Laboratory rpt, Alenaio Stream sludge, sample collected 1 ...

SDMSDocID 2024201

2024201

Environmental Laboratory of the Pacific Date: 17-Jan-OI

CLIENT:Project:Lab Order:

Date Received:

PENCOAlenaio Stream Sludge0101010

1/3/2001

Work Order Sample Summary

Lab Sam pie ID Client Sample ID0101010-01A Alenaio 1

Collection Date Sample On Hold1/2/2001 11:00:00 AM Q

Environmental Laboratory of the Pacific Date;CLIENT: PENCO

Project: Alenaio Stream Sludge CASE NARRATIVELab Order: 0101010

Samples were analyzed using the methods outlined in the following references:

Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, 3rd Edition.

All method blanks, laboratory spikes, and/or matrix spikes met quality assurance objectives.

The reporting limit was raised for method 8270 to dilution required to minimize matrix interferences.

Q01: The spike recovery for this QC sample is outside of established control limits. Review ofassociated batch QC indicates the recovery for this analyte does not represent an out-of-controlcondition for the batch.

ironmental Laboratory of the Pacific Date: Jan 17, 2001

Client: PENCO

Work Order: 0101010

Project: Alenaio Stream Sludge

Lab ID: 0101010-01A

Client Sample ID: Alenaio 1

Tag Number:Collection Date: 01/02/200111:00

Matrix: SLUDGE

Reporting Dilution Date Date BatchAnalyses

HERBICIDES, TCLP LEACHED2,4,5-TP (Silvex)

2,4-DSurr: DCAA

ICP METALS, TCLP LEACHEDArsenicBariumCadmiumChromium

LeadSelenium

Silver

MERCURY, TCLP LEACHEDMercury

PESTICIDES, TCLP LEACHEDChlordane

r~ '-'na-BHC

hepfachlor

Heptachlor epoxide

MethoxychlorToxaphene

Surr: Decaohlorobiphenyl

Surr: Tetrachloro-m-xylene

Result

ND

ND

76.1

ND

ND

NDND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

89.9

78.2

Limit Units Factor Prepared Analyzed ID Analyst Qual Notes

SW1311/81500.00500 mg/L

0.00500 mg/L

40-140 %REC

SW1311/6010A0.500 mg/L

1.00 mg/L

0.0500 mg/L0.0500 mg/L0.200 mg/L0.500 mg/L

0.0500 mg/L

SW1 31 1/74700.000500 mg/L

SW1311/8080A0.00500 mg/L

0.000500 mg/L

0.000250 mg/L0.000250 mg/L0.000250 mg/L

0.00250 mg/L0.0250 mg/L

50-150 %REC50-150 %REC

1 1/9/2001 1/15/2001 3178 RTK

11

1 1/8/2001 1/8/2001 3172 TKL111

1

11

1 1/8/2001 1/8/2001 3170 JYD

1 1/9/2001 1/15/2001 3179 RTK1

1

11

1

11

1

'tiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quaitfitation range

I of 2

vironmental Laboratory of the Pacific Date: Jan 17, 2001

Client: PENCOWork Order: 0101010


Lab ID: 0101010-01A

Analyses

SEMIVOLATILES, TCLP LEACHED1 ,4-Dichlorobenzene

2,4,5-Trichlorophenol2,4,6-Trichlorophenol

2,4-DinitrotolueneHexachlorobenzene

Hexachlorobutadiene

HexachloroethaneNitrobenzene

PentachlorophenolPyridineCresols, Total

Surr: 2,4,6-TribromophenolSurr: 2-FluorobiphenylSum 2-Fluorophenol

Surr: 4-Terphenyl-d14~urr: Nitrobenzene-d5

,urr: Phenol-d6

VOLATILES, TCLP LEACHED1,1-Dichloroethene1 ,2-Dichloroethane1 ,4-Dichlorobenzene2-Butanone

BenzeneCarbon tetrachloride

ChlorobenzeneChloroformTetrachloroetheneTrichloroetheneVinyl chloride

Surr: 1 ,2-Dichloroethane-d4

Surr: 4-Bromofluorobenzene

Surr: Dibromofluoromethane

Surr: Toluene-d8

Client Sample ID: Alenaio 1Tag Number:

Collection Date: 01/02/200111:00

Matrix: SLUDGE

Result

NDNDNDNDNDNDNDNDNDNDND

71.496.486.8106

95.689.8

NDNDNDND

11.9NDNDNDNDNDND117105120102

Reporting Dilution Date Date BatchLimit Units Factor Prepared Analyzed ID Analyst Qual Note;

SW1311/8270A1.00 mg/L1.00 mg/L5.00 mg/L1.00 mg/L1.00 mg/L1.00 mg/L1.00 mg/L1 .00 mg/L5.00 mg/L1 .00 mg/L1.00 mg/L

10-123 %REC

43-116 %REC21-100 %REC

33-141 %REC35-114 %REC

10-94 %RECSW1 311/8260 A

0.400 mg/L0.400 mg/L

0.400 mg/L5.00 mg/L

0.400 mg/L0.400 mg/L

0.400 mg/L0.400 mg/L

0.400 mg/L0.400 mg/L

0.200 mg/L68-144 %REC

72-140 %REC76-133 %REC

77-146 %REC

20 1/9/2001 1/11/2001 3177 MDH20202020202020202020202020202020

\^^

10 1/16/2001 1/16/2001 R8375 KAL

1010101010101010101010101010

•liners: ND - Not Detected at the Reporting Limit



* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

2 of 2

'ronmental Laboratory of the Pacific Date: 17-Jan-Ol

CLIENT: PENCOWork Order: 0101010Project: Alenaio Stream Sludge

QC SUMMARY REPORTMethod Blank

Sample ID MB-3177

Client ID:

Analyte1 ,4-Dichlorobenzene2,4,5-Trichlorophenol

2,4,6-Trichlorophenol2,4-Dinitrotoluene

HexachlorobenzeneHexachlorobutadieneHexachloroethane

NitrobenzenePentachlorophenol

Pyridine

Cresols, TotalSurr: 2,4,6-Tribromophenol

Surr: 2-Fluorobiphenyl^urr: 2-Fluorophenol

4-Terphenyl-d14cr-.i: Nitrobenzene-d5

Surr: Phenol-d6

Sample ID MB-3170

Client ID:

AnalyteMercury

Sample ID MB-3172

Client ID

AnalyteArsenicBarium

CadmiumChromium

LeadSeleniumSilver

Batch ID: 3177

Result0.00186

ND

ND

ND

ND

NDND

ND

ND

ND

ND

0.0871

0.04435

0.065440.053290.0468

0.04987

Batch ID. 3170

ResultND

Batch ID. 3172

ResultND

0.01341

ND

ND

0 02283

ND

ND

Test Code:

Run ID:

PQL DF0.010 10.010 10.050 10.010 10.010 10.010 10.010 10.010 10.050 10.010 10.010 1

0 10 10 10 10 10 1

Test Code:

Run ID:

PQL DF0.00050 1

Test Code:

Run ID:

PQL DF0.50 1

1.0 10.050 10.050 10.20 10.50 1

0.050 1

SW1311/8270A

MSD3_010111A

Spike SpikeValue RefVal

0.1 00.05 0

0.1 00.05 0

0.05 0

0.1 0

SW1 31 1/7470

MERC_010108B


SW1311/6010A

ICP1_010108C


Units: mg/L

SeqNo: 80964

%REC%REC Limits

87.1 10 12388.7 43 116

65.4 21 100

107 33 141

93.6 35 114

49.9 10 94

Units: mg/L

SeqNo: 80365

%REC%REC Limits

Units: mg/L

SeqNo: 80443

%REC%REC Limits

Prep Date 1/9/2001

Analysis Date: 1/11/2001

RPDRefVal RPD

000000

Prep Date

RPDimit Qual Note

J

1/8/2001


RPDRefVal RPD

Prep Date

RPDimit Qual Note

1/8/2001


RPDRefVal RPD

RPDImit Qual Note

J

J

•«iers: ND - Not Detected at the Reporting Limit



%REC - % Recovery

S - Spike Recovery outside established recovery limits

R - RPD outside established recovery limits

DF - Dilution Factor

RPD - Relative Percent Difference

C .NT: PENCOWork Order: 01 010 10Project: Alenaio Stream Sludge

QC SUMMARY REPG^Method Blank

Sample ID BLK011601 Batch ID: R8375

Client ID:

Analyte1,1-Dichloroethene1 ,2-Dichloroethane1 ,4-Dichlorobenzene

2-Butanone

BenzeneCarbon tetrachforideChlorobenzene

ChloroformTetrachloroethene

TrichloroetheneVmyl chloride

Surr: 1,2-Dichloroethane-d4Surr: 4-BromofluorobenzeneSurr: Dibromofluoromethane

Surr: Toluene-dS

ResultND

ND

ND

ND

ND

ND

ND

ND

ND

NDND

0.5780.55660.59280.5154

Test Code: SW1311/8260A

Run

PQL0.0400.040

0.0400.50

0.040

0.0400.0400.040

0.0400.0400.020

0000

ID: MSD1_010116A

Spike SpikeDF Value RefVal

111111111111 0.5 01 0.5 01 0.5 01 0.5 0

Units: mg/L

SeqNo: 81627

%REC%REC Limits

116 68 144111 72 140119 76 133103 77 146

Prep Date 1/16/2001


RPDRefVal RPD

0000

RPDimit Qual Note

'ifiers: ND - Not Detected at the Reporting Limit



%REC - % Recovery





vironmental Laboratory of the Pacific Date: 17-Jan-Ol

CLIENT: PENCOWork Order: 0101010Project: Alenaio Stream Sludge

QC SUMMARY REPORTSample Matrix Spike

Sample ID 0101017-01AMS Batch ID: 3170

Client ID:

Analyte ResultMercury 0.00967

Sample ID 0101017-01AMSD Batch ID: 3170

Client ID:

Analyte ResultMercury 0.00956

Sample ID 0101010-01AMS Batch ID: 3172

Client ID: Alenaio 1

Test Code:

Run ID:

PQL DF0.00050 1

Test Code:

Run ID:

PQL DF0.00050 1

Test Code:

Run ID:

SW1311/7470

MERC.010108B


0.01 0

SW1 31 1/7470

MERC_010108B


0.01 0

SW1 31 1/601 OA

ICP1JJ10108C

Units:

SeqNo:

%REC

mg/L

80368

%RECLimits

96.7 75 125

Units:

SeqNo:

%REC

mg/L

80369

%RECLimits

95.6 75 125

Units:

SeqNo:

mg/L

80454

Prep Date 1/8/2001


RPDRefVal RPD

0

RPDimit Qual Note

Prep Date 1/8/2001


RPDRefVal RPD

0.00967 1.14

RPDimit Qual Note20

Prep Date 1/8/2001


Analyte'c

L _ ,1CadmiumChromiumLeadSeleniumSilver

Result1.1081.0741.0111.01

1.0020.9756

0.09489

PQL0.50

1.00.0500.0500.200.50

0.050

SpikeDF Value

1 11 11 11 11 11 11 0.1

SpikeRefVal

00.04788

00

0.0208200

%REC111103101101

98.197.694.9

%RECLimits

80 12080 12080 12080 12080 12080 12080 120

RPDRefVal

0000000

RPDRPD Imit Qual Note

*

Sample ID 0101010-01AMSD Batch ID: 3172

Client ID: Alenaio 1

Test Code: SW1311/6010A

Run ID: ICP1 010108C

Units: mg/L

SeqNo: 80455

Prep Date 1/8/2001


inalyte ResultarsenicJariumCadmium 0Chromium.ead 0Selenium 0

1.0331.063.98920.991.9831.9886

Silver 0.09485

PQL0.50

1.00.0500.050

0.200.50

0.050

SpikeDF Value

1 11 11 11 11 11 11 0.1

SpikeRefVal

00.04788

00

0.0208200

%REC103101

98.999.196.298.994.8

%RECLimits

80808080808080

120120120120120120120

RPDRefVal

1.1081.0741.011

1.011.002

0.97560.09489

RPDRPD imit Qual Note7.031.032.181.881.9

1.330.0401

20202020202020

"Mfiers: ND - Not Detected at the Reporting Limit



%REC - % Recovery





C ,NT: PENCO

Work Order: 0101010


QC SUMMARY REPC :̂

Sample Matrix Spike

Sample ID 01 01 078-01 BMS

Client ID:

Analyte1,1-DichloroetheneBenzeneChlorobenzeneTrichloroethene

Surr: 1,2-Dichloroethane-d4Surr: 4-BromofluorobenzeneSurr: DibromofluoromethaneSurr Toluene-d8

Sample ID 0101078-01BMSD

Client ID:

Analyte1,1-DichloroetheneF <sneC .obenzeneTrichloroethene

Surr: 1,2-Dichloroethane-d4Surr: 4-BromofluorobenzeneSurr: DibromofluoromethaneSurr: Toluene-d8

Batch ID: R8375

Result0.56540.50420.4790.664

0.57320.52580.53540.5126

Batch ID: R8375

Result0.556

0.50480.49180.65960.57420.52980.5426

0.52

Test Code:

Run

PQL0.0400.0400.0400.040

0000

ID:

DF11111111

Test Code:

Run

PQL0.0400.0400.0400.040

0000

ID:

DF11111111

SW1311/8260A

MSD1_010116A

SpikeValue

0.50.50.50.50.50.50.50.5

SpikeRefVal

00000000

SW1311/8260A

MSD1_010116A

SpikeValue

0.50.50.50.50.50.50.50.5

SpikeRefVal

00000000

Units: mg/L

SeqNo: 81630

%REC113101

95.8133

115

105

107

103

Units:

%RECLimits

60 14060 14060 14060 14068 14472 14076 13377 146

mg/L

SeqNo: 81631

%REC111101

98.4132115106109104

%RECLimits

60 14060 14060 14060 14068 14472 14076 13377 146

Prep Date 1/16/2001


RPDRefVal

00000000

Prep

RPD

Date

RPDimit Qual

*

•

Note

1/16/2001


RPDRefVal0.56540.5042

0.4790.664

0000

RPD1.68

0.1192.64

0.6650000

RPDimit Qual2525 *2525 N~-0000

Note

s

'lifiers: ND - Not Detected at the Reporting Limit



%REC - % Recovery





F iron mental Laboratory of the Pacific Date: 17-Jan-Ol

CLIENT: PENCOWork Order: 0101010


QC SUMMARY REPORT

Laboratory Control Spike Duplicate

Sample ID LCSD-3177

Client ID:

Analyte1 ,4-Dichlorobenzene2,4-DinitrotoluenePentachlorophenol

SUIT: 2,4,6-TribromophenolSurr: 2-FluorobiphenylSurr: 2-FluorophenolSum 4-Terphenyl-d14Surr: Nitrobenzene-d5Sum Phenol-d6

Sample ID LCS-3177

Client ID:

/ !

1,-. _,chlorobenzene2,4-DinitrotoluenePentachlorophenol

Surr: 2,4,6-TribromophenolSurr: 2-FluorobiphenylSurr: 2-FluorophenolSurr: 4-Terphenyl-d14Surr: Nitrobenzene-d5Surr: Phenol-d6

Sample ID LCS-3170

Client ID:

AnalyteMercury

Batch ID: 3177

Result0 028690 022950.053430.0956

0 047950.059470 054490 049520.04366

Batch ID: 3177

Result0.026820.021830.05150.0951

0.048010.057760.052720.049150.04226

Batch ID: 3170

Result0.00966

Test Code:

Run ID:

PQL0.0100.0100.050

000000

DF

Test Code:

Run

PQL0.0100.0100.050

000000

ID:

DF111111111

Test Code:

Run

PQL0.00050

ID:

DF1

SW1311/8270A

MSD3_010110A

SpikeValue0.0250.0250.050.1

0.050.1

0.050.050.1

SpikeRefVal

000000000

SW1311/8270A

MSD3_010111A

'SpikeValue0.0250.0250.05

0.1

0.050.1

0.050.050.1

SpikeRefVal

0.0018600000000

SW1 31 1/7470

MERC_

SpikeValue

0.01

010108B

SpikeRefVal

0

Units: mg/L

SeqNo: 80889

%REC115

91.8107

95.695.959.510999

43.7

Units:

%RECLimits

36 9724 969 103

10 12343 11621 10033 14135 11410 94

mg/L

SeqNo: 80965

%REC99.887.3103

95.196

57.8105

98.342.3

Units:

%RECLimits

36 9724 96

9 10310 12343 11621 10033 14135 11410 94

mg/L

SeqNo: 80366

%REC96.6

%RECLimits

80 120

Prep Date 1/9/2001

Analysis Pate: 1/10/2001

RPDRefVal RPD

000000000

Prep Date

RPDimit Qual Note

S Q01

S Q01

1/9/2001


RPDRefVal RPD

000000000

Prep Date

RPDimit Qual Note

1/8/2001


RPDRefVal RPD

0

RPDimit Qual Note

'Tiers: ND - Not Detected at the Reporting Limit



%REC - % Recovery





C .NT: PENCO

Work Order: 0101010


QC SUMMARY REPG_.Laboratory Control Spike - generic

Sample ID LCS-3172

Client ID:

AnalyteArsenicBariumCadmiumChromiumLeadSeleniumSilver

Sample ID LCS011601

Client ID:

Analyte1,1-DichloroetheneBenzeneC ^benzeneTi.> ..oroethene

Surr: 1 ,2-Dichloroethane-d4Surr: 4-BromofluorobenzeneSurr: DibromofluoromethaneSurr: Toluene-d8

Batch ID: 3172

Result1.0481.0371.0081.016

0.99381.025

0.09841

Batch ID: R8375

Result0.59840.51840.49380.52280.52080.48460.59780.504

Test Code:

Run ID:

PQL0.501.0

0.0500.050

0.200.50

0.050

DF1111111

Test Code:

Run

PQL0.0400.0400.0400.040

0000

ID:

DF11111111

SW1311/6010A

ICP1_010108C

SpikeValue

111111

0.1

SpikeRefVal

00.01341

00

0.0228300

SW1311/8260A

MSD1_

SpikeValue

0.50.50.50.50.50.50.50.5

010116A

SpikeRefVal

00000000

Units: mg/L

SeqNo: 80452

%REC105102101102

97.1102

98.4

Units:

%RECLimits

80 12080 12080 12080 12080 12080 12080 120

mg/L

SeqNo: 81626

%REC120

104

98.8

105104

96.9

120101

%RECLimits

65 13570 13070 13070 13068 14472 14076 13377 146

Prep Date 1/8/2001


RPDRefVal RPD

0000000

Prep Date

RPDimit Qual Note

*

*

1/16/2001


RPDRefVal RPD

00000000

RPDimit Qual Note

*

S -̂̂

'ifiers: ND - Not Detected at the Reporting Limit



%REC - % Recovery





Environmental Laboratory of the fa{ c

930 Mapunapuna Street, Suite \OO Honolulu. Hawaii 96&19Telephone: (8O&)831-3090 Fax: (808)831-3O9& E-mail: BLfacHtc&aol^om

Chain of Custody / Analysis Request Form

LABORATORY USE <">NLY

LAB JOB NO..

LOCATION _

CONTAINERS

Report To

Company Name

Phone Fax

-Z747* of Samples in Shipment

1

Client Sample I.D.

Project Identification

Job Number

Data of Sample Shipment

Matrix

0*1* Result* Needed

Sampling

&aQ

3

*8

IndicateAnalysis

Requested

j__2

_3

_4

_5

_f3

_7

_8_

_9_

10

1106

Released by(Print/Signature)

Date/TimeReleased

Delivery MethodReceived by

(Print/Signature)Company / Agency

AffiliationDate / TimeReceived

Condition Noted

Comments:

White - E.L. Pacific Yellow - E.L. Pacific Pink - Client

Please Check BoxQ Dispose by LabQ Return to ClientO Archive

Page.

PACIFIC ENVIRONMENTALC O R P O R A T I O N

65 N. Nimite Hwy., Pier 14Honolulu HI 96817-5333

Phone (808) 545-5195Fox (808) 524-2307

KL1DEPART Mf

•rican Marine Services Croup ofCompr '-'.

JAN 25 A H : 3 M

HEER OFFICE

January 24,2001

Mr. Mike CrippsState of Hawaii DOH HEER919AlaMoanaBlvd,Honolulu, HI 96814-4249

RE: Alenaio Stream Sludge Case #20001219-1415

Dear Mr. Cripps:

Enclosed is the original certified analytical report for samples collected from theabove referenced site on January 2, 2001. Please feel free to call with any questions orcomments you may have.

Sincerely,

Lainie TamashiroHazmat SpecialistPacific Environmental Corporation

6000 'A" Street, Anchorage, AK 99518-1815Phone (907) 563-9584 Fox (907) 562-5426

1500 S. Barracuda St., Berth 270/271 LA.Terminal Island, CA 90731 -7357 Phone (310) 547-0919 Fax (310) 547-0031

ital Laboratory of the PacmtEnvironmental Laboratory of the Pacific

930 Mapunapuna Street, Suite 1OO Honolulu, Hawaii 96&19Telephone: (808)831-3090 Fax (808)831-3098 E-mail: ELPactflc@oceantc-tat>e com

January 17,2001

Teal CrossPENCO65 North Nimitz Highway., Pier 14Honolulu, HI 96817TEL: (808)545-5195FAX (808)524-2307

RE: Alenaio Stream Sludge Order No.: 0101010

Dear Teal Cross:

Environmental Laboratory of the Pacific received 1 sample on 1/3/2001 1:30:00 PM for theanalyses presented in the following report.

All data presented in the following report are relevant only to the samples as received and to theitems tested by the laboratory. The report shall not be reproduced except in full, without thewritten approval of the laboratory.

There were no problems with the analyses and all data for associated QC met laboratoryspecifications except where noted in the Case Narrative.

Applicable samples will be stored at no extra charge for a period of 30 days following the finalreport. Samples will be properly disposed of after 30 days, unless notified otherwise hi writing.

If you have any questions regarding these tests results, please feel free to call.

Very truly yours,ENVIRONMENTAL LABORATORY OF THE PACIFIC

Aidan Scott

Project Manager

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