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T.E. LABORATORIES LI Trading as

Loughmartin Business low, Co.

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Page 2 of 3

ANALYSIS OF AQUEOUS SAMPLE.

Date Sampled: 22/11/2018 Date Rec'd: 23/1 f/2018 Date Analysis Commenced: 23/1 Our Ref: WS-46590 & 18-27894 Certificate No. L/18/1859

unless stated otherwise

Note 1 : Subcontracted due to inst

= INAB Accredited Tests ++ = Su = Non-INAB Accredited 'Pests

The above results relate only to the sample ith the consent of T.E. Laboratories Ltd.

I .E. Laboratories

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EPA Export 16-02-2019:03:53:06

LQ-E004/DG01 a Issue No.21

TelLab Issue Date: 29.1 1.2018 Issued By: Anna Karabin

1 Appendix to results

TERMS AND CONDITIONS

1 All reports issued by T.E. Laboratories Ltd. are copy right and shall not be used either in whole or in part for the purposes of advertising, publicity or litigation without the written consent of a director of T.E. Laboratories Ltd.

2 If copied, reports shall only be reproduced in full and with the consent of T.E. Laboratories Ltd.

3 No action or legal proceedings shall be taken (except in the case of wilful neglect or default) against T.E. Laboratories Ltd. or any employees or representatives of the company by reason of or arising out of the carrying out of any research, investigation, test or analysis or the publication of results thereof by or in the name of T.E. Laboratories Ltd. and furthermore no responsibility is accepted by T.E. Laboratories Ltd. to any third party in sespect of any information, report or results compiled as a result of the carrying out of any research, investigation, test or analysis by or on behalf of T.E. Laboratories Ltd. and any third party relying on such information does so at their own risk absolutely.

4 Samples received for testing shall be disposed of after testing unless instructions to the contrary have been notified by the sender at time of placing of order.

5 Non-perishable samples received for testing or laboratory work shall be disposed of after one month from the date of reporting results unless instructions to the contrary have been notified by the sender at time of placing of order.

6 The total liability of T.E. Laboratories Ltd. for loss or damage, caused by or resulting from improper or purported performance or non-performance of work shall not exceed a sum equal to that period for the work.

7 This report sets out the results of the analysis of the samples specifically referred to in it. T.E. Laboratories Ltd. ("TelLab) warrants that the results as stated are accurate in so far they relate to that sample as received in the TelLab laboratory, TelLab accepts no other liability or responsibility to any party whatsoever. In particular, but without prejudice to generality of the foregoing, TelLab shall have no liability or responsibility whatsoever in respect of or in any way by reference to:

a The taking of the sample, the accuracy of the sample or its suitability for the purpose(s) for which taken or applied, the designation, handling, storage or transport of the sample prior to its delivery to the TelLab laboratory or its condition upon such delivery.

b The interpretation of this report and/or the application of the results as stated andlor the accuracy and reliability of any advice based thereon; and

c Any (or any alleged) lack of competence, negligence, failure or breach of duty on the part of any person engaged in or responsible for any of the activities or functions referred to above, whether or not such agent is described as an Agent of TelLab or otherwise. All such persons shall be deemed to be agents of the person to whom this report is issued and not to be agents or representative in any capacity of TelLab.

8 In the event of any claim arising against TelLab, TelLab expressly excludes liability for any consequential loss or damage or any loss values, profit, business revenue, goodwill, yields, production or anticipated savings which may arise in respect of or in any way by reference to any report, analysis, advice or information given orally by any person or contained in any report leaflet, book, pamphlet, brochure or other document, whether prepared, published or issued by TelLab or otherwise.

9 T.E. Laboratories Ltd. terms and general conditions of sales shall apply to all work carried out (available on request).

10 The laws of the Republic of Ireland will apply to any matters in relation to this report.

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EPA Export 16-02-2019:03:53:06

LQ-E004/DG01 a Issue No.21

Ammonia as NH4 Ammonia as N Cadmium Calcium

Issue Date: 29.11.2018 Issued By: Anna Karabin

Spectrophotometric

Direct aspiration/flame AAS Ion Chromatorrraphv

TelLab 8

Chloride Chromium ,:

Methods of analysis INAB Accredited tests

~ ~~

Ion chromatography Direct aspiration/flame AAS

pm- TECHNIQUE

Conductivity Copper

Elec trometry Direct asr?iratiodflame AAS

Iron Lead Magnesium

/Cobalt IDirect aspiratiodflame AAS

~

Direct aspiratiodflame AAS Direct aspiratiodflame AAS Ion Chromatorrraphv

/COD IDigestion/colorimetric

Manganese Nickel Nitrate Nitrate as N

Direct aspirationhlame AAS Direct aspiratiodflame AAS Ion chromatography

IFluoride Ikon chromatorrraDhv

Nitrite Nitrite as N Orthophosphates Orthophosphate as P

PH Potassium Sodium Sulphate Suspended Solids TON Total Hardness

Ion chromatography

Ion chromatography

Hydrogen ion selective electrode Ion Chromatography Ion chromatograohy Ion chromatography Gravimetric Sum of Nitrate & Nitrite Calculation based on Calcium &

Total Phosphorous Zinc

Digestion/ Spectrophotometric-- Direct aspiratiodflame AAS

IMamesiuni results

DETECTION 1 METHOD LIMIT REFERENCE

0. 1Oppm as NH4 TP012 0.08ppmasN 1

0.03 ppm TP001 2.5 ppm TP004 - 0 .5mm I TP002

5uSlcm 6.3 20°C I TP005

0.20 ppm TPOO 1 1 ppm TP004

0.03mm 1 TPOOl 0.10 ppm TPOOl 0.5 ppm TP002

0.2 ppm TP002 0.06 tmm 1.0 ppm TP002

0.33 tmm I L I

2- 12 pH Units 1 TP003 1 m m 1 TP004

TP004 0.25 ppm TP002

TPO 15

0;OSppmasP 1 TPOll 0.01 ppm TPOO 1

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EPA Export 16-02-2019:03:53:06

LQ-E004/DG01 a Issue No.21

Issue Date: 29.1 1.2018 Issued By: Anna Karabin

Methods of analysis NON-INAB Accredited tests

DETERMINAND TECHNIQUE

Acid Soluble Alkali Calculation

Alkalinity Titration

Aluminium ICP-MS (Unless specified

- BOD D 0 Probe Chlorine (total) Colorimetry Chlorine (free) Colorimetry Chlorine ( residual) Difference of Total C12

and Free Cl?

I O Our

Photometry

Icon duc t ivi ty Electrometry

IDetergents as MBAS Colourimetry

IGravimetric lDensity Dissolved oxygen D 0 Probe Dissolved Organic Heated-Persul fate Carbon Oxidation Dry residue (at 180 C) Fats Oils and Grease Fats Oils and Grease

Gravimetric Partition Gravimetric Soxhlet / gravimetric

IHexavalent Chromium IColorimetry

Kjeldahl Nitrogen Digestion/ Distillation/

Moisture content Loss on drying at 105C

DETECTION METHOD LIMIT REFERENCE 0.001 YO In house

5 ppm SMEWW 2320B

lOppb SMEWW 3125 ICP-

0.01 ppm SMEWW 4500-NH31 -+----- Method 10023 2 ppm 0 2

0.05 ppm DPD Method 0.05 ppm DPD Method

SMEWW 52 1 OB

2 Pt-Co Units APHA Platinum-Cobalt IStandat-d Method I .-

1 yS/cm@ lTPOO5 20°C I

0.2 ppm SMEWW 5540C

g/cm3 In-house

1 tmm ISMEWW 2540 C 2 ppm ISMEWW 5520B 0.01%

0.01 ppm SMEWW 3500-Cr D

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EPA Export 16-02-2019:03:53:06

LQ-E004/DG01 a Issue No21

Issue Date: 29.1 1.2018 Issued By: Anna Karabin

TeI Methods of analysis

DETERMINAND TECHNIQUE DETECTION METHOD NON-INAB Accredited tests (contd)

LIMIT REFERENCE Nitrite (low level) Colourimetry 0.03 ppm Method 8507

pH (soils) Hydrogen ion selective 2-12 pH Units TP003

Phenols Distillation / Colourimetry O.05ppm SMEWW 5530 D

Phosphate (low level) Colourimetry 0.01 ppm SMEWW 4500-P E Phosphate (MW) 6: Colourimetric O.05ppm Method 8190 Sulphide Colorimetry 0.01 ppm In house

electrode

Solids, Volatile Ignition 1PPm SMEWW 2540E {% Organic Matter) SMEWW 25406 Settleable Solids Gravimetric 1 ppm SMEWW 2540F

9'0 Dry Solids Gravimetric 0 Yo SMEWW 2540B

'I'eiiiperature "C Oiisite thermocouple 0-50 "C Direct measurement ___

Total Cyaiiide Distillation / Colourimetry 0.01ppm SMEWW 4500CN C&E __. -

'I'o&3rganic Carbm heated-Persulfate Oxidation 0.25 ppm SMEWW 53 1OC L I I I Il'urbidity IAtteiiuated Radiation Method I 2 FTU IAdapted form IS0

method 7027 b a l Viable Count k u r Plate Method 1 cfu/inl SMEWW 9215B p i r o c o c c i Membrane Filtration 1 cfk / loom1 SMEWW 9230 C

l ~ o r j l coliforms T s m b r a n e Filtration 1 cfu / 1OOml SMEWW 9222B

jTTaeca1 Coliforms /Membrane Filtration 1 cfu / 1OOml SMEWW 9222D --+ I

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