ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013...

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1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: ATOF Product #: 287xxx Series Issue Date: February 25, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the ATOF series RoHS-Compliant series products manufactured by Littelfuse, Inc. Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 RemarksNon-HF contains Chlorine (Cl) in white foil & orange colorant. Decemeber 01, 2005 Littelfuse, Inc. Page 1

Transcript of ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013...

Page 1: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: ATOF

Product #: 287xxx Series

Issue Date: February 25, 2013

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,

2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts

This document covers the ATOF series RoHS-Compliant series products manufactured by

Littelfuse, Inc.

< Raw Materials Used

Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1

Remarks:

Non-HF contains Chlorine (Cl) in white foil & orange colorant.

Decemeber 01, 2005 Littelfuse, Inc. Page 1

Page 2: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s)

1 057357 Molding Resin 3-12

2 955412-001 Plated Zinc Strip 13-17

3 425498 White Foil 18-26

4 057874 Colorant- Gray 27-36

5 057875 Colorant- Violet 37-45

6 057876 Colorant- Pink 46-54

7 057878 Colorant- Brown 55-63

8 057879 Colorant- Red 64-72

9 057880 Colorant- Blue 73-82

10 057877 Colorant- Tan 83-91

11 057883 Colorant- Green 92-100

12 057884 Colorant- Orange 101-109

13 057899 Colorant- Yellow 110-118

Page 3: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00299229

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0299229* Page 1 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse, S.A. de C.V. Date : Feb 25, 2013 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : VYDYNE 21SP-C Nylon Part Number : 057357 Date Sample Received : Feb 19, 2013 Date Test Started : Feb 19, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 4: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 2 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary: Result

Test Item Unit Test Method Semitransparent plastic pellets

RL

Heavy Metal

Cadmium (Cd) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Mercury (Hg) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Chromium VI (Cr6+) Content ppm

With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.

ND 1

Page 5: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 3 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Result

Test Item Unit Test Method Semitransparent plastic pellets

RL

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB)

ppm ND 5

Dibrominated Biphenyls (DiBB)

ppm ND 5

Tribrominated Biphenyls (TriBB)

ppm ND 5

Tetrabrominated Biphenyls (TetraBB)

ppm ND 5

Pentabrominated Biphenyls (PentaBB)

ppm ND 5

Hexabrominated Biphenyls (HexaBB)

ppm ND 5

Heptabrominated Biphenyls (HeptaBB)

ppm ND 5

Octabrominated Biphenyls (OctaBB)

ppm ND 5

Nonabrominated Biphenyls (NonaBB)

ppm ND 5

Decabrominated Biphenyl (DecaBB)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE)

ppm ND 5

Dibrominated Diphenyl Ethers (DiBDE)

ppm ND 5

Tribrominated Diphenyl Ethers (TriBDE)

ppm ND 5

Tetrabrominated Diphenyl Ethers (TetraBDE)

ppm ND 5

Pentabrominated Diphenyl Ethers (PentaBDE)

ppm ND 5

Hexabrominated Diphenyl Ethers (HexaBDE)

ppm ND 5

Heptabrominated Diphenyl Ethers (HeptaBDE)

ppm ND 5

Octabrominated Diphenyl Ethers (OctaBDE)

ppm ND 5

Nonabrominated Diphenyl Ethers (NonaBDE)

ppm ND 5

Decabrominated Diphenyl Ether (DecaBDE)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Page 6: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 4 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Result

Test Item Unit Test Method Semitransparent plastic pellets

RL

Phthalates Di(2-ethylhexyl) Phthalate (DEHP)

ppm ND 50

Dibutyl Phthalate (DBP) ppm ND 50

Benzyl Butyl Phthalate (BBP) ppm

With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. ND 50

Halogen Content

Fluorine (F) ppm ND 50

Chlorine (Cl) ppm ND 50

Bromine (Br) ppm ND 50

Iodine (I) ppm

With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

ND 50

Others

Hexabromo cyclododecane (HBCDD)

ppm

With reference to USEPA 3540C, by solvent extraction and determined by GC-MS.

ND 10

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample

Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Feb 19, 2013 Test Period : Feb 19, 2013 to Feb 21, 2013

(Ⅱ) Limit: RoHS Limit

Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 7: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 5 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized water and add diphenyl-carbazide solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Weigh sample and add alkaline solution

Definite temp. extraction

Cool and filter the extract

Cr6+

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Page 8: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 6 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Page 9: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 7 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 10: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 8 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 11: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 9 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 12: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299229

Test Conducted

*THJ0299229* Page 10 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 13: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00254946

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : May 04, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : PLATED ZINC STRIP Part Number : 955412-001 Date Sample Received : Apr 27, 2012 Date Test Started : Apr 28, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 14: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00254946

Test Conducted

Page 2 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item (1) (2)

Heavy Metal

Cadmium (Cd) content ND 54 Lead (Pb) content 14 112 Mercury (Hg) content ND ND

Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative

(< 0.02)(#) Negative

(< 0.02)(#)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample

surface of 24 cm2 was used and the dilution factor was adjusted accordingly.

Tested Components (1) Silvery Metal Base Material (2) Silvery Plating Layer

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Apr 27, 2012 Test Period : Apr 28, 2012 To May 03, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 15: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00254946

Test Conducted

Page 3 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 16: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00254946

Test Conducted

Page 4 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

Page 17: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00254946

Test Conducted

Page 5 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 18: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00281437

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

*THJ0281437* Page 1 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse, S.A. de C.V. Date : Oct 23, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : TAPE WHITE FOIL Part Number : 425498 Date Sample Received : Oct 16, 2012 Date Test Started : Oct 17, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 19: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 2 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic Film

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) 12260 Bromine (Br) ND Iodine (I) ND

Page 20: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 3 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic Film

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Oct 16, 2012 Test Period : Oct 17, 2012 To Oct 22, 2012

(Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 21: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 4 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.

50 ppm

Hexabromocyclododecane (HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 22: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 5 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 23: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 6 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 24: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 7 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 25: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 8 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 26: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00281437

Test Conducted

*THJ0281437* Page 9 of 9

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 27: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00299230

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0299230* Page 1 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse, S.A. de C.V. Date : Feb 25, 2013 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : Color concentrate gray Part Number : 057874 Date Sample Received : Feb 19, 2013 Date Test Started : Feb 19, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 28: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 2 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary: Result

Test Item Unit Test Method Dark gray plastic pellets

RL

Heavy Metal

Cadmium (Cd) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Mercury (Hg) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Chromium VI (Cr6+) Content ppm

With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.

ND 1

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB)

ppm ND 5

Dibrominated Biphenyls (DiBB)

ppm ND 5

Tribrominated Biphenyls (TriBB)

ppm ND 5

Tetrabrominated Biphenyls (TetraBB)

ppm ND 5

Pentabrominated Biphenyls (PentaBB)

ppm ND 5

Hexabrominated Biphenyls (HexaBB)

ppm ND 5

Heptabrominated Biphenyls (HeptaBB)

ppm ND 5

Octabrominated Biphenyls (OctaBB)

ppm ND 5

Nonabrominated Biphenyls (NonaBB)

ppm ND 5

Decabrominated Biphenyl (DecaBB)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Page 29: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 3 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Result

Test Item Unit Test Method Dark gray plastic pellets

RL

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE)

ppm ND 5

Dibrominated Diphenyl Ethers (DiBDE)

ppm ND 5

Tribrominated Diphenyl Ethers (TriBDE)

ppm ND 5

Tetrabrominated Diphenyl Ethers (TetraBDE)

ppm ND 5

Pentabrominated Diphenyl Ethers (PentaBDE)

ppm ND 5

Hexabrominated Diphenyl Ethers (HexaBDE)

ppm ND 5

Heptabrominated Diphenyl Ethers (HeptaBDE)

ppm ND 5

Octabrominated Diphenyl Ethers (OctaBDE)

ppm ND 5

Nonabrominated Diphenyl Ethers (NonaBDE)

ppm ND 5

Decabrominated Diphenyl Ether (DecaBDE)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Phthalates Di(2-ethylhexyl) Phthalate (DEHP)

ppm ND 50

Dibutyl Phthalate (DBP) ppm ND 50 Benzyl Butyl Phthalate (BBP) ppm

With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. ND 50

Halogen Content

Fluorine (F) ppm ND 50

Chlorine (Cl) ppm ND 50

Bromine (Br) ppm ND 50

Iodine (I) ppm

With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND 50

Others

Hexabromo cyclododecane (HBCDD)

ppm

With reference to USEPA 3540C, by solvent extraction and determined by GC-MS.

ND 10

Page 30: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 4 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample

Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Feb 19, 2013 Test Period : Feb 19, 2013 to Feb 21, 2013

(Ⅱ) Limit: RoHS Limit

Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 31: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 5 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized water and add diphenyl-carbazide solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Weigh sample and add alkaline solution

Definite temp. extraction

Cool and filter the extract

Cr6+

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Page 32: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 6 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Page 33: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 7 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 34: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 8 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 35: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 9 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 36: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299230

Test Conducted

*THJ0299230* Page 10 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 37: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00265154

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jul 06, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING Part Number : 057875 Date Sample Received : Jul 02, 2012 Date Test Started : Jul 02, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 38: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Brown Plastic Pellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Page 39: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Brown Plastic Pellets

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 02, 2012 Test Period : Jul 02, 2012 To Jul 05, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 40: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 41: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 42: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 43: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 44: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 45: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265154

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 46: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00265156

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jul 09, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING COLORANT Part Number : 057876 Date Sample Received : Jul 02, 2012 Date Test Started : Jul 02, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 47: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Red Plastic Pellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Page 48: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Red Plastic Pellets

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 02, 2012 Test Period : Jul 02, 2012 To Jul 06, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 49: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 50: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 51: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 52: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 53: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 54: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265156

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 55: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00265157

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jul 06, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : BROWN COLORANT Part Number : 057878 Date Sample Received : Jul 02, 2012 Date Test Started : Jul 02, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 56: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Brown Plastic Pellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Page 57: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Brown Plastic Pellets

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 02, 2012 Test Period : Jul 02, 2012 To Jul 05, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 58: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 59: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 60: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 61: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 62: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 63: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265157

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 64: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00265158

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jul 06, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : RED COLORANT Part Number : 057879 Date Sample Received : Jul 02, 2012 Date Test Started : Jul 02, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 65: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Red Plastic Pellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Page 66: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Red Plastic Pellets

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 02, 2012 Test Period : Jul 02, 2012 To Jul 05, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 67: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 68: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 69: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 70: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 71: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 72: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265158

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 73: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00299231

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0299231* Page 1 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse, S.A. de C.V. Date : Feb 25, 2013 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : Color concentrate blue Part Number : 057880 Date Sample Received : Feb 19, 2013 Date Test Started : Feb 19, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 74: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 2 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary: Result

Test Item Unit Test Method Blue plastic pellets

RL

Heavy Metal

Cadmium (Cd) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Mercury (Hg) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Chromium VI (Cr6+) Content ppm

With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.

ND 1

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB)

ppm ND 5

Dibrominated Biphenyls (DiBB)

ppm ND 5

Tribrominated Biphenyls (TriBB)

ppm ND 5

Tetrabrominated Biphenyls (TetraBB)

ppm ND 5

Pentabrominated Biphenyls (PentaBB)

ppm ND 5

Hexabrominated Biphenyls (HexaBB)

ppm ND 5

Heptabrominated Biphenyls (HeptaBB)

ppm ND 5

Octabrominated Biphenyls (OctaBB)

ppm ND 5

Nonabrominated Biphenyls (NonaBB)

ppm ND 5

Decabrominated Biphenyl (DecaBB)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Page 75: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 3 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Result

Test Item Unit Test Method Blue plastic pellets

RL

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE)

ppm ND 5

Dibrominated Diphenyl Ethers (DiBDE)

ppm ND 5

Tribrominated Diphenyl Ethers (TriBDE)

ppm ND 5

Tetrabrominated Diphenyl Ethers (TetraBDE)

ppm ND 5

Pentabrominated Diphenyl Ethers (PentaBDE)

ppm ND 5

Hexabrominated Diphenyl Ethers (HexaBDE)

ppm ND 5

Heptabrominated Diphenyl Ethers (HeptaBDE)

ppm ND 5

Octabrominated Diphenyl Ethers (OctaBDE)

ppm ND 5

Nonabrominated Diphenyl Ethers (NonaBDE)

ppm ND 5

Decabrominated Diphenyl Ether (DecaBDE)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Phthalates Di(2-ethylhexyl) Phthalate (DEHP)

ppm ND 50

Dibutyl Phthalate (DBP) ppm ND 50 Benzyl Butyl Phthalate (BBP) ppm

With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. ND 50

Halogen Content

Fluorine (F) ppm ND 50

Chlorine (Cl) ppm ND 50

Bromine (Br) ppm ND 50

Iodine (I) ppm

With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND 50

Others

Hexabromo cyclododecane (HBCDD)

ppm

With reference to USEPA 3540C, by solvent extraction and determined by GC-MS.

ND 10

Page 76: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 4 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample

Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Feb 19, 2013 Test Period : Feb 19, 2013 to Feb 21, 2013

(Ⅱ) Limit: RoHS Limit

Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 77: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 5 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized water and add diphenyl-carbazide solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Weigh sample and add alkaline solution

Definite temp. extraction

Cool and filter the extract

Cr6+

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Page 78: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 6 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Page 79: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 7 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 80: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 8 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 81: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 9 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 82: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00299231

Test Conducted

*THJ0299231* Page 10 of 10

Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 83: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00265155

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jul 06, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : TAN COLORANT Part Number : 057877 Date Sample Received : Jul 02, 2012 Date Test Started : Jul 02, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 84: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Tan Plastic Pellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Page 85: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Tan Plastic Pellets

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 02, 2012 Test Period : Jul 02, 2012 To Jul 05, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 86: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 87: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 88: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 89: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 90: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 91: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265155

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 92: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00265160

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jul 06, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : GREEN COLORANT Part Number : 057883 Date Sample Received : Jul 02, 2012 Date Test Started : Jul 02, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 93: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Green Plastic Pellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Page 94: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Green Plastic Pellets

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 02, 2012 Test Period : Jul 02, 2012 To Jul 05, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 95: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 96: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 97: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 98: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 99: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 100: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00265160

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 101: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00264346

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse, S.A. de C.V. Date : Jul 04, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description: One (1) group of submitted samples said to be : Part Description : COLORANT ORANGE Part Number : 057884 Date Sample Received : Jun 26, 2012 Date Test Started : Jun 27, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 102: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Dark Orange PlasticPellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) 1707 Bromine (Br) ND Iodine (I) ND

Page 103: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Dark Orange PlasticPellets

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jun 26, 2012 Test Period : Jun 26, 2012 to Jul 03, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 104: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 105: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 106: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 107: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 108: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 109: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00264346

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 110: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Test Report Number : TWNC00268652

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse, S.A. de C.V. Date : Jul 30, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : YELLOW COLOR CONCENTRATE Part Number : 057899 Date Sample Received : Jul 25, 2012 Date Test Started : Jul 25, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 111: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Orange Plastic Pellets

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Page 112: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Orange Plastic Pellets

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 25, 2012 Test Period : Jul 25, 2012 To Jul 27, 2012

(Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 113: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.

50 ppm

Hexabromocyclododecane (HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 114: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 115: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 116: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 117: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 118: ICP Test Report Certification Packet - Littelfuse2013/02/25  · Date Sample Received :Feb 19, 2013 Test Period :Feb 19, 2013 to Feb 21, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances

Number : TWNC00268652

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

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