Materials and Design...thin elastic films such that mode-I crack growth (i.e., K II =0)exists along...

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Spiral cracking pattern in asphalt materials Behzad Behnia a, , William G. Buttlar b , Henrique Reis c a Department of Civil and Environmental Engineering, Western New England University, Springeld, MA, USA b Department of Civil and Environmental Engineering, University of Missouri, Columbia, MO, USA c Department of Industrial and Enterprise Systems Engineering, University of Illinois, Urbana, IL, USA HIGHLIGHTS 3D spiral-shaped fracture pattern was discovered in a biaxially stressed layer of asphalt material bonded to alumi- num substrate. A logarithmic spiral model was selected to mathematically represent three-di- mensional spiral cracks. The spiral tightness parameter, b, was used in characterization of spiral cracks in different asphalt materials. Shape of spiral cracks was independent of thickness and shape of samples and inuenced by fracture properties of as- phalt materials. The embrittlement temperatures and fracture energies of asphalt materials were consistent with corresponding characteristic parameters of spiral cracks. GRAPHICAL ABSTRACT abstract article info Article history: Received 27 July 2016 Received in revised form 20 November 2016 Accepted 21 November 2016 Available online 24 November 2016 The present work for the rst time reports observations and modeling to characterize three-dimensional spiral- shaped fracture patterns in a bi-axially stressed layer of asphalt material bonded to an aluminum substrate. Five different asphalt materials with different fracture characteristics are investigated. A logarithmic spiral model was found to mathematically represent the 3D helix-shaped cracks observed. A spiral tightness parameter is proposed for the characterization of spiral fracture patterns in asphalt. Results of acoustic emission and compact tension tests are also presented and employed in the evaluation of observed spiral cracks. The shape of spirals are found to be inuenced by the fracture properties of the asphalt materials tested and appear to be independent of the thickness and shape of the test sample. The embrittlement temperature and fracture energy of tested as- phalt materials were found to correspond to the characteristic parameters of spiral cracks. Published by Elsevier Ltd. Keywords: Asphalt materials Spiral cracking pattern Acoustic emission test Compact tension test Embrittlement temperature Spiral tightness parameter 1. Introduction As a viscoelastic heterogeneous composite with complex thermo- rheological properties, asphalt materials may experience cracking upon rapid cooling. Thermal cracking, a.k.a. low temperature cracking, Materials and Design 116 (2017) 609615 Corresponding author. E-mail addresses: [email protected] (B. Behnia), [email protected] (W.G. Buttlar), [email protected] (H. Reis). http://dx.doi.org/10.1016/j.matdes.2016.11.077 0264-1275/Published by Elsevier Ltd. Contents lists available at ScienceDirect Materials and Design journal homepage: www.elsevier.com/locate/matdes

Transcript of Materials and Design...thin elastic films such that mode-I crack growth (i.e., K II =0)exists along...

  • Materials and Design 116 (2017) 609–615

    Contents lists available at ScienceDirect

    Materials and Design

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    Spiral cracking pattern in asphalt materials

    Behzad Behnia a,⁎, William G. Buttlar b, Henrique Reis ca Department of Civil and Environmental Engineering, Western New England University, Springfield, MA, USAb Department of Civil and Environmental Engineering, University of Missouri, Columbia, MO, USAc Department of Industrial and Enterprise Systems Engineering, University of Illinois, Urbana, IL, USA

    H I G H L I G H T S G R A P H I C A L A B S T R A C T

    • 3D spiral-shaped fracture pattern wasdiscovered in a biaxially stressed layerof asphalt material bonded to alumi-num substrate.

    • A logarithmic spiral model was selectedto mathematically represent three-di-mensional spiral cracks.

    • The spiral tightness parameter, “b”, wasused in characterization of spiral cracksin different asphalt materials.

    • Shape of spiral cracks was independentof thickness and shape of samples andinfluenced by fracture properties of as-phalt materials.

    • The embrittlement temperatures andfracture energies of asphalt materialswere consistent with correspondingcharacteristic parameters of spiralcracks.

    ⁎ Corresponding author.E-mail addresses: [email protected] (B. Behnia

    (W.G. Buttlar), [email protected] (H. Reis).

    http://dx.doi.org/10.1016/j.matdes.2016.11.0770264-1275/Published by Elsevier Ltd.

    a b s t r a c t

    a r t i c l e i n f o

    Article history:Received 27 July 2016Received in revised form 20 November 2016Accepted 21 November 2016Available online 24 November 2016

    The present work for the first time reports observations and modeling to characterize three-dimensional spiral-shaped fracture patterns in a bi-axially stressed layer of asphalt material bonded to an aluminum substrate. Fivedifferent asphaltmaterials with different fracture characteristics are investigated. A logarithmic spiralmodel wasfound tomathematically represent the 3Dhelix-shaped cracks observed. A spiral tightness parameter is proposedfor the characterization of spiral fracture patterns in asphalt. Results of acoustic emission and compact tensiontests are also presented and employed in the evaluation of observed spiral cracks. The shape of spirals arefound to be influenced by the fracture properties of the asphalt materials tested and appear to be independentof the thickness and shape of the test sample. The embrittlement temperature and fracture energy of tested as-phalt materials were found to correspond to the characteristic parameters of spiral cracks.

    Published by Elsevier Ltd.

    Keywords:Asphalt materialsSpiral cracking patternAcoustic emission testCompact tension testEmbrittlement temperatureSpiral tightness parameter

    ), [email protected]

    1. Introduction

    As a viscoelastic heterogeneous composite with complex thermo-rheological properties, asphalt materials may experience crackingupon rapid cooling. Thermal cracking, a.k.a. low temperature cracking,

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  • 610 B. Behnia et al. / Materials and Design 116 (2017) 609–615

    is a major form of deterioration in asphalt roads built in regions withcold climates. As a result, a number of studies have been conducted inan effort to experimentally characterize and control asphalt propertiesrelated to the low temperature performance of asphalt pavements.

    While linear crack patterns are commonly reported in asphalt mate-rials subjected to tensile stresses, spiral cracking patterns have neverbeen reported for this material. The present work reports on the mech-anisms and characterization of a unique type of low temperature crack-ing pattern consisting of spiral-shaped cracks, observed in biaxiallystressed layer of asphalt bonded to aluminum substrate, see Fig. 1.

    As a fascinating class of fracture patterns, spiral cracks and the mys-tery of their origin have occupied the thoughts of researchers from var-iousfields for a long time. Spiral cracking patterns have been reported inother materials including thin brittle adhesive layers bonding glassplates together [1,7], inside the delaminated areas of drying precipitatesof different compounds, including nickel phosphate, ferric hydroxide[12,14], inside silicate sol-gel films [13], and inside thin films of Mo/Simultilayer systems [9,10].

    What makes this study different from all previously reported casesof spiral cracks in other materials is that all previous cases were two-di-mensional spirals developed in a thin film of materials, whereas the ob-served spiral fracture pattern in asphalt is a three-dimensional, helix-like crack formed in a relatively thicker layer of asphalt material (3, 6,and 10 mm thick), adding the third dimension (height) to the crackingpattern. The orthogonal projection of the 3D helix-shape cracks on theasphalt-aluminum interface plane is a 2D spiral in shape. This study pre-sents a quantitative as well as qualitative interpretation of the observedspiral fracture pattern in asphalt materials. Characteristic parameters ofspiral cracks are determined for five different asphalt materials andcompared against the embrittlement temperatures and fracture ener-gies of those materials obtained from acoustic emission (AE) and com-pact tension [C(T)] tests, respectively.

    2. Experimental procedure

    The following five different asphalt materials with different Perfor-mance Grades (PG), i.e. PG58-16, PG64-16, PG64-22, PG70-22, andPG58-28 were utilized in the present study. The standard notation forPG grading system for asphalt materials is PG XX–YY, where XX (a.k.a.PG high temperature) is the average seven daymaximumpavement de-sign temperature and YY (a.k.a. PG low temperature) is the minimumpavement design temperature. Asphalt samples used in this experimentwere prepared using aluminum molds with Teflon tape wrappedaround them as a debonding aid, placed on a clean, untreated aluminumsubstrate plate. A 10 mm thick aluminum plate was used as the sub-strate. To ensure proper bonding between the asphalt material and alu-minum substrate, asphalt heated to 135 °C was poured into the

    Fig. 1. Typical spiral cracking pattern observed in asphalt materials bounded to aluminumsubstrate.

    preheated aluminum mold and plate assembly. Samples were allowedto cool slowly at room temperature (~20 °C) for 1 h. The dimensionsof the beam-shaped asphalt samples bonded to the aluminum substrateis schematically presented in Fig. 2.

    Prepared asphalt samples on aluminum substrate were positionedinside a ULT-25 freezer and cooled from 20 °C to −50 °C at an averagerate of−2 °C/min. The average coefficient of thermal contraction of as-phalt binders (aAsphalt = 300 × 10−6 1/oC) is about 15 times greaterthan that of aluminum material (aAluminum = 20 × 10−6 1/oC). As a re-sult, as the asphalt sample cools down, differential thermal contractionbetween the aluminum substrate and asphalt material induces progres-sively higher tensile stresses within the asphalt layer, resulting in theformation of straight, channeling thermal cracks with regular spacing.The transversely-oriented channeling cracks subdivide the beam-shaped sample into a series of prism-shaped fragments (typicallyseven segments are formed for this geometry). As the temperature con-tinues to drop, asphalt fragments develop equi-biaxial in-plane tensilestresses that eventually lead to the formation of spiral cracks withinthem. It should be noted that the spiral cracks within asphalt sampleswere hidden until the asphalt specimens were opened for examinationat the end of the test. Upon opening of each asphalt fragment, an in-ward-growing spiral crack which had propagated for a number of revo-lutions towards the fragment center was observed.

    The shape of observed spiral fracture patterns was analyzed and amathematical model was selected to represent them. In addition, twoasphalt performance tests (i.e. acoustic emission test and compact ten-sion test) were also conducted to further quantify the spiral crackingpatterns and to link their characteristic parameters to other importantlow temperature cracking properties of asphalt materials such as frac-ture energy and embrittlement temperature.

    2.1. Acoustic emission (AE) test

    Acoustic emission tests were performed to assess the low tempera-ture cracking behavior and the corresponding “embrittlement tempera-tures” of asphalt materials. As the temperature of an asphalt sampledecreases, progressively higher thermal stresses in the binder eventual-ly result in formation of thermal cracks, which are accompanied by therelease of mechanical elastic strain energy in the form of transient me-chanical waves. This manifests itself as a cluster of high amplitudewaves during the test. The temperature corresponding to the AE eventwith the first peak energy level has been termed the “embrittlementtemperature”which is considered as the onset of damage in asphaltma-terial [3,4,16]. The greater the low temperature cracking resistance ofasphalt materials, as would be expected with ‘softer’ asphalt gradesintended for colder climates, the lower its embrittlement temperature.

    To perform the AE test, 6 mm thick beam-shaped asphalt samplesbonded to aluminum substrates (as previously described) were usedas testing specimens. Again, samples were cooled from 20 °C to−50 °C at the rate of −2 °C/min. A K-type thermocouple placed adja-cent to the sample at the interface of asphalt and substrate was usedto record the sample temperature. Acoustic activities of the sampleswere monitored during the tests and recorded using wideband AE pie-zoelectric sensors (Digital Wave, Model B1025) with a nominal fre-quency range of 50 kHz to 1.5 MHz, Fig. 3. Details regarding the AEtesting setup and signal processing can be found in Behnia et al. [6]and [4].

    Fig. 2. Beam-shaped layer of asphalt sample.

  • Fig. 3. Schematic illustration of acoustic emission testing for asphalt samples usingpiezoelectric sensors and K-type thermocouple [5].

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    2.2. Compact tension [C(T)] test

    Compact tension testing was performed in accordance with ASTME399-05 to evaluate the low temperature fracture energy of the asphaltbinders used in this study. The geometry and dimensions of the C(T) as-phalt specimens are depicted in Fig. 4(a). The C(T) testswere conductedby applying a tensile load to loading holes and measuring the crackmouth opening displacement (CMOD) using a clip-on gauge as shownin Fig. 4(b). The C(T) samples were fabricated by pouring 135 °C asphaltin to the prepared C(T) silicon rubber mold. The compact tension testswere performed at −22 °C by applying a closed-loop controlledCMOD loading at a rate of 0.2 mm/min measured with a 1 kN loadcell. The fracture energy (Gf) of asphalt materials, which is defined asthe energy required to generate a unit cracked surface area, was calcu-lated by dividing the calculated area under the load-CMOD curve bythe area of the fractured surface.

    3. Spiral cracking mechanism in asphalt material

    At low temperatures, a brittle layer of asphalt material under tensilestress usually fails through fracture and/or delamination [8]. In the pres-ent study, initially when asphalt samples were cooled down, due to thethermal contraction mismatch between asphalt layer and aluminumsubstrate, tensile stresses built up within the sample. When the ther-mally-induced stresses exceeded the local tensile strength of the mate-rial, transversely-oriented straight channeling cracks begin to developin the asphalt layer. Ultimately, an array of through-thickness uniformlyspaced parallel channeling crackswas observed in the sample. Channel-ing cracks such as these are also known as “mud cracks”, see Fig. 5. Mudcracks subdivide the asphalt sample in to several prism-shaped frag-ments. Straight mud cracks continue to form until some characteristiccrack spacing is achieved. The characteristic crack spacing is obtained

    CMOD

    (a)

    Fig. 4. Compact tension test: (a) Geometry and dimens

    when the fragment dimensions become small enough such that thereis not sufficient stored strain energy available to propagate anotherthrough-thickness straight mud crack. Our observations showed thatfor asphalt material, the characteristic crack spacing (fragment length)is approximately three times the asphalt layer thickness.

    The formation of straight through-thicknessmud cracks temporarilyrelieves tensile stresses in the sample. However, as the specimen con-tinues to cool down, the biaxial in-plane tensile stresses will continueto increase in magnitude within the prism-shaped fragments of asphaltmaterial. However, due to the small size of the fragments, there is notsufficient energy available to propagate more through-thickness mudcracks within fragments. Instead, spiral cracks begin to nucleate at ornear the fragment edges and then spiral inward towards the center ofthe fragment. Thermally-induced stresses are concentrated at the inter-face. Therefore, spiral cracks begin to propagate at the interface withabout 50% penetration depth into the asphalt layer thickness. It was ob-served that as the spiral crack propagates towards the center of the sam-ple, the penetration depth of the crack gradually decreases from 50% atnear the edges to almost 0% near the fragment center. This can be linkedto the gradual reduction in stored strain energy within the fragment asthe crack front gets closer to the center of the sample. Creation of newfractured surfaces requires energy. The penetration depth of crack, i.e.the size of new fractured surfaces, is proportional to the amount ofavailable stored strain energy within the sample. At the beginning,when the stored strain energy in the fragment is maximum, the spiralcrack initiates at the interface penetrating upward to about half of thesample thickness. However, as the crack advances from the edge to-wards the center of the fragment, stored strained energy is gradually di-minished to create new surfaces. Therefore less stored energy would beavailable to overcome the fracture resistance and form new fracturefaces which leads to a gradual reduction in the penetration depth ofthe spiral crack until it finally reaches almost zero at the center of sam-ple. Fig. 6 schematically shows the three-dimensional spiral crackingpattern with the gradual reduction of crack penetration depths fromhalf the thickness at the edge to zero in the center of the sample.

    Fracture mechanics-based studies of cracking patterns in biaxiallystressed films has analytically proven the existence of spiral cracks inthin elastic films such that mode-I crack growth (i.e., KII = 0) existsalong the crack trajectory. In the case of a spiral cracking pattern, thecrack preferentially moves along a curved path to maximize the storedstrain energy release rate [7]. According to the principle of local symme-try in fracture mechanics, crack propagation in an isotropic, homoge-neous material occurs in such a way that the Mode II crack intensityfactor is zero (i.e., KII = 0). Xia and Hutchinson presented a two-

    gauge

    (b)

    ions of the C(T) specimen, (b) C(T) testing setup.

  • AsphaltStraight Channeling Cracks

    (Mud Cracks)

    Spiral Crack

    h

    Fig. 5. Array of straight channeling cracks (mud cracks) in an asphalt layer accompanied by formation of spiral cracks within each fragment.

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    dimensional model of thin elastic film bonded to an elastic substrate tosimulate the crack propagation path within a thin elastic layer. Theyprovided a theoretical explanation for the existence of spiral crackingand explained the spiral cracking phenomena in terms of the crack in-teraction and fracture crackingmode-mixity effects [15]. It was demon-strated that a spiral cracking pattern represents the crack trajectorywith maximum energy release rate [15].

    4. Mathematical representation of spiral cracks

    The cracking pattern within each asphalt fragment was observedto have a three-dimensional helix shape, see Fig. 7(a), upon removalof the top of the asphalt fragments from the substrate. After scrapingaway the helix material with a spatula while the binder is still coldand brittle, very clear and visible deposit remains on the aluminumsurface. This deposit is in the form of two-dimensional spiral, Fig.7(b). In other words, the observed 2D spiral cracking pattern onthe aluminum plate shown in Fig. 1, was in fact the ‘footprint’ or pro-jection of the 3D helix-shaped crack on the asphalt-aluminum inter-face plane.

    The spiral cracking patterns were digitally photographed andthen analyzed to explore possible mathematical models to representthem. It was found that the logarithmic spiral function, also knownas the equiangular spiral, provides an excellent fit to the experimen-tally observed spiraling deposit patterns. The mathematical repre-sentation of the logarithmic spiral in Cartesian as well as cylindricalcoordinate systems is presented in Eqs.uations (1) and (2), respec-tively, where “A” and “b” are logarithmic spiral parameters with

    (a)

    Unwrap

    Direction of crack propag

    Crack penetration d(0 D h/2)

    Fig. 6. Visualization of spiral crack formation: (a) Three-dimensional representation of spiral cdenotes the asphalt layer thickness; (b) Simplified unwrapped shape of 3D spiral crack withinand zero at the center of the sample.

    constant values, r(θ) is the distance from the spiral origin, and θ isthe angle from the x-axis [11].

    P r; θ; Zð Þ�����! ¼ Aebθ cos θð Þ i!þ Aebθ sin θð Þ j!þ θ2θ f

    h k! ð1Þ

    r θð Þ ¼ Aebθ; Z θð Þ ¼ θ2θ f

    h ð2Þ

    Parameter “A” is the apparent length scale and parameter “b” is thespiral tightness parameter which controls how tightly and in which di-rection spiral is wrapped. The sign of “b” determines whether the spiralis clock-wise (b b 0) or counter clock-wise (b N 0). When b = 0, spiralbecomes a circle of radius “A”. On the other hand, when “b” approachesinfinity, spiral turns in to a straight half-line. Fig. 8(a) depicts themath-ematical definition of “b”where φ is the constant pitch angle of the spi-ral. In general, the lower the “b” value, the tighter the spiral, whichmeans more crack revolutions within the spiral. Fig. 8(b) schematicallyshows two logarithmic spiral cracks formed in the same size fragmentswhere the overall dimensions of two spirals are approximately thesame; however, spiral #2 is much tighter than spiral #1 with morecrack revolutions. The tighter the spiral, the lower the angle φ, whichleads to a lower spiral “b” value (i .e.,b1Nb2).

    5. Results and discussion

    Themathematical model for the logarithmic spiral was employed tocharacterize spiral cracks in five different asphalt materials with

    (b)

    spiral ation

    epth

    rack in asphalt material with varying penetration depth ranging from h/2 to 0, where “h”the asphalt fragment with the highest crack penetration depth of h/2 (50%) at the edge

  • (a)

    2D deposit patterns

    3D Helix

    Projection of 3D

    &

    crack on XY

    (c)

    (b)

    Fig. 7. Geometry of three-dimensional spiral cracks; (a) Three-dimensional helix-shaped crack within asphalt layer (b) Remains of 3D helix-shaped crack on the asphalt-aluminuminterface plane in the form of two-dimensional spiral crack (c) Schematic depiction of 3D spiral crack in cylindrical coordinate and its projection on XY plane in the form of 2D spiral.

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    different Performance Grades (PG). Fig. 9 shows a typical characteristicfit of a two-dimensional spiral crack trajectory in polar coordinates forasphalt materials using the ln(r(θ))=bθ+ ln(A) equation, where θcan take any value between 0 and θf (0≤θ≤θf) and is not restricted to[0,2π]. The final angle (θf) is the angle corresponding to the outmostpoint of spiral in the sample, Fig. 7(c). The slope of the linear fit in themathematical model represents the tightness parameter, “b”, of thespiral.

    The embrittlement temperatures and the fracture energies of as-phalt materials were determined through conducting AE and C(T)tests, respectively. Table 1 summarizes the measured spiral parametersof cracks in 6 mm thick beam-shaped samples for five different asphaltmaterials alongwith AE embrittlement temperatures of thosematerials.In addition, fracture energies of three asphalt binders (PG64-22, PG70-22, and PG58-28) are also presented in Table 1. Each spiral parameter

    (a)

    Fig. 8. (a) Concept of spiral pitch angle (φ) and the formula to calculate the spiral tightness pparameters (b1Nb2), displaying effect of parameter “b” on shape and number of crack revolutio

    and the embrittlement temperature listed in Table 1 is the average ofsix test replicates. For the fracture energy results, four replicates C(T)testswere tested for eachmaterial and the average fracture energy is re-ported in Table 1.

    At the first glance, the overall shape of spiral cracking patterns fordifferent asphalt materials may appear to be almost the same, howeveranalyses showed that the shape of the spirals were influenced by thematerial properties. The spiral tightness parameter and hence the num-ber of crack revolutions in each deposit patternwere different for mate-rials with different viscoelastic and cracking characteristics. The spiraltightness values measured in 6 mm thick beam-shaped samples for dif-ferent asphalt materials were found to be in the range of 0.0421 to0.0447. Comparison of “b” values of asphalt materials shows that thePG58-28 asphalt has the lowest “b” value, followed by PG70-22 as com-pared to those of other asphalt materials. This demonstrates that spiral

    (b)

    1 2

    arameter, “b”, (b) Comparison between two logarithmic spirals with different tightnessns within spiral.

  • Table 1Characteristic parameters of spiral cracks from 6 mm thick beam-shaped samples for fivedifferent asphalt materials: PG56-16, PG58-28, PG64-16, PG64-22, and PG70-22, alongwith their AE embrittlement temperatures and C(T) fracture energies.

    Asphaltmaterial

    Spiral parameters AEembrittlementtemp (°C)

    Fracture energy @−12 °C (J/m2)

    b Cov% A(mm)

    φ(°)

    PG58-16 0.0447 3.29% 0.62 2.56 −29.26 –PG64-16 0.0443 5.87% 0.49 2.54 −28.01 –PG64-22 0.0444 1.34% 0.66 2.54 −31.76 3.10PG70-22 0.0429 4.72% 0.56 2.46 −32.36 7.50PG58-28 0.0421 2.67% 0.55 2.41 −35.78 13.10

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    cracks developed in PG58-28 and PG70-22 materials are tighter inshape and possess a higher number of crack revolutions within the spi-ral. This can be linked to the fact that both aforementioned asphalt ma-terials have higher resistance against low temperature cracking. In thecase of PG58-28, this was the softest binder tested, as evidenced bythe−28 low temperature grade. In the case of PG70-22, a styrene-buta-diene-styrene (SBS) polymer was present, providing additional resis-tance against low temperature cracking as compared to the PG64-22grade. As discussed, spiral cracks choose their trajectory to maximizethe stored energy release rate. The orientation of the crack front is con-stantly bending away from the instantaneous direction of propagation(spiral pitch angle) such that the Mode II crack intensity factor remainszero (i.e., KII = 0). Higher resistance of thematerial to fracture makes itmore difficult for the crack front to deviate from its instantaneous direc-tion of propagation, which results in lower spiral pitch angle (φ), andconsequently lower “b” (b = tan (φ)), as compared to a material withlower fracture resistance.

    The AE and C(T) test results were used to assess low temperaturefracture resistance of tested asphalt materials in micro- and macro-scales, respectively, and to help better understand the observed differ-ent spiral patterns in different asphalt materials. The embrittlementtemperatures (TEMB) and fracture energies of the five asphalt materialstested were found to be consistent with the spiral tightness parameter.Analysis of the asphalt embrittlement temperature data shows that thePG58-28 binder exhibited the lowest TEMB followed by PG70-22, whichindicates that PG58-28 has the highest resistance against microcrackingat low temperatures amongst all tested binders. The C(T) fracture ener-gy results also showed the same trendwhere the highest fracture ener-gy belonged to PG58-28 followed by PG70-22.

    The spiral crackingpattern dependence upon the asphalt layer thick-ness and the shape of asphalt sample were investigated by comparingthe parameters of spiral cracks developedwithin asphalt samples of dif-ferent shapes and thicknesses. To explore the thickness effect, beam-shaped sampleswith two different thicknesses (3 and 6mm)were pre-pared and examined. The sample shape effect was explored by compar-ing the spiral cracking pattern of beam-shaped samples and those ofdeveloped within 10 mm thick 25 mm diameter cylindrical asphaltspecimens. Table 2 lists spiral parameters for 3 mm thick beam samplesas well as cylindrical samples. Each spiral parameter presented in Table2 is the average of six test replicates. Fig. 10 presents and compares the“b” values of all three different geometries of five different asphaltbinders. It is observed that for each asphaltmaterial, the variation in spi-ral tightness parameter values, “b”, of spirals developed in samples withdifferent thicknesses and shapes is negligible, which indicates that thespiral cracking pattern in the five asphalt binders studied was indepen-dent of the asphalt layer thickness and shape of the sample. This results

    Fig. 9. Typical plot of characteristic fit for spiral crack trajectory in polar coordinates forPG58-16 asphalt material.

    suggests that material properties, such as fracture characteristics andviscoelastic properties of the asphalt binder are fundamentally tied tothe spiral cracking patterns observed, as characterized by the parameter“b”.

    6. Concluding remarks and recommendations

    The formation of three-dimensional spiral fracture patterns in as-phalt binder samples at low temperatures has been presented andmathematically characterized. Five different asphalt materialsencompassing a range of fracture characteristics were utilized in thisstudy. It was observed that as beam-shaped asphalt samples are cooleddown, primary fragmentation occurs first subdividing the sample intoseveral prism-shaped fragments. The fragmentation is then followedby the formation of inward-growing helix-shaped cracks within eachbi-axially stressed fragment at lower temperatures. A logarithmic spiralshapewas selected for themathematical representation of the observedspiral cracks in asphalt binders, and a spiral tightness parameter, “b”,which controls the overall shape of the spiral, was used to characterizethe spiral cracks in the different asphalt binders.

    It was observed that spiral cracks propagate in the direction of max-imum stress relief, where the constant pitch angle (φ) of the spiral indi-cates that the orientation of the maximum stress relief keeps bendingaway from the instantaneous direction of propagation. It was also ob-served that asphalt materials with higher fracture resistance (e.g.,PG58-58), encountered tighter spiral cracks with higher number ofcrack revolutions (i.e., possessed a lower “b” value).

    Two binder performance tests (acoustic emissions and compact ten-sion) were conducted to evaluate low temperature cracking resistanceof five asphalt binders at micro- and macro-levels. The AE embrittle-ment temperatures and C(T) fracture energy test results were in agree-ment with the spiral cracking tightness parameter “b”. These resultssuggest that the shape of spiral cracks in asphalt binders are influencedby the low temperature fracture characteristics of the material, and arelargely independent of the thickness and shape of the asphalt test sam-ples. As a consequence, the shape of the developed spiral cracks in as-phalt materials appears to have the potential to be used in thecharacterization of their low temperature fracture resistance.

    Table 2Characteristic parameters of spiral cracks for five different asphaltmaterials in 3mm thickbeam-shaped samples as well as 25 mm diameter 10 mm thick cylindrical samples.

    Material Spiral parameters3 mm thick beam 25 mm diameter cylinderb A (mm) φ (°) b A (mm) φ (°)

    PG58-16 0.0445 0.65 2.55 0.0446 1.88 2.55PG64-16 0.0442 0.51 2.53 0.0441 1.94 2.53PG64-22 0.0440 0.57 2.42 0.0446 2.04 2.55PG70-22 0.0430 0.58 2.46 0.0431 2.18 2.47PG58-28 0.0411 0.53 2.35 0.0423 2.08 2.42

  • Fig. 10. Comparison of spiral tightness parameters of different asphalt materials sampleswith different shapes and thicknesses.

    615B. Behnia et al. / Materials and Design 116 (2017) 609–615

    The difference between the thermal contraction coefficients of as-phalt and the substrate material influences the magnitude of thermal-ly-induced stresses as well as the amount of stored strain energywithin the asphalt sample, i.e. the higher the thermomechanical mis-match between asphalt and the substrate, the higher the amount ofstored strain energy and the thermal stresses in the sample. Storedstrain energy affects the driving force of the crack front. As such, changein the magnitude of stored strain energy would influence the overallshape of the spiral pattern in asphalt sample. Considering the impor-tance of the thermomechanicalmismatch between asphalt and the sub-strate material, for future studies it is recommended to investigate thespiral cracking pattern in asphalt using other substrate materials suchas granite or steel.

    While the results of this investigation appear promising, furtherstudies should be performed to explore and establish the relationshipbetween the spiral crack tightness parameter and the fracture mechan-ics parameters such as fracture energy and fracture toughness aswell asrheological parameters such as the glass transition temperature and

    embrittlement temperature of asphalt materials. In addition, links be-tween spiral cracking parameters and other binder parameters fromthe SUPERPAVE performance tests such as Bending Beam Rheometer(BBR), Dynamic Shear Rheometer (DSR), and Rotary Viscometer (RV)tests should be investigated.

    References

    [1] A.S. Argon, Distribution of cracks on glass surfaces, Proceedings of the Royal Societyof London A: Mathematical, Physical and Engineering Sciences 250 (1263) (1959)482–492.

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    Spiral cracking pattern in asphalt materials1. Introduction2. Experimental procedure2.1. Acoustic emission (AE) test2.2. Compact tension [C(T)] test

    3. Spiral cracking mechanism in asphalt material4. Mathematical representation of spiral cracks5. Results and discussion6. Concluding remarks and recommendationsReferences