ICP Test Report Certification Packet/media/electronics_technical/icp_test_reports/tvs_diode... · 1...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: Lightning Surge Protection – TVS Diode arrays Product #: SP4061-04UTG, SP4062-04UTG

Issue Date: August 1, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the Diode Array RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：.

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 N/A Wafer 1 3-6 2 N/A Wafer 2 7-11 3 N/A C194_PPF Plating Lead frame 12-42 4 N/A Adhesive 8600 43-47 5 N/A Copper Bonding Wire 48-59 6 N/A Epoxy Molding Compound 60-67

Validit nownFor QueatiPlease Co ith scs

TeSt RepOft No. rcE2o11/11s52 Date " 2o11to1ha

EPISIL TECHNOLOGIES INC.NO. 3. INNOVATION RD 1, SCIENCE BASED INDUSTRIAL PARK,HSIN-CHU. TAIWAN, R, O, C.

Page :1o f 4

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The following sample(s) was/were aubmitted and ideniifi€d by/on behalf of th€ client as :

Sample De6ciptionStyle/ltem No.Sample Receiving DateTesting Period

IC WAFERALUIVINUI/| PROCESS2011t01111201 1 tl1t1 1 TO 2011 tO V18

Test Requ*tod

To3t l$ethod

ln accordance with the RoHS Direclive 200295/EC, and itsamendment directives.

With reference to IEC 62321: 2008Procedures for the Determination of Levels of Regulated Substancesin Electrotechnical Prcducls.

(1 )(2)(3)(4)

Detemination of Cadmium by ICP-AES.Determination of Load by ICP"AES.Determination of Mercury by ICP-AES.Determination of Hexavalent Chromium by UV y'isSpeclrometry.

Please refer to next Page(6).Test Result(s)

Ibl.St|Fd lbtSGS TAIWAII Icft.,r crl lrbontory - Trlpd

CnFry +:ti€t.r, . .r !Erl r:r.lil, ;;1rllt ll r' ,!i'lli+14r1\rii;:l _::. f-{1!ftE dlrlmed 3 sdth6mpaf u . 6 o d m . l o m a l d m s f u s 6 ]

tudms i ' .y fte k@tssdb,slb..ohtsadobl€d'oisgndgihe@

/ i , 4 i i , i - eo4 rs r r

Test Report No. : CE/201li 11952 Date : 2011/01/18 P a g e : 2 o f 4

EPISIL TECHNOLOGIES INC.NO. 3, INNOVATION RD 1, SCIENCE BASED INDUSTRIAL PARK,HSIN.CHU. TAIWAN, R, O, C.

Test results by chemical method (Unilt mg/kg)

Ilflfltnfirlt]l

TEST PART DESCRIPTION:: IIULTICOLOR WAFERNo.1

Note : '1. mg/kg = ppm; 0.1wt% = 1000ppm2. n.d. = Not Detecled3. MDL = Method Detection Limit

npsG)rsdd rh3 rd r@n 6nd bcmFry 4rfij€re,. "r iri:r!:/*:|; ;i:jl l:.a ( . rtiil{114]) =:j:!t.f!l::163Dtrdffd3adbyh6mFny&6JdlofuGmd|cddfuBdsgvfu6.dm.lbmdd€]T3d336]

rdo.! fany th. cmFnts so€ r6pfsb,9nro 6cisr'd63tu

rf I r "Et!'frJr)i+s6orre

Te€t ltem (s): mdhod(Rofor to)

R€6ultI/|DLNo.1

Cadmium (Cd) ( 1 ) n.d. 2Lead (Pb) (2:) n.d-Mercury (Hg) (3) n.d.Hexavalenl Chromium Cr(Vl) byalkaline extraotion

(4) n.d. 2

Test Report No. i cE/2011/11es2 Date:2011t01t18EPISIL TECHNOLOGIES INC.NO. 3, INNOVATION RD 1, SCIENCE BASED INDUSTRIAL PARK,HSIN.CHU, TAIWAN, R. O. C.

Page : 3 of4

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1) These samples w€re dissolved totally by preronditioning method accoding to betow flow man.( Cf test method exctuded )

2) Name of the person who made mgasurement: Climbgreatyang3) Name of lhe person in charg€ of measurement: Troy Chang

Cuttjng / PrepaEtion

Sample Measurcment

Acid digestion by suitable aciddepended on diferent samplematerial {as b€low table)

Microlvave digestion with

HNO3/HCt/HFAdd appropriate amount ofdigeslion rcegent

Heat to appropriate

temperature to exttact

Cool, filter digestate

lhrough filter

Add diphenyl-cabazide for

color development

mea6ure the eboorbance

at 540 nm by UV-VIS

Sample Material Digestion Acid

Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, HrO,

Glass HNO3/HF

Gold, platinum, palladium, ceramic &ua regiaSilver HNOg

Plastic HzSOr, HzOz, HNOg, HCI

OtherB Any acid to tobl digestion

cmtsny 4+r jfr:thrl . I lits,l4!r{?jr; -.i1.rlli'tl rt . }}i+ iX,i-{rr\ r :ii. Fil . j.ij ,ftf;tr.6d@m€d ! sd by h cdhFny &br.d ro G Gmdcddi66 or sw

&4rd b Ims sd cmdiioB ior E m snoamsdhm Abd;6&5*;h,i.cr-d"b ^i

fttr,'ehisandobrearo3undgrhgrd p.ry aryumdhoddabd;m

r ! I r . x . + r ! t t l rn i? r+s610r )28

Test Report No. : CE2011/11952 Date: 2011/0'1/18 P a g e : 4 o f 4

EPISIL TECHNOLOGIES INC,NO. 3, INNOVATION RD 1, SCIENCE BASED INDUSTRIAL PARK.HSIN-CHU, TAIWAN. R. O. C.

ll| tt][ttIlIl

" EndofReport '*

oclr0nd T[t bsl r@d €nd b €c@Bry +j,j{:f,,! . _r]]p:trr:r{i.; :1ir1t]:i:q r.{:it:\rl!t\ iij i, 1. 1. I .,J.,!f t sd@nd ts *u6d ' ! r 6comFnysub rd lobGn9Ecmd toBds*

a b ] a d b r m s s i d c m d f u B b . E g l o l h a l m e l o i o i € b t y

@Bb 9Gro 6c i 61 ' ^dbs tu

a i i s6 o zenD r r e D , -

Test Report No. TSNEC1100213801 Date: 01 Jun 2011 Page I ofs

BEIJING YAN DONG IVIICROELECTRONIC CO,,LTDNO.2,WANHONG ST.XIBAJIANFANG,CHAOYANG DISTRICT.BEIJINGCHINA

The following sample(s) was^^/ere submitted and identified on behatfofthe ct;enb as :TRANSISTOR

SGS Job No.Model No.Client Rei Information

'1068557 - TJTransistorModel No.: Digital Transistor. Switching Diode. Schottky Diode. VariableCapacitance Diode. TVS. Zener. Photo-D. Photo-T. J-FET. Standardline€rVoltage Regulator. Low Dropout Regutatof. DC-DC Convertor. Audio powerAmplmer. Operational Amptifer. Voltage Compafators. Hall Sensors. DIAC.scR. TRAtc27 May 201127 May2011-01Jun2011

S€lected test(s) as requested by ctient.

Ple€se refer to next page(s).

Please refer to next page(s).

Date of Sample ReceivedTesting Pedod

Test Requested

Test Method

Test Results

Signed for and on behalf ofscs-csTc Ltd.

7@Reab€ca ZhouApproved Signatory

ar @F.d. ordby br cdqi o, rkN !.d rip.llw {r.ffi.nr_Tq_.-.!4!!!r

f"i#ffi 'FrHl'!ffi;tu"[1]lt:tlih1{{l"itrT::#'#1l#{kYfrh.tun.i.tu dh,;

sosM.rion,t'lo,a1,Th. 6m Aq6 TEoAtbdtn,cnh. 30a5? r lt6€t66aam | 6"?2t2529e5etr.:!lqgt!!l!!g!!!Flr!9s*r rrr3mar r(s2)652eo6 r(&a6re56c

, :I

Mrmberor Ih6 SGScrouD(SGS SAt

Test Report

Test Results:lD for specimen '1

Description for specimen 1

H€w m&l{s)

Test ltem(s)Cadmium (Cd)Lead (Pb)Mercrry (Hg)Hexavalent Chromium (C t) byalkaline extraclion

Nole:1. mg/kg = ppm2. N.D. = Not Detecled (< MDL)3. MDL = lrlethod Deteciion Limit

Fhn€ Rgtardenfis

Test ltem(s)

Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTelrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobrornodiphenyl etherDibromodiphenyl etherTribrornodiphenyl elherTetrabromodiphenyl etherPenlabromodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl etherOclabrornodiphenyl etherNonabromodiphenyl etherDec.bromodiphenyl elher

No. TSNECl100213901 Datq Ol Jun 2011 page2of5

: TSNl l-002138.001: yellowsilver-glay sheet with gr€y reseau (mix all)

UnitmgKgmgkgmgftsmg/Kg

Test lr€thod (Reference)IEC 62321 Ed. 1 : 2008, AASIEC62321Ed.1:2008,AAS

IEC 62321 Ed.1: 2008, ICP-OESIEC 62321 Ed.1:2008, UV-Vis

Result MDLN-D. 2N.D, 2N.D, 2N,D. 2

Result lrDLN.D.N,D. 5N,D. 5N.D. 5N.D. 5N.D, 5N.D, 5N.D, 5N.D, 5N.O. 5N.D. 5N.D,N.D, 5N.D, 5N.D. 5N.D, 5N.O. 5N.D, 5N.D, 5N.O. 5N.D. 5N.D. 5

Unit

mgkgmg-/ksmsngmg/rgmg/Kgmg/(gmg/Kgmg/(gmgKsmgKsmgKgng/K9mgKgmgKgm9K9mgKgm9Kgmg/K9mg/kgmg/Kgmg/xgm9Kg

Test lllethod (Reference)

IEC 62321 Ed-1:2008, GGMSIEC 62321 Ed.l:2008, GGMSIEC 62321 Ed. l: 2008, GGMSIEC 62321 Ed.1: 2008, GGMSIEC 62321 Ed.1:2008, GC-MSIEC 62321 Ed.1:2008, GC-MSIEC 62321 Ed.1: 2008, GC-I.4S|EC62321 Ed.1: 2008, GC]VSIEC 62321 Ed.1: 2008, cC]tISIEC 62321 Ed.1:2008, cc-ltrls

IEC 62321 Ed.1: 2008. cC-[4SIEC 62321 Ed.1: 2008, cc-lrsIEC 62321 Ed.1: 2008, cC-lrsIEC 62321 Ed.1: 2008, cC-[4SIEC 62321 Ed.1: 2008, cC-[4SIEC 62321 Ed.l: 2008, GC-lllSIEC 62321 Ed.1: 2008, GC]llSIEC 62321 Ed.1: 2008, GGMSIEC 62321 Ed.1r2008, GC-MSIEC 62321 Ed.'l:2008, GC-MS

rh.turr.bdnys.con .ir&brdb(.G.or.rcftrerors.mdd_&qrio ed @ftdr,.ultd b rlm.nd cdik r r0 osflltr.r q.{r qoiq.n! <+a!r h6_iffi-iirf, 66lf,EtF?

d 6 d h A . ' M d h d o e dl lehhi.dcr.d ffil n.ry. ri.c.@ryr or.lsdb r

i@bn t.u..tu cdh.a.ri.k, iy. fir{. ..filmdri.c.@ryr ebwdb r Lb 6.d.0.eb.tu.6i

. idtrh si.bn@d!*r.rtbrh.drb(.)b.E

| (s-24698&O I t&ra6?E5er (ts-2)654&O r €&4me

: I SCSM.io.,l|oa1,Tn sdr rvruTEo4l|.jtn,dli|!s.5?

I tr.:l!_r-$44q!I1a,!qe4! !?!i!9gqM€mbor ol t'. sOS grcup (SGS SA)

Test Report

Nole:1. mg/kg = ppm2. N.D. = Not Deteded (< tvDL)3. MDL = Method Detection Limit4. '-" = Not regulat€d

The sample(s) waJwere analyzed on behalf of lhe applic€nt as mixing sample in one testing. The aboveresult(s) was^/vere only given as lhe informality value and only for refurence.

No. TSNECl100213801 Dale: 01 Jun 2011 Page 3 of5

[email protected].,rrbrh.n.b(.)r.d.

scs rldidlno,al, n 5or a..orEoAltr4h,chs 3oo.5tSl.:ltlttt{tati*j.1||scstt tt:3oa5r

r {*-24632l& r (&2a29$e| (!-?a354&0 i (&{4@ . |!.drrcF9.@

M6nbd ol |h. AGS G|oup {SGS SA}

Test Report No. TSNEC1100213801 Dale: 01 Jun 2011 Page 4 of 5

ATTACHMEl{T8

cd/pb/Hg,rcP/pEEtspBoEt Ftow chtlt

1) Namo ofth6 pErson \ryho made tssting: Aaron Wang/Jason Li /Angell yao

4 Nam6 ofthe person in charg6 otteEting: Cindy yin/R€x Zhu3) Thgse sampl€s wel€ dissolvsd totally by pre-condilionang method according to

b.low now chai- (Cl end PBBS/PBDEs test meihod .)(cludsd)

ireqdro(ro.E.. codb.dedhtreild&bldbr.m.d na.tu.&tr.dlii. aldFDtiffiibiFffidb&qd b r.m.d ccdrn br F.did.c bM i ns.ei/h.-.eo!.d,ih ^ir6;i 6--6lliiii6, t

ddh .dndd | ' i . c@ ' ' r ih l i b d q | d h f u . @ ' r | i t r h . c . [ F i

i i 6rr bn ryn.rrr olLy ro r. !nrNG) r.{.d

scs Msrh.,rb,41,Tlr 5fl Av.MI:DAIEnjrn,ChiE:S.57 | (S-,2)65A&+l.llli{*ittt8li*r11rls0s*f Il:s45r r(s-?)os@@

1W4W2 ff-6..!!6I i&4&2 . t!.cl*ro.r.6

Sample Preparation

Sample M€aBurem€nt

Acid dig88tion rithmacro$ava/ holplat6

Sample solv6ftertraclion

Adding digestion reagsd

Concsntretiod0ilution of€xtfaction

s0tutDn

Fihralion and pHadjustment

1)AlkeliFusion /0ryAshinga Acid lodissolYe

Adding 1,+diph6nylcarbazide for

color daYelopmenl

Pbr'Cd/tlg PB.T./PBDE.

M6nb ol rh. SGS 9rorD {SCS SA}

Test R€port No. TSNEC1100213801 Date: 01 Jun 2011 Page 5 of 5

Sample photo:

TSN11-002138.001

SGS authenticate the photo on original report only"' End of Report '"

k & h ' . i y r . i c h r a h d e d

uE.nbrnt&4dandb[prdud.rc.et|i ' ! l | 'dh' ',dd,i l.n'dud.rc.pt|i ' ! l | 'dh' ',dd,

rhos { sh rd,Fn d.. oirr ro 6.rp.(.rrd

scs .ra6,Noa1.n. $h ,vdM1EDr,ft4in.drd 300.st r {s-?466am | {ts-?2125er552 lw.hlc..dFl.iliiE i+*lali*r,|r.tscs*l al:3m4r r (!-a6t e t6-245aQ52 ..e.drEortd" , I

M6hbrt or th6 SGS Groro {SGS SA)

Test Report No. I CE12011t42129

SAMSUNG TECHWIN CO,, LTD,42, SUNGJU-DONG. CHANGWON. KOREA

Dale:201114120 Page: 1 of 31

Validi nownFor QueaPlease C ith scs

lll]tIltt]flllllll

The following sample(s)

Sample DescdptionMaterialStyle/ltem No.Buyer/Order No.Sample Receiving DateTesting Period

AYAU11-01607 (ONE SAMPLE OF LEAD FRAME)METALALLOYC194-UPPFLF_RoHS-1 1 040GE0(X2011t04t132011tMh3 70 2011n4t20

was/were submittod and identified by/on behalf of the client as:

T65t Result(s) : Please refer to next page(s).

Ch-dcd Lk brY-TdFd

p€(9 bied ris bn,eood €iior.acomranv i ' r ! 1 , i l r ' r r - 1 ' : r . r r r . " J i l n . l [ . t ; i l l i i l ] 1 . . , ! . J . r . r 3 ' ! 11 .

iygbjdlo6cene6fuiditonsdse0'6qidaddal5't'! ' 'deon€q

ont :nd vhn rh. ihrs or c ,6d s ns

chehke L{* nw!.hldiadwd L lr.FjlE;1,,:{1@60lre

lor|rSi|tldftrr|d

Test Report No. . CE12O11142129 Dale: 2O11l4l2O P a g e : 2 o f 3 1

SAMSUNG TECHWIN CO,. LTD,42, SUNGJU-OONG, CHANGWON, KOREA

SILVER COLORED METAL SHEET

lll ]|l! |l[] !

Test Resultls)

PART l.lAME No.1

Test ltem (s): Unit lrethod I'DLResultNo.l

Cadmium (Cd) mg/Kg With refe.enc€ to IEC 62321r 2008 andperfomed by ICP-AES.

2 n.o,

Lead (Pb) mg/Kg With reference to IEC 6232 1 : 2008 andperformed by ICP-AES.

2

Mercury (Hg) mg/Kg With referenc€ to IEC 62321: 2008 andperformed by ICP-AES.

2 n.d.

Hexavalent Chromium Cr(Vl) bySpot test / boiling water extraction

With referenc€ to IEC 6232 1 : 2008 andperformed by Spot test / boiling waterextraclion Method. (See Note 8)

0.02mg/kgwith 50 cm'z

surtace

Negative

Antamony (Sb) mgikg Wilh reference to US EPA Method30508 forAntimony Content. Anatysi6was performed by ICP-AES.

2 n.d.

Beryllium (Be) mgikg With reference to US EPA Method30508 for Beryllium Content. AnalysiswEs performed by |CP4ES.

2 n.d.

Bromochloromethane (CAS No.:74-97-5)

mgKg With reference to US EPA 502 1method. Analysis was performed byGC/MS.

1 n.d.

Sulfur Hexafluofide (SF6) (CASNo.:2551-62-4)

mg/kg With eference to US EPA 5021method. Analysis ! ras pedormed byGC/MS.

1 n.d.

2- (3,tui-ten-buty12-hydroxyphenyl)-2H-benzotriazole(CAS No.: 38,{+71-7)

mg/kg With reference to US EPA 3540Cmethod- Analysis was performed byGC/MS.

5 n.d.

PVC Analysis uras performed by FTIR andFLAME Te6t.

Negative

Bromomethane (CAS No.: 74-83-e)

mgikg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

compant 4" .1 . i J l , - :R i r r r r j i l l n r j , i i , . ! I * f !1 r1r I I , r r lu l t l t rrh s dneil s ,su8d br be cohpany rqed b b &israr co.d ' ois dr s

- " 'o: " o "" dh. .-.r,o d si ,

o^t rnd v bn rh. rmis d c 6 s 'ns

! rds.dzo@ N4rriF.'rrdqio/! I Ir!!. !:a6j3,,,;t+s6olree

Me6bnd6e*s6relp66s5AJ

Test Report No.'.CE12011142129 Dai:e 2011t4t20 page: 3of 31

SAMSUNG TECHWIN CO., LTD.42, SUNGJU.DONG, CHANGWON, KOREA

itl tllt]lltNl

Test ltem (s): Unlt lrethod MDLResultNo.l

Polychlorinated Biphenyls (PCBS)(CAS No.: 1336-36-3)

mg/Kg With reference to US EPA 3540Cmethod. Analysis was pedormed byGC/l,,lS.

0.5 n.d.

Polychlorinated Terphenyls(PcTs)

mg/Kg With reference to US EPA 3540Cmethod. Analysis was pertormed byGC/MS.

0.5 n.d.

Alkanes, C1G13, chloro (ShodChain Chlorinated Paraffins) (CASNo.:85535-84-8)

With reference to US EPA 3540Cmethod. Analysis was performed byGC/MS.

0.01 n.o,

Polychlorinated Naphthalene(PCNS)

m9Kg With reference to LJS EPA 3540Cmethod. Analysis was pertormed byGC/MS.

5 n-d-

Perf I uorooctane sulf onate6(PFOS)PFOS - AcidPFOS - lletal SaltPFOS -Amide

mg/Kg With reference to US EPA 3540C:1996 method for PFOS Content.Analysis was perform€d by LC/MS.

1 0 n.d.

PFOA (CAS No.: 335€7-1) mg/Kg With reference to US EPA 3F!40C:1996 method for PFOA Content.Analy6is was performed by LC/MS.

1 0 n.d.

Organic-tln compoundsTributylTin (TBT) (CAS No.r 688-73-3)

mdks With reference to DIN 38407-13.An€lysis ,,r€s performed by GC/FPD.

0.03 n.d-

TriphenylTin (TphT) (CAS No.:66&34-S)

mg/kg With referenc€ to DIN 38407-13.Analysis wes performed by GC/FPD.

0.03 n.d.

Tributyl Tin Oxide (TBTO)"' (CASNo.: 56-35-9)

mg/Kg With reference to DIN 38407-13.Analysis\ ras performed by GC/FPD.

n.d.

HalonsHalon-1211 (CAS No.: 353-59-3) mg/Kg With reference to US EPA 5021

method. Analysis was performed byGC/MS.

'I n-d.

Halon-1301 (CAS No.: 75S3-8) msyKg With r€f€rence to US EPA 5021method. Analysis ',,€s performed byGC/MS.

1 n.d.

Halon-2402 (CAS No.: 124-7!2) mSikS With reference lo US EPA 5021method. Analysis \r/as performed byGC/MS.

1 n.d.

pstsli€$ed rhs Gn,eood e^idl becomp.ny i i r i : I l t . , ! -F ' r r r l , ' r l l i l r4 i r . t l i i i ! j t t - ! I 1 . r . l t j ) * .rhsdodhffrE sEdbyi[econpaiyslb]edb bG.iEE condloisd s

f r : r i r . i l , { : r , i t | i i ] r r l r46or rs

Test Report No.:CE12011142129 Date:201114t2O pager4of 31

SAI,IISUNG TECHWIN CO., LTD.42. SUNGJU.DONG, CHANGWON. KOREA

tt []|| lttttlt

Test ltem (a): Unit l/lethod I/|DL ResultNo.l

Sum of PBBa

mg/Kg With reference to IEC 62321: 2008 andperfomed by GC/MS.

n.d.lllonobromobiphenyl 5 n.o.Dibromobiphenyl n.d.Tribromobiphenyl n.o.fetrabromobiphenyl n.o,Pentabromobiphenyl 5 n,o.Hexabromobiphenyl 5 n.o.Heptabromobiphenyl 5 n.o.Octabromobiphenyl n.d.Nonabromobiphenyl n.o.Decabromobiphenyl n.d.Sum of PBDE3 n_o.lVonobromodiphenyl ether n.d.Dibromodiphenyl ether 5 n-d.Tribromodiphenyl ether 5 n.d.Tetrabromodiphenyl ether 5 n-d.Pentabromodiphenyl ether n.d.HexabromodiDhenvl ether 5 n.d.Heptabromodiphenyl ether n.d.Octabromodiphenyl ether n.d-Nonabromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n.d.AstrestosAclinolite {CAS No.: 77536S6-4) % With reference to NIOSH 9000 method.

Analysis wa6 perfomed by XRD.I Negative

Amqsite (CAS No.: 12172-73-5) % With reference to NIOSH 9000 method.Analy6js !€s pedormed by XRD-

'I Negative

Anthophyllite (CAS No.r 2536€7- With reference to NIOSH 9000 methodAnalysis was pertormed by XRD.

'I Negative

Chrysotife (CAS No.: 12@1-29-5) o/o With reference to NIOSH 9000 method.Analy6is was performed by XRD.

1 Negative

Crocidolite (CAS No.: 120U-2A4\ % With eference to NIOSH 9000 method-qnarysis wa6 performed by XRD.

1 Negative

a o m p a n y f i ' ! , r . r r l , i r i i i l i r r ] l r ' l r ' , i i : i . t f t t : . l \ . ' t . 4 I l r / j i r t .

ont 3nd wb'n rhs im k or c enr3,ftr@oB {ary rh. comp,ny 5 ero €srorsbrty F ro {s c sdandssdd

u idsrtdzoie N€vtdFi.l,rtrwr/ri_L,t:t- i::i4i+,,,tl86t0r)ree

Msb8iorrhe 56s6rcup(scs stu

Test Report No. I CEnU1l42129 Dzd'e :20jI4nO page : O of 3.1

SAMSUNG TECHWIN CO., LTD.42, SUNGJU-DONG, CHANGWON, KOREA

[[||||mn||!ll]l

T.8t ltem (s): Unit Method MDL RerultNo.1

Tremolite (CAS No.: 77536-68S) With referenc€ to NIOSH 9000 method.Analysis was performed by XRD.

1 Negative

AZO1): 4-AMINODIPHENYL (CAS No.:9247-1)

mg/Kg With reference to LFGB 82.02-2.Analysis wEs performed by GC/MS.

3 n.d.

2): BENZIDINE (CAS No.: 92-87-s)

mg/Kg With referenc€ to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.

3 n.d.

3): 4-CHLORO-O-TOLUIDINE(CAS No.: 95€9-2)


3 n.d.

4): 2-l.lAPHTHYLAl,illNE (CASNo.:91-59-8)


3 n.d.

5): O-AMTNOAZOTOLUENE (CASNo.: 97-5+3)

mg/Kg With reference to LFGB 82.02-2.Analysis wEs perfomed by GC/MS.

3 n.d.

6): 2-AMINO-4-NITROTOLUENE(CAS No.: 99-55-8)

mg/Kg With referenc€ to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

7): PCHLOROANILINE (CAS No.:10647-8)

mg/Kg With reference to LFGB 82.02-2.Analysis wa6 performed by GC/MS.

3 n.cl.

8): 2,4-DIAMINOANISOLE (CASNo.:6'15-05-4)

mg/Kg With reference to LFGB 82.02-2.Analysis wa6 performed by cc/l!ls.

3 n.o.

g): 4,4-DIAMINODIPHENYLMETHANE(CAS No.:101-77-9)

mgKg With reference to LFGB 82.02-2.Analysis ',vas performed by GC/MS.

3 n.d.

10): 3,3-DICHLOROBENZIDINE(CAS No.:91-94-1)

mgftg With reference to LFGB 82.02-2.An€lysis was perfomed by GC/MS.

3 n.d.

1 1): 3,3'-DIMETHOXYBENZIDINE(CAS No.: 119-9G4)

mg/Kg With reference to LFGB 82.02-2.Analysis w€s performed by GC/MS-

3 n.d.

1 2): 3,3'-DIMETHYLBENZIDINE(CAS No.: 119-93-7)

mg/Kg With reference to LFGB 82.02-2.Analysi6 was performed by GC/MS.

3 n.d.

13): 3,3'-DIMETHYL-4,4!OIAMINODIPHENYLMETHANE(CAS No.: 838-88{)

mgKg With reference to LFGB 82.02-2-Analysis u/as performed by GC/IVS.

3 n.o.

14): P-CRESIDINE (2-METHOXY-tMETHYLANILINE) (CAS No.:12G71€)

mgftg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

prals) r€d.d Tn 3 bd rsPod ennor bscompany ; r 1 , ! r ' l . r r _n ' : l , r i . r J ; i i l j l , l

' 1 , . , l l l ; l i i l r : r t , 1 . r i r ] r d l ! .

u Dd4(rzoiqN4rdF.[rTdwiD]!. tl r?r i::r.iitl..'t]s6(orre

rref, be, of 'he 9{9cdp 66s !Ar

Test ReportSAMSUNG TECHWIN CO., LTD.42, SUNGJU.DONG, CHANGWON, KOREA

No. : CE12O11142129 Oale : 201114120 Page :6o f31

l [ | l I l t tIt]ul

Test lt6m (s): Unit Method MDLRgsultNo.1

15): 4,4'-METHYLENE-B|S- (2-CHLOROANILINE) (CAS No.:101-144)

mg/Kg With referenc€ to LFGB 82.02-2.Analysis was perfomed by GC/MS.

3 n.d.

16): 4,4'-OXYDIANILINE (CASNo.: | 01-80.4)

mg/Kg With reference to LFGB 82.02-2.Analysas was performed by GC/MS.

3 n.d.

'17)r 4,4'-THIODIANILINE (CASNo.: 139€5-1)

mg/Kg With reference to LFGB 82.02-2.Analysis wEs performed by GC/MS-

3 n.d.

'18): O-TOLUIDINE (CAS No.: 95-53-4)

mg/Kg With reference to LFGB 82.02-2.Analysis was perfomed by GC/MS.

3 n.d.

1 9): 2,4-TOLUYLENEDIAMINE(CAS No.: 95-80-7)

mg/Kg With reference to LFGB 82.02-2.Analy6i6 was per{ormed by GC/lvlS.

3 n.d.

20): 2,4,s-TRIMETHYLANILINE(CAS No.: 137-17-7)

mg/Kg With reference to LFGB 82.02-2.Analysis was pertormed by cC/l\IS.

3 n,o,

21): O{NISIDINE (CAS No.: 9G.04-0)

mg/Kg With reference to LFGB 82.02-2.Analysi6 was performed by GC/l S.

3 n.o.

22): P-AMINOAZOBENZENE(CAS No.:60-09-3)

mg/Kg With reference to LFGB 82.02-2.Analysis was pertormed by GC/lllS.

3 n.o.

23): 2,4-XYLIDINE (CAS No.: 95-68-1)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by co/l\rs.

3 n.o.

24): 2,6-XYLIDINE (CAS No.:87-62-7)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/l\rS.

3 n,o,

HalogenHalogen-Fluodne (F) (CAS No.:14762-94-At

ms}/Kg v\/ith reference to BS EN 14582:2007.Analysis was performed by lC.

50 n.d.

Halogen-Chlorine (Cl) (CAS No.:22537 -15-1't

mgftg With reference to BS EN 14582:2007.Analysis ,l|€s performed by lC.

50 n.d-

Halogen-Bromine (80 (CAS No.:10097-32-21

mgftg With refer€nce to BS EN 145E2:2007 .Analysis was perfomed by lC.

50 n.d.

Halogen-lodine (l) (CAS No.:14 244-8)

mg/Kg With referenc€ to BS EN fl5A2:2OO7.Analysis wEs performed by lC.

50 n.d.

CFC's (Chlorofl uorocarbons)Group IChlorcf luorocarbon-1 1 (CAS No.:7s€94)

mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/[,rS.

1 n.o.

c o m p a n y ; " ! r / r l r ' L _ i ' i 1 r r j J i i i j r i ^ i : ! . r r l r l u i t i

j t + €6 ronrec r^ r+ o6lorree ry @!je,@h

Test ReportSAMSUNG TECHWIN CO., LTD.42. SUNGJU-DONG. CHANGWON, KOREA

No.: CE12011142129Da|e | 201114120 Page : 7 of 31

t l|t[ItlN]l

Test ltem (s): Unit Method MDLResultl{o.1

Chlorofluoroc€bon-12 (CAS No.:75-71-8)

mg/Kg With feference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

Chlorofluorocalbon- 1 13 (CAS No.;76-1!1)

mSikg With reference to uS EPA 5021method. Analysis was pertormed byGC/MS.

n-d.

(;htorof tuoaocarbon-1 14 (CAS No.:76-1+2t

msasWith reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Chlorofluorocarbon-1 15 (CAS No.:76-15-3)

mS/kS With reference to US EPA 5021method. Analysis was perfo.med byGC/MS.

n.d.

Group lllChlorofl uorocarbon-1 3 (CAS No.:75-72-9)

mgKg With reference to uS EPA 502 1method. Analysis wa6 pedormed byGC/MS.

n.o.

Chlorof luorocarbon-l 1 1 (CAS No.:3s+56-3)

mdks With reference to US EPA 5021method. Analybi6 was performed byGC/MS.

n.o.

Chlorof luorocarbon-l 12 (CAS No.:76-12-O)

mg/Kg With reference to US EPA 502 1mothod. Analysis was perfomed byGC/MS.

n.d.

Chlorof luorocarbon-21 1 (CAS No.:422-78-8)

mg/Kg With reference to US EPA 5021method. Analysis was pedomed byGC/MS,

n.o.

Chlorof luorocarbon-212 (CAS No.:3182-26-1)

mg/Kg With reference to US EPA 5021method. Analysis wtss performed byGC/MS,

n.o.

Chlorofluorocarbon-21 3 (CAS No.:2354{6-5)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Chlorof luorocarbon-2 14 (CAS No.:29255-31-0)

mgftg With reference to uS EPA 5021method. Analysis was performed byGC/MS.

n.d.

c o m F i ) ; i r r t l j l i . j , F i , l r l i r , ! r i t r + i : i . I , r t i r 1 , : j , . 1 , 7 . E l l r r l l l .Th5dodne i lA ! skhy1h6companysb jedbG6e ie€ | cond loBds€

suted b rems aid condloi3 br E Ad€doi s dram ro rhe rm,ho d ,ah ry,

spss ib ' t y€ l obce i l , nds3dd

Test Report No. '. CE12011142129 Dal..e | 201114120 page:8of31

SAMSUNG TECHWIN CO., LTD,42, SUNGJU-DONG, CHANGWON, KOREA

tl] flttl uttt|l

Test ltem (s): Unit Method MDLR€€ultI'lo.l

Chlorof luorocalbon-21 5 (CAS No. :425943-2')

mgikg With reference to IJS EPA 502'1method. Analy6is was per{ormed byGC/MS.

1 n.d.

Chlorof luorocarbon-216 (CAS No.:661-97-2)

mgftg With reference to uS EPA 5021method. Analysis was pedormed byGC/MS.

'I n.d.

Chlorofluo.ocarbon-21 7 (CAS No.:422-6-6)

mg/Kg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.

1 n.o.

HCFCs(Hydrochlorofl uorocaJbons)HCFC-21 (CAS No.: 75-43-4) mg/Kg With reference to uS EPA 5021

method. Analysis v/as performed byGC/MS.

1 n.o,

HCFC-22 (CAS No.: 75-456) mgftg With reference to uS EPA 502'1method. Analysis was perform€d byGC/MS.

1 n.d.

HCFC-31 (CAS No.: 593-704) mSI(g With reference to uS EPA 5021method. Analy6i6 was performed byGC/MS.

'I n,d,

HCFC-121 (CAS No.: 354-1+3) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

1 n.d.

HCFC-122 (CAS No.: 354-21-2) mg/Kg With r€ference to US EPA 5021method. Analysis was pertomed byGC/MS.

I n.o.

HCFC-I23 (CAS No.: 306-83-2) mgKg With reference to US EPA 5021method. Analy6i6 was performed byGC/MS.

1 n.o.

HCFCI24 (CAS No.: 2837-89-0) mg/Kg With reference to US EPA 5021method. Analysis wa6 pedormed byGC/MS.

'| n.o.

HCFCI3l (CAS No.: 3s9-284) mdkg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.

1 n.d.

hrrs(s) bi€d rh s led epdd eind bc o m p a n y f : " , 1 , i r l , a t i l , ' r i i t j | i i : i . t : u , i t ' , l t i i n r l r . r ! t l ] n . 'Th s @m6d 3 'ged by 6e cmpa

h€rm€dc derud6n

h* nghb 3nd obr9aiom u^der lis ra

i . : r i t , - 1 r r d r " , , : l l s6 iD8

M!nerdhes.s €,oup 11695a)

Test Report No.: CE12O11142129 Oale | 2O11|4DO paqe : 9 of 31

SAMSUNG TECHWIN CO., LTD.42, SUNGJU-DONG, CHANGWON. KOREA

It|tIm |ltt I

Test ltem (s): Unit Method MDLR€aultNo.l

HCFCj32b (CAS No.: 1649-08-7) mg/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n-d.

HCFC-133a (CAS No.: 75-88-7) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

HCFC-141b (CAS No.: 1717-005) mg/kg With reference to US EPA 5021method. Analysis \ /as performed byGC/MS.

n-d.

HCFCI42b (CAS No.i 75S8-3) mgikg With reference to uS EPA 5021method. Analysis \/as pedormed byGCiMS.

n.d.

HCFG221 (CAS No.: 422-26.4) m9/Kg With reference to US EPA 5021method- Analysis $ras performed byGC/t\rs.

1 n.d.

HCFG222 (CAS No.: 422-491) mg/K(l With reference to US EPA 502'tmethod. Analysis was peformed byGC/MS.

'l n-d-

HCFC-223 (CAS No.: 422-52€) mg/Kg With reference to US EPA 5021method. Analysis $/as performed byGC/MS.

'l n.d.

HCFC-224 (CAS No.: 422-54-8) mg/Kg With reference to Us EPA 5021method. Analysis M€s pedormed byGC/MS.

'| n.d-

HCFC-22sca (CAS No.: 422-56-0) mg/Kg With reference to uS EPA 5021method. Analysis v€s pedormed byGC/MS.

I n.d.

HCFG22scb (CAS No.: 507-55-'1) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/trs.

1 n.d.

HCFC-220 (CAS No.r 431€7-8) mg/K9 With referenc€ to US EPA 502 1method. Analysis wEs performed byGC/LilS.

1 n.d.

HCFC-231 (CAS No.r 421-94-3) mg/Kg With reference to US EPA 5021method. Analysis wtss perforned byGC/MS.

1 n.d.

c o m p a n y i t i , 1 , j : r r . - i r i i r . ' , r . l i : r l r r i i i . t l i j i a r \ . t . ! 1 , ! j , t i r : { .Th s @funi s 's!ed by 6e conp.

$bjed b rems sd coiddons tor E A&iloi 3 daw^ ro ss mraron oi riab iry

on | y3 |dw 'b ' n l h6 lmcdc6 i , 3ns

":-irin rr:r..ntt ,:t + e6(or),s * i+ s6 iirrre rr @ws<on

Membe dd€3636,oup6c!sA)

Test Report No.: CEJ2o11t4212s Date | 2o11t4DOSAMSUNG TECHWIN CO., LTD.42, SUNGJU-DONG. CHANGWON, KORE}.

P a g e : ' l 0 o f 3 1

I] |l|t]|l] ]tI| u

Test ltem (s): Unit Method MDLRe6ultNo.1

HCFC-232 (CAS No.: 460-89-9) mg/Kg With reference to US EPA 5021method. Analysis vr€s pedormed byGC/[,|S.

n.d.

HCFC-233 (CAS No.: 7125-84-0) mg/kg With refer€nce lo US EPA 502'lmethod. Analysis was performed byGC/MS.

n.d.

HCFC-234 (CAS No.: 425-94-5) mgks With reference to US EPA 5021method. Analysis was perlormed byGC/MS.

n.d.

HCFC-235 (CAS No.r 460-92-4) mg./Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

Hgl-g-241 (GAS No.: 666-27-3) mg/Kg With reference to US EPA 502'1method. Analy6i6 was performed byGC/MS.

n.d.

H9t-g-242 (CAS No.: 46063-9) mg/Kg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.

n.d.

HCFC-243 (CAS No.: 46049-5) mg/Kg With reference to US EPA 502 1method. Analysis wEs performed byGC/[rlS.

n.d.

HCFC-244 mg/Kg With reference to US EPA 5021method. Analysis $/as performed byGC/MS.

n.d.

HCFC-251 (CAS No.: 421-41-0) mg/Kg Wath reference lo US EPA 5021method. Analysis vr€s pedormed byGC/MS.

n-d.

HCFC-252 (CAS No.: 819-001) mg/kg With reference to US EPA 502'1method. Analysis was performed byGC/MS.

n.d.

HCFC-253 (CAS No.: 460-35-5) msikg With reference to US EPA 5021method. Analysis was peformed byGC/MS.

n.d.

HCFC-261 (CAS No.: 420-97-3) mgft9 With reference to US EPA 502'1method. Analysis was performed byGC/MS.

n.d.

conp . i i r i l r l l j r r ' j : L i ' i r . , i _ r r - 1 r j r i i r . t l i l : l j r l i r t I ! ! i r : l .r[ s dfuheil 5 'su.d bi be conp'

aqed b rems aid coid{o.s ror E aredon 3 d€". ro he Lmraroi or ,ab,,

tu r isia 5id od'qdioN under b0 r'

r:-rrlr!1 r:irrr :t1s6lo,rrerD ias6101pner, ___a*",

Test Report No. . CE12011142129 D e 201114120 Page: 11 of 31

SAIVSUNG TECHWIN CO,, LTD.42. SUNGJU-DONG, CHANGWON, KOREA

flrlr[ttflm rl

Test ltem (s): Unit Method MDLR€aultNo.'l

HCFC-262 (CAS No.: 421-02-03) mg/K9 With reference to US EPA 502 1method. Analysis wEs performed byGC/|VS.

1 n.d.

HCFC-271 (CAS No.: 430-55-7) mg/Kg With refercnce to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HBFCs(Hydrcbromof luo.ocarbona)HBFC-2182 (CHFBr2) (CAS No.:186&53-7)

mg./Kg With reference to US EPA 502 1method. Analysis wa6 perfomed byGC/MS.

'I n.d.

HBFo-2281 (CHF2Br) (CAS No.:1511{,2-2]-

m!/Kg With reference to US EPA 502 1method. Analysis \,vas pertormed byGC/MS,

I n.o.

HBFC-3181 (CH2FBr) (CAS No.:3735241

mS/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

HBFC-12184 (C2HFB14) mg/Kg With reference to US EPA 5021method. Analysis wEs perfonned byGC/MS.

I n.d.

HBFC-12283 /c2HF2BI3) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/t\4S.

1 n.d.

HBFC-12382 (C2HF3812) mg/kg With refefence to US EPA 5021method, Analysis wEs performed byGC/t S.

1 n.d.

HBFC-12481 (C2HF4Bt\ mg/Kg With referenc€ to US EPA 5021method. Analysis was performed byGC/[rS.

1 n.d.

HBFC-'13183 (C2H2FBr3) mg/Kg With reference to US EPA 5021method. Analysis vras performed byGC/MS.

1 n.d.

tlEF C- l 3282 lC2H2F2Br2\ mgikg With reference to US EPA 502 1method. Analysis was performed byGC/MS.

1 n.d.

Ij'-etll,tY""! b1 T.9T1.'sadv6d'ha ddnab;@ddmdh-6 hahsdrsmroNod;i

! L I t t : . { t r . r i : i , , . i +$6Fnxe

M€obsof ihe 6s6@p6G5 r1)

Test ReportSAMSUNG TECHWIN CO,, LTD.42. SUNGJU-DONG. CHANGWON, KOREA

No.: CE12O11142129Dale :201114120 Page | 12 of 31

r|tfl||t||[||r||l

Test ltem (s): Unit Method MDL RosultNo.l

HBFC-13381 (C2H2F3Br) mgikg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.o.

HBFC-l4182 (C2H3FBr2\ mdkg With ref€rence to uS EPA 5021method. Analysis we6 pedormed byGC/MS.

n.d.

HBFC-14281 (C2H3F2Br) mgxg With reference to US EPA 5021method. Analy6i6 was performod byGC/MS.

n.d.

HBFC-15181 (C2H4FBr) mgKg With reference to LJS EPA 502 1method. Analysis was performed byoc/MS.

n.d.

HBFC-22186 (C3HFB6) mg/Kg with reference to us EPA 5021method. Analysis wEs performed byGC/MS.

n.d.

HBFC-22285 (C3HF2B15) mg/Kg With reference to uS EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

HBFC-22384 (C3HF3814) mg/kg With reference to US EPA 5021method. Analysis was peafomed byGC/MS.

n.d.

HBFC-22483 (C3HF4B13) mg/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

HBFC-22582 (C3HF582) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

HBFC-22681 (C3HF6Br) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

HBFC-23185 (C3H2FB15) mg/Kg With r€ference to US EPA 5021method. Analysis was pertomed byGC/MS.

n.d.

tlBF C-23284 IC3H2F zBt 4) mdks With reference to US EPA 5021method. Analysis was performed byGC/MS.

n,o.

c o m F i y i i : , l 1 r r . j - F ' i , ! 1 i : . r i r r i f i . ! t i r i 1 . : t i l , 4 n L r t t ! , { .rhA dddnsl € 3ssd by he comp,

Test Report No.: CE12011142129 Date 201114120 Page: 13 of 31

SAMSUNG TECHWIN CO,. LTD.42, SUNGJU-DONG, CHANGWON, KOREA

I||||lrlt tI|ttll

T€€t ltem (s): Unit Method MDLResultNo.l

HBFC-23383 (C3H2F3Br3) mg/Kg With reference to t_JS EPA 5021method. Analysis was perform€d byGC/MS.

1 n.o.

HBFC-23482 (C3H2F4Bi2) m9/Kg With reference to US EPA 5021method. Analysis was performed byGC/t S.

1 n.d.

HBFC-2358,| (C3H2F58r) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

1 n.d.

HBFC-24184 (C3H3FB14) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HBFC-24283 (C3H3F2B13) mSikS With r€ference to US EPA 5021method. Analysis was pertormed byGC/MS.

'I n.cl.

HBFC-24382 (C3H3F3B12) mgikg With reference to IJS EPA 502 1method. Analysis was performed byGC/MS.

1 n,o.

HBFC-24481 (C3H3F4Br) mg/Kg With reference to Us EPA 5021method. Analysis was performed byGC/t\rs.

'I n.d.

HBFC.251B3 (C3H4FB€) mg/Kg With referenc€ io US EPA 5021method. Analysis \a€s performed byGC/t\4S.

1 n.d.

HBFC-25282 rc3H4F2BE\ mg/Kg With reference to US EPA 502 1method. Analysis wEs performed byGC/MS.

1 n.d.

HBFC-25381 (C3H4F3Bd mg/Kg With r€ference to US EPA 5021method. Analysis was perfomed byGC/MS.

I n.d.

HBFC-26'1 82 (C3H5FB12) m!/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

HBFG262Bl (C3H5F2Br) mg/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

p€1e) r€d.d tt bn cpod €nioi bec o m p a n y f / r , : t r l . L _ i ' i r | r J r l i j : t i r ' L l i i l | l , 1 . . r . , i r r t l ! .

o n | y 3 n d w ' b [ l b ! m b d c 6 i l 3 ' n s

TestReport No.:cEt2o11t4212s Date:2011t4t20SAMSUNG TECHWIN CO., LTD.42, SUNGJU-DONG, CHANGWON, KOREA

Page : 14 of 31

llr tlt t lr

Test ltem (s): Unit Method MDL ResultNo,l

HBFC-27181 (C3H6FB0 mg/kg With referenc€ to US EPA 5021method. Analysis wEs perfomed byGC/|VS.

1 n.d.

HFCa (Hydrofl uorocaJbon)HFC-23 (cHF3) (CAS No.:7546-7')


1 n.d.

HFC-32 (cH2F2) (CAS No.: 75-1G5)

mg/kg With reference to US EPA 5021method. Analy6i6 was performed byGC/MS.

1 n.d.

HFC41 (CH3F) (CAS No.: 593-s3-3)

mgftg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.

1 n.o.

HFC43l0mee (C5H2F10) mgftg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.o.

HFC-125 (C2HF5) mg/(g With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

HFC-134 (C2H2F4) mg/Kg With reference to US EPA 502'tmethod. Analysis was performed byGC/t S.

1 n-d.

HFCI34a (CH2FCF3) (CAS No.:811-97-2)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/t\rs.

,l n.d.

HFC-143 (CH3F3) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

1 n.d.

HFC-143a (CH3F3) mg/Kg With reference to uS EPA 5021method. Analysis wEs perfomed byGC/tVlS.

1 n.d.

HFC-152a (C2H4F2) (CAS No.:75-376)

mg/Kg With reference to US EPA 5021method. Analysis wEs performed byGC/MS.

1 n.d.

HFC-227ea (C3HF7) (CAS No.:431-89-0)

mg/Kg With reference to uS EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

mprec) bn€d rh e €3r '€pod €nnd *conF i y + r r 1 i , l . . 1 1 ' i , r l ] j , t : i i r ' i i : i . I l l i i . i t lrh s dotun6i1 s i$ud b) be comp'ny eled b ft c$srar cod i ois of setu € pinrd ov.dest avaiade on €qf o l e b . n o n c l o m a l d o d m s t s $ b l b h a L m l a l o n o i l a b ' t y

'.1r,:!? r: iilarr:...t + s6 {oare

Test Report No. I CE12O11142129 Dale. 2011t4t20 Page : 15 of 31


[r] rIla tmflll

Test ltem (s): Unit Meihod MDLResultNo.l

HFc-236fa (C3H2F6) mg/Kg With reference to US EPA 5021method. Analy6is was performed byGC/MS.

'I n.d.

HFC-236ea (C3H2FG) (CAS No.:43163-0)

mg/Kg With reference to US EPA 5021method. Analysis \ /as performed byGC/[rS.

1 n-d.

HFC-24sca (C3H3F5) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/r\4S.

1 n.d-

HFC-24sfa (C3H3F5) mg/Kg With reference to US EPA 5021method. Analysis wa6 perfomed byGC/MS.

1 n.d.

HFC-365mfc (C4H5F5) mg/Kg With reference to US EPA 502 1method. Analysis wEs performed byGC/MS.

'I n.d.

PFCS (Perfluorocadon)F14 (CAS No. 75-73-0) mgKg With reference to US EPA 502 1

method. Analysis was performed byGC/MS,

1 n.d.

Fluorocabon 116 (CAS No.: 76-164)

mg/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

Freon 218 (CAS No.: 7619-7) m9/Kg With feference to US EPA 5021method. Analysis ,.,ras performed byGC/t\rs.

1 n.d.

Decafluorobutane (CAS No.: 35t25-9)

mg/kg With reference to US EPA 5021method. Analysis vras pedormed byGC/[IS,

1 n.d.

Freon C318 (CAS No.: 115-25-3) mg/Kg With referenc€ to US EPA 5021method. Analysis w€s performed byGC/|VS.

I n.d.

Perfluor-l-butene (CAS No.: 357-26€)


I n.d.

perfluorisobutene (CAS No.: 382-21 { )

mS/kS With reference to US EPA 502 1method. Analysis was pedormed byGC/MS.

I n.d.

p3G)€srad rh s red €poneiiorsc m p . d y + i l r l i t . r r l ' i , i i . r ! i t l r r i r . I t i , l r r ! { 1 : . , r , r , , r l f r l .rh,3dodrem rs sued br'he cdhi,

a F . o . 1 6 - t " 6 l a b m d € d j

Test Report No. I CU2011142129 Date:2011t4t20 page:.t6of 3.1

SAII,TSUNG TECHWIN CO., LTD.42, SUNGJU-DONG, CHANGWON, KOREA

t l | ft lrrltt] l

Test ltem (s): Unit lrlethod MDLResultNo.1

1,4-dihydrooclaf luorobutane (CASNo.:377-36€)

mg/Kg With reference to US EPA 5021method. Analysis w€s perfomed byGC/[rS.

n.d.

Nonaf luorr- (trif luoomethyl)butane (CAS No.: 594-91-2)

mg/Kg With reforence to US EPA 5021method. Analysis was performed byGC/[rS.

n.d.

Perf luoron-pentane (CAS No. :678-26-2)

mg/Kg With reference to US EPA 5021method. Analysis M€s pedormed byGC/MS.

n.d.

2-pertluoromethylpentane (CASNo.:355-04-4)

mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/MS.

n.d.

Perfluorohexane (CAS No.: 35S42-O)

mg/Kg With reference to US EPA 5021method. Analysis was pedormed byGC/[IS.

n.d.

CHCS (Chlorinate hydrocarbon)1 , 1 ,'1 ,2-Tetrachloroethane (CASNo.:630-206)

mg/Kg With reference to US EPA 5021method. Analysis $/es performed byGC/[IS.

n-d.

1 ,1 ,1-Trichloroethane (CAS No.:71-556)

mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/MS.

n-d.

1 ,'1 ,2,2-Tetrachloroethane (CASNo.:79-34-5)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/[rS.

n.d.

1, 1,2-Trichloroethane (CAS No.:79-00-5)

mg/Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

n.d.

1,1-Dichloroethane (CAS No.: 7+34n)

mg./Kg With reference to US EPA 502 1method. Analysis was perfomed byGC/MS.

n.d.

'1,l-Dichloroethene (CAS No-: 75-354)

mgikg With reference to uS EPA 5021method. Analy6is was pedormed byGC/MS.

n.d.

1 ,1-Dichloropropene (CAS No.:563-586)

mgikg With reference to l-JS EPA 5021method. Analysis wa6 pedormed byGC/MS.

n-d.

pelst €sied rhKGd BpdeniolbEr , . r r _ l . n L l t r : . ! . i r : i t , l i r r . i 1 _ r r { a .

r:.ir i::r:+ti r +s61orPren,

Test Report No. : CE12011142129 Date 20'1114t20 Paoe: 17of 3i


tl]ltltl] r!tttt

Test ltem (s): Unit Method MDLRe3ultNo.l

'1,2,3-Trichloropropane (CAS No.:96-184)

mg/Kg With reference to US EPA 5021method. AnalFis $/as performed byGC/MS.

1 n.d.

1,2-Dichloroethane (CAS No.:107-06-2)

mg/Kg With reference to US EPA 5021method. Analysis wEs performed byGC/t\4S.

1 n.d.

1,2-Dichloropropane (CAS No.:78€7-5)

mg/Kg With reference to US EPA 5021melhod. Analysis wE6 performed byGC/MS.

1 n.d.

1,&Dichloropropane (CAS No.:142-28-9')

m9Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

I n.d.

2,2-Dichloropropane (CAS No.:594-20-7)

mS/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

Cabon tetrachloride (CAS No.:56-23-5)


1 n.d.

Chloroethane (CAS No.: 7t0G3) mS/kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

I n.o.

Chloroform (CAS No.: 67-66-3) mg/Kg With reference to US EPA 502 1method. Analy6is was performed byGC/MS.

'I n.o.

Chloromethane (CAS No.: 74-87-3)

mg/(g With reference to uS EPA 502 1method. Analysis \ ras peformed byGC/MS.

'I n.d.

cis-1,2-Dichloroethene (CAS No. :156-59-2)

mg/K(l With rcference to US EPA 502'lmethod. Analysis was performed byGC/MS.

1 n.o,

cis-1,3-Dichloropropene (CAS No.:10061-01-s)

mg/(g With refer€nce to US EPA 502'1method. Analysis was porformed byGC/MS.

1 n.o.

Hexachlorobutadiene (CAS No.l87€8-3)

mg/Kg With reference to US EPA 5021fiethod. Analysis u/as pedormed byGC/MS.

1 n.d.

con?zny . ; ) i , ) t ) + ,N i , r : r . ! l t i i i . I I 1 i ! 1 , - r i n , 4 ! r ] r l r , { .rhs6aftnE sEdbyrdcom@iysqedb G cei€..r cond i ois or s

r.o,,9hcaidob,earn3lido.irera iidrbarprdu@dereprdru pay Ailmalihorz.dajb€ioiroae,y o, rasrdrdn ofihe codenrd e i, d €nsi;r$e aw

rr ri,lt r:1,!{!!! :t rd6{0r)2B rD r+ s6lor)rs * w!sqrom

Test Report No.: CE12011142129Oale : 2011 l4l2\ Page :18o f3 ' t


l|| |lIl| ttmlr

Test ltem (8): Unit Method I/|DL ResultNo.1

Methylene Chloride (CAS No.: 7t09-2)

mg./Kg With referenc€ to US EPA 5021method. Analysjs was performed byGC/MS.

n.d.

Tetrachloroethene (CAS No.: 127-18-4)

mg./r$ With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

t€n91,2-Dichloroethene (CASNo.: 1566G5)

mgKg With reference to Us EPA 5021method. Analysis wa6 performed byGC/MS.

n.d.

trans-1,lDichloropropene (CASNo.: 10061-02€)

mS/kS With .eference to US EPA 5021method. Analysi6 was performed byGC/MS.

n.d.

Tdchloroethylene (CAS No.: 79-01s)

mS/kg With reference to LJS EPA 5021method. Analysis was pedormed byGC/MS.

n.d.

PFOS Referenco Information : Dircctive 2005/12ZEC(1) May not be placed on the maakel or used as a substance or constituent of preparations in a concentrationequalto or higherthan 0.005 % by mass.(2) [,,lay not be placed on the market in semi-finished prodlcls or adictes, or parts thereof, if the concenkation ofPFOS is equalto o. higher than 0.1 7o by mass calculated with reference to the mass of skuctura y ormiqostructurally distinct parts that contain PFOS or, for textiles or other coated materials, if the amount of PFOSis equalto or higherthan 1lg/m'?ofthe coated materiat.

:3fiTi"#iTil ,5ir.rl.:,:l.".".fi:gjrr:p1,lxe"l,iili:rl.e,,:r:llfil.-**""",,"."

s p o n j b l l y A b l s c L € d a n d s 3 d f u

Fry Any m,,,MEd dbcrionor*r*e"iirre a"

Test Report No.: CEnOlll42129 Dale 2O1 4t2O page: 19 of 31

SAI'SUNG TECHWIN CO., LTD,42, SUNGJU-DONG, CHANGWON, KOREF.

Note :1. mg/kg = ppm | o.1wtyo = lOOOppm2. n.d. = Not Detected3. MDL = Method Detection Limit4 . " - "=No tRegu la ted5. " = Qualitative anatysis (No Unit)6. Negative = Unde,tectabte / Positive = Detectabte7. Asbestos : Negative = "< 1.0 0/6", Positive =.'> 1.0 %,,8. Spot-test:

rmlit[ tttt]!

Negative = Absence of Cr(Vl) coating / surface tayer; positive = presence of C(Vl) coating / surface tayer;(The tested sample should be fu(hervedfied by boiling-water-extraction method ifthe spot test result cannotbe confirmed.)

Boiling-u€ter-extraction:Negative = Absence of Cr(Vl) coating / surface layer; posilive = presence of C(Vl) coating / sudace layer;The detected concentralion in boiling-wster-extraction sotutaon is equal or greater than O.O2 rng/kg with 50 cm,sample Sudace area.

9. "*r The substance was calculated by the test re6utt of Tributyt Tin. The I\,DL was evatuated for Tributyt Tin.

ld(s) b3rd rh e bd €pon €n^or e Icmpany i i : r r i rL . r : t ; r , r l , j r l ,n r1 , . r i1 11 ! .L :1 4 -4 r l ! ,1 .

i , g 6 i e d b t G . i f t l c o n d l o i 3 d *

3 p s s b l t y 6 l o $ c | € d a n d h € d 6 u

L r Lr:- r: r r;Ji.,'l I s6 (oaree

Test ReportSAMSUNG TECHWIN CO., LTD,42, SUNGJU-DONG, CHANGWON, KOREr'.

No.: CEnOl142129 Dale:201114120 Page | 20 of 31

ll][tt fltNl||]]

1) Thes€ samples were d|ssotved totatly by preconditioning method according to betow flow cnan.( Cf'test method excluded )

2) N€me of the person who made measurement: Ctimbgreat yang3) Name of the pecon in aharge of measufement: Troy Chang

ICP.AES

Sample lvlaterial DigestionAcid

$ed, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H,O,

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regia

Silver HNO]

Pla€tic HrSO1, HrOr, HNO3, HCI

Others Any acid to total digestion

pralsr€scd ha re$ cpod €nioi becompany 4 r ! r / . r l l l , ! - n i l . r r ] , l i l l r t i I . L [ i i i i l , ] r I 1 . r t i L l ! .

Cutting / Preparation

Sample lVeasurement

Acid digestjon by suitable aciddepencled on different samplematerial (as b€low table)

Microwave digestion with

HNO3iHCt/FtFAdd appropdate amount otclageslion reagent

Heat to appropriate

temperalure to extract


through filterAlkali FusionHClto dissolve

measure the absorbance

at 540 nm by uV-VlS

Test ReportSAMSUNG TECHWIN CO.. LTD.42, SUNGJU-DONG, CHANGWON, KORE/'

No.: CE12011142129Dale | 201114120 Page: 21 of 31

Iftl t] fl]I] u

Analylical flow chart1) Name of the pe6on who made measurement Roman Wong2) Name of the pe6on in charge of measurement Troy Chang

I TesI Items: PBB/PBDE, TBBP-A-bis

Firsttesling process -----' Optionat screen proc€ss ,--. Confrmation process -.>

Screen analy6is

Sample extraction method

Concentrate/Dilute Extracled solution

Filter

Analy6is by GC/MS

lssue Report

p s(s) bsied rhsbd Epodeinorbcohpaiy .i l | 1 nr ' j_ l i i ,r l i t l r irri r. .r rt f. i i1i,] n , .,

"lrr!,! .

r& 6onsr E s@ byhecompa.yrqedb b csarcr cddd I ois d sslted b rems and coidioos ror E

6@ie'ashacofiFrysindnqsas p o ^ s b I l y s l o i s c e n l a d $ " d @nndbeGFduedei.eplmlu].wbou

! I rs _e"i i,r r. .*l : , F ' . r i - 6 p T r a e n n r + su idGfrr zoE, M!! Lhd cr, tu,({ 4r._

Test Report No.: CEnOl142129 Date:20l|l4n1 Page.22 ol 31

SAMSUNG TECHWIN CO., LTD,42, SUNGJU-DONG, CHANGWON, KOREA

|l] [tfl tfitl|t

Analysis flow chart for determination of PVC in material1) Name of the person who made measuemenl Ginny Chen2) Name ofthe person in charge of measurement Shinjyh Chen

cmpany r ; r , r r l r ' i r :_F ' i , ! r i | ! /n j i , r i r . . r ,1 . r .? r . t l l

for sisdroi c ,oma1 do@ nants slt 5 d.m ro rhe Lmibid d ,rbL ly.

m r y a d w ' b i n , h 6 i n c d c € d s n s m a d d e . d € x s e a ; e a i 6 b a 1 6iid ba €Fdued exep,niu, v,set prcr

",hs:pp-€ dri,s compaiy Any m,,,MEd dbcrion

f r : r r r f l r * 1 r

Sample pre{reatment

Sample analyzed by FTIR

Check wav6number of C-Cl bonding

Test Report No. : CE12011142129Dale : 2O11l4l2O

SAMSUNG TECHWIN CO., LTD.42. SUNGJU-DONG, CHANGWON. KORE'.

Page : 23 of 31

lllIll[l[][]I I|

Analytical flow chart of Soxhlet extraction (GC/MS) procedure

1) Name of the person who made measurement Roman Wong

2) Name oflhe per6on in charge ofmeasurement Shinjyh Chen

Data

mpre(n bid rh s red €Fon$iiorbc o h @ i l i ' , : . . 1 i r l . . l i i , , l ; ; i n f J + i i . l i i , L i l r l j . ' r ' \ l l .

r h s d o f u n s l A s s E d b y h e c o m p a . y s ! b ] e d b c G e H d c o . d l o | s d s

I Test ltems: Phthalate ' Benzotriazole ' HBCDD . NP ' DBBT '

Organic phosphorus compounds

Test Report No. : CEn011142129 Da'e: 201114120 Page'.24 d 31


flt ]ttr ||ttr ]

Analylical flow chart of Soxhlet extraction (LC/MS) procedure

1) Name of the perSon who made measurement: Roman Wong

2) Name ofthe person in charge of measurement: Shinjyh Chen

rTest ltems: PFOS/PFOA . Benzotriazole

Sample pretreatmenvseparation

+

Data

ps(s)rsded rh s Gd ,epd eiidl becompany 4 j r !1 , r1 | b_ i ' ! { , r t J i tn l rh r . l r i i ; { t i : r I . r r . i r r l t { .

.. i-.1. *:IFt4..:;!+s6lorrxeer7e t r s6lorrrer rr wweiion

Membsdrhescscrolp15c5sAr

Test ReportSANISUNG TECHWIN CO,, LTD.42 SUNGJU-OONG. CHANGWON. KOREA

No. : CE12011142129Dale:201114120 Page: 25 of 31

Ill[ ||[l t!flr

Analytical flow charl of volatile organic compounds (VOCS)

1) Reference method : US EPA 50212) Name ofthe oerson who made measurement : DalkiYen3) Name of the person in charge of measurement : Shinjyh Chen

: t ii irrrr,t, l

3uba4 'o lems aod coid{ons ior E

Sample pretreatment

Take sample and put it intoheadspace glassware.

Test Report No. I CE2011142129 Dale | 201114120 Paae ; 26 of 31

SAMSUNG TECHWIN CO., LTD-42, SUNGJU-DONG, CHANGWON, KOREA

tl]|l|tt|l|||t[t ]

Analysis flow chart for determination of Asbestos

1) Name of f|e oerson who made measurement Victor Kao2) Name of the person in charge of measuremenl: wendy w€i

Not containing Asbestos/Negative

mprels) EsEd frs re. codd €nnor b, - 1 i ! r , . , , r ' r , , , , : r . d f i n r t - \ r , . i . . , j t , , : .

Th s dofumenl 6 's!ed by 6e c dmpa$!ed ro rens aid cdiddoG iof E

.I j:rr !:I4i!! :,r+tr6i02)2FrDi+s6rcr)rrerr *-!*-,

;ffi""ti"" p -f __l

a6be6tos is present IDiffraction peak ofasbestos is absent

_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ -

Asbestos identification byopticalmicroscopy

Asbestos fiber is oresent Asbestos fiber is absent

Containing Asbestos/Positive

Test ReportSAMSUNG TECHWIN CO., LTD,42. SUNGJU-DONG. CHANGWON. KOREA

1 )

2\3)

No.'. CEn011142129 Dale:201114n0 Page:27 ot 3'l

|:] [ttl [!l||lll

These samples were dissolved totally by pre-conditioning method according to b€lowflowchan.Name ofthe person who made measurement: climbgreatYangName of the person in charge of measurement: Troy Chang

FlowChaft ofdigestion for the elements analysb pe.formed by ICP-AES

S'teel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, HrO,

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic HrSO4, HrOr, HNO3, HCI

Others Any acid to lolaldigestion

. r i ; r ' l J i i i ! . : , r , i . r , i . n t , l r ! r t r l

poisbr t sb c c €d 5nd rh s doam

,.t I t-|| f:l:r*;4.iiias610r)r!

Cuting / Preparation

Acid digeslion by suitable acid d€pended ondifferent sample matedal(a6 below table)

'1) Alkal iFusion2) HClto dissolve

Test ReportSAMSUNG TECHWIN CO,, LTD.42, SUNGJU-DONG, CHANGWON, KOREA

No. . CE12011142129Date :2O1114n0 Page : 28 of 31

r|rr[ttl] tl||tl

Analytical flow chart of halogen content1) Name of the oerson who made measurement: Rita Chen2) Name of the person in charge of measu@menl Troy chang

r . , r l h l n i l ; i L . x r i i . ! 1 , L1 ]ftBd@msl6 s€dbyhecomp3

spssb i r y6b bsen , . d l r sdo tumm'dcsm, *oe€ repa ; l sbs rErhetr nq[b aid ob 0dDn3 und rhe ra w hdi pr o. Mrdn.pprcva d be comp,^y hy **h-*d

" b,"i."

Sample pretreatment / Separation

Weighting and putting sample in cell

Oxygen Bomb Combustion / Absorption

Dilution to fixed volume

Analysis w€6 performed by lC

Test ReportSAI\4SUNG TECHWIN CO., LTD.42, SUNGJU.DONG, CHANGWON, KOREA

No.'. CE12O11142129Date 201114120 Page : 29 of 31

|l|| [t!] ltNrll

Analytical flow chart of Organic-Tin content

1) Name of lhe person who made measurement Ginny Chen2) Name of the person in charge of measurement Troy Chang

Data

pe(s)€jed rh s rad Gpod6iiolbec o m p a n y l ; r 1 l l l r ' r r _ i ' f , r r , h r r t i . . ! i r i r t r I t . - . L i 4 ! j !

s p . N b ' l i A l o 6 c | € d a n d h s d o c u

F^y Any*a!hm6ddbd;ntuaeryorias6Groidhe6^Gdorap!€.ranedrhsdoonenrsunas he tured 6nani;r $e bw

! i d s . r zoFN* ra iF r . v rawd / ! i t l eo r ) r ee rD r+s6 (01 rsn ,4_ * ' a , ,

Menerof ihe rsc@p rs6s sA)

Test Report No. : Ce2011142129

SAMSUNG TECHWIN CO-, LTD-42, SUNGJU-DONG. CHANGWON. KOREA

Dale | 201114n0 Page : 30 of 3 l

ut[ta|||||lrllll

Chlorinated Flame retardant analytical flow chart'1) Name of the person who made measurement Bary Tseng2) Name of the person in charge of mea6uremenl Troy Chang

r Reference method: US EPA 8270D, US EPA 3540r Test ltems: PCBS, PCNS, PCTS, Mirex, CP, |CCP

Data

p 6(s) reied rh s rd .+od €nnd bc m p a i y ; i r r I j l r ' j - l l ' r : ! - , r L r r r t t r r -r h " d d o r s l 6 $ s d b y h a c o m p a ^ y o b l e a b G c s e € | c o d l o i 3 o f s

F n , M t m s l l f u l z d d k € | d n

l1886€nnsrr f +tr6ror)rarr *-,q,--

Test Report No. : CEn011142129 Oa'e | 201114120

SAMSUNG TECHWIN CO., LTD.42, SUNGJU.DONG, CHANGWON. KOREA

" End of Report "

Page : 31 of 31

l tt |l[

p6(s)bbd rh s bd r.pd eiio, bec o n o a n v + ! r ! r , r ! _ 1 1 r , , r r r , ' J t l n N A i r : . r ; i l r l r r r i ^ . r l n l q . [ .

! rd4(rzoiqN4rdie.rrrrw,./tri i 146 i.rrf ID r l s610rPre tt w!se!@n

M€nba or se rs G&p rscs sA)

Validi nownFor QueatiPlease Co ith scs

Test Report No : cE/2Olo/A5235 Date: 2010/11/03P a g e : 1 o f 5

rIlllIrllllllrlrltl

IENIE|:3[8m$lr"t*o*'"" 'o'" o'FrcE: 14ooo TAMB.REE R.AD' TRVTNE'

oALIFORNIA. 92606 U.S A

The following sample(8) waslwere submitted and identitied by'on behalf of the client as :

Sample DescdPtionStyleJltem NoSample Receiving Date

Testing Period

: ln accodance wth the RoHS Dnective 2OOZ95/EC' and its amendment

directives.

ADHESIVE86002010110D82o1o/10/28 TO 2010i 11/03

Te$ RequeBted

Test Method

T€t Result(s)

With reference to IEC 62321: 2008l'ri ii i*" ii,i ir,. oa",.ination of Levels of Regulated substances in

Electrotechnic€l Produc'ts'

l1) Detemination of Cadmium by ICP-AES'

(2) Detemination of Lead by ICP-AES

r3l Cletemination of Mercury by ICP-AES

iii o"t"r.ina'on ot Hexavalent chromium by uv /rs spectrornetry'

iS1 Oetermlnaion of eBB and PBDE by GC/MS

Please €fer to next Page(s).

Ctst ca laqfi.Y-TJF

, j : : * : -**-" : " : . . " " , , . , - ; ; ' . * . 1. ' " : f r "" : "" -*"- . ' : ; " "" ' - ' "*" : - l - " : . : ' .

;*t+*:*;q"ll:': H**lt"i:::ffi **;q+***i*nnriiirr**li*::*l':*,:"-;";;x',r :::ffi?:"iT:;xfi J*::lli

Sfnd io.xd

Test Report No : cE/2010/A5235Date:2010/11/03 P a g e : 2 o f s

lt|l lllllllllllllt

lEillEi i3l:3tr:lt+crRoNrcs MArN oFFrcE: 14ooo JAMBoREE R.AD' TRVTNE'

CALIFoRNIA' 92606 U SA

"hami.il method (Unit:Result MDLMethod

(Refer to) o.12(1) n,02n.o.

(3) n,o 2

n-d. 2

ifficinaextradlon

(4)

n,0-SumofPB* , .MonobromoblPnenyr

I n.on.d.

6-iuromoiPnenYt I n.o,iiilomoiPnenYt n.d.iEiEt-mouiPtrenylPentabromoblPnenyl

n.d.n.d. 5

FEilulxauromotiPnenYt n.o. 5F-ptaurornobiPnenyt n.d.d;EbromobiPhenyl n.d.fi 6iaulonauromoliPhenYl n.d. 5DecabromobiPhenyl l

(5) n.d.Sum of PBDE6 n.o. 5fr -_-onoqgn'ooipnenvte!!g

n.o. 5DibromodiPhenyI ether

i I ether:nyl ether

n.d.TribromodlPnen: t n.d. 5TetrabromodiPh n.d. 5PentabromoolDhenyl elner

rhenyl ethern.d.

Hexabromodl n.d. 5HeptabrcmoolPnenyr cu's' 1-t

-ln.d.

S#",i,iiffi n.d.n.d.

DecabromodiPh€nI emer

Note :1. mg/kg = ppm; o.1wto/o = loooppm

2.nd = Not Detected3. MDL = Melthod Detection Llmll

4. '-" = Not Regulated

:;:'.::"'l * T*" -"':^ ::"-: " "- ;^, .l; . ;"; ; .;.. " ", * ;-"j,'"ix#;':-:":;,.;;l ",.i,rlr;,1**3x;'"1i;"1];,3r;;;"1;":n',:'::'.t,ilii,::;*:::"j;:i:"i{i.i"f-;,i"':,:::#: -";*r"**",*s::it:iJ*ir "" 'rr::#,*'"-h:j*."..".i-:-'n:1,1:!iirli"":.._r#i j:lr;ifu";:;;":*l:.tj:.i'xi:1i:"r:::"::l'#':i;3ir;;i:;:"{ii"#";;.':''fl:.""::;.'";"*;:;;::s;;;'j"fu";#;rr;;ft':"; rrii;:;l::l"L+l*in-"+r;:ir:*ili:iT":;;;n"t";:";r.'"*":''" T ".':i,";".:"1.:"'

No.1 : GRAY PASTE

Test Report No : cEzo1o/A5235Date:2010/11/03 Page

MAIN OFFICE: 14000 JAMBOREE ROAD'

3 o f 5

IRVINE,r!lrm||]l||$|r

lEIlEi :3ffi 3trll?f.",*o*".CALIFORNIA' 92606 U'S'A

1) These samples we€ dissolved( cf test method excluded )

totally by pre-conditioning method

me€surement Climbg€at Yang

according to belo\ / flow chan'

2) Name of the PeFon who made

;i iil" ; t;; ;;" 'n charse or measuremer{: rrov chans

#'"* j;'"::::;,:;:r' "-i "r"r* *,r,,1r*.?:-:::;i:*':,:"j":"*:";:$";::'..qil:"I*ri;::r:fi""":?i*"",i.,;*'; ;:::,rr:ixr:!:"ii.:ii;.ii"i#i*.*;ii"fi.iii;;ix';l,,iir:i"*,"*"i:li'l:"ti;;::""q;ilj:-;"":-":i.11'X;"ll'","*li,i,lljji*ii:::i{}:lfi;'ir"i::;rf;:!U,i:-l{,;::,:i;:,ijji:rir:llir",i:i ili:;;li*;i,""**:1"'**ii";:j:;i=T::#:"";*i"",;;'i"#i:;:.;; ';::;:,.:: ,:r,::'l:;fl'j{',;lrffirfffffi!:i'q"}:'ir""}lq:X*:*:*,mi*'ttt*:ii:il"'*r*:rkr*sr;'"r"c"'momv-auo-aa"o"

cf.

Add appropriate amount of

digestion reagent-cid digestion bY suitable aciddepended on diff erent.samplem-ieriat (as tetow taote)

Heat to aPpropnale

t€mperature to extlacr


throughfilter1) AlkaliFusion2) HClto di$soMe

Add diphenyl-carbazide f or

color develoPment

measure the abso$ance

at 540 nm bY UV-MSAqua regia, HNOg HCI' HF H'?O?Steel, copper, aluminum' solder

Gold, platinum palladium c€€mic

HzSOl HzOa HNOg, HCI

Any actd to total digestion

Test Report No : cE/2010/As235 Date : 2010/11/03P a g e : 4 o f s

HEIIE|:3lHmlEl,"'*o"'"t "^'* o'FrcEl 14ooo JAMBoREE RoAo' TRVTNE'

CALIFORNIA, 92606 U.S'A

PBBIPBDE analytical FLOW CHART

1) Mnp of the p€6on who ftEde neasurerEnt Rod€n Wong

,i N"* of,n" o"*n 'n charge of lYpasurefiFnt: Trcy chang

Iillrlll[illll |rl

First testing Procesa -+

OptionalscreenProcess __

ConfinrEtion Proce6s - '>

I Sannh I

' I

I Sanple Pretreatment I---_--_,-

Screen amlYslsi . . . ' . . . . ' . + " " " " " "

I Sanple extractiorv II Soxhlet netnoo I<

t l

I concertratdDilne II Ef€cted solution I

I Fitter I

I

I Analysis bY GC/MS I

'tr's ose:^$. ieriiT:t::: r iry; qli iilr:.ijl jfjiLl *;;*:,j1fl:i::":".;:;:" -"*" '":. . " -:-.::;#,",i:,':i;:;i5.:i:111".::''"".'.x,"-' -"".:i:ll1t-""jlili"1"$.;::":':::,';;l:;;;:J{i.::'"*i:'ii':-*":::;ij{ni.l*:':":lr;:';:,:*:l;*:xi:ii:i;l.l".}ii;:ixI#1;::r*::.? l{";i.: .""":l:'-:.::r.:'":i::::'1ryi.::Tr:"r':t"ir'"::"'":,'"%:: ::1.'::'r lli;: i":;ri::nr";;':.':{"r:i..:1,:,,:p*:,^it}i*:;;+":':;"';"':!:i}:;}::i.".:;"1;};':'"';:""':''.:'";"':":"'-,.,,,, .,,, i,., t o,s a, '*- nwosi tui.wdq tr_:_:".lt1_1j:-i-=:' ll

Test Report No : cE/2010/A5235 Date:2010/11/03P a g e : 5 o f s

HENKEL CORPORATIONiiEr.iiEl noHesrves-eLEcrRoNlcs MAIN oFFlcEcALlFoRNlA, 92606 U.S.A

1r] lIllllllllllll

l4OOO JAMBOREE ROAD, IRVINE'

" End of Report "

;-i"d[*iT::d 1;;;ffi # .;tr ;: *ti*+*ffi # r',='qffi:l':ql$-:.i.-i:iliJ:r-itli::t*ilF=**"":tl*:+'**:1,'*;tt'*i3;"';"; '-* " '" "'-" ""''-"

No. : KLl201 0/80970A{)1 Date:2010/08/31P a g e : 1 o f 1 2

i o r QPlease

|ltttl||ttI|tttl|lrHERAEUS IIIATERIALS SINGAPORE PTE LTDALK 5OO2 ANG MO KIO AVE 5, #O+05 TECHPLACE II, SINGAPORE 569871

The followlng sample(s) was/were submttted and idenfified by/on beh.tf of ihe ctient as :

Test Report

Sample DescriptionStyle/ltem No.ColorSample Receiving DateTesting Period

Cu BONDING WIREicu, DHF, l,4axsofl and MaxSoftLDCOPPER2010/08/132010/08/13 TO 201 0/08/31

Teat Resul(s) Please reler to ne)d page(s).

: d i , : ' ; ! E ; { r t - : t r 1 l j " * i

comFatr'3tudielrs"lncdtu dc a itudor fsiy rh.tuntsnyE&b

i-

Ele|rd to. |nd oo b.tdtgGS T.k |r Llnit d

HEMEUS I'ATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG I\4O KIO AVE 5, #0445 TECHPLACE II, SINGAPORE 569871

Test Report

Te3t R6sul(a)

PART NAIVIE NO.1

No. : r\r',/201 0/809704{1 Date:2010/08/31 Page ,2 ol 12

CU BONDINGWIRE

||] |l:|r tr|tl||]tl

T€si ltem (s): lJnit Methocl MOL Re3ultNo.l

Cadmium (Cd) mg/Kg with reference to lEc 62321:2008 andperformed by ICP-AES.

2 n,d,

Lead (Pb) mg/Kg With reference to tEC 62321:2oo8 andpedormed by ICP-AES.

2 n.d.

Mercury (Hg) mg/kg Wth reference to IEC 62321: 2008 andperformed by ICP-AES.

2 n_o.

Hexavalent Chromium Cr(Vl) by Spottesl / boiling water extraction

With refefence to tEC 62321t2008 andpeformed by Spot test / boiling waterextraction l\rethod. (See Note 5)

0.02mg/kgwith 50 cm,6urface area

Negative

He)€valent Chromium Cr(Vl) mgftg With reference to US EPA Method 3060A& 7196Afor Hexavalent Chromium.Analysis was perfomed by uv-VisSpectromelry.

2 n.d.

Anlimony (Sb) mg/Kg With reference to US EPA Method 3052for Anlimony Content- Analysis wasperfomed by ICP-AES.

2

Perfl uorooclane sulfonales (PFOS)PFOS - AcidPFOS - Metal SattPFOS -Amide

mg/Kg vv]th reference to US EPA 3540C: 1 996method for PFOS Content. Analysiswaspeformed by LC/MS.

1 0

PFOA (CAS No.r 00033547-1) mg/Kg Vvith reference to US EPA 3540C: 1996method for PFOA Content Analvsiswasperlormed by LC/l,,lS.

1 0

Test Report No.:KA/2010/80970A{1Date:2010/08/31 Page :3ol 12

HERAEUS I\4ATERIALS SINGAPORE PTE LTDgLK5OO2 ANG MO KIO AVE 5, #O+05 TECHPLACE II, SINGAPORE 5€9871

n t €d& rh6Ed rcFdemderel i ! r , " " . r - , i r ^ r

coh t sn t6 tud i csd$c rned R .E

| , ' s *o l - , " "

rtl

To3t llem (B): Unit Method MDL Re3ultNo.1

Sum ot PBBS

mg/xg Wilh reference to IEC 62321:2008 andperformed by GC/MS.

n.d.Monobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.TribromobiphenylTetrabromobiphenyl 5 n.d.Penlabromobiphenyl 5 n,d.HeEbromobiph€nyl 5 n.d.Heplabrcmobiph€ny' 5Octabromobiphenyl n.d.Nonabromobiphenyl 5 n.d.Decabromobiphenyl 5 n.d.Sum of PBDE3

mg/Kg Wilh reference to IEC 62321:2008 andpedormed by cC/1,4S.

n.d.Monobromodiphenyl ether 5 n.d.Dibrcmodiphenyl elher 5 n.d.Trib.omodiphenyl ether n.d,Tetrabromodiphenyl elher 5 n.d.Pentabromodiphenyl elher 5 n.d.HeEbomodiphenyl ether 5 n,d,Heptabromodiphenyl ether 5 n,d,Octabromodiphenyl ether 5 n.d.Nonabromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n,d.HaloqenHalogen-Fluorine (F) (CAS No.:014762-94-A'

mg/Kg Wilh reference to BS EN 14582:2007.Analysis was pedormed by lC.

50

Halogen4hloin€ (Cl) (CAS No.:022537-15-1)

mg/Kg wilh reference lo Bs EN 14582:2007.Analysis was performed by lC.

50 n.d.

Halogen-Bromine (Br) (CAS No.:01009732-2)

m9/kg Wth reference to BS EN 14582:2007.Analysis was performed by lC.

50 n.d.

Halogen-lodine (l) (CAS No.: 014362-4€)

mg/Kg Wth reference to BS EN 14582:2007.Analysis was perfomed by lC.

50 n.d,

Test Report No. : KA,/201 0/80970A-01 Date : 2010/08/31 Page :4 ot 12

HERAEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG IIIO KIOAVE 5, #04{5 TECHPLACE II, SINGAPORE 56987,I

Note : 1. mg/kg = ppm i 0.1M% = 1000ppm2. n.d. = Not Delected3. MDL = Melhod Detection Limit4 . ' - " = N o t R e g u l a t e d5. SDotlesl:

Negative = Absence of Cr(Vl) coating / surface layer,Positive = Presence of Cr(Vl) coating / surface tayer;(The tested sample should be fudher verified by boiling-water-extraction method ifthespot l€st r€sult cannot be confirmed.)

Boiling-water-extraction:Negative = Absence of Cr(Vl) coating / sudace layer.Positive = Presence of Cr(Vl) coating / surface layer;lhe dolected concentration in boiling-water-€xlractlon solution i6 equal or greaterlhan O.O2 mg/kg with 50 cm2 sample surface area.

llt [ttt]l|lttt[ll ll

*hsbdoc rary rh! cdp.itr &

Test ltem (3): Unit Method MDL R€ultNo. l

PhthalatesBaP (Benzyl butyl phthalate) (CAS No.:000085€8-7)

o wth reference to EN 14372. Analysiswasperrormed by GC/MS.

0.003 n.d.

DBP (Dibutyl phthalate) (CAS No.:ooooa4-7+2)

With reference to EN 't4372. Anatysis wasperfomed by cc/MS.

0.003 n.d.

DEHP (Di- (2-€thylh€ry|) phthalate)(CAS No.: 000117{1-7)

% \Mth reference to EN 14372. Analysis wasperfomed by GC/l!lS.

0.003 n.d,

DIDP (Di-jsodecyt phthatate) (cAs No.:026761-4G0)

\Mth reference to EN 14372. Analysiswasperfomed by GC/MS.

0.01

DINP (Di-isononyl phthalate) (CAS No.:028553-12-0)

o./a wjth feference to EN 14372. Anatysiswasoedormed bv GC/MS.

0.01 n.d.

DNOP (Di-n-octyl phtharate) (CAS No.:000117-84{)

With refe€nce to EN 14372. Analysiswa6pedormed by GC/MS.

0.003 n.d.

DNHP (Di-n-heryl phthalate) (CAS No.:000084-75-3)

% With reference to EN 14372- Analysis waspedomed by GC/MS.

0.003

DMEP (Bis (2-methoryethyl) phthalate)1CAS No.:000117€2-8)

vo Wilh reference to EN 14372, Analysiswasperfofined by GC/MS.

0.003 n.d.

Test Report No. : KA/2010/80970A-01 Date : 2OlO/OB/3i

HEMEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIOAVE 5, flX45 TECHPLACE II, SINGAPORE 569871

P a g e i 5 o f 1 2

n |lll]||Ittllfl|lr

6. " = Qualitative anatysas (No unit)7. This isthe additionanest rcport of K /2010/80970 which was issued on 2010/08/31.

Please refer to Ky'/2010/80970 for odginat infomation.

PFOS Reierence Information : DiEcttve 2006r122/EC(1) May not be placed on the ma*et or used a5 a substanc€ or constiluent of preDaralions in a

concentEljo. equalto or higherthan 0.005 % by mass.(2) May not be placed on the market in semi-finished products oraftictes, or pads thereof, ifthe

concentration of PFOS is equalto or higherlhan 0.1 % by mass calculated wilh rcference lo rnemass ot struclurally or microstruclurally distinct parts that contain PFOS of, foa textiles or olhercoaled matedals, if lhe amount of PFOS is equatto or highe. than ttgh, ot lhe coated matenar.

._....__ila'ie*g

Test Report No. : KA2010/80970A-01Date:2010/08/31 page:6 of 12

HERAEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIOAVE 5, #04{5 TECHPLACE II, SINGAPORE 569871

ll| ttt] rtllI ||]tr

1) These sampleswere dissolved totatty by pre-conditioning method according to betownow chan. (CI6+te6tmethod excluded )

2) Name of lhe pe6on who made measuGmenl:Atex Chang3) Name ofthe person in charue of measu€menl: Ray Chang

1 " "

r ; i . d r

Sample Meas0remenl

Acid dageslion by suibble acid

depended on different sample

material (as below table)

IvicrowEve digestion wilh

HNO3/HCI/HFAdd appfopriate amount

of digestion reagenl

Heat to appropdale

temperature to extracl


thfough liller

Add diphenyfcatbazide

for color developmenl

llleasure the absobance

at 540 nm by UV-VIS$el, copper, aluminum, solder &ua regia, HNO3, HCl, HF, HrO,

Glass HNO3/HF

Gold, plalinum, palladium, ceEmic

Silvsr HNO3

HrSO1, H,q, HNO3, HCI

Olhers Any acid to rotal digesrion

Test Report No- : KA/2010/80970A41 Date:2010/08/3t Paoe :7 of 12

HERAEUS I'ATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG IVO KIO AVE 5, #04-05 TECHPLACE II, SINGAPORE 569871

I ]]]t n |lrlt]||r

PBB/PBDE analytical FLOW CHARTI ) Name of hc p€Eon who made measurement Anson Tsao

2) Name of the peMn in charge of me€surcment Ray Chang

Optional scre€n process

I Sample exlracliorv II

soxhret metiod I

I Concenlraie/Dilute I

I Exlracled solution

I

a ,I Firtef I_ - - - - - - - - - - - - - - _

i

Test Report No. : KA/201 0/80970A-01 Date:2010/08/31 Page.8 ot 12

HEMEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIOAVE 5, #04-05 TECHPLACE II, SINGAPORE 569871

1) These samples were dissotved totatty by pre-conditioning method accoding to betownow drart.

2) Name of lhe pe6on who made measurementi Alex Changi3) Name ofthe pe6on in charge of measurement: Ray Chang

Flow Chart of digestion forthe elements anatt|sis performed by lCP-AES

ICP.AES


Glass HNO3/HF

Gold, plalinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic HrSO,, H,O,, HNO3 HCI

Others Any acid lo total digestion

rl| ltt|| r|r]utrt l

. o n t s r y . 3 ' i d i q ! a ' t . l n e d R d e

Cutling ' Preparalion

Sample ldeasurement

Acid digestion bysuitable acid depended on different sampte materht(as betowiabl6)

2) HCllo dissolve

Test Report No. : KA/2010/80970A{1 Date : 2010/08/31 page : 9 of 12

HERAEUS IJATERIALSBLK 5OO2 ANG MO KIO

SINGAPORE PTE LTDAVE 5, #04-05 TECHPLACE II, SINGAPORE 569871

llllll ]l lut|If ltl|lttI

Anelt'tical iow chart ot PFOA/PFOS content

1) N€me of the p€rson who made measurement Anson Tsao

2) Name of lhe peFon in charge of measurcment Ray Chang

6nstudotr! r!ry ri! c@paiya 6d

Test Report No. : fJ,.i2010/80970A{1 Date :2010/08/31

HERAEUS MATERIALSBLK 5OO2 ANG MO KIO

Page : 10 of 12

]lflt:llfittttttll|lrSINGAPORE PTE LTDAVE 5, #04-05 TECHPLACE II, SINGAPORE 569871

1 )

2)

Analytical flow chartof hatogen content

Name of the peFon who made msasur€menr Jean HungNam€ ol the peEon in chaee of measur€menr Ray Chang

eG l bded . r hs€n€con€ t rdb . r !ili lrfi9rri irri*,,nI 1.,lii ;.{riJr. ":;i+ : ri:i,,,ri!q..

Sample pictu|e and €pon number

Weiqhtng and pultng sample incell

Oxygen Bomb Combustion /AbsoDtion

Dilution to nxed volume

Analysis was psrformed by lC

SGSTest ReportHERAEUS IMATERIALS SINGAPORE PTE LTDBLK5OO2 ANG I\4O KIO AVE 5, #O+05 TECHPLACE II, SINGAPORE 569871

No. I rW201 0/80970A-.01Oate:2010/08/31Page : 11 of 12

rr ]|tfi |l[t]ttlll|ltl

Analytical flow chart of phthalate content'l ) Name of the person who made measurem€nt Anson Tsao

2) Name oflhe p€Eon in chaEe ol measurement Ray Chsng

Dala

Test Report No. : KA,/201 0/80970A-01 Dafe : 2010/08/31 page: 12 ot 12

r ||I|tlLl]]l||]tl||lHERAEUS IUATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #04-05 TECHPLACE II, SINGAPORE 569871

" End of Repod "

Test Report No. : CE/2011/42646 Dale | 201110/'t127 Page : 1 of 8

HITACHI CHEMICAL CO., LTD.1772-1 KAMKUBO YUUKI.SHI

Validit nownFor QuealiPlease Co ith scs

ll]tltI|[] tII|lllIBARAKI, 307-0015, JAPAN

wa6/were submitted end identified by/on behalfofthe client as:The following sample(s)

Sample DescriptionStyle/ltem No.Sampie Receiving DateTesting Period

EPOXY MOLDING COIVPOUNDCEL-922OHF2011t04t14201 I t04t1 4 TO 201 I t04t27

!dsrdzoiqNa!7dF.&rdwr.ri : l+46i0lrerr[s610?]rrerr@!ss'rdn

Test Result(s) : Please refer to next page(s).

c o m o a n v : l n r l t r : . 1 : a ' : , r ' , " 1 . . / L r r t : ; . : r t r : ! { l i I r ' r ' r r l r t , { '

{Nwa--x

E$rad for rid

cl|.|nicd Laboratory - TdDel

Test ReportHITACHI CHEMICAL CO., LTD.1772.1 KANAKUBO YUUKI-SHI

Test Resultlsl

PART NAME No.1

No. : CE/2011/42646Daie | 20111c/,127 Page : 2 of 8

IBARAKI, 307-0015, JAPAN

DARK GRAY LUMP

Ifl[ [[]rr|l

Test ltom (s): Unit Method I'DL ResultNo-1

Cadmium (Cd) mg/Kg With reference to tEC 62321: 2008 andperformed by ICP.AES.

2 n.d.

Lead (Pb) mg/Kg Wilh reference to IEC 62321:2008 andperformed by ICP.AES.

2 n.d.

Mercury (Hg) mg/Kg With reference to tEC 62321: 2008 andperformed by ICP-AES.

2 n.d.

Hexavalent Chromium C.(Vl) byalkaline extraction

mg/Kg Wilh eference to IEC 62321: 2008 andperformed by UV-VIS.

2 n.d.

Antimony (Sb) mg/Kg With feference to US EPA Method30508 forAntimony Conlent. Analysiswas performed by ICP-AES.

2 n.d.

HalogenHalogen-Fluodne (F) (CAS No-:14762444\

m9Kg With reference to BS EN U5a22OO7.Analysis was performed by lC.

50 n .d .

Halogen-Chlorine (Cl) (CAS No.:22537-1+1'

50 n.cl.

Halogen-Bromine (Bf) (CAS No.:10097-32-2)

50 n.o.

Halogen-lodine (l) (CAS No.:14€6244-8)

50 n.d.

Sum of PBBS

mg/kg With reference to IEC 62321: 2008 andDer{ofmed bv GC/IVS.

n.d.llonobromobiphenyl n.d.Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.o.Pentabromobiphenyl 5 n.d-Hexabromobiphenyl 5 n.d.Heptabromobiphenyl 5 n.d.

Octabromobiphenyl 5 n.d.Nonabromobiphenyl 5 n.d.Decabromobiphenyl n.d.

coroa iy . i : . I rL . l J - l ' r , r i r r l , :1 r . i : i r i . t l i l l l l r ' i

s p o n g b l y s b b c l a d s i d l h 3 d o d

. : l . . r t i . ' i i t r : , i l + *6o : tDenD i r $6o r r r t s t t * * ! ! od

Test ReportHITACHI CHEMICAL CO., LTD.1772.'1 KANAKUBO YUUKI-SHI

No.'. CEl2011l42U6 Daie: 20111c/'n7 Page : 3 of 8

IBARAKI, 307-0015, JAPANlll llltI||lu]|l]t

Test ltem (s): Unit lrlethod MDL ReaultNo,1

Sum of PBDES

mgftg With refe.ence to IEC 62321: 2008 andpeformed by GC/lllS.

n.d-lvlonobromodiphenyl ether 5 n.d.Dibromodiphenyl ether 5 n.d.fribromodiphenyl ether 5 n.d.fetrabromodiphenyl ether 5 n.d.Pentabromodiphenyl ether 5 n.d.Hexabromodiphenyl ether 5 n.o.Heptabromodiphenyl ether 5 n.o.Oclabromodiphenyl ether 5 n.o.Nonabromodiphenyl ether n.o,Decabromodiphenyl ether 5 n.d.

Note :1. mg/kg = ppm ; 0.lM% = 1000ppm2. n.d. = Not Detected3. MDL = Method Detec{ion Limit4 . " - "=No tRegu la ted

c o m F r y i i : . I i ! . - - R i I l : . r r ' . i r : r N . L * . i : , . 1 j r t ! ! ..ysqedb c cse6r codd r om of s

ior s sdrod . rom.r dodme^6 slbr ro ha m rar oo 0r 'ab !t

rn' ! i J ri:i1..i;t+s6 tr:ee

Test Report No. I CE12011/4264€ Date:2011t04t27 paoe:4of8

HITACHI CHEIVICAL CO., LTD.'1772-1 KANAKUBO YUUKI.SHI IBARAKI. 307-OO'15, JAPANfltlt[ttt! ||I|t|l

1) These samples were dissotved totally by pre-conditioning method eccording to betowflow chart.( Cr"' test method exctuded )

2) Name of the pe6on who made measurement: Climbgr€at yang3) Name of the pe6on in charge of measurement: Troy Chang

ICP.AES

Sample Material DigestionAcid

S-teel, copper, aluminum, solder Aqu€ regia, HNO3, HCl, HF, HrO,

Glass HNOy'HF

Gold, platinum, palladium, ceramic Aqua regra

Silver HNO3

Plastic H,SO. H,O,, HNO3, HCI

Others Any acid to total digestion

c o m o a n v ; " I : : , 1 , r : - i : I r l J i , 1 ' r t i . , : : I t r ' r . r i 1 : , r ' : I t r ! l { 'a sub ]ad lo ' 6cene laco id [omds

Cutling / Preparaiion

Acid digestion by suitable aciddepended on different samplemalerial (as below table)

l\Iicrowave digestion wih

HNO3/HCUHFAdd appropriate amount of

digestion reagent

Heat to appropriate

temperature to exfact


through filter'1) Alkali Fusion2) HClto dissolve

Add diphenyl-carbazide for

color development

measure the absorlcance

at g0 nm by UV-VIS

Test ReportHITACHI CHEMICAL CO., LTD.1772.1 KANAKUBO YUUKI-SHI

No. I CEl2011l42UO Dale 2011t04t27 paoe | 5 of I

IBARAKI, 307-0015, JAPAN||fl11 rflr] ||l|

'1) These samples were dis6olved totatty by pre-condilioning method according to betow flowcnan.

2) Name of the person who made measurement Ctimbgreat yang3) Name of the person in charge of measurement: Troy Chang

Flow Chaft of digestlon for the etemenb anatysts pertormod by tCp-AES


Glass HNO3/HF

Gold, platinum, palladium, cefamic Aqua fegia

Silver HNO3

Plastic HrSO4, HrO?, HNO3, HCI

Others Any acid to totaldigestion

Pe(tbbd rh sbd Gpon€nidbc o m o a n v ; i , r t i i r , r r _ i i , : , . , 1 J . 1 , I - r i L : . r i r : : i t t - l . . . r r ) ! * .rhsad,mm, sc&d by b.cmpa

tld,ois I any rhs companyssoac

lL ' - : r i l , l i l i . a l r u6 r0 : r r e

Acid digestion by suitable acid depended ondifferent sample material(a6 below table)

1) Alkal iFusion2) HClto dissolve

Test ReportHITACHI CHEMICAL CO., LTD,1772.1 KAMKUEO YUUKI-sHI

No. I CU2011l42646 Date:


2011104127 Page:6 ot A

[ffI |||l[] ll

Analytical f,ow chart of halogen content1) Name ofthe person who made measufement Rita Chen2) Name of the peEon in charge of measurement Troy Chang

c o h @ i y r i . . I i l , . . r ( ' r , r , i i i : i i , i i : i t l i l i l i , l ioyeqedb G 6ercrcond r ois oi s

s u b ] e d l o T e m s a n d c o d l o i 6 ' o l E A t € d o i s d r o r . l o h e l m L b l o i o i ' a b l J

$mple pretreaiment / Separ€tion

Weighting and putting sample in cell

Oxygen Bomb Combustion / Absorpton

Dilution to nxed volume

Analysis was perfomed by lC

Mlmbe, orrhe %!crcup iscs sal

Test ReportHITACHI CHEMICAL CO-, LTD,1772-1 KANAKUBO YUUKI-SHI

No. : CEl2011l42U6 Dale:2O11lMn7 Page i 7 of 8


Analytical flow chart1) Name of the person who made measurement: Roman Wong2) Name of the person in charge of meaaurement Troy Chang

r Test |tems: PBB/PBDE, TBBP.A-bis

|r||[]|| |lfltt!

First testing prccess -----f OplionatscEen process --... Confi.malion proc€ss -.>

:ji!!rScreen analysis

1' ' ' ' ' ' . . . . . . . . . . . .

1_n , : i l : : r ' ; ; 1 . . i i + s6o l xe

SamDle extaction method

Concentrate/Drlute Extracted solution

t

Filter

V

Analysis by GC/MS

lssue Report

r_ ri i ,1, :: i,:rrtr i: . r. { .l.i;,.:l.yslqedb c Gener,r cd.d r dis di s

p o i s b ] l y € l o c c | 3 d a n d l h 3 d d f u m

Test ReportHITACHI CHEMICAL CO,, LTD.1772.,I KAMKUBO YUUKI-SHI

No. : CE12011142646Date:2011104127 Page : 8 of 8


'. End of Report *'

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