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Intermetallic Matrix Composites
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Cambridge University Press978-1-107-41006-0 - Materials Research Society Symposium Proceedings: Volume 194:Intermetallic Matrix CompositesEditors: D. L. Anton, P. L. Martin, D. B. Miracle and R. McMeekingFrontmatterMore information
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Cambridge University Press978-1-107-41006-0 - Materials Research Society Symposium Proceedings: Volume 194:Intermetallic Matrix CompositesEditors: D. L. Anton, P. L. Martin, D. B. Miracle and R. McMeekingFrontmatterMore information
MATERIALS RESEARCH SOCIETY SYMPOSIUM PROCEEDINGS VOLUME 194
Intermetallic Matrix Composites
Symposium held April 18-20, 1990, San Francisco, California, U.S.A.
EDITORS:
D. L. AntonUnited Technologies Research Center, East Hartford, Connecticut, U.S.A.
P. L. MartinRockwell International Science Center, Thousand Oaks, California, U.S.A.
D. B. MiracleWright Research & Development Center, Wright-Patterson Air Force Base,Ohio, U.S.A.
R. McMeekingUniversity of California, Santa Barbara, California, U.S.A.
IMIRIS1 MATERIALS RESEARCH SOCIETYPittsburgh, Pennsylvania
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Cambridge University Press978-1-107-41006-0 - Materials Research Society Symposium Proceedings: Volume 194:Intermetallic Matrix CompositesEditors: D. L. Anton, P. L. Martin, D. B. Miracle and R. McMeekingFrontmatterMore information
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Cambridge University Press978-1-107-41006-0 - Materials Research Society Symposium Proceedings: Volume 194:Intermetallic Matrix CompositesEditors: D. L. Anton, P. L. Martin, D. B. Miracle and R. McMeekingFrontmatterMore information
Contents
PREFACE xi
MATERIALS RESEARCH SOCIETY SYMPOSIUM PROCEEDINGS xii
PART I: MODELING OF INTERMETALLIC MATRIX COMPOSITES
•MODELS FOR THE STRENGTH OF DUCTILE MATRIX COMPOSITES 3Gang Bao, Francesco Genna, John W. Hutchinson, andRobert M. McMeeking
ON THE FLOW AND CREEP STRENGTH OF POWER LAW MATERIALSCONTAINING RIGID REINFORCEMENTS 15
Ming Y. He
MICROMECHANICAL MODEL OF CRACK GROWTH IN FIBER REINFORCEDBRITTLE MATERIALS 23
Asher A. Rubinstein and Kang Xu
PART II: PROCESSING OF INTERMETALLICMATRIX COMPOSITES
•INNOVATIVE PROCESSING TECHNIQUES FOR INTERMETALLICMATRIX COMPOSITES 31
N.S. Stoloff and D.E. Alman
DUCTILE PHASE TOUGHENING OF BRITTLE INTERMETALLICS 45D.L. Anton and D.M. Shah
REACTION SINTERING OF MOLYBDENUM DISILICIDE BASEDCOMPOSITES 53
Martin W. Weiser, Sherisse R. Smelser, andJohn J. Petrovic
EFFECT OF THERMOMECHANICAL TREATMENTS ON SOLIDIFICATIONINHOMOGENEITY IN INGOT METALLURGY GAMMA TITANIUMALUMINIDES 59
J.D. Bryant, S.L. Semiatin, J.R. Maisano,D.T. Winter, and A.R.H. Barrett
INTERMETALLIC MATRIX COMPOSITES BY PHYSICAL VAPORDEPOSITION 65
Dallis A. Hardwick and Richard C. Cordi
TAILORED MICROSTRUCTURES OF NIOBIUM-NIOBIUM SILICIDESBY PHYSICAL VAPOR DEPOSITION 71
Rabi S. Bhattacharya, A.K. Rai, M.G. Mendiratta,and Y.T. Cheng
REACTIVE SYNTHESIS OF NbAl3 MATRIX COMPOSITES 79L. Lu, Y.S. Kim, A.B. Gokhale, and R. Abbaschian
•Invited Paper
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Cambridge University Press978-1-107-41006-0 - Materials Research Society Symposium Proceedings: Volume 194:Intermetallic Matrix CompositesEditors: D. L. Anton, P. L. Martin, D. B. Miracle and R. McMeekingFrontmatterMore information
SOLIDIFICATION PROCESSING ROUTES TO HIGH ASPECT RATIOREINFORCEMENTS IN -TiAl 89
J.J. Valencia, J.P.A. Lofvander, J. Rosier,C.G. Levi, and R. Mehrabian
AXIAL ALIGNMENT OF SHORT-FIBER TITANIUM ALUMINIDECOMPOSITES BY DIRECTIONAL SOLIDIFICATION 97
S.L. Kampe, G.H. Swope, and L. Christodoulou
SOLIDIFICATION PROCESSING OF NbCr2 ALLOYS 105D.J. Thoma and J.H. Perepezko
THE EFFECTS OF COOLING RATE UPON XDtm TiAl WELDMICROSTRUCTURE 113
Erica Robertson, Mary Ann Hill, andRicardo B. Schwarz
PART III: MICROSTRUCTURE/PROPERTY RELATIONSHIPSOF INTERMETALLIC MATRIX COMPOSITES
SiC REINFORCED-MoSi2 ALLOY MATRIX COMPOSITES 123J.J. Petrovic, R.E. Honnell, and A.K. Vasudevan
&ND Nb REINFORCED MoSi2David H. Carter and Patrick L. Martin
Ta AND Nb REINFORCED MoSi2 131
139J.-M. Yang and S.M. Jeng
MICROSTRUCTURES AND MECHANICAL PROPERTIES OF NiAl+MoIN-SITU EUTECTIC COMPOSITES 147
P.R. Subramanian, M.G. Mendiratta, D.B. Miracle,and D.M. Dimiduk
SURVEY OF EUTECTIC SYSTEMS AS POTENTIAL INTERMETALLICMATRIX COMPOSITES FOR HIGH TEMPERATURE APPLICATION 155
S. Mazdiyasni and D.B. Miracle
MICROSTRUCTURE AND MECHANICAL PROPERTIES OF Ni3Al-Al203COMPOSITES PRODUCED BY HOT EXTRUSION 163
C.G. McKamey and E.H. Lee
MICROSTRUCTURE AND MECHANICAL BEHAVIOR OF Ni3Al-MATRIXCOMPOSITES 169
P.C. Brennan, W.H. Kao, S.M. Jeng, and J.-M. Yang
DUCTILE-PHASE TOUGHENING IN NIOBIUM-NIOBIUM SILICIDEPOWDER PROCESSED COMPOSITES 175
Rama M. Nekkanti and Dennis M. Dimiduk
DUCTILE-PHASE TOUGHENING OF Cr3Si WITH CHROMIUM 183Joseph W. Newkirk and J. Alan Sago
DUCTILITY ENHANCEMENT FROM INTERFACE DISLOCATIONSOURCES IN A DIRECTIONALLY SOLIDIFIED 0+( + ')Ni-Fe-AlCOMPOSITE ALLOY 191
M. Larsen, A. Misra, S. Hartfield-Wunsch, R. Noebe,and R. Gibala
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DISLOCATION MORPHOLOGIES IN TiB2/NiAl 199L. Wang and R.J. Arsenault
DEVELOPMENT OF HIGHLY IMPACT RESISTANT NiAl MATRIXCOMPOSITES 205
Vincent C. Nardone, James R. Strife, andKarl M. Prewo
1300 K COMPRESSIVE PROPERTIES OF A REACTION MILLEDNiAl-AIN COMPOSITE 211
J. Daniel Whittenberger, Eduard Arzt, andMichael J. Luton
CREEP BEHAVIOR AND MICROSTRUCTURE OF XD™ TITANIUMALUMINIDE 219
C.R. Feng, H.H. Smith, D.J. Michel, and C.R. Crowe
STRUCTURE/PROPERTY COMPARISONS IN PARTICULATE ANDSHORT FIBER Y-BASED TITANIUM ALUMINIDE COMPOSITES 225
S.L. Kampe, J.A. Clarke, and L. Christodoulou
CONSTANT STRESS CREEP OF XD™ TiAl CONTAININGNITROGEN 233
Erica Robertson and Patrick L. Martin
THE HIGH TEMPERATURE BEHAVIOUR OF TiAl CONTAININGCARBIDE REINFORCEMENTS 241
J. Rosier, J.J. Valencia, C.G. Levi, A.G. Evans,and R. Mehrabian
SIMPLE MEASUREMENTS OF TOUGHNESS AND CRACK FORMATIONIN SEVERAL INTERMETALLIC-MATRIX COMPOSITE SYSTEMS 249
Robert L. Fleischer
STRENGTH AND TOUGHNESS OF SINGLE-PHASE AND DUAL-PHASEHIGH-TEMPERATURE INTERMETALLICS 257
Stephen M. Bruemmer, John L. Brimhall, andCharles H. Henager, Jr.
DETERMINATION OF FIBER/MATRIX INTERFACE MECHANICALPROPERTIES IN BRITTLE-MATRIX COMPOSITES 263
Ronald J. Kerans, Paul D. Jero,Triplicane A. Parthasarathy, and Amit Chatterjee
THE EFFECT OF NOTCHES ON THE FATIGUE LIFE OF SCS-6/Ti3AlCOMPOSITE 271
Kenneth R. Bain, Mary Lee Gambone, andRichard D. Zordan
MECHANICAL BEHAVIOR AND FAILURE MECHANISMS OF SCS-6/Ti3AlCOMPOSITES 277
S.M. Jeng, C.J. Yang, J.-M. Yang, D.G. Rosenthal,and J. Goebel
EFFECT OF XD™ TiB2 VOLUME FRACTION ON THE MICROSTRUCTUREOF A CAST NEAR-GAMMA TITANIUM ALUMINIDE ALLOY 285
Donald E. Larsen, Jr., Stephen Kampe, andLeo Christodoulou
vii
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INTERFACIAL SHEAR BEHAVIOR OF SAPPHIRE-REINFORCED NiAlCOMPOSITES 293
C.A. Moose, D.A. Koss, and J.R. Hellmann
MICROSTRUCTURE AND INTERFACE BEHAVIOR IN DIFFUSIONBONDED Ni3Al+B MATRICES CONTAINING CONTINUOUS A12O3FIBERS 3 01
C. Lee, D.S. Grummon, and G. Gottstein
PARTICLE-REINFORCED Nb-26at%Ti-48at%Al COMPOSITES 307R.M. Aikin, Jr., P.E. McCubbin, andL. Christodoulou
HEAT TREATMENTS AND THERMAL FATIGUE OF SCS-6/ALPHA-2TITANIUM ALUMINIDE COMPOSITES 315
Y-W. Kim and J.J. Kleek
INITIAL EVALUATION OF CONTINUOUS FIBER REINFORCED NiAlCOMPOSITES 323
R.D. Noebe, R.R. Bowman, and J.I. Eldridge
FEASIBILITY STUDY OF INTERMETALLIC COMPOSITES 333D.M. Shah, D.L. Anton, and C.W. Musson
MICROSTRUCTURAL STUDIES OF /3-NiAl AND a-Re COMPOSITESPRODUCED BY EUTECTIC SOLIDIFICATION 341
D.P. Mason, D.C. Van Aken, and J.G. Webber
STUDIES OF TITANIUM ALUMINIDE COMPOSITES CONTAININGMETALLIC FIBER/MATRIX INTERFACE LAYERS 349
C.G. Rhodes, C.C. Bampton, and J.A. Graves
CYCLIC OXIDATION RESISTANCE OF A REACTION MILLEDNiAl-AIN COMPOSITE 355
Carl E. Lowell, Charles A. Barrett, andJ. Daniel Whittenberger
HIGH TEMPERATURE OXIDATION OF Ni3Al COMPOSITES 361P.F. Tortorelli, J.H. DeVan, C.G. McKamey,and M. Howe11
PART IV: COMPATIBILITY OF INTERMETALLICMATRIX COMPOSITES
*CHEMICAL STABILITY OF FIBER-METAL MATRIX COMPOSITES 3 69J.H. Norman, G.H. Reynolds, and L. Brewer
COMPATIBILITY OF POTENTIAL REINFORCING CERAMICS WITHNi AND Fe ALUMINIDES 379
J.A. Moser, M. Aindow, W.A.T. Clark, S. Draper,and H.L. Fraser
CHEMICAL COMPATIBILITY OF HIGH TEMPERATURE INTERMETALLICCOMPOUNDS WITH VARIOUS POTENTIAL REINFORCEMENTS 385
J.-M. Yang, S.M. Jeng, C.J. Yang, and D.L. Anton
*Invited Paper
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PHASE STABILITY OF SIGMA + BETA MICROSTRUCTURES IN THETERNARY Nb-Ti-Al SYSTEM 393
D.T. Hoelzer and F. Ebrahimi
DUCTILE PHASE TOUGHENING OF MoSij-CHEMICAL COMPATIBILITYAND FRACTURE TOUGHNESS 399
L. Xiao, Y.S. Kim, and Reza Abbaschian
DECOMPOSITION REACTIONS AND TOUGHENING IN NiAl-Cu ALLOYS 405W.P. Allen, J.C. Foley, R.F. Cooper, andJ.H. Perepezko
REACTION ZONE GROWTH IN Ti-BASE/SiC COMPOSITES 413Ann M. Ritter, Ernest L. Hall, and Nathan Lewis
OXIDATION OF POWDER PROCESSED NbAl3 MATRIX COMPOSITES 423Paul S. Korinko and D.J. Duquette
INTERFACE MODIFICATION FOR FIBER-REINFORCED TITANIUMALUMINIDE COMPOSITES 429
Daniel E. Boss and J.M. Yang
AUTHOR INDEX 437
SUBJECT INDEX 439
MATERIALS RESEARCH SOCIETY SYMPOSIUM PROCEEDINGS 441
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Preface
MRS has been a leader in publishing current research resultscovering the area of intermetallic compound development. Threeprior symposia in 19 84 (Vol. 39), 19 86 (Vol. 81) and 19 88(Vol. 13 3) were devoted primarily to monolithic ordered systems.The current volume is the first to concentrate on issuesparticular to intentional multiphase intermetallic systems.
Our intent was to bring together the myriad of disciplinesneeded to understand the complex processing-microstructure-property relationships in intermetallic matrix compositematerials. It may appear to the reader that some of the workreported in this volume does not bear on this question, but itshould be remembered that intermetallic compounds have propertiessimilar to both ceramics (at low temperatures) and metals (at hightemperatures). Thus the techniques for toughening brittle matrixcomposites at ambient temperatures as well as those for strength-ening ductile matrix composites at elevated temperatures need tobe applied to the intermetallic situation. For this reason, thesession on microstructure-based modeling of the behavior ofintermetallic matrix composites drew heavily on ceramic and metalmatrix experience. The session discussing processing was also amix of ceramic and metallurgical approaches, while stressing novelmethods particular to composite microstructures. Thermodynamiccompatibility and conventional microstructure-mechanical propertystudies made up the bulk of the contributed papers as they addressa large deficiency in our understanding in this important area.
The breadth of sponsorship reflects the large number oforganizations which recognize the need for intermetallic matrixcomposites. The sponsors were GE Aircraft Engines, Los AlamosNational Laboratory, Martin Marietta Laboratories, NASA LewisResearch Center, Office of Naval Research, United TechnologiesResearch Center, and Rockwell Science Center. Their financialsupport is gratefully acknowledged. In addition, we would liketo thank Ms. Joyce Hurlburt for her diligent secretarial supportduring the meeting and assistance in compiling this proceedingsafterward and to the session chairmen and all those who helpedreview the submitted papers.
D. AntonP. MartinD. MiracleR. McMeeking
May 199 0
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Cambridge University Press978-1-107-41006-0 - Materials Research Society Symposium Proceedings: Volume 194:Intermetallic Matrix CompositesEditors: D. L. Anton, P. L. Martin, D. B. Miracle and R. McMeekingFrontmatterMore information
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MATERIALS RESEARCH SOCIETY SYMPOSIUM PROCEEDINGS
Recent Materials Research Society Symposium Proceedings
Volume 157—Beam-Solid Interactions: Physical Phenomena, J.A. Knapp, P. Borgesen,R.A. Zuhr, 1989, ISBN 1-55899-045-3
Volume 158—In-Situ Patterning: Selective Area Deposition and Etching, R. Rosenberg,A.F. Bernhardt, J.G. Black, 1989, ISBN 1-55899-046-1
Volume 159—Atomic Scale Structure of Interfaces, R.D. Bringans, R.M. Feenstra,J.M. Gibson, 1989, ISBN 1-55899-047-X
Volume 160—Layered Structures: Heteroepitaxy, Superlattices, Strain, andMetastability, B.W. Dodson, L.J. Schowalter, J.E. Cunningham,F.H. Pollak, 1989, ISBN 1-55899-048-8
Volume 161—Properties of II-VI Semiconductors: Bulk Crystals, Epitaxial Films,Quantum Well Structures and Dilute Magnetic Systems, J.F. Schetzina,F.J. Bartoli, Jr., H.F. Schaake, 1989, ISBN 1-55899-049-6
Volume 162—Diamond, Boron Nitride, Silicon Carbide and Related Wide BandgapSemiconductors, J.T. Glass, R.F. Messier, N. Fujimori, 1989,ISBN 1-55899-050-X
Volume 163—Impurities, Defects and Diffusion in Semiconductors: Bulk and LayeredStructures, J. Bernholc, E.E. Haller, DJ. Wolford, 1989,ISBN 1-55899-051-8
Volume 164—Materials Issues in Macrocrystalline Semiconductors,P.M. Fauchet, C.C. Tsai, K. Tanaka, 1989, ISBN 1-55899-052-6
Volume 165—Characterization of Plasma-Enhanced CVD Processes, G. Lucovsky,D.E. Ibbotson, D.W. Hess, 1989, ISBN 1-55899-053-4
Volume 166—Neutron Scattering for Materials Science, S.M. Shapiro, S.C. Moss,J.D. Jorgensen, 1989, ISBN 1-55899-054-2
Volume 167—Advanced Electronic Packaging Materials, A. Barfknecht, J. Partridge,C-Y. Li, C.J. Chen, 1989, ISBN 1-55899-055-0
Volume 168—Chemical Vapor Deposition of Refractory Metals and Ceramics,T.M. Besmann, B.M. Gallois, 1989, ISBN 1-55899-056-9
Volume 169—High Temperature Superconductors: Fundamental Properties and NovelMaterials Processing, J. Narayan, C.W. Chu, L.F. Schneemeyer,D.K. Christen, 1989, ISBN 1-55899-057-7
Volume 170—Tailored Interfaces in Composite Materials, C.G. Pantano, E.J.H. Chen,1989, ISBN 1-55899-058-5
Volume 171—Polymer Based Molecular Composites, D.W. Schaefer, J.E. Mark, 1989,ISBN 1-55899-059-3
Volume 172—Optical Fiber Materials and Processing, J.W. Fleming, G.H. Sigel,S. Takahashi, P.W. France, 1989, ISBN 1-55899-060-7
Volume 173—Electrical, Optical and Magnetic Properties of Organic Solid-StateMaterials, L.Y. Chiang, D.O. Cowan, P. Chaikin, 1989,ISBN 1-55899-061-5
Volume 174—Materials Synthesis Utilizing Biological Processes, M. Alper, P.D. Calvert,P.C. Rieke, 1989, ISBN 1-55899-062-3
Volume 175—Multi-Functional Materials, D.R. Ulrich, F.E. Karasz, A.J. Buckley,G. Gallagher-Daggitt, 1989, ISBN 1-55899-063-1
Volume 176—Scientific Basis for Nuclear Waste Management XIII, V.M. Oversby,P.W. Brown, 1989, ISBN 1-55899-064-X
Volume 177—Macromolecular Liquids, C.R. Safinya, S.A. Safran, P.A. Pincus, 1989,ISBN 1-55899-065-8
Volume 178—Fly Ash and Coal Conversion By-Products: Characterization, Utilizationand Disposal VI, F.P. Glasser, R.L. Day, 1989, ISBN 1-55899-066-6
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Cambridge University Press978-1-107-41006-0 - Materials Research Society Symposium Proceedings: Volume 194:Intermetallic Matrix CompositesEditors: D. L. Anton, P. L. Martin, D. B. Miracle and R. McMeekingFrontmatterMore information
MATERIALS RESEARCH SOCIETY SYMPOSIUM PROCEEDINGS
Volume 179—Specialty Cements with Advanced Properties, H. Jennings, A.G. Landers,B.E. Scheetz, I. Odler, 1989, ISBN 1-55899-067-4
Volume 180—Better Ceramics Through Chemistry IV, CJ. Brinker, D.E. Clark,D.R. Ulrich, BJ.J. Zelinsky, 1990, ISBN: 1-55899-069-0
Volume 181—Advanced Metallizations in Microelectronics, A. Katz, S.P. Murarka,A. Appelbaum, 1990, ISBN: 1-55899-070-4
Volume 182—Polysilicon Thin Films and Interfaces, B. Raicu, T.Kamins,C.V. Thompson, 1990, ISBN: 1-55899-071-2
Volume 183—High-Resolution Electron Microscopy of Defects in Materials, R. Sinclair,D.J. Smith, U. Dahmen, 1990, ISBN: 1-55899-072-0
Volume 184—Degradation Mechanisms in III-V Compound Semiconductor Devices andStructures, V. Swaminathan, SJ. Pearton, O. Manasreh, 1990,ISBN: 1-55899-073-9
Volume 185—Materials Issues in Art and Archaeology II, J.R. Druzik, P.B. Vandiver,G. Wheeler, 1990, ISBN: 1-55899-074-7
Volume 186—Alloy Phase Stability and Design, G.M. Stocks, D.P. Pope, A.F. Giamei,1990, ISBN: 1-55899-075-5
Volume 187—Thin Film Structures and Phase Stability, B.M. Clemens, W.L. Johnson,1990, ISBN: 1-55899-076-3
Volume 188—Thin Films: Stresses and Mechanical Properties II, W.C. Oliver,M. Doerner, G.M. Pharr, F.R. Brotzen, 1990, ISBN: 1-55899-077-1
Volume 189—Microwave Processing of Materials II, W.B. Snyder, W.H. Sutton,D.L. Johnson, M.F. Iskander, 1990, ISBN: 1-55899-078-X
Volume 190—Plasma Processing and Synthesis of Materials III, D. Apelian, J. Szekely,1990, ISBN: 1-55899-079-8
Volume 191—Laser Ablation for Materials Synthesis, D.C. Paine, J.C. Bravman, 1990,ISBN: 1-55899-080-1
Volume 192—Amorphous Silicon Technology, P.C. Taylor, M.J. Thompson,P.G. LeComber, Y. Hamakawa, A. Madan, 1990, ISBN: 1-55899-081-X
Volume 193—Atomic Scale Calculations of Structure in Materials, M.A. Schluter,M.S. Daw, 1990, ISBN: 1-55899-082-8
Volume 194—Intermetallic Matrix Composites, D.L. Anton, R. McMeeking, D. Miracle,P. Martin, 1990, ISBN: 1-55899-083-6
Volume 195—Physical Phenomena in Granular Materials, T.H. Geballe, P. Sheng,G.D. Cody, 1990, ISBN: 1-55899-084-4
Volume 196—Superplasticity in Metals, Ceramics, and Intermetallics, M.J. Mayo,J. Wadsworth, M. Kobayashi, A.K. Mukherjee, 1990, ISBN: 1-55899-085-2
Volume 197—Materials Interactions Relevant to the Pulp, Paper, and Wood Industries,J.D. Passaretti, D. Caulfield, R. Roy, V. Setterholm, 1990,ISBN: 1-55899-086-0
Volume 198—Epitaxial Heterostructures, D.W. Shaw, J.C. Bean, V.G. Keramidas,P.S. Peercy, 1990, ISBN: 1-55899-087-9
Volume 199—Workshop on Specimen Preparation for Transmission ElectronMicroscopy of Materials II, R. Anderson, 1990, ISBN: 1-55899-088-7
Volume 200—Ferroelectric Thin Films, A.I. Kingon, E.R. Myers, 1990,ISBN: 1-55899-089-5
Earlier Materials Research Society Symposium Proceedings listed in the back.
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