Kiruna Iron Metallurgical Summary

40
Scandinavian Resources Metallurgical Summary Click to edit Master subtitle style Click to edit Master subtitle style > RESOURCE PROJECTS > TECHNOLOGY > INTEGRATED SERVICES > Mineral Processing > Engineering Design > Specialist Services > Simulation & Optimisation > EPCM > Risk Management > Training

description

Two phases of metallurgical studies have been performed and a third is currently underway (Davis Tube Recovery tests)

Transcript of Kiruna Iron Metallurgical Summary

Page 1: Kiruna Iron Metallurgical Summary

Scandinavian Resources

Metallurgical Summary

Click to edit Master subtitle styleClick to edit Master subtitle style

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Page 2: Kiruna Iron Metallurgical Summary

> DISCLAIMERWith respect to all the information contained herein, neither Mineral Engineering TechnicalServices Pty Ltd nor any officer servant employee agent or consultant thereof make anyServices Pty Ltd, nor any officer, servant, employee, agent or consultant thereof make anyrepresentations or give any warranties, expressed or implied, as to the accuracy, reliability orcompleteness of the information contained herein, including but not limited to opinions,information or advice which may be provided to users of the document. No responsibility isaccepted to users of this document for any consequence of relying on the contents hereofaccepted to users of this document for any consequence of relying on the contents hereof.

> ACKNOWLEDGEMENTSThis document is a dynamic record of the knowledge and experience of personnel at MineralEngineering Technical Services. As such it has been built upon over the years and is acollaborative effort by all those involved. We are thankful for the material supplied by andreferenced from various equipment manufacturers, vendors, industry research and projectpartners.

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Page 3: Kiruna Iron Metallurgical Summary

Introduction - Kiruna

> A well known iron ore province in northern Sweden

> The location of the worlds largest underground iron ore mine

> Orebodies usually comprise of magnetite, martite, hematite and apatite

> Many orebodies exhibit a high iron grade (in excess of 60% Fe)

> Typically, Kiruna iron ore contains higher levels of phosphorus which requires processing to removerequires processing to remove.

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Introduction - Kiruna

> The Kiruna Project lies to the jsouth west of Luossavaara-Kiirunavaara Altiebolag (LKAB) mine and Kiruna

> The boreholes tested include Vieto, Laukkujärvi, Ekströmsberg Puoltsa Gäddmyr Ekströmsberg,Puoltsa, Gäddmyr, Rakkurijärvi, Rakkurijoki and Sautasvaara

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Metallurgical Testwork

> Two phases of metallurgical studies have been performed and a third is currently underway (Davis Tube Recovery tests)

> Phase 1: Mineral Engineering Technical Services (METS)– Puoltsa (1 hole), Gäddmyr (1 hole), Vieto (1 hole), Laukkujärvi (2 holes)and

Ekströmsberg (1 hole)Ekströmsberg (1 hole)– Head grades– Magnetic Separation by Davis Tube Recovery (DTR)

> Phase 2: JK Tech– Sautasvaara (2 holes)– Comminution (crushing and grinding)– Davis Tube Recovery

> Phase 3: METS– Rakkurijärvi (5 holes), Rakkurijoki (5 holes)– Currently underway

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Phase 1 - METS

> Puoltsa borehole - Assay

– Head assay returned iron grade up to 66% Fe (average of 48% Fe)

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Phase 1 - METS

> Puoltsa borehole - Davis Tube Recovery– Head assay returned iron grade up to 66% Fe (average of 48% Fe)– Iron recoveries over 90% were achieved in the magnetic products – Majority of the iron was contained in magnetite.– DTR concentrate averaged 70.3% Fe

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Phase 1 - METS

> Puoltsa borehole– Low alumina and silica levels. Within iron ore specification limit

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Phase 1 - METS

> Puoltsa borehole– Low levels of phosphorus and sulphur

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Page 10: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Vieto Borehole – Head Assay– Iron grades ranged from 10 – 58% Fe.– Good correlation between iron grade and magnetic susceptibility (the g g (

majority of the iron is present in magnetite)

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Phase 1 - METS

> Vieto Borehole – Davis Tube Recovery– Iron upgrades readily by magnetic separation

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Phase 1 - METS

> Vieto Borehole – Davis Tube Recovery– Alumina, and silica grades of the DTR concentrates were low.

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Phase 1 - METS

> Vieto Borehole – Davis Tube Recovery– Sulphur grades a little inflated. Reverse flotation processing is available

to remove sulphur

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Page 14: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Laukkujärvi borehole – Assay– Head assay returned iron grade of 45.4 and 49.6% Fe– Small mineralised (high grade) zone( g g )

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Page 15: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Laukkujärvi borehole – Davis Tube Recovery– Magnetic concentrate was over 71% Fe grade

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Page 16: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Laukkujärvi borehole – Davis Tube Recovery– High DTR concentrate iron grade complimented by very low silica and alumina

grades

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Phase 1 - METS

> Laukkujärvi borehole – Davis Tube Recovery– And very low phosphorus and sulphur grades

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Phase 1 - METS

> Ekströmsberg borehole – Assay– Head assay averaged 52.2% Fe with a maximum of 64.1% Fe– A high grade zone of ~60 meters averaging 61.8% Fe could potentially be DSO g g g g p y

except for high levels of phosphorus

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Page 19: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Ekströmsberg borehole – Davis Tube Recovery– Magnetic concentrate 70-71% Fe– Some high grade intervals gave low DTR recoveries indicating hematiteg g g g

Insufficient sample for assay

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Page 20: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Ekströmsberg borehole – Davis Tube Recovery– High DTR concentrate iron grade complimented by very low silica and alumina

grades

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Page 21: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Ekströmsberg borehole – Davis Tube Recovery– Very low sulphur grades (most below detection limit of 0.001%)– Some phosphorus grades above the nominal iron ore specificationp p g p

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Page 22: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Gäddmyr borehole – Assay– Head assay returned iron grade up to 69% Fe (average of 65% Fe)– Results indicate potential for direct shipping ore (DSO)p pp g ( )– Phosphorus and sulphur grade too high for DSO but can be reduced after

processing

701.2

50

60

%

Target Fe

0.8

1.0

%

20

30

40

Hea

d G

rade

,

0.4

0.6

Hea

d G

rade

, %

0

10

20

SiO2Al2O3 0.0

0.2

0 5 10 15 20 25 30

PS

Limit Limit 

0 5 10 15 20 25 30

Depth, m

0 5 10 15 20 25 30Depth, m

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Page 23: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Gäddmyr borehole – Davis Tube Recovery– Iron assay upgraded further through magnetic separation to over 70% Fe– Non-magnetic fraction also high at >64% Feg g– Only ~20% of samples are magnetite, ie. ~80% of iron is hematite and not

recovered by LIMS

50

60

70Target Fe

30

40

50

e Gra

de, %

0

10

20

Fe

DTR Fe

Feed Fe

00 5 10 15 20 25 30

Depth, m

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Page 24: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Gäddmyr borehole – Davis Tube Recovery– Alumina and silica grades were very low and should not be considered as an

issue.

4 0

4.5

5.0

SiO2Limit

2 5

3.0

3.5

4.0

ade,

%

SiO2

Al2O3

Limit 

Limit

1 0

1.5

2.0

2.5

DT

R G

ra

0.0

0.5

1.0

0 5 10 15 20 25 300 5 0 5 0 5 30

Depth, m

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Page 25: Kiruna Iron Metallurgical Summary

Phase 1 - METS

> Gäddmyr borehole – Davis Tube Recovery– A high level of phosphorus and sulphur in the unprocessed ore– Phosphorus and sulphur reduced to acceptable levels by magnetic

separationseparation– In the high hematite ores, phosphorus and sulphur can potentially be

reduced by further processing (magnetic, gravity or flotation)0.10

0.07

0.08

0.09

%

0.04

0.05

0.06

DT

R G

rade

, %

PLimit

0.01

0.02

0.03

D

SLimit 

0.000 5 10 15 20 25 30

Depth, m

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Page 26: Kiruna Iron Metallurgical Summary

Phase 2 - JKTech

> Sautasvaara borehole – Head Assay– Hole 65708: high grade iron; up to 63.6% Fe, medium silica, high S and P– Hole 65715: medium grade iron; 27.6-52.1% Fe; high silica, sulphur

70

Target Fe65708                                      65715

2.5

3.0

65708                                                        65715

40

50

60

de, %

2.0

2.5

de, %

20

30

40

Hea

d G

rad

1.0

1.5

Hea

d G

rad

0

10

0 50 100 150 200 250 300

Al2O3SiO2

0.0

0.5

0 50 100 150 200 250 300

PSLimit  

Depth, m Depth, m

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Phase 2 - JKTech

> Sautasvaara borehole – DTR testwork– DTR tests returned magnetic products exhibiting iron grades greater than

69% Fe ti d t hibit d l ili h h d l h– DTR magnetic products exhibited low silica, phosphorus and sulphur

– Iron recoveries ranged from 72 – 98%

50

60

70

65708                                      65715

Target Fe

30

40

50

e Gra

de, %

0

10

20

F

DTR Fe

Feed Fe

00 50 100 150 200 250 300

Depth, m

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Page 28: Kiruna Iron Metallurgical Summary

Phase 2 - JKTech

> Sautasvaara borehole – DTR testwork– DTR tests returned magnetic products exhibiting iron grades greater than

69% Fe i d f 2 98%– Iron recoveries ranged from 72 – 98%

70

50

60

%

65708                                      65715

Target Fe

20

30

40

Fe G

rade

, %

0

10

20

DTR Fe

Feed Fe

0 50 100 150 200 250 300

Depth, m

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Page 29: Kiruna Iron Metallurgical Summary

Phase 2 - JKTech

> Sautasvaara borehole – DTR testwork– DTR magnetic products exhibited low silica, phosphorus– Some high sulphur

4.0

4.5

5.0

SiO2Limit 

1 20

1.40

1.60

2 0

2.5

3.0

3.5

Gra

de, %

Al2O3Limit

0.80

1.00

1.20

R G

rade

, % 65708                                      65715

0 5

1.0

1.5

2.0

DT

R G 65708                                      65715

0.20

0.40

0.60DT

S

0.0

0.5

0 50 100 150 200 250 300

Depth, m

0.000 50 100 150 200 250 300

Depth, m

Plimit 

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Page 30: Kiruna Iron Metallurgical Summary

Phase 2 - JKTech

> Sautasvaara borehole – Comminution testwork

– Crushing characteristics reflect consistent crushing indices (GeMCitests)

– Grinding characteristics indicate two grinding domains – related to mineralogy

– Further testwork is required to estimate grinding indexFurther testwork is required to estimate grinding index

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Page 31: Kiruna Iron Metallurgical Summary

Phase 3 - METS

> Rakkurijoki – Assay Rjo11001– Head assay averaged 38% Fe with a maximum of 60% Fe– Silica is high in the iron mineralised zonesg– Alumina, phosphorus and sulphur grades are moderate to high

3.5

4.0

70

Target Fe

2.5

3.0

de, %

40

50

60

e, %

Target Fe

1.0

1.5

2.0

Hea

d G

rad

20

30

40

Hea

d G

rade

0.0

0.5

80 100 120 140 160 180

PS

limit  

0

10

80 100 120 140 160 180

Al2O3SiO2

Limit

Depth, mDepth, m

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Page 32: Kiruna Iron Metallurgical Summary

Phase 3 - METS

> Rakkurijoki, Roj 11001 – Davis Tube Recovery– Magnetic concentrate averaged 69% Fe at up to 99% recovery (average 83%)

60

70Target Fe

40

50

60

de, %

Feed Fe

DTR Fe

20

30

Fe G

rad

0

10

80 100 120 140 160 180

Depth, m

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Page 33: Kiruna Iron Metallurgical Summary

Phase 3 - METS

> Rakkurijoki, Roj 11001 – Davis Tube Recovery– High DTR concentrate iron grade complimented by very low silica and alumina

gradesThe very high silica in the low iron feed grade area of the hole (>50%) has been – The very high silica in the low iron feed grade area of the hole (>50%) has been reduced significantly but is still above the target 4%

8 0

9.0

6.0

7.0

8.0

%

3.0

4.0

5.0

TR

Gra

de, %

SiO2Al2O3

Limit Limit

0 0

1.0

2.0DT

0.075 95 115 135 155 175 195

Depth, m

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Page 34: Kiruna Iron Metallurgical Summary

Phase 3 - METS

> Rakkurijoki, Roj 11001– Davis Tube Recovery– Low sulphur grades (most below target grade of 0.03%)– Two composites of 5% S at end of mineralised zonep– Phosphorus grades acceptable

0.09

0.10

0.06

0.07

0.08

ade,

%

0.03

0.04

0.05

DT

R G

ra

P

S

Limit 

Limit

0.00

0.01

0.02

80 100 120 140 160 180

Depth, m

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Page 35: Kiruna Iron Metallurgical Summary

Phase 1 Summary - METS

> Laukkujärvi Borehole– Head grades were low <10% Fe however, DTR

magnetic product recovered over 70% of the iron with magnetic product recovered over 70% of the iron with low impurity levels.

– This suggests that the majority of the iron is present as magnetiteM ti ti l i t bl i – Magnetic separation alone is acceptable processing for this ore

> Ekströmsberg Borehole> Ekströmsberg Borehole– Head iron grades were high, many reached 60% Fe.– The high grade iron zones exhibited acceptable levels

of alumina, silica and sulphur– DTR magnetic product exhibited high iron grades (70%

Fe) low in silica, alumina and sulphur and phosphorus– Testwork suggests that a mixture of magnetite,

hematite/martite is presenthematite/martite is present

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Phase 1 - Summary

> Puoltsa borehole– Outstanding magnetic separation results– Low phosphorus, sulphur, silica and alumina in the magnetic productp p , p , g p– Magnetic product recovered over 90% of the iron (mainly magnetite)– Testwork suggests that only magnetic separation would be required to

produce a high grade saleable productC ld b it bl f di t d ti (DR) f d– Could be suitable for direct reduction (DR) feed

– Comparable with LKAB’s Kiruna B and Malmberget A fines

Gädd b h l> Gäddmyr borehole– High iron grades achieving up to 72% Fe (equivalent to 99% magnetite)– Lower iron recoveries than Puoltsa.

Significant iron remaining in the non magnetic product suggests the presence – Significant iron remaining in the non-magnetic product suggests the presence of hematite

– Non-magnetic product contained high phosphorus and sulphur suggesting that both are associated with hematite

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Phase 1 - Summary

> Vieto, Laukkujärvi and Ekströmsberg– A range of head iron grades present– Many head iron grades were greater than 60% FeMany head iron grades were greater than 60% Fe– DTR magnetic product exhibited high Fe grades from each borehole– Many DTR magnetic products exhibited low silica, alumina and

sulphur levelsi i i– Some moderate phosphorus levels exhibited which may be removed

by further beneficiation

> QEMSCAN mineralogical analysis (Gäddmyr deposit) has > QEMSCAN mineralogical analysis (Gäddmyr deposit) has identified that the phosphorus contaminant of the ore is the mineral apatite and the sulphur contaminant is in the form of pyrite and pyrrhotite form of pyrite and pyrrhotite

> The contaminant minerals are liberated at 45 microns and should be rejected by a beneficiation processand should be rejected by a beneficiation process

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Summary

Puoltsa Gaddmyr Vieto Laukkujarvi Ekstromsberg Sautasvaara Rakkurijoki

Head Fe grade 49.3 64.6 32.8 10.3 52.6 47.7 38.5

% Magnetite 62.4 No data 47.9 69.9 28.2 No data 30.9% Magnetite 30.9

Mass Recovery, % 67.9 17.9 42.2 65.7 25.9 54.5 49.5

DTR Fe recovery 96.2 20.4 82.8 98.4 44.6 88.5 85.4

DTR conc Fe grade 70.3 71.9 70.0 71.0 70.8 71.1 69.8g

DTR conc SiO2 grade 0.58 0.01 1.2 0.6 0.7 0.5 1.1

DTR conc Al2O3 grade 0.16 0.07 0.2 0.02 0.1 0.2 0.3

DTR conc P grade 0.0017 0.02 0.01 0.002 0.04 0.05 0.01g

DTR conc S grade 0.005 0.005 0.06 0.001 0.003 0.3 0.2

Note: 1. Where the iron is predominantly present as magnetite, then the mass recovery will follow the % magnetite in

the ore2. The mass recovery and iron recovery are related by the iron feed grade . Ie. If the iron grade is 10% Fe and

this is present as only magnetite (equivalent to14% magnetite in the feed) then a mass recovery of 14%, in a perfect separation, would achieve 100% iron recovery

3. If the iron grade is made up of 50:50 magnetite:hematite then a mass recovery of 7% would achieve 50% 3. If the iron grade is made up of 50:50 magnetite:hematite then a mass recovery of 7% would achieve 50% iron recovery. If the mass recovery was 14%, as a result of gangue included with the magnetic concentrate, the iron recovery would still be ~50%, if the gangue material did not contain iron

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Page 39: Kiruna Iron Metallurgical Summary

Summary – Further Testwork

> The DTR testwork has been carried out at 45 microns

> Further work will optimise the grind size for magnetic separation> Further work will optimise the grind size for magnetic separation

> With the low grade feeds, rejection of some waste at coarse sizes (coarse cobbing) is a possibility and will be investigated

> Further testwork will investigate the reduction of sulphur and u e es o es ga e e educ o o su p u a d phosphorus from the magnetite and hematite ores by beneficiation

> The ores tested produce a concentrate of very low silica and alumina

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Page 40: Kiruna Iron Metallurgical Summary

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