORIES, INC. 1835 EMAX Batch … LABORATORIES, INC. 1835 W. 205th Street Torrance, CA...

MAX LABORATORIES, INC. 1835 W. 205th Street Torrance, CA 90501

Te!: (310) 618-8889 Fax: (310) 618-0818

Date: 03-18-2015 EMAX Batch No.: 15B126

Attn: Sarah Von Raesfeld

MWH 2121 N. California Blvd., #600 Walnut Creek, CA 94596

Subject: Laboratory Report Project: BOEING SSFL - 201501

Enclosed is the Laboratory report for samples received on 02/17/15. The data reported relate only to samples listed below:

Sample ID

WS-08 021615 03

Control # Col Date Matrix Analysis

B126-01 02/16/15 WATER URANIUM BY 908.0 (PARTICULATE) URANIUM BY 908.0 (DISSOLVED) GROSS ALPHA/BETA BY 900 (PARTICULATE) GROSS ALPHA/BETA BY 900 (DISSOLVED)

Note : Subcontracted to GEL Lab.

The results are summarized on the following pages.

Please feel free to call if you have any questions concerning these results.

sincerely/':JJ~:· j .,

-~-~ spar J. Pang boratory Director

This report is confidential and intended solely for the use of the individual or entity to whom it is addressed. This report shall not be reproduced except in full or without the written approval of EMAX.

EMAX certifies that results included in this report meets all NELAC & DOD requirements unless noted in the Case Narrative.

NELAC Accredited Certificate Number 02116CA L-A-B Accredited DoD ELAP and ISO/IEC 17025 Certificate Number L2278 Testing

LABORATORY REPORT FOR

MWH

BOEING SSFL- 201501

URANIUM BY 908.0 (PARTICULATE) URANIUM BY 908.0 (DISSOLVED)

GROSS ALPHA/BETA BY 900 (PARTICULATE) GROSS ALPHA/BETA BY 900 (DISSOLVED)

SDG#: 15B126

March 05, 2015 Mr. Ye Myint EMAX Laboratories 1835 W. 205th Street Torrance, California 90501 Re: Boeing SSFL - 2015Q1 Work Order: 367333 Dear Mr. Myint:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for thesample(s) we received on February 17, 2015. This original data report has been prepared and reviewed inaccordance with GEL’s standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needson time every time. We trust that you will find everything in order and to your satisfaction. If you have anyquestions, please do not hesitate to call me at (843) 556-8171, ext. 4487.

Sincerely, PM_SIGN_HERE Sylainna Rivers Project Manager

Chain of Custody: MWH20150216_00 Enclosures

Hope Taylor for

Table of Contents

Case Narrative......................................................................................1

Chain of Custody and Supporting Documentation...............................3

Laboratory Certifications......................................................................6

Radiological Analysis...........................................................................8

Sample Data Summary...............................................................17

Quality Control Data..................................................................20

Alpha Spectroscopy Raw Data...................................................25

Continuing Calibration Data...............................................39

Background and Efficiency Data........................................43

RAD Standards Traceability...............................................84

Runlogs...............................................................................92

Gas Flow Raw Data....................................................................95

Continuing Calibration Data.............................................111

Background and Efficiency Data......................................119

RAD Standards Traceability.............................................142

Runlogs.............................................................................151

Case Narrative

Page 1 of 153

Receipt Narrative for

EMAX Laboratories, LLC - Boeing SSFL SDG: 367333

March 05, 2015 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171

Summary:

Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on February 17,2015 for analysis. The samples were delivered with proper chain of custody documentation and signatures. Allsample containers arrived without any visible signs of tampering or breakage. There are no additional commentsconcerning sample receipt.

Sample Identification: The laboratory received the following samples:

Laboratory ID Client ID367333001 WS-08_021615_03367333002 WS-08_021615_03

Case Narrative:

Sample analyses were conducted using methodology as outlined in GEL’s Standard Operating Procedures. Anytechnical or administrative problems during analysis, data review, and reduction are contained in the analyticalcase narratives in the enclosed data package.

The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler ReceiptChecklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry.

PM_SIGN_HERE Sylainna Rivers Project Manager

Hope Taylor for

Page 2 of 153

Chain of Custody andSupporting

Documentation

Page 3 of 153

of 153

LaboratoryCertifications

Page 6 of 153

State CertificationAlaska

ArkansasCLIA

California Colorado

ConnecticutDelaware

DoD ELAP/ ISO17025 A2LAFlorida NELAP

Foreign Soils PermitGeorgia

Georgia SDWAHawaii

Idaho ChemistryIdaho Radiochemistry

Illinois NELAPIndiana

Kansas NELAPKentucky SDWA

Kentucky WastewaterLouisiana NELAPLouisiana SDWA

MarylandMassachusetts

MichiganMississippiNebraskaNevada

New Hampshire NELAPNew Jersey NELAP

New MexicoNew York NELAP

North CarolinaNorth Carolina SDWA

OklahomaPennsylvania NELAPPlant Material Permit

South Carolina ChemistrySouth Carolina GVL

South Carolina RadiochemiTennessee

Texas NELAPUtah NELAP

VermontVirginia NELAP

Washington

UST−11088−0651

42D09040462940 Interim

SC00012PH−0169

SC000122013−102567.01E87156

P330−12−00283, P330−12−00284SC00012

967SC000122013−10

SC00012SC00012200029

C−SC−01E−10332

9012990129

03046 (AI33904)LA150001

270M−SC012

9976SC000122013−10NE−OS−26−13SC000122014−1

2054SC002

SC0001211501233

457099904

68−00485PDEP−12−00260

101200012361100110120002TN 02934

T104704235−15−10SC000122014−16

VT87156460202

C780−12

List of current GEL Certifications as of 05 March 2015

Page 7 of 153

Radiological Analysis

Page 8 of 153

Radiochemistry Technical Case Narrative

EMAX Laboratories, LLC - Boeing SSFL (EMAX) SDG #: 367333

Method/Analysis Information

Product: Alphaspec U, Liquid - dissolved

Analytical Method: DOE EML HASL-300, U-02-RC Modified

Analytical Batch Number: 1459242

Sample ID Client ID367333001 WS-08_021615_031203268722 MB for batch 14592421203268724 Laboratory Control Sample (LCS)1203268723 367333001(WS-08_021615_03) Sample Duplicate (DUP)

The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC asStandard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance withGL-RAD-A-011 REV# 25.

Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and usedbefore the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 367333001 (WS-08_021615_03). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and theduplicate, 1203268723 (WS-08_021615_03DUP) and 367333001 (WS-08_021615_03), did not meet the U-238

Page 9 of 153

relative percent difference requirement; however, they do meet the relative error ratio requirement with a valueof 1.33.

Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts None of the samples in this sample set were recounted.

Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. A data exception report (DER) was not generated for this SDG. Manual Integration Manual integration of alpha spectroscopy spectra 1203268722 (MB) was performed to fully separate counts inRegions of Interest which would have been biased. Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC. Additional Comments Additional comments were not required for this sample set.

Qualifier Information Manual qualifiers were not required. Method/Analysis Information

Product: Alphaspec U, Filter

Analytical Method: DOE EML HASL-300, U-02-RC Modified

Prep Method: Filter Prep


Prep Batch Number: 1459429

Sample ID Client ID367333002 WS-08_021615_031203269519 MB for batch 14595241203269521 Laboratory Control Sample (LCS)

Page 10 of 153

1203269520 367333002(WS-08_021615_03) Sample Duplicate (DUP)



Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 367333002 (WS-08_021615_03). QC Information All of the QC samples met the required acceptance limits.

Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts None of the samples in this sample set were recounted.

Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. A data exception report (DER) was not generated for this SDG. Manual Integration No manual integrations were performed on data in this batch. Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Page 11 of 153

Additional Comments Additional comments were not required for this sample set.


Product: GFPC, Gross A/B, liquid - dissolved

Analytical Method: EPA 900.0/SW846 9310


Sample ID Client ID367333001 WS-08_021615_031203269828 MB for batch 14596561203269832 Laboratory Control Sample (LCS)1203269829 367333001(WS-08_021615_03) Sample Duplicate (DUP)1203269830 367333001(WS-08_021615_03) Matrix Spike (MS)1203269831 367333001(WS-08_021615_03) Matrix Spike Duplicate (MSD)



Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 367333001 (WS-08_021615_03).

Page 12 of 153

QC Information All of the QC samples met the required acceptance limits.

Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moistureabsorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flameuntil a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that properalpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium,polonium and cesium may be lost during sample heating. Recounts None of the samples in this sample set were recounted.

Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC. Additional Comments The matrix spike and matrix spike duplicate, 1203269830 (WS-08_021615_03MS) and 1203269831(WS-08_021615_03MSD), aliquots were reduced to conserve sample volume.


Product: GFPC, Gross A/B, filter

Analytical Method: EPA 900.0/SW846 9310/SM 7110B Modified

Prep Method: Filter Prep


Page 13 of 153

Prep Batch Number: 1459429

Sample ID Client ID367333002 WS-08_021615_031203269854 MB for batch 14596641203269858 Laboratory Control Sample (LCS)1203269855 367333002(WS-08_021615_03) Sample Duplicate (DUP)1203269856 367333002(WS-08_021615_03) Matrix Spike (MS)1203269857 367333002(WS-08_021615_03) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC asStandard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance withGL-RAD-A-001B REV# 17.

Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. The discrimination settings are calibrated inbeta discriminating mode to reduce beta to alpha crosstalk. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and usedbefore the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 367333002 (WS-08_021615_03). QC Information All of the QC samples met the required acceptance limits.

Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Page 14 of 153

Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moistureabsorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flameuntil a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that properalpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium,polonium and cesium may be lost during sample heating. Recounts Samples were recounted due to high MDCs. The recounts are reported.

Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC. Additional Comments The matrix spike and matrix spike duplicate, 1203269856 (WS-08_021615_03MS) and 1203269857(WS-08_021615_03MSD), aliquots were reduced to conserve sample volume.

Qualifier Information Manual qualifiers were not required. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of therequirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Page 15 of 153

GEL LABORATORIES LLC2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com

EMAX011 EMAX Laboratories, LLC - Boeing SSFL

Client SDG: 367333 GEL Work Order: 367333

GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverablesreceive a third level review of the fractional data package.

The following data validator verified the information presented in this data report:

The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a Tracer compoundU Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

forQualifier Definition Report

Signature: Name:

Date: Title:05 MAR 2015

Heather McCarty

Analyst II

Review/Validation

Page 16 of 153

Sample Data Summary

Page 17 of 153

Certificate of Analysis


Rad Alpha Spec Analysis

Rad Gas Flow Proportional Counting

Solid Preparation

Parameter Result UnitsQualifier Analyst Date Time

Alphaspec U, Liquid - dissolved "As Received"

GFPC, Gross A/B, liquid - dissolved "As Received"

Laboratory Filtration for dissolved "As Received"

1459242

1459656

1119

1226

pCi/LpCi/LpCi/L

pCi/LpCi/L

Uranium-233/234Uranium-235Uranium-238

AlphaBeta

02/24/15

02/28/15

MXS2

AXJ1

U0.7750.5060.209

2.902.73

RL

2.002.002.00

3.004.00

DF

Mr. Ye MyintContact:

EMAX LaboratoriesCompany :1835 W. 205th Street

Torrance, California 90501 March 5, 2015Report Date:

Address :

Boeing SSFL - 2015Q1Project:

367333001Water16-FEB-1517-FEB-15

WS-08_021615_03 EMAXSSFLGWProject:EMAX011Client ID:

Client

1.250.129

1.12

3.774.33

+/-0.688+/-0.317+/-0.568

+/-2.11+/-1.78

Sample ID:

Receive Date:

Client Sample ID:

Matrix:Collect Date:

Collector:Batch Mtd.

The following Analytical Methods were performed Method Description

+/-0.708+/-0.317+/-0.588

+/-2.20+/-1.91

1

2

3

DOE EML HASL-300, U-02-RC Modified

EPA 900.0/SW846 9310

GL-RAD-A-026

1

2

Notes:

Uranium-232 Tracer Alphaspec U, Liquid - dissolved "As Received" 79.2 (15%-125%)1459242

Acceptable LimitsTest Recovery%Batch IDSurrogate/Tracer Recovery

MDC TPUUncertainty

TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).

Page 18 of 153

Certificate of Analysis


Rad Alpha Spec Analysis

Rad Gas Flow Proportional Counting

Parameter Result UnitsQualifier Analyst Date Time

Alphaspec U, Filter "As Received"

GFPC, Gross A/B, filter "As Received"

1459524

1459664

0951

1248

pCi/LpCi/LpCi/L

pCi/LpCi/L

Uranium-233/234Uranium-235Uranium-238

AlphaBeta

03/03/15

03/04/15

MXS2

AXJ1UU

0.06520.03040.0652

2.493.03

RL

2.002.002.00

3.004.00

DF


EMAX LaboratoriesCompany :1835 W. 205th Street

Torrance, California 90501 March 5, 2015Report Date:

Address :

Boeing SSFL - 2015Q1Project:

367333002Filter16-FEB-1517-FEB-15

WS-08_021615_03 EMAXSSFLGWProject:EMAX011Client ID:

Client

0.08580.0304

0.119

0.3131.31

+/-0.0601+/-0.0409+/-0.0681

+/-1.24+/-1.78

Sample ID:

Receive Date:

Client Sample ID:

Matrix:Collect Date:

Collector:Batch

The following Prep Methods were performed

Filter Prep Filter Prep 02/23/15 14594290908CXC1

Method Description Analyst Date Time Prep Batch

Mtd.

The following Analytical Methods were performed Method Description

+/-0.0613+/-0.0411+/-0.0701

+/-1.24+/-1.78

1

2

DOE EML HASL-300, U-02-RC Modified

EPA 900.0/SW846 9310/SM 7110B Modified

1

2

Notes:

Uranium-232 Tracer Alphaspec U, Filter "As Received" 86.8 (15%-125%)1459524

Acceptable LimitsTest Recovery%Batch IDSurrogate/Tracer Recovery

MDC TPUUncertainty


Page 19 of 153

Quality Control Data

Page 20 of 153

QC Summary


Rad Alpha Spec1459242

1459524

Batch

Batch

Uranium-233/234

Uranium-235

Uranium-238

Uranium-233/234

Uranium-235

Uranium-238

Uranium-233/234

Uranium-235

Uranium-238

Uranium-233/234

Uranium-235

Uranium-238

Parmname


EMAX LaboratoriesClient :1835 W. 205th Street

Torrance, California

March 5, 2015Report Date:

Units

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

Anlst Date Time

MXS2

MXS2

MXS2

MXS2

02/24/15

02/24/15

02/24/15

03/03/15

11:19

11:19

11:19

09:51

QC

1.69

0.114

0.616

54.9

2.66

58.1

-0.312

-0.0349

-0.0582

0.0959

0.0731

0.133

NOM Sample

1.25

0.129

1.12

0.0858

0.0304

0.119

Range

(0% - 100%)

N/A

(0%-20%)

(70%-130%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

Qual

U

U

U

U

QC1203268723 367333001

QC1203268724

QC1203268722

QC1203269520 367333002

QC1203269521

REC%

10754.3

DUP

LCS

MB

DUP

LCS

367333Workorder:

*

U

+/-0.688

+/-0.317

+/-0.568

+/-0.0601

+/-0.0409

+/-0.0681

+/-0.689

+/-0.280

+/-0.432

+/-3.72

+/-0.923

+/-3.82

+/-0.259

+/-0.167

+/-0.275

+/-0.0653

+/-0.0588

+/-0.0661

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

+/-0.708

+/-0.317

+/-0.588

+/-0.0613

+/-0.0411

+/-0.0701

+/-0.725

+/-0.280

+/-0.440

+/-8.28

+/-0.990

+/-8.71

+/-0.259

+/-0.167

+/-0.275

+/-0.0667

+/-0.0597

+/-0.0686

30

0

57.7

11

82.6

11.5

RPD%

Page 1 of 4

Page 21 of 153

QC Summary


Rad Alpha Spec

Rad Gas Flow

1459524

1459656

Batch

Batch

Uranium-233/234

Uranium-235

Uranium-238

Uranium-233/234

Uranium-235

Uranium-238

Alpha

Beta

Alpha

Beta

Alpha

Beta

Alpha

Parmname Units

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

Anlst Date Time

MXS2

MXS2

AXJ1

AXJ1

AXJ1

AXJ1

03/03/15

03/03/15

02/28/15

02/28/15

02/28/15

02/28/15

09:51

09:51

12:26

12:26

12:26

12:26

QC

5.06

0.224

5.56

0.0468

0.0104

0.00845

3.25

3.63

94.6

361

0.304

-1.19

282

NOM Sample

3.77

4.33

3.77

Range

(70%-130%)

(0% - 100%)

(0% - 100%)

(70%-130%)

(70%-130%)

(50%-150%)

Qual

U

U

U

U

U

QC1203269519

QC1203269829 367333001

QC1203269832

QC1203269828

QC1203269830 367333001

REC%

102

117

114

115

5.43

81.1

316

243

MB

DUP

LCS

MB

MS

367333Workorder:

+/-2.11

+/-1.78

+/-2.11

+/-0.376

+/-0.090

+/-0.394

+/-0.0502

+/-0.0401

+/-0.0324

+/-1.96

+/-1.54

+/-8.91

+/-12.4

+/-0.666

+/-1.11

+/-29.9

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

+/-2.20

+/-1.91

+/-2.20

+/-0.797

+/-0.0952

+/-0.866

+/-0.0507

+/-0.0401

+/-0.0325

+/-2.04

+/-1.65

+/-17.8

+/-61.5

+/-0.668

+/-1.11

+/-55.7

14.8

17.6

RPD%

Page 2 of 4

Page 22 of 153

QC Summary


Rad Gas Flow1459656

1459664

Batch

Batch

Beta

Alpha

Beta

Alpha

Beta

Alpha

Beta

Alpha

Beta

Alpha

Beta

Alpha

Beta

Parmname Units

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

pCi/L

Anlst Date Time

AXJ1

AXJ1

AXJ1

AXJ1

AXJ1

AXJ1

02/28/15

03/04/15

03/04/15

03/04/15

03/05/15

03/04/15

12:26

12:48

16:06

12:48

06:22

12:48

QC

1120

291

1150

-0.29

1.28

98.1

386

0.698

0.852

282

1150

267

1070

NOM Sample

4.33

3.77

4.33

0.313

1.31

0.313

1.31

0.313

1.31

Range

(50%-150%)

(0%-20%)

(0%-20%)

N/A

N/A

(70%-130%)

(70%-130%)

(50%-150%)

(50%-150%)

(0%-20%)

(0%-20%)

Qual

U

U

U

U

QC1203269831 367333001

QC1203269855 367333002

QC1203269858

QC1203269854

QC1203269856 367333002

QC1203269857 367333002

REC%

118

118

121

121

122

116

122

110

113

948

243

948

81.1

316

243

948

243

948

MSD

DUP

LCS

MB

MS

MSD

367333Workorder:

U

U

U

U

U

U

+/-1.78

+/-2.11

+/-1.78

+/-1.24

+/-1.78

+/-1.24

+/-1.78

+/-1.24

+/-1.78

+/-39.0

+/-30.0

+/-39.3

+/-1.05

+/-2.14

+/-9.20

+/-13.2

+/-1.35

+/-2.14

+/-26.0

+/-38.5

+/-26.3

+/-38.1

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

Uncert:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

TPU:

+/-1.91

+/-2.20

+/-1.91

+/-1.24

+/-1.78

+/-1.24

+/-1.78

+/-1.24

+/-1.78

+/-191

+/-57.3

+/-194

+/-1.05

+/-2.14

+/-9.30

+/-14.4

+/-1.35

+/-2.14

+/-26.2

+/-42.1

+/-26.6

+/-41.4

3.17

2.44

0

0

5.44

6.97

RPD%

Page 3 of 4

Page 23 of 153

QC Summary


Parmname

Page 4 of 4

Units Anlst Date TimeQCNOM Sample RangeQual

The Qualifiers in this report are defined as follows:

REC%

367333Workorder:

**

<

>

BD

FA

H

J

K

L

M

M

N/A

N1

ND

NJ

Q

R

U

UI

UJ

UL

X

Y

^

h

Analyte is a Tracer compound

Result is less than value reported

Result is greater than value reported

Results are either below the MDC or tracer recovery is low

Failed analysis.

Analytical holding time was exceeded

Value is estimated

Analyte present. Reported value may be biased high. Actual value is expected to be lower.

Analyte present. Reported value may be biased low. Actual value is expected to be higher.

M if above MDC and less than LLD

REMP Result > MDC/CL and < RDL

RPD or %Recovery limits do not apply.

See case narrative

Analyte concentration is not detected above the detection limit

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

One or more quality control criteria have not been met. Refer to the applicable narrative or DER.

Sample results are rejected

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Gamma Spectroscopy--Uncertain identification

Gamma Spectroscopy--Uncertain identification

Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

Other specific qualifiers were required to properly define the results. Consult case narrative.

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

Preparation or preservation holding time was exceeded

N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.** Indicates analyte is a surrogate/tracer compound.^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater thanfive times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- theRL is used to evaluate the DUP result.For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELACstandard unless qualified on the QC Summary.

RPD%


Notes:

Page 24 of 153

Alpha SpectroscopyRaw Data

Page 25 of 153

of 153

Jessica

Jessica Davis

Jessica

Typewritten Text

03/05/15

of 153

Alpha Spectroscopy Software Version 3.5.1 effective date: 18-Feb-2015

GEL Laboratories LLCALPHA SPECTROSCOPY REPORT

Instrument SOP: GL-RAD-I-009 Analytical SOP: GL-RAD-A-011

BATCH NUMBER : 1459242SAMPLE ID : S0367333001_UU

SAMPLE QTY : 0.050 LSAMPLE DATE : 16-Feb-2015 00:00:00

ANALYST : MXS2% YIELD : 79.2 +/-6.664 %

+/-0.500 %

CHAMBER : 015DETECTOR S/N : 80055

AVERAGE %EFFICIENCY : 32.2878AVERAGE %EFF ERROR : 0.6217

COUNT DATE : 24-Feb-2015 11:19:49ELAPSED LIVE TIME(SEC) : 30300.00

LIB FILE : UUBKG FILE : B015.CNF;1663

BKG DATE : 20-Feb-2015BKG LIVE TIME(SEC) : 60000.00

EFF FILE : W015.CNF;487CAL DATE : 03-Feb-2015

TRACERID : 1564-G

NUCLIDE : U-232NOMINAL : 4.7269E+00 dpmRESULTS : 3.7448E+00 dpm

NUCLIDE ACTIVITY SUMMARY1.96-sigma 1.96-sigma

NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Lc cnt UncENERGY ENERGY FWHM AREA AREA AREA StDev pCi/L pCi/L pCi/L pCi/L pCi/L

U-232 5302.10 5324.62 37.526 615.000 610.455 4.545 2.1319 100.000 4.26E+01 6.73E+00 8.10E-01 3.00E-01 3.40E+00U-3/4 4763.02 4779.44 28.553 22.000 17.960 4.040 2.0100 100.000 1.25E+00 7.08E-01 7.75E-01 2.83E-01 6.88E-01U-235 4391.00 4423.42 39.158 2.000 1.495 0.505 0.7106 80.900 1.29E-01 3.17E-01 5.06E-01 1.24E-01 3.17E-01U-238 4184.73 4198.41 6.118 16.000 16.000 0.000 0.0000 100.000 1.12E+00 5.88E-01 2.09E-01 0.00E+00 5.68E-01

2382 2776 3175 3579 3987 4400 4818 5240 5668 6100 6537 6978 7425

Energy (keV)

1

7

13

19

25

31

37

43

49

55

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

5000

keV

5397

keV

U-2

32

U-232: 5000-5397 keV

Page 29 of 153

Alpha Spectroscopy Software Version 3.5.3 effective date: 02-Mar-2015






+/-0.500 %







TRACERID : 1564-G




U-232 5302.10 5340.86 48.987 769.000 760.415 8.585 2.9300 100.000 4.26E+01 6.38E+00 8.30E-01 3.31E-01 3.05E+00U-3/4 4763.02 4654.51 4.872 1.000 -5.565 6.565 2.5622 100.000 -3.12E-01 2.59E-01 7.47E-01 2.90E-01 2.59E-01U-235 4391.00 4397.17 0.000 0.000 -0.505 0.505 0.7106 80.900 -3.49E-02 1.67E-01 4.06E-01 9.93E-02 1.67E-01U-238 4184.73 4148.19 160.763 3.000 -1.040 4.040 2.0100 100.000 -5.82E-02 2.75E-01 6.22E-01 2.27E-01 2.75E-01

2393 2785 3182 3583 3989 4400 4816 5237 5662 6091 6526 6965 7409

Energy (keV)

1

7

13

19

25

31

37

43

49

55

61

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

4999

keV

5422

keV

U-2

32

U-232: 4999-5422 keV

NOTES: * Regions have been manually adjusted

Page 30 of 153







+/-0.500 %







TRACERID : 1564-G




U-232 5302.10 5313.64 35.495 694.000 690.465 3.535 1.8802 100.000 4.26E+01 6.52E+00 6.53E-01 2.34E-01 3.19E+00U-3/4 4763.02 4767.37 34.320 30.000 27.475 2.525 1.5890 100.000 1.69E+00 7.25E-01 5.80E-01 1.98E-01 6.89E-01U-235 4391.00 4469.61 0.000 2.000 1.495 0.505 0.7106 80.900 1.14E-01 2.80E-01 4.47E-01 1.09E-01 2.80E-01U-238 4184.73 4181.36 9.806 11.000 9.990 1.010 1.0050 100.000 6.16E-01 4.40E-01 4.35E-01 1.25E-01 4.32E-01

2370 2764 3163 3567 3974 4387 4803 5224 5650 6080 6514 6953 7396

Energy (keV)

1

8

15

22

29

36

43

50

57

64

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

5000

keV

5397

keV

U-2

32

U-232: 5000-5397 keV

Page 31 of 153







+/-0.500 %







TRACERID : 1564-G


LCS ID

NUCLIDENOMINAL (pCi/L)

% RECOVERY

1600-DU-238

5.4346E+01



U-232 5302.10 5316.67 68.350 660.000 653.940 6.060 2.4617 100.000 4.26E+01 6.62E+00 8.42E-01 3.23E-01 3.29E+00U-3/4 4763.02 4769.77 36.336 846.000 843.475 2.525 1.5890 100.000 5.49E+01 8.28E+00 6.13E-01 2.09E-01 3.72E+00U-235 4391.00 4415.93 31.801 33.000 33.000 0.000 0.0000 80.900 2.66E+00 9.90E-01 2.41E-01 0.00E+00 9.23E-01U-238 4184.73 4196.70 43.157 894.000 891.980 2.020 1.4213 100.000 5.81E+01 8.71E+00 5.69E-01 1.87E-01 3.82E+00

106.857

2378 2772 3170 3574 3983 4396 4814 5238 5666 6099 6537 6979 7427

Energy (keV)

1

9

17

25

33

41

49

57

65

73

81

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

5000

keV

5397

keV

U-2

32

U-232: 5000-5397 keV

Page 32 of 153

of 153

Jessica

Jessica Davis

Jessica

Typewritten Text

03/05/15

of 153







+/-1.118 %



COUNT DATE : 03-Mar-2015 09:51:23ELAPSED LIVE TIME(SEC) : 30300.00




TRACERID : 1564-G




U-232 5302.10 5307.59 39.466 521.000 519.990 1.010 1.0050 100.000 4.26E+00 7.06E-01 5.78E-02 1.66E-02 3.67E-01U-3/4 4763.02 4763.12 7.443 12.000 10.485 1.515 1.2309 100.000 8.58E-02 6.13E-02 6.52E-02 2.03E-02 6.01E-02U-235 4391.00 4396.76 138.940 3.000 3.000 0.000 0.0000 80.900 3.04E-02 4.11E-02 3.04E-02 0.00E+00 4.09E-02U-238 4184.73 4157.81 9.924 16.000 14.485 1.515 1.2309 100.000 1.19E-01 7.01E-02 6.52E-02 2.03E-02 6.81E-02

2368 2767 3169 3575 3985 4398 4815 5236 5660 6088 6519 6955 7393

Energy (keV)

1

6

11

16

21

26

31

36

41

46

51

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

5000

keV

5397

keV

U-2

32

U-232: 5000-5397 keV

Page 35 of 153





SAMPLE QTY : 0.500 LSAMPLE DATE : 02-Mar-2015 00:00:00


+/-1.118 %







TRACERID : 1564-G




U-232 5302.10 5271.36 70.929 503.000 498.960 4.040 2.0100 100.000 4.26E+00 7.16E-01 9.48E-02 3.46E-02 3.76E-01U-3/4 4763.02 4715.00 232.299 7.000 5.485 1.515 1.2309 100.000 4.68E-02 5.07E-02 6.80E-02 2.12E-02 5.02E-02U-235 4391.00 4482.75 0.000 2.000 0.990 1.010 1.0050 80.900 1.04E-02 4.01E-02 7.44E-02 2.14E-02 4.01E-02U-238 4184.73 4163.39 177.931 2.000 0.990 1.010 1.0050 100.000 8.45E-03 3.25E-02 6.02E-02 1.73E-02 3.24E-02

2406 2803 3205 3611 4021 4436 4855 5277 5705 6136 6571 7011 7455

Energy (keV)

1

5

9

13

17

21

25

29

33

37

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

5000

keV

5397

keV

U-2

32

U-232: 5000-5397 keV

Page 36 of 153






ANALYST : MXS2% YIELD : 104 +/-6.734 %

+/-1.118 %







TRACERID : 1564-G




U-232 5302.10 5310.59 32.443 577.000 575.485 1.515 1.2309 100.000 4.26E+00 6.87E-01 5.90E-02 1.84E-02 3.49E-01U-3/4 4763.02 4759.80 53.342 17.000 12.960 4.040 2.0100 100.000 9.59E-02 6.67E-02 8.22E-02 3.00E-02 6.53E-02U-235 4391.00 4414.70 133.976 9.000 7.990 1.010 1.0050 80.900 7.31E-02 5.97E-02 6.45E-02 1.85E-02 5.88E-02U-238 4184.73 4174.31 58.304 19.000 17.990 1.010 1.0050 100.000 1.33E-01 6.86E-02 5.22E-02 1.50E-02 6.61E-02

2388 2786 3189 3595 4005 4418 4835 5256 5680 6108 6540 6975 7414

Energy (keV)

1

7

13

19

25

31

37

43

49

55

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

5000

keV

5397

keV

U-2

32

U-232: 5000-5397 keV

Page 37 of 153





SAMPLE QTY : 0.500 LSAMPLE DATE : 02-Mar-2015 00:00:00


+/-1.118 %







TRACERID : 1564-G


LCS ID

NUCLIDENOMINAL (pCi/L)

% RECOVERY

1600-DU-238

5.4346E+00



U-232 5302.10 5300.30 61.589 592.000 587.455 4.545 2.1319 100.000 4.26E+00 6.85E-01 8.41E-02 3.12E-02 3.47E-01U-3/4 4763.02 4754.22 42.886 699.000 699.000 0.000 0.0000 100.000 5.06E+00 7.97E-01 2.17E-02 0.00E+00 3.76E-01U-235 4391.00 4396.52 48.986 25.000 25.000 0.000 0.0000 80.900 2.24E-01 9.52E-02 2.69E-02 0.00E+00 9.00E-02U-238 4184.73 4186.41 42.880 769.000 767.485 1.515 1.2309 100.000 5.56E+00 8.66E-01 5.77E-02 1.80E-02 3.94E-01

102.328

2377 2771 3170 3573 3980 4392 4808 5229 5654 6083 6517 6956 7398

Energy (keV)

1

7

13

19

25

31

37

43

49

55

61

Act

ivity

(C

OU

NT

S)

3976

keV

4286

keV

U-2

38

U-238: 3976-4286 keV

4312

keV

4483

keV

U-2

35

U-235: 4312-4483 keV

4592

keV

4865

keV

U-3

/4

U-3/4: 4592-4865 keV

5000

keV

5397

keV

U-2

32

U-232: 5000-5397 keV

Page 38 of 153

Continuing CalibrationData

Page 39 of 153

of 153

Background andEfficiency Data

Page 43 of 153

of 153

RAD StandardsTraceability

Page 84 of 153

of 153

Standard Traceability Log Rad

Source Material Info

Parent Code: 1564

Prepared By: Ashley Drochter

Carrier Conc: 2M HNO3

Reference Date: 09/12/2011

Ampoule Mass (g): 5.06048 g

Uncertainty: +/- 4.9 %

LogBook No: RC-S-060-109

A Solution Material Info

Isotope: Uranium-232


Prep Date: 11/15/2012

Verification Date: 12/10/2014

Expiration Date: 12/10/2015

Primary Code: 1564-A

Dilution(mL): 100 mL

Mass of Parent(g): 4.9067 g

Density(g/mL): 1.0615 Balance ID: 38080204

Calculations Converting parent activity to dpm/mL|dpm/g

(Mass of parent(g)) * (Parm Activity (Bq)) * (conversion dpm to Bq) / (Ampoule Mass(g) *(Dilution Vol)) = Parent Activity (dpm/mL)

(Mass of parent(g)) * (Parm Activity (Bq)) * (conversion dpm to Bq) / Density / (Ampoule Mass (g) * (Dilution Vol)) = ParentActivity (dpm/g)

(4.9067 g) * (33930 Bq) * (60 dpm/Bq) / (5.06048 g * 100 mL ) = 19739.3525 dpm/mL

(4.9067 g) * (33930 Bq) * (60 dpm/Bq) / ( 1.0615 g/mL)/ (5.06048 g * 100 mL) = 18595.7160 dpm/g

Secondary Standards

Prep Date PreparerMass

PrimaryDilution

(mL)Code

Conc dpm/mL

Verification Date

Expiration Date

11/16/2012Ashley

Drochter2.6179 1000 1564-B

48.6817 dpm/mL

11/13/2013 11/13/2014

01/15/2013Christina Kimball

.265 250 1564-C19.7115 dpm/mL

01/13/2014 01/13/2015


.116 500 1564-D4.31421 dpm/mL

02/16/2015 02/13/2016

01/02/2014Gregory Ramsay

2.6936 1000 1564-E50.08942 dpm/mL

12/10/2014 12/10/2015


.266 250 1564-F19.78584 dpm/mL

03/20/2014 03/20/2015

12/10/2014 Tim Chandler 2.6312 1000 1564-G48.929

dpm/mL12/10/2014 12/10/2015

GEL Laboratories LLC Version 1.0 9/18/2000

Page 86 of 153

of 153

of 1

53



Parent Code: 1600


Carrier Conc:UO2(NO3)2 in dilute

HNO3


Ampoule Mass (g):

7.0521 g

Uncertainty: +/- 1.18 %



Isotope: Uranium-238

Prepared By:Ashley

Drochter

Prep Date: 09/04/2012

Verification Date:

03/31/2014




Mass of Parent(g):

6.8204 g

Density(g/mL): 1.0789Balance

ID:38080204


(Mass of parent(g)) * (Parm Activity (kbq)) * (conversion dpm to kbq) / (Ampoule Mass(g) *(Dilution Vol)) = Parent Activity (dpm/mL)

(Mass of parent(g)) * (Parm Activity (kbq)) * (conversion dpm to kbq) / Density / (Ampoule Mass (g) * (Dilution Vol)) =Parent Activity (dpm/g)

(6.8204 g) * (18.42 kbq) * (60000 dpm/kbq) / (7.0521 g * 100 mL ) = 10688.8814 dpm/mL

(6.8204 g) * (18.42 kbq) * (60000 dpm/kbq) / ( 1.0789 g/mL)/ (7.0521 g * 100 mL) = 9907.0626 dpm/g

Secondary Standards


PrimaryDilution

(mL)Code

Conc dpm/mL

Verification Date

Expiration Date

09/04/2012Ashley

Drochter1.4579 500 1600-B

28.8913 dpm/mL

09/04/2012 09/04/2013

09/11/2012Ashley

Drochter3.0288 500 1600-C

60.0219 dpm/mL

09/04/2013 09/04/2014

03/27/2014Tim

Chandler3.0445 500 1600-D

60.3241 dpm/mL

03/31/2014 03/31/2015


Page 90 of 153

of 1

53

Runlogs

Page 92 of 153

Instrument Run Log

ALPHA SPECTROMETERInstrument Type:

367333001120326872212032687231203268724

SampleID

SampleType

MXS2MXS2MXS2MXS2

Analyst

1015101610171018

Instrument

FEB-24-15 11:19:49FEB-24-15 11:19:49FEB-24-15 11:19:49FEB-24-15 11:19:49

Run Date

DONEDONEDONEDONE

Status Geometry

03-FEB-15 12:0703-FEB-15 12:0903-FEB-15 12:0903-FEB-15 12:09

Calibration Date

Batch ID:1459242

SAMPLEMBDUPLCS

Page 93 of 153

Instrument Run Log

ALPHA SPECTROMETERInstrument Type:

367333002120326951912032695201203269521

SampleID

SampleType

MXS2MXS2MXS2MXS2

Analyst

1141114211431144

Instrument

MAR-03-15 09:51:23MAR-03-15 09:51:24MAR-03-15 09:51:27MAR-03-15 09:51:29

Run Date

DONEDONEDONEDONE

Status Geometry

16-JAN-15 13:5216-JAN-15 13:5316-JAN-15 13:5317-FEB-15 12:53

Calibration Date

Batch ID:1459524

SAMPLEMBDUPLCS

Page 94 of 153

Gas Flow Raw Data

Page 95 of 153

of 153

Continuing CalibrationData

Page 111 of 153

of 153

Background andEfficiency Data

Page 119 of 153

Denotes Outlier

+3 Sigma 0.33

-3 Sigma -0.089

+2 Sigma 0.26

-2 Sigma -0.019

Mean 0.12

-0.0468

-0.00477

0.0373

0.0793

0.12

0.16

0.21

0.25

0.29

0.33

07/0

107

/06

07/1

207

/17

07/2

407

/31

08/0

708

/14

08/2

108

/27

08/3

109

/07

09/1

409

/19

09/2

409

/30

10/0

510

/10

10/1

510

/21

10/2

810

/31

11/0

511

/10

11/1

711

/22

11/2

912

/08

12/1

512

/22

12/2

801

/04

01/1

101

/18

01/2

501

/29

02/0

402

/11

02/1

802

/23

02/2

6

DATE

LB4100E1 ALPHA BKG Generated 02/28/2015

CP

M

+3 Sigma 11610

-3 Sigma 10500

+2 Sigma 11400

-2 Sigma 10700

Mean 11060

10611

10722

10833

10944

11055

11166

11277

11388

11499

11610

07/0

107

/07

07/1

207

/17

07/2

307

/29

08/0

408

/09

08/1

508

/21

08/2

709

/02

09/0

709

/12

09/1

709

/22

09/2

710

/02

10/0

710

/12

10/1

710

/23

10/2

911

/04

11/0

711

/13

11/1

811

/20

11/2

512

/01

12/0

812

/13

12/1

812

/23

12/2

901

/04

01/0

901

/14

01/1

901

/25

01/2

902

/04

02/0

902

/14

02/1

802

/22

02/2

7

DATE

LB4100E1 ALPHA EFF

CP

M

+3 Sigma 0.22

-3 Sigma 0.17

+2 Sigma 0.21

-2 Sigma 0.18

Mean 0.2

0.18

0.18

0.19

0.19

0.2

0.2

0.21

0.21

0.22

0.22

07/0

107

/07

07/1

207

/17

07/2

307

/29

08/0

408

/09

08/1

508

/21

08/2

709

/02

09/0

709

/12

09/1

709

/22

09/2

710

/02

10/0

710

/12

10/1

710

/23

10/2

911

/04

11/0

711

/13

11/1

811

/20

11/2

512

/01

12/0

812

/13

12/1

812

/23

12/2

901

/04

01/0

901

/14

01/1

901

/25

01/2

902

/04

02/0

902

/14

02/1

802

/22

02/2

7

DATE

LB4100E1 ALPHA EFF Cross Talk

+3 Sigma 2.15

-3 Sigma 0.6

+2 Sigma 1.89

-2 Sigma 0.86

Mean 1.38

0.76

0.91

1.07

1.22

1.38

1.53

1.69

1.84

2

2.15

07/0

107

/06

07/1

207

/17

07/2

407

/31

08/0

708

/14

08/2

108

/27

08/3

109

/07

09/1

409

/19

09/2

409

/30

10/0

510

/10

10/1

510

/21

10/2

810

/31

11/0

511

/10

11/1

711

/22

11/2

912

/08

12/1

512

/22

12/2

801

/04

01/1

101

/18

01/2

501

/29

02/0

402

/11

02/1

802

/23

02/2

6

DATE

LB4100E1 BETA BKG

CP

M

Page 120 of 153

Denotes Outlier

+3 Sigma 18580

-3 Sigma 16850

+2 Sigma 18290

-2 Sigma 17130

Mean 17710

17023

17196

17369

17542

17715

17888

18061

18234

18407

18580

07/0

107

/08

07/1

207

/16

07/2

107

/28

08/0

408

/11

08/1

808

/25

08/3

109

/07

09/1

309

/18

09/2

510

/01

10/0

710

/13

10/2

010

/24

10/3

111

/07

11/1

411

/20

11/2

512

/02

12/1

012

/16

12/2

212

/29

01/0

601

/12

01/1

801

/25

02/0

102

/06

02/1

002

/15

02/1

902

/24

DATE

LB4100E1 BETA EFF Generated 02/28/2015

CP

M

+3 Sigma 00

-3 Sigma -0

+2 Sigma 00

-2 Sigma 00

Mean 00

0.0000157

0.0000765

0.000137

0.0001981

0.000259

0.00032

0.0003804

0.000441

0.00050202

0.000563

07/0

107

/08

07/1

207

/16

07/2

107

/28

08/0

408

/11

08/1

808

/25

08/3

109

/07

09/1

309

/18

09/2

510

/01

10/0

710

/13

10/2

010

/24

10/3

111

/07

11/1

411

/20

11/2

512

/02

12/1

012

/16

12/2

212

/29

01/0

601

/12

01/1

801

/25

02/0

102

/06

02/1

002

/15

02/1

902

/24

DATE

LB4100E1 BETA EFF Cross Talk

Page 121 of 153

Denotes Outlier

+3 Sigma 0.36

-3 Sigma -0.112

+2 Sigma 0.28

-2 Sigma -0.033

Mean 0.12

-0.0648

-0.0173

0.03009

0.0775

0.12

0.17

0.22

0.27

0.31

0.36

07/0

907

/20

07/2

608

/01

08/0

708

/13

08/1

908

/25

08/3

109

/07

09/1

109

/17

09/2

109

/27

10/0

310

/07

10/1

210

/17

10/2

210

/28

11/0

111

/05

11/1

111

/17

11/2

311

/30

12/0

812

/14

12/2

012

/24

12/3

101

/07

01/1

101

/17

01/2

201

/26

01/3

102

/04

02/1

002

/16

02/2

102

/25

DATE


CP

M

+3 Sigma 11130

-3 Sigma 8926

+2 Sigma 10800

-2 Sigma 9290

Mean 10030

9150

9370

9590

9810

10028

10200

10500

10700

10900

11130

07/1

607

/19

07/2

507

/31

08/0

608

/12

08/1

808

/23

08/2

909

/04

09/0

909

/14

09/1

809

/24

09/2

910

/03

10/0

810

/13

10/1

910

/24

10/3

011

/05

11/1

111

/16

11/2

111

/26

12/0

212

/09

12/1

412

/19

12/2

412

/30

01/0

501

/08

01/1

001

/15

01/2

001

/25

01/3

002

/05

02/1

002

/15

02/1

802

/23

02/2

8

DATE

LB4100E3 ALPHA EFF

CP

M

+3 Sigma 0.68

-3 Sigma -0.172

+2 Sigma 0.54

-2 Sigma -0.03

Mean 0.26

-0.0867

-0.0011

0.0845

0.17

0.26

0.34

0.43

0.51

0.6

0.68

07/0

107

/08

07/1

407

/18

07/2

508

/01

08/0

808

/15

08/2

208

/29

09/0

509

/11

09/1

709

/23

09/2

910

/04

10/1

010

/16

10/2

310

/30

11/0

611

/13

11/1

911

/25

12/0

212

/10

12/1

612

/22

12/2

901

/05

01/0

901

/12

01/1

801

/25

01/3

002

/06

02/1

202

/18

02/2

202

/28

DATE


+3 Sigma 2.06

-3 Sigma 0.51

+2 Sigma 1.8

-2 Sigma 0.77

Mean 1.28

0.66

0.82

0.97

1.13

1.28

1.44

1.59

1.75

1.9

2.06

07/0

107

/07

07/1

207

/17

07/2

307

/29

08/0

408

/10

08/1

608

/22

08/2

809

/04

09/0

909

/14

09/1

909

/24

09/3

010

/06

10/0

910

/15

10/2

110

/25

10/3

011

/04

11/0

811

/14

11/2

011

/26

12/0

312

/11

12/1

712

/23

12/2

801

/04

01/0

901

/14

01/2

001

/25

01/2

802

/02

02/0

702

/13

02/1

802

/23

02/2

7

DATE

LB4100E3 BETA BKG

CP

M

Page 122 of 153

Denotes Outlier

+3 Sigma 19910

-3 Sigma 17560

+2 Sigma 19500

-2 Sigma 18000

Mean 18740

17795

18030

18265

18500

18735

18970

19205

19440

19675

19910

07/0

107

/08

07/1

407

/17

07/2

207

/28

08/0

408

/08

08/1

508

/22

08/2

809

/04

09/1

009

/16

09/2

209

/28

10/0

410

/10

10/1

610

/22

10/2

811

/04

11/0

811

/15

11/2

011

/26

12/0

312

/11

12/1

712

/22

12/2

901

/06

01/1

001

/16

01/2

201

/29

02/0

502

/11

02/1

702

/22

02/2

8

DATE


CP

M

+3 Sigma 00

-3 Sigma -0

+2 Sigma 00

-2 Sigma 00

Mean 00

0.0000195

0.00008084

0.000142

0.0002036

0.000265

0.000326

0.000388

0.000449

0.0005103

0.000572

07/0

107

/08

07/1

407

/17

07/2

207

/28

08/0

408

/08

08/1

508

/22

08/2

809

/04

09/1

009

/16

09/2

209

/28

10/0

410

/10

10/1

610

/22

10/2

811

/04

11/0

811

/15

11/2

011

/26

12/0

312

/11

12/1

712

/22

12/2

901

/06

01/1

001

/16

01/2

201

/29

02/0

502

/11

02/1

702

/22

02/2

8

DATE


Page 123 of 153

Denotes Outlier

+3 Sigma 0.29

-3 Sigma -0.057

+2 Sigma 0.24

-2 Sigma 00

Mean 0.12

-0.022005

0.0131

0.0483

0.0834

0.12

0.15

0.19

0.22

0.26

0.29

07/0

107

/06

07/1

107

/17

07/2

307

/29

08/0

408

/10

08/1

608

/22

08/2

809

/04

09/1

009

/16

09/2

210

/07

10/1

110

/15

10/2

210

/28

11/0

111

/05

11/0

811

/13

11/1

911

/22

11/2

812

/04

12/1

212

/16

12/2

012

/24

12/3

101

/07

01/1

001

/16

01/2

201

/26

01/3

002

/04

02/1

002

/16

02/2

002

/24

02/2

8

DATE


CP

M

+3 Sigma 11380

-3 Sigma 9192

+2 Sigma 11000

-2 Sigma 9550

Mean 10280

9410

9630

9850

10100

10286

10500

10700

10900

11200

11380

07/0

107

/07

07/1

107

/14

07/1

807

/21

07/2

807

/31

08/0

708

/14

08/2

008

/25

08/3

009

/12

09/2

109

/27

10/0

310

/08

10/1

410

/19

10/2

511

/01

11/0

811

/15

11/2

111

/28

12/0

412

/12

12/1

812

/24

12/3

101

/07

01/1

301

/19

01/2

502

/01

02/0

702

/13

02/1

802

/23

DATE

LB4100E4 ALPHA EFF

CP

M

+3 Sigma 0.26

-3 Sigma 0.23

+2 Sigma 0.26

-2 Sigma 0.23

Mean 0.24

0.23

0.23

0.24

0.24

0.24

0.25

0.25

0.26

0.26

0.26

07/0

107

/07

07/1

107

/14

07/1

707

/21

07/2

607

/29

08/0

408

/11

08/1

808

/21

08/2

709

/03

09/0

909

/14

09/1

809

/24

09/3

010

/06

10/1

110

/17

10/2

210

/29

11/0

511

/12

11/1

811

/24

12/0

112

/09

12/1

512

/21

12/2

801

/04

01/1

001

/16

01/2

201

/28

02/0

402

/10

02/1

602

/20

02/2

6

DATE


+3 Sigma 1.79

-3 Sigma 0.78

+2 Sigma 1.62

-2 Sigma 0.95

Mean 1.28

0.88

0.98

1.08

1.18

1.28

1.38

1.48

1.58

1.69

1.79

07/0

107

/06

07/1

107

/17

07/2

307

/29

08/0

408

/10

08/1

608

/22

08/2

809

/04

09/1

009

/16

09/2

210

/07

10/1

110

/15

10/2

210

/28

11/0

111

/05

11/0

811

/13

11/1

911

/22

11/2

812

/04

12/1

212

/16

12/2

012

/24

12/3

101

/07

01/1

001

/16

01/2

201

/26

01/3

002

/04

02/1

002

/16

02/2

002

/24

02/2

8

DATE

LB4100E4 BETA BKG

CP

M

Page 124 of 153

Denotes Outlier

+3 Sigma 22580

-3 Sigma 19020

+2 Sigma 21987

-2 Sigma 19613

Mean 20800

19376

19732

20088

20444

20800

21156

21512

21868

22224

22580

07/0

107

/08

07/1

607

/21

07/2

508

/01

08/0

808

/15

08/2

208

/29

09/0

509

/11

09/1

709

/23

09/2

910

/05

10/1

110

/17

10/2

210

/28

11/0

411

/11

11/1

711

/22

11/2

912

/05

12/1

312

/19

12/2

412

/31

01/0

801

/12

01/1

801

/25

02/0

102

/07

02/1

202

/18

02/2

3

DATE


CP

M

+3 Sigma 00

-3 Sigma 00

+2 Sigma 00

-2 Sigma 00

Mean 00

0.0000453

0.0000673

0.0000893

0.000111

0.000133

0.000155

0.000177

0.000199

0.000221

0.000243

07/0

107

/08

07/1

407

/18

07/2

307

/30

08/0

608

/13

08/2

008

/27

09/0

309

/09

09/1

509

/21

09/2

710

/03

10/0

910

/15

10/2

210

/25

11/0

111

/08

11/1

511

/20

11/2

612

/03

12/1

112

/17

12/2

212

/29

01/0

601

/10

01/1

601

/22

01/2

902

/05

02/1

102

/16

02/2

102

/27

DATE


Page 125 of 153

Denotes Outlier

+3 Sigma 0.34

-3 Sigma -0.032

+2 Sigma 0.27

-2 Sigma 0.03

Mean 0.15

0.00443

0.0412

0.07802

0.11

0.15

0.19

0.23

0.26

0.3

0.34

07/1

407

/19

07/2

307

/27

07/3

108

/03

08/0

708

/13

08/1

908

/26

08/3

009

/04

09/1

009

/16

09/2

209

/27

10/0

310

/09

10/1

510

/21

10/2

711

/02

11/0

811

/12

11/1

811

/24

12/0

112

/09

12/1

512

/21

12/2

801

/04

01/1

101

/17

01/2

301

/29

02/0

402

/10

02/1

502

/20

02/2

6

DATE

LB4100I1 ALPHA BKG Generated 02/28/2015

CP

M

+3 Sigma 11620

-3 Sigma 10300

+2 Sigma 11400

-2 Sigma 10500

Mean 10960

10432

10564

10696

10828

10960

11092

11224

11356

11488

11620

07/1

507

/19

07/2

507

/29

08/0

408

/09

08/1

508

/21

08/2

709

/02

09/0

709

/12

09/1

709

/22

09/2

709

/30

10/0

510

/10

10/1

510

/21

10/2

711

/01

11/0

711

/13

11/1

811

/23

11/2

912

/04

12/1

112

/15

12/1

812

/23

12/2

901

/04

01/0

701

/12

01/1

701

/21

01/2

702

/02

02/0

702

/12

02/1

602

/20

02/2

5

DATE

LB4100I1 ALPHA EFF

CP

M

+3 Sigma 0.2

-3 Sigma 0.15

+2 Sigma 0.19

-2 Sigma 0.15

Mean 0.17

0.15

0.16

0.16

0.17

0.17

0.18

0.18

0.19

0.19

0.2

07/0

107

/08

07/1

507

/22

07/2

608

/02

08/0

908

/16

08/2

308

/30

09/0

609

/12

09/1

809

/24

09/2

910

/04

10/1

010

/16

10/2

310

/30

11/0

611

/13

11/1

911

/25

12/0

212

/10

12/1

512

/19

12/2

701

/02

01/0

701

/12

01/1

801

/23

01/3

002

/06

02/1

202

/17

02/2

202

/28

DATE

LB4100I1 ALPHA EFF Cross Talk

+3 Sigma 1.84

-3 Sigma 0.24

+2 Sigma 1.57

-2 Sigma 0.51

Mean 1.04

0.4

0.56

0.72

0.88

1.04

1.2

1.36

1.52

1.68

1.84

07/0

107

/07

07/1

207

/17

07/2

307

/25

07/3

008

/01

08/0

508

/11

08/1

708

/22

08/2

708

/31

09/0

509

/11

09/1

709

/22

09/2

610

/02

10/0

810

/14

10/2

110

/26

11/0

111

/07

11/1

111

/17

11/2

311

/30

12/0

812

/14

12/2

012

/27

01/0

301

/10

01/1

601

/22

01/2

802

/03

02/0

902

/14

02/1

902

/25

DATE

LB4100I1 BETA BKG

CP

M

Page 126 of 153

Denotes Outlier

+3 Sigma 17550

-3 Sigma 16570

+2 Sigma 17400

-2 Sigma 16700

Mean 17060

16668

16766

16864

16962

17060

17158

17256

17354

17452

17550

07/0

107

/07

07/1

207

/16

07/2

207

/28

08/0

208

/06

08/1

208

/18

08/2

308

/29

09/0

209

/07

09/1

209

/17

09/2

209

/27

10/0

210

/07

10/1

210

/17

10/2

310

/29

11/0

411

/10

11/1

511

/19

11/2

411

/30

12/0

512

/12

12/1

712

/22

12/2

801

/04

01/1

001

/15

01/2

001

/26

02/0

102

/06

02/1

102

/13

02/1

802

/22

02/2

7

DATE

LB4100I1 BETA EFF Generated 02/28/2015

CP

M

+3 Sigma 00

-3 Sigma -0

+2 Sigma 00

-2 Sigma 00

Mean 00

0.0000518

0.0001086

0.000165

0.0002221

0.000279

0.000336

0.000392

0.000449

0.0005058

0.000563

07/0

107

/08

07/1

407

/19

07/2

608

/02

08/0

708

/14

08/2

108

/28

09/0

209

/07

09/1

309

/18

09/2

510

/01

10/0

710

/13

10/2

010

/27

11/0

311

/10

11/1

611

/21

11/2

812

/04

12/1

212

/18

12/2

412

/31

01/0

901

/15

01/2

101

/28

02/0

402

/10

02/1

302

/18

02/2

4

DATE

LB4100I1 BETA EFF Cross Talk

Page 127 of 153

Denotes Outlier

+3 Sigma 0.29

-3 Sigma -0.06

+2 Sigma 0.23

-2 Sigma -0.001

Mean 0.12

-0.0245

0.01073

0.0459

0.0811

0.12

0.15

0.19

0.22

0.26

0.29

08/0

108

/06

08/1

108

/16

08/2

108

/26

08/3

109

/06

09/1

109

/16

09/2

109

/26

10/0

110

/06

10/1

010

/15

10/2

010

/25

10/3

011

/03

11/0

811

/13

11/1

811

/23

11/3

012

/05

12/1

212

/18

12/2

312

/29

01/0

401

/10

01/1

501

/20

01/2

501

/30

02/0

402

/09

02/1

402

/18

02/2

302

/28

DATE


CP

M

+3 Sigma 15350

-3 Sigma 14640

+2 Sigma 15200

-2 Sigma 14800

Mean 15000

14711

14782

14853

14924

14995

15066

15137

15208

15279

15350

08/0

108

/07

08/1

308

/19

08/2

508

/30

09/0

509

/10

09/1

509

/19

09/2

509

/29

10/0

410

/09

10/1

310

/19

10/2

410

/30

11/0

411

/10

11/1

511

/20

11/2

512

/01

12/0

312

/10

12/1

512

/17

12/2

012

/27

12/3

101

/07

01/0

701

/09

01/1

301

/15

01/2

001

/23

01/2

902

/04

02/0

902

/13

02/1

802

/22

02/2

7

DATE

LB4100I2 ALPHA EFF

CP

M

+3 Sigma 0.23

-3 Sigma 0.16

+2 Sigma 0.22

-2 Sigma 0.17

Mean 0.19

0.17

0.17

0.18

0.19

0.19

0.2

0.21

0.22

0.22

0.23

08/0

108

/07

08/1

308

/19

08/2

508

/30

09/0

509

/10

09/1

509

/19

09/2

509

/29

10/0

310

/08

10/1

110

/16

10/2

310

/29

11/0

411

/10

11/1

511

/20

11/2

512

/01

12/0

312

/10

12/1

512

/17

12/2

012

/27

12/3

101

/07

01/0

701

/09

01/1

301

/15

01/2

001

/23

01/2

902

/04

02/0

902

/13

02/1

802

/22

02/2

7

DATE


+3 Sigma 2.21

-3 Sigma 0.12

+2 Sigma 1.86

-2 Sigma 0.47

Mean 1.17

0.33

0.54

0.75

0.96

1.17

1.37

1.58

1.79

2

2.21

08/2

7

09/1

2

10/0

7

10/1

2

10/2

0

10/2

4

10/2

8

10/3

1

11/0

4

11/0

8

11/1

2

11/1

6

11/2

0

11/2

4

11/2

9

12/0

3

12/0

9

12/1

2

12/1

7

12/2

1

12/2

6

12/3

0

01/0

4

01/0

9

01/1

3

01/1

7

01/2

1

01/2

5

01/2

9

02/0

2

02/0

6

02/1

0

02/1

4

02/1

8

02/2

1

02/2

5

DATE

LB4100I2 BETA BKG

CP

M

Page 128 of 153

Denotes Outlier

+3 Sigma 19540

-3 Sigma 18740

+2 Sigma 19400

-2 Sigma 18900

Mean 19140

18820

18900

18980

19060

19140

19220

19300

19380

19460

19540

08/0

108

/07

08/1

308

/19

08/2

508

/30

09/0

509

/10

09/1

509

/19

09/2

509

/30

10/0

510

/10

10/1

510

/21

10/2

711

/01

11/0

711

/12

11/1

611

/21

11/2

612

/02

12/0

912

/14

12/1

912

/24

12/3

001

/07

01/1

201

/17

01/2

201

/28

02/0

202

/06

02/1

102

/13

02/1

802

/22

02/2

5

DATE


CP

M

+3 Sigma 00

-3 Sigma 00

+2 Sigma 00

-2 Sigma 00

Mean 00

0.000126

0.0001608

0.000196

0.0002309

0.000266

0.0003011

0.000336

0.000371

0.0004063

0.000441

08/0

108

/07

08/1

308

/19

08/2

508

/30

09/0

509

/10

09/1

509

/19

09/2

509

/30

10/0

510

/10

10/1

510

/21

10/2

711

/01

11/0

711

/12

11/1

611

/21

11/2

612

/02

12/0

912

/14

12/1

912

/24

12/3

001

/07

01/1

201

/17

01/2

201

/28

02/0

202

/06

02/1

102

/13

02/1

802

/22

02/2

5

DATE


Page 129 of 153

Denotes Outlier

+3 Sigma 0.28

-3 Sigma -0.052

+2 Sigma 0.23

-2 Sigma 00

Mean 0.11

-0.0185

0.0149

0.0482

0.0816

0.11

0.15

0.18

0.21

0.25

0.28

07/1

407

/20

07/2

608

/01

08/0

708

/11

08/1

708

/23

08/2

909

/04

09/1

009

/16

09/2

209

/28

10/0

410

/10

10/1

610

/23

10/2

911

/02

11/0

811

/12

11/1

811

/20

11/2

612

/03

12/1

112

/16

12/2

212

/29

01/0

501

/12

01/1

801

/24

01/3

002

/05

02/1

102

/17

02/2

202

/26

DATE


CP

M

+3 Sigma 12610

-3 Sigma 10820

+2 Sigma 12300

-2 Sigma 11100

Mean 11720

10999

11178

11357

11536

11715

11894

12073

12252

12431

12610

07/0

107

/19

07/2

507

/29

08/0

408

/09

08/1

508

/21

08/2

709

/02

09/0

709

/12

09/1

709

/22

09/2

709

/30

10/0

510

/09

10/1

410

/20

10/2

510

/31

11/0

611

/12

11/1

711

/22

11/2

812

/03

12/1

012

/14

12/1

712

/22

12/2

801

/03

01/0

701

/11

01/1

601

/21

01/2

602

/01

02/0

602

/11

02/1

502

/19

02/2

4

DATE

LB4100I4 ALPHA EFF

CP

M

+3 Sigma 0.2

-3 Sigma 0.14

+2 Sigma 0.19

-2 Sigma 0.15

Mean 0.17

0.15

0.16

0.16

0.17

0.17

0.18

0.19

0.19

0.2

0.2

07/0

107

/08

07/1

407

/21

07/2

608

/01

08/0

808

/15

08/2

208

/29

09/0

509

/11

09/1

709

/23

09/2

910

/03

10/0

910

/13

10/2

010

/27

11/0

311

/10

11/1

611

/22

11/2

912

/05

12/1

212

/16

12/2

212

/29

01/0

501

/09

01/1

501

/21

01/2

702

/03

02/0

902

/14

02/1

902

/25

DATE


+3 Sigma 1.42

-3 Sigma 0.33

+2 Sigma 1.24

-2 Sigma 0.51

Mean 0.88

0.44

0.55

0.66

0.77

0.88

0.99

1.09

1.2

1.31

1.42

07/0

107

/07

07/1

207

/17

07/2

307

/29

08/0

408

/08

08/1

408

/20

08/2

609

/02

09/0

709

/13

09/1

809

/25

10/0

110

/07

10/1

310

/20

10/2

610

/30

11/0

511

/11

11/1

511

/19

11/2

311

/30

12/0

812

/13

12/1

912

/26

01/0

201

/09

01/1

501

/21

01/2

702

/02

02/0

802

/14

02/1

902

/25

DATE

LB4100I4 BETA BKG

CP

M

Page 130 of 153

Denotes Outlier

+3 Sigma 22380

-3 Sigma 20880

+2 Sigma 22100

-2 Sigma 21100

Mean 21630

21030

21180

21330

21480

21630

21780

21930

22080

22230

22380

07/1

507

/21

07/2

808

/04

08/0

808

/15

08/2

208

/29

09/0

409

/10

09/1

609

/22

09/2

810

/03

10/0

810

/14

10/2

110

/27

10/3

111

/07

11/1

311

/17

11/2

111

/28

12/0

412

/11

12/1

612

/19

12/2

312

/29

01/0

501

/12

01/1

801

/23

01/2

802

/02

02/0

702

/11

02/1

402

/16

02/1

802

/20

02/2

302

/28

DATE


CP

M

+3 Sigma 00

-3 Sigma -0

+2 Sigma 00

-2 Sigma 00

Mean 00

0.0000194

0.0000853

0.000151

0.0002171

0.000283

0.000349

0.000415

0.0004806

0.000547

0.000612

07/0

107

/08

07/1

407

/19

07/2

608

/02

08/0

708

/14

08/2

108

/28

09/0

309

/09

09/1

509

/21

09/2

710

/02

10/0

710

/13

10/2

010

/27

10/3

011

/06

11/1

311

/17

11/2

011

/26

12/0

312

/10

12/1

512

/18

12/2

212

/28

01/0

501

/11

01/1

701

/23

01/2

702

/02

02/0

602

/10

02/1

302

/16

02/1

802

/19

02/2

302

/27

DATE


Page 131 of 153

Denotes Outlier

+3 Sigma 0.35

-3 Sigma -0.046

+2 Sigma 0.29

-2 Sigma 0.02

Mean 0.15

-0.006072

0.03404

0.0741

0.11

0.15

0.19

0.23

0.27

0.31

0.35

07/0

107

/07

07/1

107

/17

07/2

307

/29

08/0

408

/10

08/1

608

/22

08/2

809

/04

09/1

009

/14

09/1

809

/24

09/3

010

/06

10/1

210

/19

10/2

510

/29

11/0

411

/08

11/1

411

/18

11/2

211

/29

12/0

412

/11

12/1

712

/23

12/3

001

/06

01/1

201

/18

01/2

501

/30

02/0

502

/11

02/1

702

/22

02/2

8

DATE

PIC1A ALPHA BKG Generated 03/05/2015

CP

M

+3 Sigma 10950

-3 Sigma 10330

+2 Sigma 10800

-2 Sigma 10400

Mean 10640

10392

10454

10516

10578

10640

10702

10764

10826

10888

10950

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/31

09/0

709

/13

09/1

809

/24

09/3

010

/06

10/1

210

/19

10/2

511

/01

11/0

811

/15

11/2

111

/28

12/0

412

/12

12/1

812

/24

12/3

101

/07

01/1

301

/19

01/2

602

/01

02/0

702

/13

02/1

802

/23

03/0

1

DATE

PIC1A ALPHA EFF

CP

M

+3 Sigma 0.31

-3 Sigma 0.27

+2 Sigma 0.3

-2 Sigma 0.28

Mean 0.29

0.27

0.28

0.28

0.28

0.29

0.29

0.3

0.3

0.3

0.31

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/31

09/0

709

/13

09/1

809

/24

09/3

010

/06

10/1

210

/19

10/2

511

/01

11/0

811

/15

11/2

111

/28

12/0

412

/12

12/1

812

/24

12/3

101

/07

01/1

301

/19

01/2

602

/01

02/0

702

/13

02/1

802

/23

03/0

1

DATE

PIC1A ALPHA EFF Cross Talk

+3 Sigma 1.28

-3 Sigma -0.015

+2 Sigma 1.06

-2 Sigma 0.2

Mean 0.63

0.11

0.24

0.37

0.5

0.63

0.76

0.89

1.02

1.15

1.28

07/0

107

/07

07/1

107

/17

07/2

307

/29

08/0

408

/10

08/1

608

/22

08/2

809

/04

09/1

009

/14

09/1

809

/22

09/2

810

/04

10/1

010

/16

10/2

310

/28

11/0

211

/08

11/1

211

/16

11/2

111

/26

12/0

312

/09

12/1

512

/21

12/2

801

/04

01/1

001

/16

01/2

201

/28

02/0

302

/09

02/1

502

/20

02/2

603

/05

DATE

PIC1A BETA BKG

CP

M

Page 132 of 153

Denotes Outlier

+3 Sigma 21630

-3 Sigma 20720

+2 Sigma 21500

-2 Sigma 20900

Mean 21180

20811

20902

20993

21084

21175

21266

21357

21448

21539

21630

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/29

09/0

509

/11

09/1

709

/19

09/2

610

/02

10/0

810

/14

10/2

110

/28

11/0

411

/11

11/1

711

/20

11/2

612

/03

12/1

112

/17

12/2

312

/30

01/0

601

/08

01/1

001

/16

01/2

101

/28

02/0

402

/10

02/1

602

/20

02/2

603

/04

DATE

PIC1A BETA EFF Generated 03/05/2015

CP

M

+3 Sigma 00

-3 Sigma -0

+2 Sigma 00

-2 Sigma 00

Mean 00

0.000047

0.000179

0.000311

0.000444

0.000576

0.0007081

0.0008403

0.000973

0.001105

0.00124

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/29

09/0

509

/11

09/1

709

/19

09/2

610

/02

10/0

810

/14

10/2

110

/28

11/0

411

/11

11/1

711

/20

11/2

612

/03

12/1

112

/17

12/2

312

/30

01/0

601

/08

01/1

001

/16

01/2

101

/28

02/0

402

/10

02/1

602

/20

02/2

603

/04

DATE

PIC1A BETA EFF Cross Talk

Page 133 of 153

Denotes Outlier

+3 Sigma 0.35

-3 Sigma -0.02

+2 Sigma 0.28

-2 Sigma 0.04

Mean 0.16

0.0163

0.0528

0.0894

0.13

0.16

0.2

0.24

0.27

0.31

0.35

07/0

107

/05

07/1

007

/15

07/2

107

/27

08/0

108

/06

08/1

108

/17

08/2

208

/27

09/0

209

/08

09/1

309

/18

09/2

510

/01

10/0

710

/13

10/1

910

/26

11/0

611

/12

11/1

911

/25

12/0

212

/10

12/1

612

/21

12/2

801

/04

01/0

801

/14

01/2

001

/26

02/0

102

/07

02/1

302

/18

02/2

403

/02

DATE

PIC3B ALPHA BKG Generated 03/04/2015

CP

M

+3 Sigma 13790

-3 Sigma 13260

+2 Sigma 13700

-2 Sigma 13400

Mean 13530

13313

13366

13419

13472

13525

13578

13631

13684

13737

13790

07/0

107

/07

07/1

307

/19

07/2

608

/02

08/0

808

/15

08/2

208

/28

08/3

109

/07

09/1

309

/17

09/2

309

/29

10/0

610

/11

10/1

710

/24

10/3

111

/07

11/1

211

/17

11/2

111

/28

12/0

212

/08

12/1

212

/15

12/1

812

/22

12/2

412

/31

01/0

701

/13

01/1

901

/26

02/0

202

/08

02/1

402

/18

02/2

403

/02

DATE

PIC3B ALPHA EFF

CP

M

+3 Sigma 0.27

-3 Sigma 0.23

+2 Sigma 0.26

-2 Sigma 0.24

Mean 0.25

0.24

0.24

0.24

0.25

0.25

0.26

0.26

0.26

0.27

0.27

07/0

107

/07

07/1

307

/19

07/2

608

/02

08/0

708

/14

08/2

108

/28

08/3

009

/06

09/1

209

/16

09/2

209

/28

10/0

410

/09

10/1

510

/22

10/2

911

/05

11/1

011

/15

11/1

811

/24

12/0

112

/04

12/0

912

/15

12/1

512

/19

12/2

212

/28

01/0

401

/10

01/1

601

/22

01/2

902

/05

02/1

102

/17

02/2

102

/27

DATE

PIC3B ALPHA EFF Cross Talk

+3 Sigma 2.38

-3 Sigma -0.33

+2 Sigma 1.93

-2 Sigma 0.12

Mean 1.02

-0.0597

0.21

0.48

0.75

1.02

1.29

1.56

1.83

2.11

2.38

07/0

107

/05

07/0

907

/14

07/1

907

/25

07/3

008

/04

08/0

708

/12

08/1

808

/22

08/2

608

/30

09/0

609

/11

09/1

609

/22

09/2

810

/04

10/1

010

/14

10/1

710

/29

11/0

811

/17

11/2

311

/30

12/0

512

/11

12/1

712

/22

12/2

901

/05

01/0

901

/15

01/2

101

/27

02/0

202

/08

02/1

402

/19

02/2

503

/02

DATE

PIC3B BETA BKG

CP

M

Page 134 of 153

Denotes Outlier

+3 Sigma 22510

-3 Sigma 20970

+2 Sigma 22300

-2 Sigma 21200

Mean 21740

21124

21278

21432

21586

21740

21894

22048

22202

22356

22510

07/0

107

/07

07/0

907

/15

07/2

107

/28

08/0

408

/11

08/1

808

/25

08/3

009

/05

09/1

109

/17

09/2

409

/30

10/0

610

/12

10/1

910

/25

11/0

111

/07

11/1

211

/17

11/2

211

/25

12/0

112

/02

12/0

212

/05

12/1

212

/18

12/2

312

/30

01/0

601

/12

01/1

601

/22

01/2

602

/01

02/0

702

/13

02/1

802

/23

03/0

1

DATE

PIC3B BETA EFF Generated 03/04/2015

CP

M

+3 Sigma 0.02

-3 Sigma 00

+2 Sigma 0.02

-2 Sigma 0.01

Mean 0.01

0.00462

0.00624

0.00785

0.00947

0.01109

0.01271

0.0143

0.0159

0.0176

0.0192

07/0

107

/07

07/0

907

/15

07/1

807

/25

08/0

108

/08

08/1

508

/22

08/2

909

/03

09/0

909

/15

09/2

209

/28

10/0

410

/10

10/1

610

/23

10/3

011

/06

11/1

111

/16

11/2

011

/24

11/2

912

/01

12/0

212

/05

12/1

012

/15

12/2

112

/27

01/0

301

/09

01/1

301

/19

01/2

201

/28

02/0

402

/10

02/1

602

/20

02/2

603

/02

DATE

PIC3B BETA EFF Cross Talk

Page 135 of 153

Denotes Outlier

+3 Sigma 0.35

-3 Sigma 0.01

+2 Sigma 0.29

-2 Sigma 0.07

Mean 0.18

0.0475

0.08083

0.11

0.15

0.18

0.21

0.25

0.28

0.31

0.35

07/0

107

/07

07/1

107

/17

07/2

307

/29

08/0

408

/13

08/2

008

/28

09/0

609

/11

09/1

809

/23

10/0

110

/08

10/1

410

/22

10/2

811

/01

11/0

611

/12

11/1

811

/20

11/2

612

/02

12/0

912

/13

12/1

912

/26

01/0

201

/08

01/1

401

/20

01/2

602

/03

02/0

702

/13

02/1

802

/23

02/2

803

/04

DATE

PIC4D ALPHA BKG Generated 03/04/2015

CP

M

+3 Sigma 17420

-3 Sigma 16940

+2 Sigma 17341

-2 Sigma 17019

Mean 17180

16988

17036

17084

17132

17180

17228

17276

17324

17372

17420

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/31

09/0

709

/14

09/1

909

/26

10/0

210

/08

10/1

410

/21

10/2

811

/04

11/1

111

/17

11/2

311

/30

12/0

812

/14

12/2

012

/27

12/3

101

/07

01/1

301

/19

01/2

301

/30

02/0

602

/12

02/1

802

/22

02/2

8

DATE

PIC4D ALPHA EFF

CP

M

+3 Sigma 0.27

-3 Sigma 0.25

+2 Sigma 0.26

-2 Sigma 0.25

Mean 0.26

0.25

0.26

0.26

0.26

0.26

0.26

0.26

0.26

0.27

0.27

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/31

09/0

709

/13

09/1

809

/25

10/0

110

/07

10/1

210

/19

10/2

511

/01

11/0

811

/15

11/2

111

/28

12/0

412

/12

12/1

812

/24

12/3

101

/05

01/1

101

/17

01/2

101

/28

02/0

402

/10

02/1

602

/20

02/2

603

/04

DATE

PIC4D ALPHA EFF Cross Talk

+3 Sigma 2.2

-3 Sigma 1.17

+2 Sigma 2.03

-2 Sigma 1.34

Mean 1.68

1.27

1.37

1.48

1.58

1.68

1.79

1.89

1.99

2.1

2.2

07/0

107

/08

07/1

407

/21

07/2

708

/02

08/0

908

/16

08/2

108

/28

09/0

409

/09

09/1

409

/19

09/2

510

/04

10/1

110

/17

10/2

411

/01

11/0

611

/12

11/1

711

/21

11/2

812

/03

12/0

912

/14

12/2

012

/27

01/0

201

/07

01/1

201

/17

01/2

201

/29

02/0

402

/08

02/1

302

/17

02/2

102

/25

03/0

2

DATE

PIC4D BETA BKG

CP

M

Page 136 of 153

Denotes Outlier

+3 Sigma 45180

-3 Sigma 42800

+2 Sigma 44800

-2 Sigma 43200

Mean 43990

43038

43276

43514

43752

43990

44228

44466

44704

44942

45180

07/0

107

/07

07/1

007

/16

07/2

107

/28

08/0

408

/11

08/1

808

/25

08/3

109

/06

09/1

309

/19

09/2

409

/30

10/0

610

/11

10/1

710

/24

10/3

111

/04

11/0

811

/14

11/1

811

/24

11/2

812

/04

12/1

212

/18

12/2

212

/24

12/3

101

/07

01/1

301

/19

01/2

201

/27

01/3

002

/06

02/0

902

/12

02/1

802

/22

02/2

603

/03

DATE

PIC4D BETA EFF Generated 03/04/2015

CP

M

+3 Sigma 0.01

-3 Sigma 0.01

+2 Sigma 0.01

-2 Sigma 0.01

Mean 0.01

0.00677

0.00766

0.00854

0.00942

0.010306

0.0112

0.01207

0.013

0.0138

0.0147

07/0

107

/07

07/1

007

/17

07/2

307

/31

08/0

808

/16

08/2

308

/31

09/0

609

/13

09/1

909

/25

10/0

210

/08

10/1

410

/22

10/3

011

/04

11/1

011

/15

11/1

911

/24

12/0

112

/10

12/1

712

/22

12/2

701

/03

01/1

001

/17

01/2

201

/27

02/0

102

/08

02/1

002

/16

02/2

102

/26

03/0

4

DATE

PIC4D BETA EFF Cross Talk

Page 137 of 153

Denotes Outlier

+3 Sigma 0.38

-3 Sigma -0.041

+2 Sigma 0.31

-2 Sigma 0.03

Mean 0.17

0.000777

0.04302

0.0853

0.13

0.17

0.21

0.25

0.3

0.34

0.38

07/0

107

/06

07/1

307

/20

07/2

708

/03

08/1

008

/15

08/2

208

/28

09/0

709

/14

09/2

209

/29

10/0

610

/13

10/2

110

/26

11/0

211

/08

11/1

311

/17

11/2

111

/29

12/0

312

/05

12/1

212

/19

12/2

401

/02

01/0

901

/14

01/2

001

/26

01/2

802

/02

02/0

702

/11

02/1

502

/19

02/2

403

/02

DATE

PIC5A ALPHA BKG Generated 03/04/2015

CP

M

+3 Sigma 11600

-3 Sigma 10610

+2 Sigma 11400

-2 Sigma 10800

Mean 11100

10709

10808

10907

11006

11105

11204

11303

11402

11501

11600

07/0

107

/07

07/1

207

/17

07/2

307

/29

08/0

408

/09

08/1

508

/22

08/2

809

/03

09/0

809

/13

09/1

809

/23

09/2

810

/03

10/0

810

/13

10/1

910

/24

10/3

011

/05

11/1

111

/16

11/2

211

/28

12/0

412

/11

12/1

612

/21

12/2

412

/30

01/0

501

/10

01/1

501

/20

01/2

602

/01

02/0

602

/11

02/1

602

/19

02/2

403

/01

DATE

PIC5A ALPHA EFF

CP

M

+3 Sigma 0.28

-3 Sigma 0.23

+2 Sigma 0.27

-2 Sigma 0.24

Mean 0.26

0.24

0.24

0.25

0.25

0.26

0.26

0.27

0.27

0.28

0.28

07/0

107

/07

07/1

207

/17

07/2

307

/29

08/0

408

/09

08/1

508

/21

08/2

709

/02

09/0

709

/12

09/1

709

/22

09/2

710

/02

10/0

710

/12

10/1

710

/23

10/2

911

/04

11/1

011

/15

11/2

011

/26

12/0

312

/10

12/1

512

/20

12/2

312

/29

01/0

401

/09

01/1

401

/19

01/2

501

/30

02/0

502

/10

02/1

502

/18

02/2

302

/28

DATE

PIC5A ALPHA EFF Cross Talk

+3 Sigma 1.93

-3 Sigma -0.785

+2 Sigma 1.48

-2 Sigma -0.333

Mean 0.57

-0.514

-0.243

0.0286

0.3

0.57

0.84

1.11

1.38

1.66

1.93

07/0

107

/07

07/1

307

/19

07/2

507

/31

08/0

608

/12

09/2

309

/29

10/0

510

/11

10/1

710

/23

10/2

610

/30

11/0

411

/08

11/1

211

/15

11/1

911

/24

12/0

112

/04

12/0

512

/11

12/1

712

/22

12/2

801

/04

01/1

001

/14

01/2

001

/25

01/2

701

/31

02/0

402

/08

02/1

102

/14

02/1

802

/23

02/2

703

/03

DATE

PIC5A BETA BKG

CP

M

Page 138 of 153

Denotes Outlier

+3 Sigma 18760

-3 Sigma 17660

+2 Sigma 18600

-2 Sigma 17800

Mean 18210

17770

17880

17990

18100

18210

18320

18430

18540

18650

18760

07/0

107

/07

07/1

007

/14

07/1

807

/23

07/2

908

/01

08/0

608

/12

08/1

808

/26

09/0

309

/10

09/1

709

/24

09/3

010

/06

10/1

310

/17

10/2

510

/31

11/0

811

/14

11/2

111

/28

12/0

412

/13

12/2

012

/28

01/0

501

/12

01/1

901

/26

02/0

202

/05

02/1

002

/15

02/1

802

/19

02/2

503

/02

DATE

PIC5A BETA EFF Generated 03/04/2015

CP

M

+3 Sigma 0.01

-3 Sigma 00

+2 Sigma 0.01

-2 Sigma 00

Mean 00

0.000972

0.00155

0.00213

0.002704

0.00328

0.00386

0.00444

0.005013

0.005591

0.00617

07/0

107

/07

07/1

007

/14

07/1

807

/23

07/2

908

/01

08/0

608

/11

08/1

608

/23

08/3

109

/08

09/1

509

/22

09/2

910

/03

10/1

010

/14

10/2

210

/29

11/0

511

/12

11/1

811

/24

12/0

312

/10

12/1

712

/24

01/0

201

/09

01/1

601

/22

01/3

002

/04

02/0

902

/12

02/1

702

/18

02/2

302

/27

DATE

PIC5A BETA EFF Cross Talk

Page 139 of 153

Denotes Outlier

+3 Sigma 0.35

-3 Sigma -0.022

+2 Sigma 0.29

-2 Sigma 0.04

Mean 0.17

0.0152

0.0529

0.09059

0.13

0.17

0.2

0.24

0.28

0.32

0.35

07/0

107

/07

07/1

307

/19

07/2

507

/31

08/0

608

/12

08/1

808

/23

08/2

809

/04

09/0

909

/16

09/1

909

/23

09/3

010

/06

10/1

210

/16

10/2

210

/26

10/3

011

/06

11/1

111

/14

11/1

811

/25

12/0

112

/05

12/1

212

/18

12/2

312

/30

01/0

401

/09

01/1

501

/20

01/2

601

/31

02/0

402

/10

02/1

602

/21

02/2

503

/03

DATE

PIC5C ALPHA BKG Generated 03/04/2015

CP

M

+3 Sigma 10900

-3 Sigma 10450

+2 Sigma 10800

-2 Sigma 10500

Mean 10680

10495

10540

10585

10630

10675

10720

10765

10810

10855

10900

07/0

107

/09

07/1

607

/24

08/0

108

/08

08/1

608

/25

09/0

209

/09

09/1

509

/21

09/2

810

/05

10/1

210

/20

10/2

811

/03

11/0

811

/14

11/2

211

/30

12/0

912

/14

12/1

612

/21

12/2

712

/31

01/0

701

/08

01/1

201

/13

01/1

901

/23

01/2

702

/04

02/0

902

/16

02/2

102

/28

DATE

PIC5C ALPHA EFF

CP

M

+3 Sigma 0.27

-3 Sigma 0.26

+2 Sigma 0.27

-2 Sigma 0.26

Mean 0.27

0.26

0.26

0.26

0.26

0.27

0.27

0.27

0.27

0.27

0.27

07/0

107

/09

07/1

607

/24

08/0

108

/07

08/1

508

/23

08/3

109

/08

09/1

509

/19

09/2

710

/04

10/1

110

/19

10/2

711

/01

11/0

711

/13

11/2

011

/29

12/0

812

/13

12/1

512

/20

12/2

712

/31

01/0

701

/08

01/1

201

/13

01/1

901

/23

01/2

702

/04

02/0

902

/16

02/2

102

/28

DATE

PIC5C ALPHA EFF Cross Talk

+3 Sigma 1.7

-3 Sigma -0.074

+2 Sigma 1.41

-2 Sigma 0.22

Mean 0.81

0.1

0.28

0.46

0.64

0.81

0.99

1.17

1.35

1.53

1.7

07/0

107

/08

07/1

507

/22

07/2

908

/05

08/1

208

/19

08/2

408

/28

09/0

309

/09

09/1

709

/19

09/2

309

/29

10/0

610

/13

10/1

610

/22

10/2

410

/28

11/0

311

/08

11/1

211

/14

11/1

711

/23

11/2

912

/03

12/1

012

/17

12/2

312

/30

01/0

401

/09

01/1

601

/21

01/2

602

/01

02/0

602

/13

02/1

902

/24

03/0

3

DATE

PIC5C BETA BKG

CP

M

Page 140 of 153

Denotes Outlier

+3 Sigma 23010

-3 Sigma 22300

+2 Sigma 22886

-2 Sigma 22414

Mean 22650

22371

22442

22513

22584

22655

22726

22797

22868

22939

23010

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/31

09/0

709

/13

09/1

809

/25

10/0

110

/07

10/1

310

/20

10/2

711

/03

11/1

011

/16

11/2

311

/30

12/0

812

/14

12/2

012

/27

01/0

301

/09

01/1

501

/21

01/2

802

/01

02/0

202

/07

02/1

302

/18

02/2

303

/01

DATE

PIC5C BETA EFF Generated 03/04/2015

CP

M

+3 Sigma 00

-3 Sigma 00

+2 Sigma 00

-2 Sigma 00

Mean 00

0.00154

0.00192

0.002304

0.00269

0.003069

0.00345

0.00383

0.00422

0.0046

0.00498

07/0

107

/08

07/1

407

/21

07/2

808

/04

08/1

108

/18

08/2

508

/31

09/0

709

/13

09/1

809

/25

10/0

110

/07

10/1

310

/20

10/2

711

/03

11/1

011

/16

11/2

311

/30

12/0

812

/14

12/2

012

/27

01/0

301

/09

01/1

501

/21

01/2

802

/01

02/0

202

/07

02/1

302

/18

02/2

303

/01

DATE

PIC5C BETA EFF Cross Talk

Page 141 of 153

RAD StandardsTraceability

Page 142 of 153

of 153



Parent Code: 1243

Prepared By: Daniel Roy

Carrier Conc: 0.1M HCL



Uncertainty: +/- .85 %



Isotope: Strontium-90


Prep Date: 12/19/2008












Secondary Standards


PrimaryDilution

(mL)Code Conc dpm/mL

Verification Date

Expiration Date

01/21/2010Bethany

Fiem2.2467 1000 1243-B

510.329369 dpm/mL

01/21/2010 01/21/2011

08/03/2010Bethany

Fiem2.5604 1000 1243-C

581.5851 dpm/mL

08/03/2010 08/03/2011

01/12/2011Bethany

Fiem2.4946 1000 1243-D

566.6389 dpm/mL

01/12/2011 01/12/2012

08/12/2011Tim

Chandler3.3115 100 1243-G

18.7877 dpm/mL

03/26/2014 03/25/2015

08/17/2011Tim

Chandler2.5541 100 1243-H

14.49064 dpm/mL

03/26/2014 03/25/2015

06/21/2011Tim

Chandler.0235 100 1243-E

53.37936 dpm/mL

03/19/2014 06/20/2014

07/05/2011Bethany

Fiem2.6072 1000 1243-F

592.2156 dpm/mL

07/05/2011 07/05/2012


2.6792 1000 1243-I608.5701 dpm/ml

01/31/2012 01/31/2013

Page 144 of 153

08/29/2012Bethany

Fiem2.6799 1000 1243-J

608.729104 dpm/mL

09/14/2012 09/11/2013


2.6526 1000 1243-K 602.528 dpm/ml 01/15/2014 01/15/2015


2.5347 1000 1243-L575.747476

dpm/ml12/04/2013 12/04/2014


2.7006 1000 1243-M613.431 dpm/mL

08/12/2014 08/12/2015


Page 145 of 153

of

153

of 153



Parent Code: 1242


Carrier Conc: 0.5M HNO3



Uncertainty: +/- 2 %



Isotope: Thorium-230


Prep Date: 11/10/2009












Secondary Standards


PrimaryDilution

(mL)Code Conc dpm/mL

Verification Date

Expiration Date

12/01/2009Bethany Fiem 6.3855 500 1242-B279.79548 dpm/mL

12/02/2009 12/02/2010


12.8745 1000 1242-C282.063 dpm/mL

07/30/2013 07/30/2014

07/05/2011Bethany Fiem 12.1975 1000 1242-D267.2309 dpm/mL

06/22/2012 06/22/2013


.105 500 1242-E4.6008

dpm/mL01/13/2015 01/13/2016

01/08/2013Bethany Fiem 12.5093 1000 1242-F274.062 dpm/mL

01/07/2014 01/07/2015


.012512 100 1242-G2.74129 dpm/mL

08/25/2014 08/25/2015

02/17/2014Tim Chandler .2121 100 1242-H46.46827 dpm/mL

02/17/2015 02/17/2016


6.16 500 1242-I269.9147 dpm/mL

08/12/2014 08/12/2015

Page 148 of 153


Page 149 of 153

of

153

Runlogs

Page 151 of 153

Instrument Run Log

GFPCInstrument Type:

36733300112032698281203269829120326983012032698311203269832

SampleID

SampleType

AXJ1AXJ1AXJ1AXJ1AXJ1AXJ1

Analyst

LB4100I1LB4100I2LB4100I4LB4100E1LB4100E3LB4100E4

Instrument

FEB-28-15 12:26:04FEB-28-15 12:26:04FEB-28-15 12:26:04FEB-28-15 12:26:14FEB-28-15 12:26:14FEB-28-15 12:26:15

Run Date

DONEDONEDONEDONEDONEDONE

Status

2 inch Planchett2 inch Planchett2 inch Planchett2 inch Planchett2 inch Planchett2 inch Planchett

Geometry

01-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:00

Calibration Date

Batch ID:1459656

SAMPLEMBDUPMSMSDLCS

Page 152 of 153

Instrument Run Log

GFPCInstrument Type:

36733300212032698541203269855120326985712032698581203269856

SampleID

SampleType

AXJ1AXJ1AXJ1AXJ1AXJ1AXJ1

Analyst

PIC5CPIC3BPIC5APIC4DPIC4DPIC1A

Instrument

MAR-04-15 12:48:27MAR-04-15 12:48:42MAR-04-15 12:48:46MAR-04-15 12:48:56MAR-04-15 16:06:54MAR-05-15 06:22:31

Run Date

DONEDONEDONEDONEDONEDONE

Status

2 inch Planchett2 inch Planchett2 inch Planchett2 inch Planchett2 inch Planchett2 inch Planchett

Geometry

01-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:0001-OCT-13 00:00

Calibration Date

Batch ID:1459664

SAMPLEMBDUPMSDLCSMS

Page 153 of 153

MAX LABORATORIES, INC. 1835 EMAX Batch … LABORATORIES, INC. 1835 W. 205th Street Torrance, CA...

Documents

Transcript of MAX LABORATORIES, INC. 1835 EMAX Batch … LABORATORIES, INC. 1835 W. 205th Street Torrance, CA...