ICP Test Report Certification PacketSGS Job No. : Date of Sample Received : Testing Peiod : Test...

$: ICP Test Report Certification PacketSGS Job No. : Date of Sample Received : Testing Peiod : Test Requested : Test Method : Test Results : C,onclusion : xrvtl390111gEC - Xl\,1 '18 Jun$
1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: 5x20 Cartridge

Product #: 213xxxP Series

Issue Date: October 17, 2012

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,

2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts

This document covers the 5x20 Cartridge RoHS-Compliant series products manufactured

by Littelfuse, Inc.

＜ Raw Materials Used

Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1

Remarks：

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 C910541 Cap – Base & plating 3-6

2 C909543 Soda Lime Glass Tubes 7-11

3 C909542 Borosilicate Glass Body 12-16

4 11-0595 (082xxx-001) Element - 99% Sn Plated Cu 17-23

5 687xxx-001 Element – Ag-Cu Sn Plated 24-33

6 YTW102 (692535-002) Solder 34-38

7 934-077 (C030208) Overcap – Cap Base & plating 39-42

8 934-077 (C030208) Overcap – Wire Base & plating 39-42

9 648115 Yarn 43-51

10 648150 Yarn 52-60

11 425907 Ink- Green 61-75

12 425902 Ink - Black 76-90

13 425901 Ink - Red 91-105

14 425903 Ink- Yellow 106-120

15 425904 Ink- Blue 121-134

16 425906 Ink- Brown 135-149

nov'TEST REPORT

NO.jA002E11121307'1R02 DaG:Dec.t5,2Oi1 page 1 of4Custom6i Suzhou FuHong Eteclronic IndustialCo., L6.AddT€sg: NO.89 WEIDU ROAD, WANGTINGTOWN. XIANGCHENG oIsTRIcT. sUzHoU. CHINAReport on tie subnitied samptes.id to beSample name: Copper shellModsl: /

Materlal: /D€cripiion: /Buyer: /Supplier: /

SamPle rcceiwd date: Elec.'13,2011T€dng poriod: From Dec.13,2011 lo Dec.15,2o.l1

T€lino Reou6tedAs sp€cified by client, to detemine the L€ad, Cadmium, Mercury & Hexavat€nt Chromilm content an the slbmified sampte inaccordance wilh Dircctive 200295/EC (RoHS).

Te.Uno method:

T€sling liem Measuring instrument MQL

Lead (Pb) IEC 62321:2008, section I rcP-oEs 2mg/kgcadmium (cd) IEC 62321:20t,3, s€clion 9 tcPoEs 2 mg/kgllercury (Hg) IEC 62321:2008, section 7 lcPoEs 2 mg/kg

Chromrum (Cr l'1) IEC 62321:2008, Annex B 0 o2mgkg'

---FOR FURTHER DETAILS, PLEASE REFERTOTHE FOLLOWNG PAGE(ST**'

leg-' 0.02 mg/kg reGrc lo the MQL of sampte extraction tiquid.

99!9!cis!i-When tesled as specined the submi(ed sample compli€d wilh the rcquirements of commission Decision of 18 Aug 2005amending Directive 2002/95/EC notilied undef document 2005/618/EC.

Pro,ect Leader /{bjA-L(Engine€r) J 4

lnsoected bv

,**'*''*,n-, [,[rlg-,i ti-Y\

,ffi:::j:,,44

SHENZHEnl AOVTESTINC TECHNO!OGY CO..L.TD,KUI\ISIIAI\I BRANCIi Holline86.512.5510 8000

nov.NO,: A002E11121307-1 R02

TEST REPORT

Tesled by ICP-OES

Add the digestion sotutioni thevessel is healed until the sampl€has b€€n dissolved

Weigh the sample into

F*_-l-Content (Melal substEle)

Add the digeslion solutjon, ctose

the micfowave ves:€|.

F;;1.-and l\Iercury Content (Plaling)

To Detenn exavalenl Chromium Content (bojting- wateF extraction): (Metat substrate)

The sample is digesred in the

mrcrowave oven iollowing a sp€citic

decomposilion program.

Tesl lh€ s€mple solution and the 0.02mg/kg standard solution by UV-VIS.

Hotline86-512-5510 8000

To

+Cooling the vessel, fltet washed and

filled to the ma* with distilled wat€r.

Remove the sample, and coolthe beaker to room lemperature,and do the color leadion

sample in the beaker.Heat 50 mL of Dl waler in the

beaker to boiling ior 10 min

To Delemine

___+l coorins. rirtei washed and lilled l_-_----|l resteo oy l+fl_*l

I t o t he ma*w i th D twa te r .

I l r n " r ,u rn "n , I l " * ' I

SHENZHsN AOV TG6TING ICCHITOI"OGY CO.,L'O.KUNAHAN BRANCH a

nov'NO.i 4002E11121307-rR02

5. To O€temine Hexavalent Chromium

,':"j":::i v^02

Place 1-5

TEST REPORToste:oec15,2011

Contentin colorless and cotorcd cnromaE coating on metats(Plaljng)

5 2 Eoiling- wat6F extraction

Tako the (50+5) cm'?

sample in the beaker.

S!IENZHEN AOV'CSTING IECIINOIOGY CO..ITD,KUNSHAN gNANCH Hotlinea6-512-5510 8000

lf the tesl rcsult is posilive,

the sample is considercd tohave hexavalenl chromilm

Compare the

and lhe 0.02 mg/(qstanda.d solution

Eoiling- wateF ext€ctjonprccedurc shall be used to

lfthere is int€rference or it is hard to decide whetherthe sampl€ have tie h€xavatent chromium

Remove tie sample, and cool

lhe beaksr to room tempeEture,

and do the color reaolion

Heat 50 mlof Dlwaier in the

beaker lo boiling for 10 min

Test the sample solution and the 0.02mg/kg standard solution by UV,VIS.

T€t Re6ult3:

Unit RoHS

Limil

Result

Substrate Plating'

Lead (Pb) mg/Kg 1000 N.O. N.O.Cadmium (cd) mg/Kg 100 N.D, N.D.lvercury (Hg) mgn(]s 1000 N.D. N.D.

chromium (Crl'I) mg/Kg 1000 Negalive Negative

nov-TEST REPORT

NO 4002E11121307.rR02

'The new RoHS directive 201 1/65/EU, on Jul. 21 , 201 1 come into lorce on Jan. 03, 20 1 3 the fomat imptementation. Direclive2002,95/EC shall be rcpeated simuttaneousty.

-specimens, which requested to determine Lead, cadmium and l,rercury conteni, have been dissorved comprererv

-N.D.=not detected(<tltoL)-MOL=ntethod Ouantitation Limit-Negative=Absence of Cr (VIir

PositivF Presence ofCr (\ll)i

Unc€rlain= can not verify whetlerthe sampte have Hexavatent Chromium by spoltest.(The test€d sample should be fufthet verified by boiling-waler-€nraction method if the spot test resutt |s uncertain ornegalive. )

-'The tesl is based on lhe following assumption:The sampte ptating is a singte tayefand each paft is uniform. The tesr resuttmaybe cannotsland br lhe physicaltruth ofsampte ptating.

Photograph ofSample

Coppershell

SHENZHEN AOVT€STING TECHNOLOGYCO.,IID,XUNSHAN ARANCTI e!:-"Jllls,.**

Test Report No. CANEC1207912201 Date: 26 Jun 2012 Page '1 of 5

XIAMEN LICHUN ELECTRONIC ELEIVENT CO''LTD

42_2XINGLIN WEST RD.,361O22,JIMEI DISTRICT,XIAI\,IEN''FUJIAN,P.R'C

The followjng sample(s) was/were submitted and identified on b€half of the ctiens as: SODA LIME GLASS

SGS Job No. :

Date of Sample Received :

Testing Peiod :

Test Requested :

Test Method :

Test Results :

C,onclusion :

xrvtl390111gEC - Xl\,1'18 Jun 2012

18 Jun 2012 - 26 Jun 2012

Selected test(s) as requested by client

Please refer to next Page(s).

Please refer to next Page(s)

Based on the performed tests on submitted samples, thg results of Lead'

I\rercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB)' -PolybrominateO diphenyl ethers (PBDE) comply with the limits as set by RoHS

Direc{ive 2011/65/EU Annex ll; rec€sting 200295/EC

Signed fof and on behalf ofscs-csrc Ltd.

Approved Signatory

:ffitili":;r,:1"'),i:;'"""ft1u1!'irlil"l'.:".-".:"^:;-:*;r::r"';',:""*i:::l;l,l:iiiiirii$ii:iii:l+*tij'"$:ff.+#.,;1]:ii::T;.^.Ji{,*isi"iilj:ilii:{fiIj,^,ti{+:i':'i!*it**

isGs96s9f 0a9o@ s t&rq L4'or!ixdatgro 510'63

4t.rii Ettt*eB*+tl&*C1e3! ml:\'0633i rs6-20ier56666 lls-20)@075r13 @'i sqeco6

| {6-201s?it55ss rie20ls2075rl3 ' lgsdm@t{sd

Mombo.olth€SGS Group (SGS SA)

Test Report No. oANEC1207912201 Date: 26 Jun 2012 Page 2 of 5

Test Results :

Test Part Descriotion :

Sp€dmon No. SGS Samplo lD D€sc.l$ion1 CAN12'079122.001 Transparentglasstube

Remarl..s :(1) 1 mg/kg= 1 PPm =00001%

(2) MDL = Method Detection Limat

(3) ND = Not Detected ( < MDL )(4) "-" = Po1 P"n''"t"d

RoHS Oit€dhe 201 1,/66/EU

Test lvethod: with reference to IEC 62321:2008(1) Determination ofCadmium bv ICP"OES(2) Determination of Lead by ICP-OES.(3) Determination of l\rercury by ICP'OES'(4) Determination of Hexavalent Chromium by Colorjmetric Method using IJV-Vis'

(5) Determination of PBBS / PBDES content by GC-I\'S

Test ltem(s)

Cadmium (Cd)

Lead (Pb)

Mercury (Hg)

Hexavalent Chromium (CrVl)

Sum of PBBSMonobrcmobiPhenylDibromobiPhenylTnbromobiphenylTetrabromobiPhenYlPentabromobiPhenYlHexabromobiphenylHeptabromobiPhenylOctabromobiPhenylNonabromobiphenyl

DecabromobiPhenYlSum of PBDESMonobromodiphenyl ether

;ili,ii' !n'i*-"i,i;r i*i.p. -t, -r, td rh. sncr'(3)r63Ed

001N D229N DNDNDN DNONONDNDNDNDNDNDN DNDND

1 6&m)SZ1555.€ 1 136-20)32075113 twcn'.qs@

l i36-e)s21s5566 iistr0)lco791s e l{schit@{3s

Memb€roilhe sGS GouP (s6SSA)

t!!i!100

1,0001,0001,0001,000

Unit MO!mg/kg 2mg/kg 2mg/kg 2mg/kg 2

mgKgmg/kg 5mg/kg 5mdkg 5mg/kg 5

mg/kg 5mS^(S 5mg/kg 5mg/kg 5mS-ftS 5

mgikg 5mg/KgmS/kg 5

1,000

ii":-iit#$:1ft +iifr fi.'q*rii';l*l'#ilriilrrryiili.iii',fi ,'i;lill"':i:istii;,,*$:,:l+3i+i*+ul+:l**-{+-;ft1fi::ilffi}ii.lq'f."'.",r'",:,l;!i"Trtritirtlm';i:i:trieifi"i#i:T#jih';#}##',*;b#;ii:ix""d..;";rl'Hri'::::r'r$";*r n1?:1:r'i''rr:irl

rs16!ltod,*tdrrllolrdutlmrTdridqt06!r{s'ro.n0tdooitr 510663

+8. , - f l € ' . t1 (+&Ef lS f lS4 t1$q '6 |6 :s10€63

Test Report

Test ltem(s)

Dibromodiphenyl etherTribromodiphenyl ethetTetrabromodiphenyl etherPentabromodiphenYl etherHexabromodiphenyl ether

HeptabromodiPhenyl elher

OctabromodiPhenyl ether

Nonabromodiphenyl ether

DecabromodiPhenyl ether

Notes :

No. CAN EC 120791220'l

titri!

Date: 26 Jun 2012

MDL 0915 N D5 N D

Page 3 of 5

5555555

'!rM ed,ed %c4g,tslEl kdEqt0'6d!ikdcqr9(Cx" 5 10663

+E.r f i .4#6n+Etsqe4i q* t$c an 51$Rj

NDN DNDN DNONDND

r r€6 2olers5ai5 I136+0J32!7t13I isHls2lSsss I €6-20)s20/5113 o tssdlBe3s'gM

MenbBf olthe sGs Group (sGs sA)

udtmg/Kg

ms,ksmg/Kg

mg/Kg

mg/Kg

mg/kg

mg/Kg

mgK9

mg/Kg

(1) The maximum permissible limit is quoted from the directive 2011/65/Eu' Annex ll

igi,i#*iffi*f:iffi iiilttll$jf*:nii.l,irJg'fr*fiiq*ts**efti#*fi*,}Iiifl,ii:le;i:,;liir,';i;i#li::li:"j#'i:rir:;*':11"""::;"'T;;;";;;:;';'::::"";:r111x11:::"r':;:'r:

Test Report

ATTACHMENTS

'1) Name of the person who madetesting: Bella Wang / Cutey Yu2t Name of the berson in charge of testing: Adams Yu / Ryan Yangii in."" Lroriti

"tt" dissolfu totally by pre-conditioning method according to below flow chaft

(cf' and PbBs/PBDEs test method excluded)

Pb/Cd/Hg PBBS/PBDE8

Positive

vrb,e,10,ico'd.uon'trNorsd!,:ilJlll"#rl:i1!':i[#.$.:.::;,,,-;!U,";q" i!il;iii:.il*.*df'#m:tilsrillil':l;:tHT:"1!}i6ii:;::i:",,xr.1"Hi:'Hl;ixlfi';i'"r:;::;*lui;1";iq;'i;,"."xii:dr;#i;lffi:1.ffi"c;i:;ifi"j|.r*;in-'i#:'-*il4!:1:i{:riii".liiliiji"i.#i::;:f.::i:r;iii;li*'*'.*:;*?:;;r::';r:r;*'

Page 4 of5

i ts6 rts21566i,5 I i36_20)3S75113 M43!5oh

' i*-mietlass r (!6eo420751'g d 4s'1i*€{3s

Momberor$e SGS GrcuP (SGS sA)

No. CANEC12O7S12201 Date:26 Jun 2012

RoHS T€sting Flow Chart

Sample PreParation

Sample Measurement

Acid digestion withrnicrowave/ hotplate

Conc€ntration/Dilution of extraction

solution

1) Alkali Fusion /Dry Ashing

2) Acid todissolve

Filtration andpH adjustment

Adding 1,5-diphenylcarbazidefor colordevelopment

Adding '1,$

diphenyloarbazidefor @lordevelopment

A red colorindicates thepresence of CF*I n€cessary,confirm with

'416rNdld$'|rotl@o tdurrbqroit{oltr0do'tgs rtu 51066J

cE.r 6 .*ts *rtEf+Eflel1e8t |!F: 110633

T€st Report

Sample photo:

No. CANEC1207912201 Datet 26 Jun 2012 Page 5 of 5

ses authenticate the photo on original report only

ri* End of Repod rd

;;:l,i;;ah"j";iffi;d+d.i'- vbt!sanpr'G)bn'd

'$6RatsdPrqdrtatdMr 6Yqr 0..@ 0@ tu9u )tr 10663

+E.r-d e8k^+tg*+lf!tf1$q l6t:sr06arI135-?01321566i6 i 135 ?0)32015113 w4!nrgson

L(s-ers2155556 1 (s5 20)3205113 { 3$dmo3osm

Membeiollhe sGS G'ouP (SOs sA)

Test Report No. CANEC1207912202 Date:26 Jun 2012 Page 1 of 5

XIAMEN LICHUN ELECTRONIC ELEMENT CO.,LTD

42 2XINGLIN WEST RD.,361O22,JIMEI DISTRICT,XIA['EN,,FUJIAN,P.R.C

Test Results :

Conclusion :

The following s€mple(s) was^/vere submitted and identified on behalf of the clients as : BOSI GLASS TUBE

SGS Job No. : XM13901119EC-XM

Date of Sample Received : 18 Jun 2012

Testing Period : 18 Jun 2012 '26 Jun 2012

Test Requested : Selected test(s) as requested by client.

Test Method : Please fefer to next page(s)

Please refer to next page(s).

Based on the oeformed tests on submitted samples, the results of Lead,Mercury, Cadmium. Hexavalent chromium, Polybrominated biphenyls (PBB),

Polybrominated diphenyl ethers (PBDE) comply with the limits as s€t by RoHSDireclive 2011/65/EU Annex ll; recasting 2002/95/EC.

Signed for and on behalf ofscs-csrc Ltd.

Luc'y WuApproved Signatory

ii:trii";df#i*iil:i":#i'Tiiiqili'",'iq;l[i+ill$]*Ji":ia"#r.:ilr.'""?ir"'i1i':"'"#-

1g(drRods&$rdorgn Edu{t1drlUDtd(FlilkEoldogtu 510€63

+q.r'rijSt&^4t8fl*dfl6gls3€ i!fr:s10663r 66-201s2r56666 ' 136-20 e07t 13r is6xre,5s5s5 r €6-20)s2o75us e 3$sd1*e4tm

Momb€.ollhdscs GrouP {scs sA)

Test Report No. CANEC1207912202 oate:26 Jun 2012 Page 2 of5

Test Results :

Test Part Descriotion :

Spodmen No. SGS Sample lD O€6cfiption1 CAN12-079122.002 Transparent glass tube

Remarks :(1) 1 mg/kg = 1 PPm = 0 0001%

(2) MDL = Method Detection Limit

(3) ND = Not Detected ( < l\rDL )(4) "-" = Not Regulated

RoHS Dlr€div6 2()l 1/85/EU

Test Method : with reference to lEc 62321:2008(1) Detemination ofCadmium by ICP-OES.(2) Determination of Lead by ICP-OES(3) Determination of lrerdiry by ICP-OES.(4) Determination of Hexavalent Chromium by Colorimetdc Method using lJV_Vis'

(5) Determination of PBBS / PBDES content by GC-MS

Test ltem{s)C.dmium (Cd)Lead (Pb)

[,lercury (Hg)

Hexavalent Chromium (crvl)

Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiPhenylPentabromobiPhenylHexabromobiphenylHeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl ether

Limit Unit MDL

100 mS/kS 2

1.000 mg/kg 2

1,000 mg/kg 2

1,000 mg/kg 2

1,000 mg/kg- mdkg 5, mg/kg 5- mdkS 5- mg/kg 5- mg/kg 5- mo/kg 5- mg/kg 5- ms/kg 5- msiks 5- mg/lq 5

1,000 mg/kg- mdkg 5

'Sield&rrdrrituttbt@rln{qtc.@d0dotdsotu 510663

F!.Ttir'F8fii*&4fl+ffl**1$q 8r:5i0663

9uNDN DNDN DNDNDNDNDNDNDNDNDNDNDNDNDND

r i!5-08a56656 I l!6_20)32075113 Mc03{tl.n

l is-Oe156s6 1(!F20)3207s113 ' {sch*€is3s

Memb€rorlh€ scs Gmw {sossA}

illi:tr1y:lr:i;i:1":'"sf;:H:l'1i5$i{,ff;1ti!.'di$:::fiirtriii,i"s.ii:'#ii#;*,r#S{s.,#lU-"tii}HilffiiltliFtldlffi"{;;tu'i d-k-.;ehd6.,"h.

Test Report

Test ltem(sl

Dibrcmodiphenyl elhet

Tribromodiphenyl ether

Tetrabromodiphenyl ether

Pentabromodiphenyl ether

Hexabromodiphenyl ether

Heptabromodiphenyl ethe.

Octabromodiphenyl etherNonabromodiphenyl ethetDecabromodiphenyl ether

Notes :

No. CANEC1207912202 Date: 26 Jun 2012 Page 3 ol 5

:q ̂ nftd soFE Prrcdd! tow tqrotT t'0dloJgslm 51m6J

4@ .r ,l1 .&fitl^f&D 6e!i! e&l$e ar' )'r$63

0!2NDNDNDNDNDNDNDNDND

j lS6 rrel$666 | 136_&)3?0751i3r (86 20) s2r555s5 r lS6-2OlS2O7t'3 e s€s dB@'3ss M

Menbe 'or lho SGs GrouP (sGS SA)

t!d! ui!mgKgmg/Kgmg/Kgmg/KgmgKgmg/Kgmg/Kgmg/Kgmg/Kg

IVDL

555555555

(1) The maximum permissible limit is quoted ftom the directive 2011/65/EU, Annex ll

i

Test Report No. CANEC1207912202 Date: 26 Jun 2012 Page 4 of 5

ATTACHMENTSRoHS Testing FlowChart

'1 ) Name of the peEon who made testing: Bella Wang / Cutey Yu2) Name of the person in charge of testing: Adams Yu / Ryan Yang3lThese samolis were dissolved tcElly by pre-conditioning method according to below flow chart'(Cf*

and PBBS/PBDES test method excluded).

ifu i.,!;"#Isi.:11*fiifi ';2l':l-:i,:lil"'li"rX=r*fr jip;;rs.#*i*t$1g$]lt$#ffi*$;'#f$$ili'l$liryh]ii:ffit*rtr*:i::i;i"r"*:?ril?!?:li:ni3*:*"

,0qcdbdprolss''*rkddq0,.r'li0.dci*Eo* r(863,ffi;:;ffi I ffi:trl,i " JX$T:sE.r- i t l .E t ,GtreEsgt iF&* la3t 6t :51

Pbrcd/Hg PBB3/PBDE8

Positive

Acid digestion withmicrcwaveJ hotplate

1) Alkali Fusion /Dry Ashing

2) Acid todissolve

Adding 1,tdiphenylcarbazidefor colordevelopment

Adding 1,5-diphenylcarbazidefor colordevelopment

A red colorindicates thepresence of CF*.f necessary,confirm with

M6mberollho sGS GrouP (SGs sA)

SGSTest Report

Sample photo:

cAN12-079122.002

SGS authenticate the photo on onginal report only

'** End of Report *-

;H:S:,I"t'*i;H'"ltT:-l::.t:,':ffi:'.-.#i":._a.r-li!;i;1".j;:r*,T::Xt;:,ru1rw,*ir.!:iitii:i,-Si,'lit1{.i:iiT:iq',iT#ilii:i::iij"::'j,*'rfl'#rffliilrl-":ll;r,lrurii:**'"r

1106-,0)&155696 I {3H0)320751r3 Mm 59rM

I (st-!o)s?155556 l 1s6-2o)s20751ls' ssscrrna€F$M

No. CANEC1207912202 Datet 26 Jun 2012 Page 5 of 5

rlt{0r! R6l5edlP'l(slr{dnEdni&di@06!hFstod'{otgaroi! 510663

+!l' et&**AE*+r*i+$*re3S 4n:s1m63MeFborolrhe SGs6DuP (SGSSA)

scsI

Test ReportPOLYFIL AGOBERALLMENDSTMSSE 2OA,

was/w6re submitted and identified by/on behalfofthe client as:

Validit nownForQueStiPlease Co ith scs

No. : CE/2011/84950 D e | 2011112101

CH€3OO ZUG / SWITZERLAND

Cu99.9MSn'1'14595

2011t1lt25201 1t11/25 rO 201I |1',01

Page: 1 or 7

rr|| [ltt!|||tlt[t

The following sample(s)

S€mple DescriptionBuyer/Order No.Sample Receiving DateTesting Period

lest Result(a) Plea6eefer to next page(s).

prqt iadsd Ds Gn ,epd eind bComFiy -r ,: !;t lLr. . . i ; l :r l i l l{ i l rt lrd r qti ' r^rl l i9i: l+,11\- em+,i , -,:r. ift",rl.

.ysuq8d b b cs€rcond rbns d ssubrd lo Tems ad cd@ l.l:

o n L y a i d w l h L n h . t m B d c | € d l n !

E d ftr|tld

clsnH L.Do'|b.t - Trhd

Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE

T66i R.6ultls)

PART t.lAME No.1

No.: CE/2011/84950 Dale :2O114ZO1

2OA, CH63OO ZUG / SWITZERLAND

Page'.2 of 7

t I] t l

SILVER COLORED METAL WIRE (INCLUDING THE PLATING LAYER)

Te3t lt6m(s) Unit Method MDLR.3ultNo,l

Cadmium (Cd) mg/KgWith reterence to IEC 62321r 2008 andperfomed by ICP-AES.

n.d.Lead (Pb) mgKg 24Mercury (Hg) mS/kS n.d.Hexavalent Chromium Cr(Vl) With reference to IEC 62321: 2008 and

pedormed by Boiling \r€ter ext€ctionMethod.#

Negative

Sum of PBBS

mgikS With reference to IEC 62321: 2008 andperfomed by GC/MS.

n.d.Monobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.o.Pontabromobiphenyl n.d,Hexabrcmobiphenyl 5 n.o.Heptabromobiphenyl n.d.Octabromobiphenyl 5 n.d.Nonabrornobiphenyl 5 n.d.Dec€bromobiphenyl 5 n .d .Sum of PBOEa n.d.Monobromodiphenyl ether n.d.Dibromodiphenyl ether 5 n.o.Tribromodipheny! ethe. 5 n.d.Tetrabromodiphenyl ether n.d.Pentabromodiphenyl ether n.d.Hexabrcmodiohenvl ether 5 n.d.Heptabromodiphenyl ether 5 n.o,Octabromodiphenyl ether n.o,Nonabromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n.d.

eGlG{d rh s ied @d €nrclb Bpdcn€ry 'l+ !r ! rlrl . .n 1!ts,:r1,rtilr. ;l'!l* rrn . imri+Al'r-\r jrl4.f4! 1r€11hsdocmdssdby'h€c.mpany&bldlobcffi6|codibGo's*to. e.d'mc romal dmstu suq

d ^ t ' n d w l h L n h r m B d c r . d ! n d p o B d r t s t o G c s r a n d r h 3 d Mldrrgh6add]Ed'on6un6lh6'm

t',i!r: :d, dri:_ 11rs6rorPre

Test Report No. : CE/2011/84950 Date | 2011h21O1 Page: 3 of 7

tl]tIlltltfltttltPOLYFILAGOBERALLMENDSTRASSE 2OA, CH€3OO ZUG / SWITZERLAND

Test ltem(s) Unit method MDLResultNo.1

HalogenHalogen-Fluorine (F)(CAS No.: 14762-94-8)

mg/Kg With reference to BS EN M5A2,2007.Analysis was perfomed by lC.

50 n,o,

HalogenChlodne (Cl)(CAS No.: 22537-1s1)

50 n.d.

Halogen-Brcmine (Br)(CAS No.r 10097-32-2)

50 n.d.

Halogen-lodine (l)(CAS No.i 14362-44-8)

50 n.d.

Note :1. mg/kg = ppm : 0.1wf/6 = 1o00ppm2. n.d. = Not Detected3. MDL = Method Detection Limit4 - " - "=No tRegu la led5. '" = Qualitative analysis (No unit)6. # = a. Positive means the presence of CrVl on the tested areas

b. Negative mgans the absence of C l on the tested areasThe dgteci€d concentration in boiling-lvater-ext€ction solution is equalor greaterthan 0.02 mg/kg with 50 cm,tested areas.

7. The sample(€) was/wer6 analyzed on behalfof the applicant as mixing sample in one testing. The above result(s)was^^/€re only giv€n as the informality value.

'nrhstar€Fnd€f ontrorbsmpq3)Idd rhEbd,etsn6ndbGComFny f l t r , l r i 9 ! r . , r l i ] l : r r ! l { : : l : : ; l i ' ! i : l j i A r i i F -5 ! , [ 1 ' e t r ; ' f ' , , ' l ] l t ) [ l i 1 'n3dumd ts6su6d ' l hscomtsny5u*db t csccond1 t r sds

sib iv 6 10 6 o er 5d b6 @mntft,ltrrsandd odd3undrth€ta mol & €pdud depr 'n ju r, ftd

+l r l *J l : r (+s610r ) re t7e f +sitlfuirL!{:,r rr ir: i - i.hsror

IlF

Test Report No. : CE201'1/84950 OaL .2011h2,01 Pager 4

according to belo\ / flo /

POLYFILAGOBERALLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND

1) These sample6were da66olved totally by pre-conditioning methoda Cf' test method excluded )

Name of the pe6on who made measurement: Climbg€at YangName ofthe pe6on in charge of measurement: Troy Chang3)

ICP-AES

Sample Material Dige€tion Acid

S1eel, copper, aluminum, sold€r Aqua regia, HNO3, HCl, HF, HrO,

Glass HNO3/HF

cold, platinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic H2SO1, HrOr, HNq, HCI

Othe.s Any acid to totral digestion

ii. irei,.or if *q oy t . cop-r " ,g .oo-maa"J ' * .6b i " - ' *dco^d ' * "6 .Edrcn ico@isbdM!os@]bi.*ddb" -'d l,nsdd 6 *,* i5r

*l iq:i";* @"* -;d.." **o.ooissr,s.ry - r"

"rd;^ a * -nd .

rtf:r:: r1lirtii+ 1l i s6 io,t,e tTe t r s lo:)2e 'r7 ffiar(om

Acid digestion by suitable aciddepended on difierent samplemderial (as belo\ , iable)

Micro\rave digestion with

HNO/HCVHF

Heat to appropriat€

temperature to e,\tract

Cool, filter digestate

through filter1) Alkal iFusion2) HCltodissolve

at 540 nm by UV-VIS

Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE 2OA,

No. : CE2011184950 Oale'. 201 lh2lo1

CH43OO ZUG / SWITZERLAND

Page: 5 of 7

t l | l [ ] | | I t t | l

PBB/PBDE1) lllanE of the person2) MnE of the person

analytical FLOW cHARTwho nEde npasurenEnt: Ronran Wongin charge of nEasurenent Troy Chang

Scrcen analysis

" " " " " 1 " " " " " "

Sanple extraction/So*rlet rEthod

ConcentratdDiluteE)dracbd solution

First testing process -----t

Optional screen process -.--

Confinmtion process - .>

-s."pb---_-]--------r-------[S-r-tp]-j-a"arn"-_l-----r----

Ft ler

Analysis by GC/liS

cm€ry r r ' r j l j r ) t r . : r i l i " . : . l ! i * i , ; i i l ' r l t : e l . t i l : i l r t / . 1 \ ' l r Fn . r ' j : 1 . ' t l 6+

to €sd'o'c ramd dm6tu suq

d^t ,nd vihin rb rmis ot cr€d s i3'lbr.ohbadd€donsu.ddsera od b. repdued eiceol itul wiher

! idsnrzorNe-tu!acirrrer/*l:r/f,!.r +!!4J1i:irlre 02)r!e

I

Test ReportPOLYFIL AGOBERALLMENDSTRASSE

No. : CE/2011/84950 Daie | 2011h21O1

2OA. CH-6300 ZUG / SWITZERLAND

Analytical flow chart of halogen content

1) Name of the p€rson who lmde rneasuredEntr Rita Chen2) llan€ of the person in charge of nEasurerEdt: Troy Chang

Page: 6 of 7

comoad N]r]F,j!:ir.. I tiir lt{!l; ;]]rltl.1!- . r. irtsih-{} I 11 FiT . f!l r19i!+l

fi"JHl"l;liiii',i!',i.iwi;c"ry"';ti"-"c*""tc"t.^a sriu*-t i*n d..",; ''jbl.n bi... .d c.d*" 6, €. a " ' ' i i a - - o e , " a a . ^ * * ' ; . n b a d " i s d l b d i b m a i o ; d k . d h ;

; ; ; q ; ; ; ; oo ,4a t ; . : 6 . ? .€6@- -hsd ; "db . - "b1 .

r L - I I i d l L a i

Sarple pretreatrnent / Separation

Weighting and putting safipte in cell

Orygen Bomb Cofibustion / Absorption

Dilution to fixed volurne

Analysisw€s perfornEd by lC

Test Report No. : CE/2011/84950 D€te 2011h2101 Paget 7 of 7

tl] tlt II][]lPOLYFILAGOBEMLLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND

* The teeted sample / pa is maaked by an arrow if ifs shown on ih€ pholo. '

" End of Report -

€(s) r6rd Th€ r6d rop.n @nd b rccomtsry rirl,,iirar.rr'ir,'r,:111!!1, iilrRj:itr r.il1' l:!11.!-em+iI, ra r';)n:ll 'Thsih{.d"**dbylh6c"np.nysub'db6G4€Ejcond1bngo{sld ,M6.6al &dmsfu' sub]rendir,e'@ d ru d dbn s€s ibrh€! n reieds rhe cmp8.r's t ndn$ 3r rhe-y .d fu " t h " i . 6dc " " c ' * dDc . {5ny r ' j e cdnF i ys9s . s$;nshisandobroa,o3@do,rbta mdsrepd@sxepr'nlu.wM,sio,MtenaFro!3 drhecompanv a

,fl.d,+E+Test Report f i , S ( N " . ) , c E / 2 0 1 2 / ] 0 8 3 5

ELSCHUrcM ELEKTROSCHUTZI{OMPONENTENBAU GIIBHCEI'ERBESTR,ASSE 87, D-98669 \EIISDORF, GE&UA\Y

E 4 ( D a t e ) : 2 0 r 2 l 0 1 / 1 1 F & ( P a 8 e ) : r o f r o

Validit nownFor Oue5llPlease Co ith scs

|l] t|| fl m

trTxlt*.5G 68P 't&, -R & *,P +*&lf*P *AnTi d e l t i f i e d h y l o n b e h a t f o f r l e c l i e n t a s ) :

i iSZ,f*(s. 'p l" D€s.r ipr ion)i f gd&(style/ I r€b N". )4 , & . E ( c o u n t i y " f o r i s i n ){ t4 A S (s. ' !1" Rec€iving Date), t lHS&l(Tesrihc P€. i od)

(The fo l loe ins saDples ra . / rc re s rbe i t tcd and

SILIER PIATED & PURE SILVM $'IRES',tr+*sR (PLEASE REFER To PAGE s)

{EE (GERI4A\"Y)

2012/0t /04

2 0 1 2 / 0 t / 0 4 ' f o 2 a t 2 / a t / t l

j i , t ,+ jR(rest Resrl ts ) ' 5 + X . F - F { P r e a , e r e f p - r o r e x r ! a s c ! r

chrnLd lrbor.tlry - Trlpdp3G)6rad rb s rad Gpon€n'orF

? r ' - ; . ! l i i r i i . : i ) . : ! t l i i r . r . r r l ! t u l .

(Alw4?\

C$Fdft.|nd

McmbF or fie !69 Gouo 6c! Sr,.r

,fla,+E+Test Report

! t45(No. ) : cE/20I2 l lodJs

ELSCHUKOM ELU(TRqSCHUTZXOMPONENTENMU GVBHGENERBESTI{ASSE 87, D-98669'IIEIISDORF, CE!.T{Ar\Y

I t** (T.st Re6ul ts)

jrl:i *r'.i (PART NAME) No.l :

E q ( D a r " ) : 2 0 1 2 0 I / l l E * { p a s e ) , 2 o i l 0

]||lt[ttl||||fiml|!

ie;qma&ein& (6{t,r) (Jt6t ) (MTXED ALL mLoR tltErAr Nrm( INCLUDING TIiE PLATINC LA\'ER) (6 TYPES) )

pelsr reded rhE bd rcpod Enid bec o n o a . y t r r , : 1 r 1 , r ! _ i ' , r r l - J i j i r n : : l , ] . r : . a i i . ; ; r t i ] 1 , . r , r j r , ! * .

iy $qd ro b cene6 cdidroc d s

onlysndwibinlh.imlsoic€nls'ns

r|iiit E +lt( U r i t )

*ittri ttt.ttrlEtl{N(rDL)

s*(Resq l t )

N o , 1,fr / cadniun (cd) +arEc 623zLt 2oo8r; i , 4&,S*{

6€*.F+&4t*.*d,h;Fl. / q'i threfe.ence to IFC 62327t 2008 anlperforfted 6y ICP-AFS.

S / Lead (Pb) ++IEc 6232rt 2008ti1, rr t$A*t+t*fr+**i*,;*d&;il. / {i ih.e fe rence to IEC 62321: 2008 and

ter fo raed by ICP- , ES.

*- / vercury (Hs) ++ lEx. 62321 : 2008t&,'r€E*4+€ {/F + **t rt ;* d, *birl . / $i r1're fe rence to IEC 62321: ?008 andper fo rned by tCP- r {XS,

, i . f lJ ' / Heaav, lent chroni !n c . (v I ) ++ \F : 62321. 2OO8li*, t)a.,fr *+Rl iAt l l . / wi th fefe.€n€e ro IEc62321. 2 iAB and per formed byB o i I i n s s a t e r e x t . a c t i o n M € t h o d . #

} f r .+B** / Perrruo.oocranesu l fonates (PF!S-Ac id . Ueta l sa l t

nglka t+us EPA 3540C: 1996t i i , ' l i liE,9*f 1[-r*&}f,4 an+,t,4*69'/ t r i th reference to us EPA 3540c1996 n€thod for PFoS Co. le. l .Analys is was per lorned by tClMS.

I O

an+6.(J+) / PFoA (cAs No.: 335 6?r )

++US EPA 3540c: l996tt ! , ,Xt l&Eif 1{r*{,*fl an+d(n) }f/ wi th refetenc€ to US EPA 3540C1996 eethod for PFOA Content .Analys is was per fofned by rc /MS.

l 0

rfla+E+Test Report f t 4 ( N o . ) : c E / 2 0 I 2 l r 0 8 3 5

ELSCHUKOM ELEKTROSCHUTZKONPONENTENBAU CMBqGMERBESTRASSE 87, D-98669 !'EIISDORF, GERMAIr\

E J q ( D a r e ) : 2 0 t 2 l 0 t E * . t e , B " / , 3 . r r o

lll l ]tl| ]t

d{t E +4o(Uni t )

,{fi,t*( Ie thod)

,illt,rlEIE{I(IDL)

r**( R e s u 1 t )

N o . lt*t**'ts / su! of PBtss

*trEc 623211 zoo$iiF, ,tfu|aE+8dl f : *d,&j r l . / $ i th rererencero IEC 62321: ?008 and per fornedby rc/MS.

:14#* / uonobronobiphenyt: i *#f ' / Dib.onobip l tenyl: ;Ad* / Tr ibronobi phenylqA#tr i / Tet rabr6nob L ohenvlI *#X i / Pentabronob r ohen! I

?!4$it / Hexabronobi phenyl 5+iASf / Heprab.onobi phe.y1 5^i t r f i A / o . rabronobipheDyl 54)qS* / Nonabromobipheryt 5+;ASf / Decabronobi phenyt 5t*AS.t&t" / suo of PBDES- ;ASf ! { / Monobronod i Dhehv l e ther 5=-r [#*e / Dibronodi phenyl ether 5: ; A # + a { / ' l r i b r o d o d i p } e n v l e r h e . 5B,*S iFa* / Te t ra6 .onod i phe.v l e rher 5i ;*Sxad / Pe.rabromodi Dh€"v l ether 5' r*S*a* / Heaabronodi phervt erher 5-k ;A#Xa{ / Heptabromodi Dh€nv l e ther 5, \ ; *SXa{ / ocrabronodi Dhe.v l e ther 5,L ; i#*e i Nonabromodi Dhenv l e t le r 5+&#i i4 / D€cabronodiDhenvl ether

a* / s"l.s."6* ( f r . ) / Halogen-Floo. ine (F) (c{sN o . : 1 4 ? 6 ? _ 9 4 - 8 )

ng/18

ltBs vt r4s82:2007, vx&+8fr{ r }* t . / s i rh reference to Bs ENI 4 5 8 2 r 2 0 0 7 . A n a l y s i s v a s

5 0

6* (5. ) / Haloeen-chlo. ine (c l ) (cAs

! o . : 2 2 5 3 7 - 1 5 - r )5 0

&* (* ) / Haloren-Bronine (Br) (cAS

l { o . : 1 0 0 9 7 - 3 2 - 2 )5 0

6fr (dU / Halocen-lodine (I) (cASN o . : 1 4 3 6 2 - 4 4 - 8 )

5 0

hrr.(s) rssbd rh s resr €pon ennd bc o n F i v ; " r 1 l l u . , [ r ' r , l : i / i r r . r I i . t l l t ! , l r ' i i q l L r L t [ ] ! .

o y g l b r e d b b 6 a i . ' a l c o n d l o i s d s

3 p d J b ' t } 6 l o b c € d a ^ d h s d o c u

,F{a+E+Test Report f f6(No.) : CE/2012l10835

EI-SCHIrXOI1I ELEKTROSCHUTZ(oVPO|iENTU\]BAU GttBHGEI/ERBE.STT.ASSE 87, D,98669 VEITSDORF. GERVIIY

aBlJzr.) . 20L2/ot/71 Ftk(pare) : 1 of r0

[]tl||t][]tI| l

f i i i ( N . t . ) :

l . m g l k g : p p m ; 0 . | w t % = l o o o p p n2 _ n _ d . = N o r D e t e c t e d ( * . t A r r )

3- MDL : Met lod Detect ion L i r i i ( r l t lA; { ts1816)

4. ' - = Not R"sulated (Sl i ,+&.6)

5 . r ' = Q u a t i t a t i v e a n a L y s i s ( N o u n i t ) _ € , B r ) * f ( * + & )6 . # : a . P o s i t i v e b e a ! s t l e p . e s e n c e o f C r V t o n t h e r € s t e d a r e a s

(po s i t i ve *,F rq,l it E q.tF jq r{ ,r{l rS)b. Negat ive neans the absence of CiVI on rh€ rested a.eas

( Nesa t i ve i nr::tl *, E 4 t.tA ).14 'r1l1g )T h e d e t e c t e d c o h c e n r r a t i o n i n b o i l ] n a - e a r € r - e x r r a c t i o n s o l u t i o n i s50 cn: tested ar .a" . / l i6 ; i {XA>0.02 nslka * i ih 50 cm, ( tested

z. tte.i,tlS{r.'Af ;F./.**isArxl:{, , *E+ titi,sA,tt:ri}: +.Tftt 4 +1Erll+-ttlt aiAE.(The sanp les sas /were ana lyzed on beha l f o f the a t f r i can t as mix ing sanpre in one resr ine . The above! e s u l t s w a s / w e r e o n l y g i v e n a s r t e i n f o . n a t i t y v a l u e , )

PFos++*d,(R"f " ' .o"€

Inf or lat ion) ' !A+ 2oo6t rzztEa (Di rect iae 2006/t2ztw)(1 ) riitrrf rTfi.'|tsld.&n,r+r+4rrf, d.Ee,Ed,rlE*tla+,i6d.n,+0. 005%.

(May no t be p laced on the marke t o . used as a sDbstance o . consr i tuent o f p reparar rons€ q u a l i o o r n i g h € r t h a n 0 . 0 0 5 % b y n a s s . )

(2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE,i.&+,i!d.i, i fo.r%,6*r&€d.4{tt i.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,.( M a y n o t b e p l a c e d o n i h e n a . k € t i n s e n i - l i n i s n e d p r o d o c t s o r a r t i c l e s , o r p a . t s r h e r e o f , i f u r ec o n c e n t . a t i o n o f P F O S i s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o fs t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . s o r , f o . r e x r i t e s o r o t h e . c o a r e dnater ia ls , i f thc anoun! o f PFOS is equa l to o . h iahcr than Ug/nr o f thc coated na ter ia t . )

c o m p a i y t r : ; r , r ; : i r l , , ; - f i t . r l J r . n i r r , . r , , t i i L t l t t r 1 i . , r " . l , r ! / , ) !

ont and ub'n ihs h b or c en'3,ns

€ q u a l o r g r € a r e r t h a b 0 . 0 2 m A l k g w i t h

- . 4 t t r - ! . ! , , : r r i r l l i - . I c i eoaF i - : . r ; : : r l n t i , , ; i +46 iD r , ss r7

,rla#+Test Report

f t ,q(No. ) : cE/20r2lr0835

EI-SCHIXOi,I ELEKTRO€CHUIZKNTPONENTENMU CVBHGEIIERBESTInSSE 87, D 98669 IEIT,SDORF. GERILUY

E S ( D a t e ) : 2 0 1 2 1 0 1 / 1 1 F * . ( p a s € ) : 5 o r l 0

[t[t tl| |||ll

t l&4!t(styl . / I t . ' N". )( B - 1 ) 1 0 1 . 0 1 4 - s i l v e r p l a t e d c o F p e . { t r e - C u . A g - - %( B - 2 ) 1 0 1 . 0 1 3 1 . - - - - - p u r e s i l v e . s i r e - A g l ( ) ( ) ( )( B - 3 ) 1 0 1 . 0 1 2 3 . 0 - - - - s i l v e r p l a t c d p u r e s t n i c k c t v i r e - N i 9 9 . 9 8 % . A g I %( B - 4 ) 1 0 r , 0 1 8 2 . 0 - - s i l v e . - c o p p e r a l l o y p l a t e d c o t p e . c l a d v i r e - E l c o n D ,( B 5 ) 1 0 1 . 0 1 2 0 . 0 - - s i l v e r p l a t e d c o n s t a n t a n w i i € - C u N i 4 4 , A A S %( B - 6 ) 1 0 1 . 0 1 5 1 . 0 - - - - c o p p e r - n i c k e t 4 4 a l l o y s v e r p l a r e d s i . e - c u N i 4 4 ,

p sG) rssr€d rh s€d Gpon€ind ecoDoanv t l r I t ! . , r - N ' | , r " l : l , i l l l i : . ! 1 1 : ; ! 1 , 1 \ ! r l l l r i l l r l .

ont 3nd *ii'n rh. hrs or c €nr s 'ns

r i . : l , ; l - " : I q : j 1

,fl-d,#+Test ReportELSCHUI{OM ELEKTROSCHUTZKOMPONENTENBAU G\!BHGEWERBESTRNSSE 8?, D 98669 WILSDoII, CERMA\Y

r)

f i { 5 ( N o . ) : C E l 2 0 1 2 l l o s 3 s E S ( D a r e ) : 2 o t z l 0 r / t t F # ( p a s € ): 6 0 f l 0

[l|[]|l t]n]l

2)3)

ll?cr,-F $,EEn zI*1+ ' *.& aia*t+ . ( *1' j&d *tt *hrl. ) / Thes€ samDtes !,€€d€sotued rolrrry by p.e-condrumhg methoo accoding lo betN now chad. cP re€t method excludeor.lri^l: $e ! / Nahe otlne ps6on who made nEsuremed: ctimbgreal yangir'13{ I i ^ : tl4* / Name of the pe6on in charge or measu€m€nlr Troy chans

f [*a{*4+*it{rtc / rcP,aEs

f!911L / samde Matedal ;filt&AJlfi / DiqesL|onAcd

51eel, @pper, allnirum, solder-t+, 4la{, !lt, nn*, el,,k /Aa@ reoia. HNO' HCl. HF. H,O,rra{,Inc / HNoJftF

A, J6, €, nit /Gold, olalinum, Dalladium, ceramic

rti!€ /HNOr&E / Plaslic *d, t{"*, s!t, td / H,so. Ho,. HNor hcl

,! \'efi*1eti*l+ / Any acld lo lotal dig€Gtion

r i l , i , j i i r i r + ! . r 1 r . t p . l i , . 1 , i f i ' ! ! l .r hcdddne i iAs€dbysgcompa^ys !b4d {ob6a i . . a | cond lo i 3ds

tr*. {rtt*s /curing. p€galaton

iqr{.&,cf ! / sdde MeasuEmenl

&lf;F n l*'.g 6t t{ f, 6 }xn!tr ai&it,tirt /LoeT t4,;) /Acid dig€slion by suitabte acid depended ondtrerenlsahdemaledat{asbetowiable)

4rt/!inlt n.i'la{&,aib /MiorcMve digestion with HNO3/HC|/HF

,"rl4rOf jit& jt.li,lilt +C( / H€i to appropriate

1) &ltgti / Alkali F6ion2) ta{*tt /HCltod$d€

4?,*i&8tt$ / coot,fher digestate lhrough liher

,i( f rf 7h-ir,g t.rLrlf,.' Iirl#B*i{Aftrcnm 6id

ab6o6ance at a/ro nm byUV-VIS

,F{a*R+Test ReportELSCHUKOM ELEI$ROSCHUTZKOIIPONENTENB,qU GMBHCETERBESTRA.SSE 87, D-98669 VEIISDORF, CER[{AI\'Y

iEIS(No.) : cE/2012l10835 E rr? (Dare) : 2012l01/11 F&(P,s")

l t l||tI l

t ttt*/t rtt+4+f *,aE / PBB/PBDE anatyticat FLOW CHARTa }l{,/\l I a_i9*, / Name ofthe person who made measuremenl: Roman Wonqr,$Ji( fr t ^ : &+le / Nam€ of the person In charge of measurement Trcy Cha;gn^ ld,ElF / First lestry proce.s ------------f€*,E&*€F / OptionalscE€n prccess ....,---.*{.€,S / Confimation orccess -. -,t

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pslsl bdad h€rad cpod€nnorb3c o m D a n ! + " , I r i r r , , : i ; r . l J : ? . l r i a 1 . : - ! i - j ! , A l r I i . , . - l : r 3 1 1 . !

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rF{-d,+E+Test ReportEI.SCHUI(OM ELEI{TROSCHUTZ(OMA)NENTENB,{U GVBIiGE9ERBESTTASSE 87, D 98669 \,'EIT-SDoRF. GEf,Vl}IY

f t 1 4 ( N o . ) , C E / 2 0 r 2 l 1 0 8 3 5E S ( D a r . ) , 2 o l 2 l l ] t / t t F & { p r s e )

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it+&fiAn / Analyticalflow chart of halogen content

jtli{,l.F : gi',g* / Nane of the person who made me€surement: Rita Chenjrl:i,A ll, : #,*e / Name of the person in cbarge of measurement: Troy Chang

*+E &t&.'sl' IAnalysis wE6 perfomed by lC

np61s) rssbd fu bn cpod €nnor b. I i r i t i - 1 " j ! : L i i i ' ! r ] - l i . ' . i i r i : l l r

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i t4(No. ) : cE/2012l10835

E-SCHUKOM EI-E(TROSCHUTZKO]\IIONENTEN&{U GMBHGEFERBESTRASSE 87, D-98669 VEIISDORF, CERMA]\ry

AS(Dare) : 201210r/ tr F*.(pase) : 9 of lo

tI|fll|t][taf, l

*Ji+n+fin€n /Analytical flow chart ofSoxhtet extraction (LC/MS) procedure

r i A/-F : ij!9*y / Name ofthe person who made meesuement Rcman Wongr t4j :{, q i,\ : tF'.*4 / Name of the person in charge of measurement: Troy Chang

( rd8,{ a : Afi.+n*.n/Afi.+rt(*) , **.:4i{bA4, /Test ltems: PFOS/PFOA . Benzotriazole )

*{* / Datia

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trl'd,#+Test ReportELSCHTJKOM ELENROSCHU'\ZKOMPONENTENBAU GMBHGEISRBESTR.ASSE 8?, D.98669 WII-SDOTF, GERVA}Y

f i6(N". ) , c-E/2072/10a35 Es(Date) : 2tr2/ar/r1 E*@aEe) : r0 of t0

trlt[tl fl|||trr

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10835

Test Report No. SHAECl216714748 Date: 25 Sep 20 1 2 Page 1 of 5

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO'' LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE' CHINA

The follorving sample(s) wasl/verc submitted and identified on behalf of the clienb as : LEAD'FREE SOLOER

WIRE

sGS Job No. :

Part No. (P/N) :

Composition :

Date ol Sample Received :

Testing Period :

Test Reqlested :

Test Method :

Test Resulb :

Condusion :

sP12-028285 - SH

YTW1o8 (692535-001' 692535-003 )

Sn3.0CuRE21 gep 2012

21 Sep 2012 - 25 seq 20 12

Seleded test(s) as requested by client.

Please refer to next page(s).

Ple€se refer to next Page(s)Based on the perfrcrmed tests on submitted samples, the results of Lead'

Mercury, cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB)' -Polybrominatecl diphenylethe6 (PBDE) comply with the limits as set by RoHS

Direciive 2011/6tEu Annex lli recasting 200295/EC.

Signed for and on behalf ofsc$csrc Ltd.

,zQv"-Fan Jingjie, JJApproved Signatory

rhb@drb &.d tt tu cqryry aDld b b-

r4rg,.giffi:iii; ftH,#'ffiffiffiffffififfii';:i;c*;ivi ;f -d.urb-r-brbcld-n

tltrridtarblnlud.'i.groh 2@+t.rt.lE6lufte+eet al:4

iElE6-?1Fa€m9 wd{rm*.oeagms . *!|h.e4(!ii

108{S.?r)61{!!anL(d-21nl4@a

ri.rnb.lol0|. Sos oollP (8oS S )

Teet Report

Test Resufts :

No. SHAEC1216714748 Date; 25 Sep 2012 Page 2 of 5

Test Part Desc.iption :

SpodmqrNo. SGSSandolD D*qiptlon1 SHA'12167147.041 Silvery wire

Rema*€ :(1 ) I mg /kg= 1 PPm=00001%(2) MDL = Method Detedion Limit

(3) ND = Not Detected ( < NIDL )(4)

"" = Not Regulated

RoHS Diradv€ 201 1/65/EU

Test Method : with reference to lEc 62321i2008(1) Determination of Cadmium by ICP-OES.(2) Oetemination of Lead by ICP-oES(3) Determination of Merdiry bv ICP'OES(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis

(5) Determination of PBBS / PBDES by GC-MS'

Test ltem(s)

Cadmium (Cd)

Lead (Pb)

Mercury (Hs)

Hexavalent Chromium (Cr(Vl))

Sum ol PBBSMonobrcmobiphenylDibrcmobiphenylTribromobiphenylTetrabromobiPhenylPentabromobiphenYlHexabromobtphenylHeptabromobiPhenylOctabromobiphenylNonabromobiphonylDecabromobiPhenylSum of PBDESMonobromodiphenyl ether

Limit ud! M0!100 mg/kS 2

1000 mSftS 2

1000 mS/kg 2o

1000 mgkg- mSikS 5- mdkS 5- mS/kS 5- ms/ks 5- mdkS 5- mg/kg 5- mg/kg 5- mgftS 5

mdkg 5- mS/kg 5

1000 mS/kg- mdkg 5

@1ND55ND

NegativeNDNDNDNDNDNDNDNDNDNDNONDND

;i;a' ir*&{.d n dnl.,.d/bb 6rr.{.tt.d '

tlrr'ttafi$bDd|rddna.{rofr !93{l -I*.*trBlt!l8aea3+l aI: 2@

rE E6+r)B1a@ IEE€GA)6|€Sdrgnj{c-2rtauozg $i6GA)4|d063

M.n&r ot fi. Soa or.r0 (8Gs sA)

sGqTest Report

Test ltem{s)

Dibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl elherPentabrcmodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl elherOctabromodiphenyl elherNonabromodiphenyl ethetDecabromodiphenyl ether

Notes :(1) The maximum permissible limit is quoted ffom direclive 2011/65/EU' Annex ll(2) ospoltest:

Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;

Ohe tested sample should be further vedfied by boiling-wateFexlraction method if the spot test result

is Negative or cannot be confimed-)oBoiling-wateFextraction:Negative = Absence of Cr(Vl) coatingpositive = Presence of Cr(Vl) coating; the detected concentration in boiling-wateFextraction solution is

equal or greater than O.O2 mg/kg with 50 crn" sample surface areaForcorosionprotectioncoatingsonmeta|s:|nformationonstorageconditionsandproducliondateofthe tested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time

of testing.

No. SHAEC1216714748 Date: 25 Sep 2012

ud! Mot @1mg/kS 5 NDmS/kS 5 NDmdks 5 NDmSikS 5 NDmg/kS 5 NDmSftS 5 NDmdkS 5 NDmS/kS 5 NDmdkS 5 ND

Page 3 of 5

tird!

iiiiir-r'ud-poa-t.ovbrk.md(.rrrd'

ttlEttlFYErto d!| |lqsrflddctrr 2@ rE E64r)6la{!54rii('-zl5r4&t4

ra€6+1F*n19f{! (6-er)6,La6t+l -ll.*tr6lurlftaer+gttl l|: 2a@

€mD.r ot !h. sGE GrcuP (8GS SA)

Test R€port No. SHAECl216714748 Date: 25 Sep 2012 Pag€ 4 of 5

ATTACHMENTS

RoHS Testing Flow Chart

1) Name of the person who made testing: Jan Shi/Yoyo Wangr'Allen XiaolGaryXu2) Name of the person in charge of testing: Jeff Zhanglceorge Xu/ Linda Li3) These sampleswere dissolved lotally by pre-conditioning method according to betow flow chart. (Cf'

and PBB!,/PBDES test method excluded)

Sample PrepaEtion

1) Alkali Fusion /DryAshing

2) Acid to dissolve

Heating to 90-957for extraction

Adding 1,5-diphenylcalbaAde

for colordevelopment

Adding 1,5-diphenylcarbaade

for colordevelopment

A rcd colorindicatesthe

presence of cr8t.necessary,

Pb/CdHg PBBs/PBDES

t6&tttY|laf{dpdtrd,st{iatr @'Fr.-*.ltrEtdttidotsr+l lr:2@3

r ErE F2!) 8r@53rll Fzl6lil&5aa

I€EF{|FMDrij F€i)i6063

lLint r ot th.sos Gro{p (8GS s,l)

Teet Report

Sample photo:

No. SHAEC1216714748 Oate: 25 Sep 2012 Page 5 of 5

sHA12-167147.041

SGS authenticate the photo on odginal report only

". End of Report '_

tu&.{drbdnrtbtu d..{d I bd rr h orFry ndd b rr oodr c.ddr o, sdi- rtu orr..r. hrlbd .rrh i!ra..!...* t'd @r'oqtuqd n rmr d c.du| @ Edmr o.eid d tlndrsso&E sEs4!ll4.r-ril_kr.rllnddb end r. dn-d b.k*r'd!. dnfu i.d| dr6 i. ct'e6r'.bffimidror. h.&,dr.dr4ffiFLb.tur&ldFcu&..rdLl&lr rd.&k, .bglfuoi.lb..oo&qan6pihtun,riMt st'ff..'|erEdctuc.ir4d|n-tu|i-.hAnrdrrrd

't6.h.nril*dnN..rnhidrtb6 |hpr.Gl6H.

fbtlnsll||lto dftnrada.cfirr ?w rEl.Fa)flroe5a r€.EFtl6&9 w.o.!.ch-tl'*,EEldJlsaol€tl i*@ u!9Fa)6l.aa!Da t{jF46ea .{.d*reg.@

[.tn!.rolfr. scaGr.{, {8GSA )

nov'TEST REPORT

NO.:4002E11121307-2R02 Oa!aiDec15,2o11 page 1 of4

Customer: Suzhou FuHong Electrcnic IndustfialCo, Ltd.Addrgs8: NO.89WEl DU ROAD, WANGTING TOWN, XTANGCHENG D|STR|CT, SUZHOU, CHTNAReport on th6 3ubmitted ssmple said io beSample name: Fusos copper shellllodol: /

Material: /D$cription: /Buyea: /supplier: /

Sa|nple recelved date: Dec.13,2011Tcatlng p€riod: Frcm Dec.13,2011 to Dec.15,2011

T€tino Reau6tedAs specined by client, to delermine the L€ad, Cadmium, Mercrry & Hexavatent Chrcmium content in the submitted sampte inaccordance wilh Direclive 2002/95/EC (RoHS).

Tcstind method:

Testing llem [,leasudng inslrument MQL

Lead (Pb) EC 62321: 2008, seclion 9 ICP-OES 2mglkg

cadmium (Cd) EC 62321: 2008, section I ICP€ES 2 mg/kg

Mercury (Hg) EC 62321r 2008, section 7 rcP-oEs 2 mg/kg

Chrom'um (Cr l'I) EC 62321:2008, Annex I 0.02mg,a(g'

ILS, PLEASE REFER TOTHE FOLLOWING PAGE(S)'**'

lsg-'0.02 mg/kg returs 10 lhe MQLofsample extEction tiquid.

99!s!.c!i9!j-ffien tesied as specifred the submitted sample complied with the requircments of commission Decision of 18 Aug 2005amending Directive 2002l95/EC nolified lnderdocument 2005/618/EC

',:,"il:::i" ryf4lffH*"",",We-i hr n

,3ffi::::1,,44

S}'EI{ZN€N AOV TGSTING T€CHNOlOGY CO.,L'D.KUNSHAN EiANCH Hotllne86-512-5510 8000

6novNO.: 4002E11121307-2R02

TEST REPORT

Add the digestion solution; thevessel is heated Lrntil lhe sampl€ Add HrO, u nlil the sampl€ is clear

F;;1.-F;;,",..;-1.-{Melal subslrat€)

Add lhe digestion solution, clos€

the macrowave vess€|.

Cooling the vessel, fllleri washed and

filled to the mark with distilled water.

The sample is digested in the

micrcwave oven following a specific

decomposilion program.

and l\rercury Content: (Praring)

_____-l coor,ns. nrr", *""n"0 ""0 r"o | ,l o*o -ill_.;*--;-l

I to the mark with Dtwater I I r*r.r*t | | -.- |

STIENZH€N AOV TESIING T€CIII{OLOGY CO.,lIO,KUII9HAN BFANCH

Hdpi/j,w.o{,6n

Hotline86-512"s510 8oO0

Cooling the vessel, filter washed and

filled to the mark with distilled water.

Remove the sample, and coollhe beaker lo rcom tempefalure,and do 1ie color reaction

Heal 50 mL ofDlwaterin lhe

beakerto boiling for 10 min

Test the sample solution and lhe 0.02mg/kg standard solution by UV-VIS.

To Detemine

nov.NO.: 4002E11121 307-2R02

5. To Detemine Hexavalent Chromium- '' ',.'1re$eo ovr I r

s.t sw-resi (M&

TEST REPORTDate: Dec.15, 2011

Contentln colorless and colored ctlromate coaling on

Page 3 ol4

metals: (Plating)

lflhe lest resull is positive,

the sample is considered 1o

have hexavalenl chromium

and the 0.02 mg/kg

Boiling- waieF extractionprocedure shall be used to

lfthe€ isrnterference orI rs hard to decide *terhellhe sample have the hexavalent chrcmium

5 2 Boiling- wEter- en€ction

Take the (5015) cm'z

sample in the beaker.

Srmple d93cription:

SH!NZHEN AOV TESTING TCCTNOIqGY CO.,L}D,KUNSHAN BFANCH nHot l ine86'512^5510 8000

Remove he sample, and cool

lhe beaker 1o room temperature,

and do the color reaction

Heat 50 mlof Olwater in the

beaker lo boiling for 10 min

Test the sample solution and the 0.02

mg/kg standard solution by UV-VIS.

Copper shell subslrateLead wle Platrng 24 Copper shell Plaling

Unil RoHS

Limit 2-3 24"Lead (Pb) mg/Kg 1000 N.D. 2.5 40.0 N.D.Cadmium {Cd) mg/kg 100 N,D. N.D. N.D. N.D.Msrorry (Hs) mg/kg 1000 N.D, N.D, N.D. N.D.Chromium (Crvl) mg/Kg 1000 Negative Negative Negalive Negative

nov.TEST REPORT

NO.r A002E11121307-2R02 Dat€iOec15,2011

-The new RoHS di.ective 2011/65/EU, on Jul 21, 2011 come into force, on Jan. 03, 2013 the fomat imotementation. Dircctive

2002l95/EC shall be reoealed simultaneouslv.

Sp€cim€ns, wnicn requested to determine Lead, Cadmium and l4ercury Conlent, have been dissotved comptetety.-mg/kg=ppm

-N.D.=not detected(<tVoL)-MQL=l'rethod Ouaniilation Limit-Negalive=Abs€nce of Cr (VI);

Posilive=Prcs€nce of Cr (VI)i

Uncedain= c€n noi ve fy whether the sample have Hexavat€nt Chrcm ium by spoliesl.(The tested s€mple should be furlher venfed by boiling-waterextradion method if the spol test result is uncertain or

-'The test is based on the following assumption:The sampte ptating is a singte tayerand each pad is unifom. The test resuttmaybe cannol sland ior rhe physicartruth of sample plating.

Photog.aph ofSample

"'End of Repod"'

S'iE'!ZH€N AOVT€STING TECXNO!OGYCO..lIO,KUNSHAN ABANCH

Hh,:/fuloi6n nHotline86-512-5510 8000

Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SHAH00299967

PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI

MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER

PAGE 1 OF 9

APPLICANT: LITTELFUSE,INC. DATE: JAN 18, 2012 800 E. NORTHWEST HWY

ATTN: A. CESISTA/ K. BACILA

SAMPLE DESCRIPTION: One(1) Submitted Sample Said To Be White Yarn. Part Description : Yarn. Part Number : 648115. Date Sample Received : Jan.11, 2012. Date Test Started : Jan.11, 2012. ***********************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 9

1 (Ⅰ) Test Result Summary :

Testing Item Result (ppm)

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million = mg/kg ND = Not detected

Responsibility Of Chemist :Ken He

(Ⅲ) Test Method:

Testing Item Testing Method Reporting Limit

Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography

50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 9

(III) Measurement Flowchart:

Test For Halogen Content Reference Standard： EN 14582

**********************************************************************TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask

make up with deionized water

sampling/grinding or cutting

analyzed by ion chromatography



TESTS CONDUCTED

PAGE 4 OF 9

2 (I) Test Result Summary :


Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 9


Responsibility Of Chemist :Dent Fang / Ken He

(II) RoHS Requirement:

Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 6 OF 9

(III) Test Method:


Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content


2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

DATE SAMPLE RECEIVED : JAN.11, 2012 TESTING PERIOD : JAN.11, 2012 TO JAN.13, 2012

**********************************************************************TO BE CONTINUED

(IV) Measurement Flowchart:



TESTS CONDUCTED

PAGE 7 OF 9

Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008

**********************************************************************

TO BE CONTINUED


weigh sample and for different

material, digest the sample with


Cd/Pb/Hg

analyzed by ICP-OES

weigh sample and add alkaline solution

definite temp.

make up with deionized water and add diphenyl-

carbazide solution

Cr6+

weigh sample and add organic

soxhlet extraction or

solvent extraction

concentrate the extract and make up with organic

PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples

boiling water extraction

metalpolymers / electronics

negative*2confirm the tested samples are totally

dissolved No

cool and filter the extract



TESTS CONDUCTED

PAGE 8 OF 9

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected. **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 9

**********************************************************************

END OF REPORT





PAGE 1 OF 9

APPLICANT: LITTELFUSE,INC. DATE: JAN 18, 2012 800 E. NORTHWEST HWY


SAMPLE DESCRIPTION: One(1) submitted sample said to be White yarn. Part Description : YARN. Part Number : 648150. Date Sample Received : Jan.11, 2012. Date Test Started : Jan.11, 2012. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 9



Halogen Content Fluorine (F) 370 Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND



(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 9



**********************************************************************TO BE CONTINUED










TESTS CONDUCTED

PAGE 4 OF 9



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 9






TO BE CONTINUED



TESTS CONDUCTED

PAGE 6 OF 9

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


DATE SAMPLE RECEIVED : JAN.11, 2012 TESTING PERIOD : JAN.11, 2012 TO JAN.13, 2012

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 9



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 8 OF 9

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 9

**********************************************************************

END OF REPORT





PAGE 1 OF 15

APPLICANT: LITTELFUSE,INC. DATE: NOV 01, 2011 800 E. NORTHWEST HWY


SAMPLE DESCRIPTION: One (1) submitted sample said to be Green ink. Part Description : Ink – green. Part Number : 425907. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15

1 PHTHALATE CONTENT TEST

WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND RESULT (%,W/W)

(MAX.) DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND ---

SUM OF THREE PHTHALATES ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 (FORMERLY KNOWN AS DIRECTIVE 2005/84/EC) FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.

DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED % = PERCENTAGE BASED ON DRY WEIGHT OF SAMPLE/COMPONENT

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

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MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS

**********************************************************************

TO BE CONTINUED

Weigh sample and place in a thimble

Extracted by Soxhlet extraction with organic solvent

Concentrate the extract

Analyze by GC-MSD

Make up with organic solvent

Transfer the extract into a volumetric flask



TESTS CONDUCTED

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Halogen Content Fluorine (F) ND Chlorine (Cl) 400 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample =

mg/kg ND = Not detected


(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15



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TESTS CONDUCTED

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Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

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TO BE CONTINUED



TESTS CONDUCTED

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(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4


TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15


WITH REFERENCE TO ASTM D3421, BY GAS CHROMATOGRAPHY-MASS

SPECTROMETRY (GC-MS) ANALYSIS.

RESULT (%, w/w) LIMIT (%, w/w) (MAX.) DIBUTYL PHTHALATE (DBP) ND 0.1 DI(2-ETHYL HEXYL) PHTHALATE (DEHP) ND 0.1 BENZYL BUTYL PHTHALATE (BBP) ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER

PRODUCT SAFETY IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.

DETECTION LIMIT = 0.01% (w/w) ND = NOT DETECTED % = PERCENTAGE BASED ON DRY WEIGHT OF SAMPLE/COMPONENT.

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

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MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS **********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

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5 (A) TEST RESULT SUMMARY:

TESTING ITEM RESULT(ppm)

HBCDD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :

TESTING ITEM TESTING METHOD REPORTING

LIMIT

HBCDD (HEXABROMOCYCLODODECANE)

WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS

10 ppm

DATE SAMPLE RECEIVED : OCT.25, 2011 TESTING PERIOD : OCT.25, 2011 TO OCT.28, 2011 **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

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MEASUREMENT FLOWCHART: TEST FOR HBCDD (Hexabromocyclododecane) CONTENT **********************************************************************

TO BE CONTINUED

Weigh sample and place into a thimble

Soxhlet extraction with organic solvent


Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT





PAGE 1 OF 15

APPLICANT: LITTELFUSE,INC. DATE: OCT 31, 2011 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA

SAMPLE DESCRIPTION: One (1) submitted sample said to be Black ink. Part Description : Ink – black. Part Number : 425902. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15


**********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 15



Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND




(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15



**********************************************************************TO BE CONTINUED










TESTS CONDUCTED

PAGE 6 OF 15



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 15






TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 15

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:




TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 12 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 13 OF 15






LIMIT



10 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 14 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT





PAGE 1 OF 15

APPLICANT: LITTELFUSE,INC. DATE: NOV 01, 2011 800 E. NORTHWEST HWY


SAMPLE DESCRIPTION: One (1) submitted sample said to be: Red ink. Part Description : Ink - red. Part Number : 425901. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


*********************************************************************** TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15


**********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 15







(II) Test Method:



50 ppm


TO BE CONTINUED