Urban Pesticide Use Patterns – Pesticides of Concern for Pesticides ...
Matrix: Derivative Certificate of Analysis · 2021. 6. 19. · Sample Method : SOP.T.20.010...
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty of measurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for the pass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310. Jorge Segredo Lab Director State License # CMTL-0002 ISO Accreditation # ISO/IEC 17025:2017 Accreditation PJLA-Testing 97164 ___________________ Signature 06/18/21 ___________________ Signed On 4131 SW 47th AVENUE SUITE 1408 DAVIE, FL, 33314, US Kaycha Labs Nocturne Cartridge 1g Nocturne Matrix: Derivative Certificate of Analysis Sample:DA10616002-003 Harvest/Lot ID: 9065 5409 1179 7761 Cultivation Facility: Tampa Cultivation Processing Facility : Tampa Processing Seed to Sale #9065 5409 1179 7761 Batch Date :04/15/21 Batch#: 1036 9141 5302 0802 Sample Size Received: 16 gram Total Weight/Volume: 704 units Retail Product Size: 1 gram Ordered : 06/15/21 sampled : 06/15/21 Completed: 06/18/21 Sampling Method: SOP.T.20.010 Jun 18, 2021 | FLUENT 82 NE 26th street Miami, FL, 33137, US PASSED Page 1 of 5 PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides PASSED Heavy Metals PASSED Microbials PASSED Mycotoxins PASSED Residuals Solvents PASSED Filth PASSED Water Activity PASSED Moisture NOT TESTED Terpenes TESTED CANNABINOID RESULTS Total THC 59.438% TOTAL THC/Container :594.387 mg Total CBD 0.186% TOTAL CBD/Container :1.865 mg Total Cannabinoids 63.590% Total Cannabinoids/Container :635.900 mg CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA % ND 0.0200 0.2690 1.9440 0.1690 0.3500 0.4069 58.3810 ND 0.8440 1.2060 mg/g ND 0.2000 2.6900 19.4400 1.6900 3.5000 4.0700 583.8099 ND 8.4400 12.0600 LOD 0.0010 0.0010 0.0010 0.0010 0.0001 0.0010 0.0010 0.0001 0.0010 0.0010 0.0010 % % % % % % % % % % % Cannabinoid Profile Test Analyzed by Weight Extraction date : Extracted By : 450 0.0972g 06/16/21 11:06:43 2198 Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 06/17/21 12:45:12 Batch Date : 06/16/21 09:42:32 Analytical Batch -DA027370POT Instrument Used : DA-LC-001 Reagent Dilution Consums. ID 110520.96 400 CE0123 061121.R26 280678841 061121.R23 11945-019CD-019C 914C4-914AK 929C6-929H Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L). Filth PASSED Analyzed By Weight Extraction date Extracted By 457 NA NA NA Analyte LOD Result Filth and Foreign Material 0.1 ND Analysis Method -SOP.T.40.013 Batch Date : 06/16/21 10:15:11 Analytical Batch -DA027379FIL Reviewed On - 06/16/21 11:11:02 Instrument Used : Filth/Foreign Material Microscope This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing waste and by-products. An SH-2B/T Stereo Microscope is use for inspection. Water Activity PASSED Analyte Analyzed by Weight Ext. date LOD A.L Result WATER ACTIVITY 457 NA NA 0.01 aw 0.85aw 0.430aW Analysis Method -Water Activity SOP.T.40.010 Batch Date : 06/16/21 10:12:31 Analytical Batch -DA027378WAT Reviewed On - 06/16/21 15:29:40 Instrument Used : DA-028 Rotronic Hygropalm
Transcript of Matrix: Derivative Certificate of Analysis · 2021. 6. 19. · Sample Method : SOP.T.20.010...
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
06/18/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsNocturne Cartridge 1g
NocturneMatrix: Derivative
Certificateof Analysis
Sample:DA10616002-003Harvest/Lot ID: 9065 5409 1179 7761
Cultivation Facility: Tampa CultivationProcessing Facility : Tampa Processing
Seed to Sale #9065 5409 1179 7761Batch Date :04/15/21
Batch#: 1036 9141 5302 0802Sample Size Received: 16 gramTotal Weight/Volume: 704 units
Retail Product Size: 1 gramOrdered : 06/15/21sampled : 06/15/21
Completed: 06/18/21Sampling Method: SOP.T.20.010
Jun 18, 2021 | FLUENT82 NE 26th streetMiami, FL, 33137, US
PASSEDPage 1 of 5
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityPASSED
MoistureNOT TESTED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
59.438%TOTAL THC/Container :594.387mg
Total CBD
0.186%TOTAL CBD/Container :1.865 mg
Total Cannabinoids
63.590%Total Cannabinoids/Container:635.900 mg
CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA
% ND 0.0200 0.2690 1.9440 0.1690 0.3500 0.4069 58.3810 ND 0.8440 1.2060
mg/g ND 0.2000 2.6900 19.4400 1.6900 3.5000 4.0700 583.8099 ND 8.4400 12.0600
LOD 0.0010 0.0010 0.0010 0.0010 0.0001 0.0010 0.0010 0.0001 0.0010 0.0010 0.0010
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 0.0972g 06/16/21 11:06:43 2198Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 06/17/21 12:45:12 Batch Date : 06/16/21 09:42:32Analytical Batch -DA027370POT Instrument Used : DA-LC-001
Reagent Dilution Consums. ID
110520.96 400 CE0123061121.R26 280678841061121.R23 11945-019CD-019C
914C4-914AK929C6-929H
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep andShimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSEDAnalyzed By Weight Extraction date Extracted By457 NA NA NAAnalyte LOD ResultFilth and Foreign Material 0.1 NDAnalysis Method -SOP.T.40.013 Batch Date : 06/16/21 10:15:11Analytical Batch -DA027379FIL Reviewed On - 06/16/21 11:11:02Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
Water Activity PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultWATER ACTIVITY 457 NA NA 0.01 aw 0.85aw 0.430aWAnalysis Method -Water ActivitySOP.T.40.010 Batch Date : 06/16/21 10:12:31Analytical Batch -DA027378WAT Reviewed On - 06/16/21 15:29:40Instrument Used : DA-028 Rotronic Hygropalm
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
06/18/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsNocturne Cartridge 1g
NocturneMatrix : Derivative
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10616002-003Harvest/LOT ID: 9065 5409 1179 7761Batch# : 1036 91415302 0802Sampled : 06/15/21Ordered : 06/15/21
Sample Size Received : 16 gramTotal Weight/Volume : 704 unitsCompleted : 06/18/21Expires: 06/18/22Sample Method : SOP.T.20.010
Page 2 of 5
Terpenes TESTEDTerpenes LOD(%) mg/g % Result (%)
CAMPHENE 0.007 ND NDBETA-MYRCENE 0.007 0.205 0.020ALPHA-PHELLANDRENE
0.007 ND ND
3-CARENE 0.007 ND NDOCIMENE 0.007 ND NDEUCALYPTOL 0.007 ND NDLINALOOL 0.007 0.438 0.043FENCHONE 0.007 ND NDISOPULEGOL 0.007 ND NDISOBORNEOL 0.007 ND NDHEXAHYDROTHYMOL
0.007 ND ND
NEROL 0.007 ND NDGERANYL ACETATE 0.007 ND NDBETA-CARYOPHYLLENE
0.007 9.369 0.936
VALENCENE 0.007 ND NDCIS-NEROLIDOL 0.007 ND NDCARYOPHYLLENEOXIDE
0.007 0.252 0.025
CEDROL 0.007 ND NDFARNESENE 0.007 1.832 0.183ALPHA-BISABOLOL 0.007 0.844 0.084ALPHA-PINENE 0.007 ND NDSABINENE 0.007 < 0.2 < 0.020BETA-PINENE 0.007 < 0.2 < 0.020ALPHA-TERPINENE 0.007 < 0.2 < 0.020LIMONENE 0.007 0.399 0.039GAMMA-TERPINENE
0.007 < 0.2 < 0.020
TERPINOLENE 0.007 < 0.2 < 0.020SABINENEHYDRATE
0.007 < 0.2 < 0.020
FENCHYL ALCOHOL 0.007 0.600 0.060CAMPHOR 0.013 ND NDBORNEOL 0.013 0.553 0.055
Terpenes LOD(%) mg/g % Result (%)
TERPINEOL 0.007 1.383 0.138GERANIOL 0.007 ND NDPULEGONE 0.007 ND NDALPHA-CEDRENE 0.007 ND NDALPHA-HUMULENE 0.007 3.117 0.311TRANS-NEROLIDOL 0.007 0.661 0.066GUAIOL 0.007 1.967 0.196
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By1082 1.002g 06/16/21 12:06:15 2651
Analysis Method -SOP.T.40.090Analytical Batch -DA027315TER Reviewed On - 06/17/21 18:22:06Instrument Used : DA-GCMS-006Running On :Batch Date : 06/15/21 10:29:16
Reagent Dilution Consums. ID
051921.14 10 CE012328067884112499402
Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.
Total (%) 2.162
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
06/18/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsNocturne Cartridge 1g
NocturneMatrix : Derivative
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10616002-003Harvest/LOT ID: 9065 5409 1179 7761Batch# : 1036 91415302 0802Sampled : 06/15/21Ordered : 06/15/21
Sample Size Received : 16 gramTotal Weight/Volume : 704 unitsCompleted : 06/18/21Expires: 06/18/22Sample Method : SOP.T.20.010
Page 3 of 5
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.1 NDACEPHATE 0.01 ppm 0.1 NDACEQUINOCYL 0.01 ppm 0.1 NDACETAMIPRID 0.01 ppm 0.1 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 0.1 NDBIFENAZATE 0.01 ppm 0.1 NDBIFENTHRIN 0.01 ppm 0.1 NDBOSCALID 0.01 PPM 0.1 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 1 NDCHLORMEQUAT CHLORIDE 0.1 ppm 1 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.2 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZINON 0.01 ppm 0.1 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 0.1 NDFENHEXAMID 0.01 ppm 0.1 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 0.1 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 0.1 NDFLUDIOXONIL 0.01 ppm 0.1 NDHEXYTHIAZOX 0.01 ppm 0.1 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 0.4 NDKRESOXIM-METHYL 0.01 ppm 0.1 NDMALATHION 0.02 ppm 0.2 NDMETALAXYL 0.01 ppm 0.1 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 0.1 NDNALED 0.025 ppm 0.25 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.1 NDPIPERONYL BUTOXIDE 0.3 ppm 3 NDPRALLETHRIN 0.01 ppm 0.1 NDPROPICONAZOLE 0.01 ppm 0.1 ND
Pesticides LOD Units Action Level ResultPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 0.5 NDPYRIDABEN 0.02 ppm 0.2 NDSPIROMESIFEN 0.01 ppm 0.1 NDSPIROTETRAMAT 0.01 ppm 0.1 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 0.1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 0.5 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0.05 PPM 5 ND
TOTAL DIMETHOMORPH 0.02 PPM 0.2 NDTOTAL PERMETHRIN 0.01 ppm 0.1 NDTOTAL SPINETORAM 0.02 PPM 0.2 NDTOTAL SPINOSAD 0.01 ppm 0.1 NDTRIFLOXYSTROBIN 0.01 ppm 0.1 NDPENTACHLORONITROBENZENE (PCNB)*
0.01 PPM 0.15 ND
PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 0.7 NDCHLORDANE * 0.01 PPM 0.1 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 0.5 NDCYPERMETHRIN * 0.01 PPM 0.5 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 , 1665 0.2675g 06/16/21 12:06:03 1665 , 1665Analysis Method - SOP.T.30.065, SOP.T.40.065, SOP.T.40.066, SOP.T.40.070 , SOP.T.30.065,SOP.T40.070Analytical Batch - DA027363PES , DA027357VOL Reviewed On- 06/16/21
11:11:02Instrument Used : DA-LCMS-003 (PES) , DA-GCMS-001Running On : 06/16/21 16:53:08 , 06/16/21 16:01:38 Batch Date : 06/16/21 09:35:11
Reagent Dilution Consums. ID060121.R12 25 6524407-03060121.R13061521.R16061621.R01092820.59
Pesticide screen is performed using LC-MS and/or GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060Sample Preparation for Pesticides Analysis via LCMSMS and GCMSMS.SOP.T40.065/SOP.T.40.066/SOP.T.40.070 Procedure for Pesticide Quantification Using LCMS and GCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
06/18/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsNocturne Cartridge 1g
NocturneMatrix : Derivative
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10616002-003Harvest/LOT ID: 9065 5409 1179 7761Batch# : 1036 91415302 0802Sampled : 06/15/21Ordered : 06/15/21
Sample Size Received : 16 gramTotal Weight/Volume : 704 unitsCompleted : 06/18/21Expires: 06/18/22Sample Method : SOP.T.20.010
Page 4 of 5
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
METHANOL 25 ppm 250 PASS ND
ETHANOL 500 ppm 5000 PASS <2500.000
PENTANES (N-PENTANE) 75 ppm 750 PASS ND
ETHYL ETHER 50 ppm 500 PASS ND
ACETONE 75 ppm 750 PASS ND
2-PROPANOL 50 ppm 500 PASS <250.000
ACETONITRILE 6 ppm 60 PASS ND
DICHLOROMETHANE 12.5 ppm 125 PASS ND
N-HEXANE 25 ppm 250 PASS ND
ETHYL ACETATE 40 ppm 400 PASS ND
BENZENE 0.1 ppm 1 PASS ND
HEPTANE 500 ppm 5000 PASS ND
TOLUENE 15 ppm 150 PASS ND
TOTAL XYLENES 15 ppm 150 PASS ND
PROPANE 500 ppm 5000 PASS ND
CHLOROFORM 0.2 ppm 2 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND
BUTANES (N-BUTANE) 500 ppm 5000 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND
TRICHLOROETHYLENE 2.5 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0223g 06/17/21 04:06:44 850
Analysis Method -SOP.T.40.032Analytical Batch -DA027387SOL Reviewed On - 06/18/21 12:38:31Instrument Used : DA-GCMS-002Running On : 06/17/21 00:46:49Batch Date : 06/16/21 11:47:46
Reagent Dilution Consums. ID
1 00268767R2017.217
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.40.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
06/18/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsNocturne Cartridge 1g
NocturneMatrix : Derivative
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10616002-003Harvest/LOT ID: 9065 5409 1179 7761Batch# : 1036 91415302 0802Sampled : 06/15/21Ordered : 06/15/21
Sample Size Received : 16 gramTotal Weight/Volume : 704 unitsCompleted : 06/18/21Expires: 06/18/22Sample Method : SOP.T.20.010
Page 5 of 5
Microbials PASSED
Analyte LOD Result Action Level (cfu/g)ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.ASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.TOTAL YEAST AND MOLD 10 <10 CFU 100000
Analysis Method -SOP.T.40.043 / SOP.T.40.044 / SOP.T.40.041Analytical Batch -DA027355MIC , DA027361TYM Batch Date : 06/16/21, 06/16/21Instrument Used : PathogenDx Scanner DA-111, PathogenDx Scanner DA-111Running On :
Analyzed by Weight Extraction date Extracted By1829, 513 NA NA NA,
Reagent Consums. ID Consums. ID Consums. ID Consums. ID060421.19021921.36
200103-274TH093G11989-024CC-02428040292803035D013
D012A16A1528070152810031D2809006
04428080092811025918C4-918J20324200507119C
914C4-914AK929C6-929H002005
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing. Pour-plating is used for quantitation and confirmation, Total Yeast and Mold hasan action limit of 100,000 CFU.
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA027364MYC | Reviewed On - 06/17/21 12:18:23Instrument Used :Running On : 06/16/21 16:52:13Batch Date : 06/16/21 09:37:14
Analyzed by Weight Extraction date Extracted By585 NA 06/16/21 04:06:57 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Heavy Metals PASSED
Reagent Reagent Dilution Consums. ID060821.R15061421.R76051121.R20060221.R33060221.R34061421.R77
061421.R02030420.08050121.01
100 11989-024CC-02489401-566
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 PPM ND 0.2CADMIUM 0.02 PPM ND 0.2MERCURY 0.02 PPM ND 0.2LEAD 0.05 PPM ND 0.5
Analyzed by Weight Extraction date Extracted By53 0.2303g 06/16/21 01:06:35 1879
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA027372HEA | Reviewed On - 06/17/21 08:07:06Instrument Used : DA-ICPMS-003Running On :Batch Date : 06/16/21 09:51:51
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.
