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Transcript of I·. I'pdf.usaid.gov/pdf_docs/PNADC787.pdf · finest quality processed foods and their partners In...
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I·. I'
r~ ultu ",led Ex.port. o ~t ;:;'.'Yo §"' e: iC}. c-U. M .~ }tl :;::) ~~ ~' :;;j
"~ kkiS.tf~t" 6th Floor Giza t 9ypt
~rEl 0 :38«1445 .AX 02w. 48Y<0129
,f, Proj(:;.·c't No" 263»>0264
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. ,;.
REGISTRATION INFORMATION CONDIMENTS
Name
TIlle
Comoanv
AdcI_
.&.ITEL _____ ~~"C __ "" ________ "_'"""_
FAX "'" _____ "
EmaH
Attendeel may regilter by CIIIIng In or faxing thil registration to Al.ES. They may ailO regilter on-Ilte. Please let us know if you plan to attend 10 that we can plan appropriately.
This program fee II 4Ol.E. Regiltrants will raceive a course notebook, coffee break and certiflcete of particpation.
Join the Egyptian Agrlbu.ln ... AMoclatlonl
Food proceHlng coinpanl., and the eervIce leCtor firms that work with and help IUpport Egypt's processed foods Industry are encouraged to apply for membership in the Egyptian Agribuslne88 Association (EAGA).
EAGA serves the makers of Egypt's finest quality processed foods and their partners In the service induatrles, Including packaging, labeling, cold stores, freezing, banking and transportation companies, just to nama a few.
EAGA members receive a 28% dl.count on ALEB workshops.
Contact EAGA at: Telephone: 749-9176 or 749-6994
Email: InfOCegagribiz.org Web lite: http://www.agagribiz.org
CONDIMENTS: FORMULATION &
PROCESSING
A Short Collrse Sponsored by
AGRICUL TURE·LED EXPORT BUSINESSES (ALE B)
Novenlber13,2001 12:00 Noon to 4:00 P.M.
F .. :40LE
ALEB Training Center 12 Dokkl Street.11h Floor
Dokkl, Giza
... --illES Is a proJlct fond!td by USAID ,
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THOMAS A. BUTTERWORTH Austin FoodTech 114 Pearl Avenue
Newport Beach, CA 92662 TEL (714) 666-8482 FAX (714) 666-1017
EIIPLOYIIENT EXPERIENCE
1988-Present Managing General Partner Austin Food Tech, Inc. -5pecia1sts in Food Product Development
1984-1998 Instructor, "FDA Better Process Control School, • Chapman University, Orange, CA
1988-1989 Lecturer, "Chemical Engineering Process Design," Department of Chemical Engineering california State University at Long Beach
1973-1988 ASSOCiate DirectoI, Research and Development BeatricelHoot-Wesson, Inc., Fulerton, C8Iifomia - Management of productIprocess development with staIf of 24
- Project budget of $1.5 miIon
- Manpower assigI nnents for product development, technical service, and non-rouIine reguIatOfy interface for the following brands: 0rvIIe Redenbacher, HLrtt's. Peter Pan, FISher, J. Hungedord Smith, and Food Producers
- Experience with state-of-the-art aseptic ~ems, tomato products, toppi1gs, sauces, dry mixes, drilk bases, Iow-acid canned foods and fruits for both food service and retail product lines
- StaIf commercialized 32 new products and Ina extensions and 30 product improvements in a five year period
1982 Instructor, "Food Engineering" Depl of Food Science and Technology Chapman University. Orange, California
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1980 -1981 Lecturer, "Chemical Engineerii19 Process Design" Dept of Chemical, Nuclear and Thermal EngineeJilg University of California at Los Angeles
1988 -1973 Teachirlg and Res881ch Assistantship Dept. of Nutrition and Food Science MIT, Cambridge, Massachusetts
1988 Chemical Engileer Weslem Regional Research LaboratOry, AlJany. CA - Work resulted in three publications
1964 -1967 Chemical Engineer B.F. Goodrich Chemical Company, Long Beach. CA
EDUCATION
Ph.D., BiOchemical EngineerirIg. 1973 Massachusetts Institute ofTec:hnoIogy
- Chemical Engineering and BiOlogy millOf$ - Thesis project concemed separation of protein
solutions by ulbar6alion covered in two publications. - Recipient of NestJe..IFT Fellowship
B.S., Chemical Engineering. 1967 Universily of C81iromia at 8eJt!:eIey
PROFESSIONAL AFFILIATIONS
Institute of Food Techilologists: -Fonner Chairman, Food Erlgineerlng DivIsion and Fonner Member. Annual Program Commiltee
Institute for Thermal Processing Specialsts American Assoc. for the Advancement of ScIence Industry Advisory CoI.IlcI. Food Science and Technology Department. Univ. Calif. Davis
Food Engineerirlg Advisory Council. Univ. Calif. Davis
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1
Condiments: Fonnulation & Processing
• Thomas A. Butterworth, Ph.D. • Austin Food Tech, Inc. • Consultant for ALEB
• E~mall: [email protected]
• www.austlnfoodtech.com
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ALEB f:...t~ IS~ .. -
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foodtech@compYserve•com www.austlnfoodtech.com -
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2
Definition, Condiment:
n. A seasoning, e.g. pepper used to flavor food
Webster's Dictionary
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3
Definition, Condiment:
FED-REGS, §170.3 Definitions .
... plain seasoning sauces and spreads, olives, pickles, and relishes, but not spices or herbs .
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4
Some Types of Condiments
• Ketchup • Mayonnaise • Mustard • Spaghetti Sauce • Tomato Sauce • Hot Sauce
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• Chili Sauce • Worcestershire • Steak Sauce • Soy Sauce • Horseradish • Pickle Relish
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5
Some Characteristics of Condiments
• pH<I= 4.6 • Most heat processed • Some have standards • Diversity: Few characteristics in common
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6
Definition, Condiment:
For this course:
Tomato Ketchup
Mayonnaise
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7
Standard of Identity
• Product name(s) • Major ingredient(s) • Method of preparation • Minor (or optional) ingredients
allowed • How it is labeled • Quality attributes
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8
(a) Identity-(1) Definition. Catsup, ketchup, or catchup is the food prepared from ...
(i) Tomato concentrate ...
(ii) The liquid derived from mature tomatoes ...
(iii) The liquid obtained from the residue from preparing such tomatoes ...
(iv) The liquid obtained from the residue from partial extraction of juice from such tomatoes.
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9
Ketchup std. of identity (cont):
Such liquid is strained so as to exclude skins, seeds, and other
coarse or hard substances in accordance with current good
manufacturing practice ...
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10
Ketchup std. of identity (cont.):
The final composition of the food may be adjusted by concentration and/or by
the addition of water.
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11
Ketchup std. of identity (cont):
The food may contain salt and is seasoned with ingredients as specified
in paragraph (a)(2) of this section.
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12
Ketchup std. of identity (cont):
The food is preserved by heat sterilization (canning), refrigeration, or freezing. When sealed in a container to be held at ambient temperatures, it is so processed by heat, before or after
sealing, as to prevent spoilage.
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13
Ketchup std. of identity (cont):
(2) Ingredients. One or any combination of two or more of the following safe and suitable ingredients in each of the following categories is added to the tomato ingredients specified in paragraph (a)( 1) of this section:
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14
Ketchup std. of identity (cont):
(i) Vinegars.
(ii) Nutritive carbohydrate sweeteners ...
(iii) Spices, flavoring, onions, or garlic.
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15
Ketchup std. of identity (cont):
i) (3) Labeling. (i) The name of the food is "Catsup," "Ketchup," or "Catchup. "
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16
Ketchup std. of identity (cont):
(iii) Label declaration. Each of the ingredients used in the food shall
be declared on the label. .. . . . except that the name "tomato
concentrate" may be used in lieu of the names "tomato puree," "tomato
pulp," or "tomato paste" ....
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17
Ketchup std. of identity (cont):
(b) Quality. (1) The standard of quality for catsup is as follows: The consistency of the finished food is such that its flow is not more than 14 centimeters in 30 seconds at 200
C when tested in a Bostwick Consistometer ...
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18
Ketchup std. of identity (cont):
(3) If the quality of catsup falls below the standard... . .. the label shall bear the general statement of substandard quality... . .. "Below Standard in Quality--Low Consistency. "
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19
Ketchup std. of identity (cont):
( c) Fill of container. (1) The standard of fill of container for catsup. .. . .. is not less than 90 percent of the total capacity except:
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20
Ketchup std. of identity (cont):
(ii) When the food is packaged in individual serving-size packages containing 56.7 grams (2 ounces) or less.
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21
Summary, Must Contain:
1. Strained tomato ingredient 2.At least one of the following:
a.Vinegar b. Nutritive sweetener c. Spices, flavoring, onion, garfic
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22
Summary, May Contain:
1.Water 2.Salt 3. Seasonings
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23
Summary, May Not Contain:
Anything not specifically permitted; Examples:
Starch Gum Artificial colors Non-nutritive sweeteners Preservatives
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24
Standards Seem Restrictive
They are intended to be restrictive but they may be used creatively:
Lemon concentrate Spices Flavorings
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25
Lemon Concentrate:
FED-REGS, §155.194 Catsup. lemon juice, concentrated or lemon juice ... ... may be used ...... to adjust the pH .. .
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26
Spices FED-REGS, §101.22 Foods; labeling of spices ... Allspice, Anise, Basil, Bay leaves, Caraway seed, Cardamon, Celery seed, Chervil, Cinnamon, Cloves, Coriander, Cumin seed, Dill seed, Fennel seed, Fenugreek, Ginger, Horseradish, Mace, Marjoram, Mustard flour, Nutmeg, Oregano. Paprika, Parsley, Pepper, black; Pepper, white; Pepper, red; Rosemary, Saffron, Sage, Savory, Star aniseed, Tarragon, Thyme, Turmeric.
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, 27
Flavorings
This category covers any approved . compound used to impart flavor
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28
How to design a Ketchup Product
"Imitation is the sincerest form of flattery"
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Product Emulation: Tools Available
• Label • Product characteristics • Chemistry • Experimentation
:e;L.,s\ its' .... i. At.; tl\ ~t • .h'
~1l:uD -•
4..a.Jd ~ .- -:1 _ ." .~
29
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30
Label: Ingredient Declaration
• Tomato concentrate
• Distilled vinegar • High fructose
corn syrup
• Corn syrup
cl--ulJ .. .J -
~I J."..........-- • .. LC,-"J-JJ" U~-
• Salt • Spice • Onion powder • Natural
flavoring
r-bL.JJ1 jS JA -
fo J;.
~ j.,s)::..j~I.;i11
j.,s)::.. -
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31
Label: Nutritional Facts
• Serving size 17 g • Total fat 0 g • Sodium 190 mg • Total carb 4 g • Fiber 0 g • Sugars 4 g • Protein 0 g
%, 1 ~tlji%."i-~~ -%."i-r~ -%."i-~ -
• Vitamin A 6% • Vitamin C (lOA,
• Calcium (lOA,
• Iron (lOA.
t+W~~
t+."i-~~ -!"4"-H. r.J:l.l.,- -
, ~ d yo;..M.fil -
t+ t+';"'~ -t+' d.tfi- -
t+ ."i- Ufa.J..)l •
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32
Product Characteristics
• Color • Consistency
• Taste • Texture
w."lll -~~I
JllJl -
rl.,ill -
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33
Chemistry
• Moisture • Fat • Fatty acid profile • Protein • pH
d~~.fi
~Y.fod t.Jl -cl--
r~.J-
~uA-W1-
• Carbohydrate • Sugar profile • Salt • Sodium • Total Acid
~.,Jm~
~.lI
~.lll uA-W t.Jl -....
(.)JJ.JY. -
t...,-lI ~jl-
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Formula Estimate: Table Ingredient Formula %
Water 0
Tomato paste I 0
Vinegar I 0
HFCS 0
Corn syrup 0
Salt 0
, Totals 100
.; 'Is ~ LS .• h t :J.e % ~.JlI ~:alI~
.).- foL..
• ~LJ.J\W"""'" ..J'-
.).- Ji.
.).- jjlSI.).II ~ jfi.,l::t.
.).- jfi .,l::t.
.).- cL. , . . ~'il
34
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Formula Estimate: Tomato Paste
Bostwick consistency: \
3 to 4 cml30 seconds I i
\
: ~ ':. na I '6..:il1 liii..\ ... l..)M'1 (,}I'J • .) •
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J
! , ,I
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36
Formula Estimate: Tomato Paste Ingredient Formula %
Water 70
Tomato paste 30
Vinegar 0
HFCS 0
Comsymp 0
Salt 0
Totals 100
~w .1Ilt (Uiu :lJls'!u /J ,h.
% ~ji.1I ~liJI ..;wUJI v. ,.t..
yo. ~I....bl\u"""""
.;i- J:..
.;i- jfolJ&ll ~ jfi ~
.;i- jfi~
.;i- ~ , .. ~'il
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37
Formula Estimate: Salt
Label: 190 mg sodium in 17 9
0.190/0.39/0.17 = 2.8% salt
,... 'v ~ r.J;lol..,.... r+--' 4\. :~
~ %Y,A - " 'V/.,Y'4\/., H.
\ i I
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I !
1 I ~ 1
I
I ;: ..
38
Formula Estimate: Salt Ingredient Formula Salt Contribution
(%) (%) (%)
Water 67.3 0 0.0
Tomato paste 30 0.3 0.1
Vinegar 0 0.0
HFCS 0 0.0
Comsymp 0 0.0 Salt 2.7 100 2.7
Totals 100 2.8
~ .. ~ .. _ :4:,J5 _ LI I.a ..
~"II~ eLo ~.JlII ~.iilI~
{%> (%) {%>
· , . .>i- ,\V," .. t..
· , , " ,. ,.. rl-l..l:JI u-*""
· , . .>i- Jo.. · , . .>i- ~jfi.JJ l'
jjiSl.)ll
" . .>i- jfi~
V,V , .. 'I',V eI..
Yf"
, .. ~'11
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Formula Estimation: Acid
Measurement:
Total Acidity (as acetic) = 1.4%
\ \ !
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i 1
I l
j
1 1 I , 11
40
Formula Estimation: Acid
Ingredient Formula Acid Contribution (0/0) (%) (%)
Water 62.8 0 0.0 Tomato paste 30 1.75 0.5 Vinegar 4.5 20 0.9 HFCS 0 0 Com syrup 0 0 Salt 2.7 0 0
Totals 100 1.4
'",n" ~ .. ullll'llna.. :4 a,S _ tJ. Ila ..
1'1f..."I' ~ u:-.-la. 4.Is.;n ~li.I\ ~I
(%) (%) (%)
· , . .;i- H,A ~L.
• ,0 , ,vo \". r-b1..J..l1,,~
• • 'I V. t,o Jo. .;i- .;i- ~jfi-,l :>
jjiSl.;iII
.;i- .;i- jfi~
.;i- .;i- V,v eI.. ,.t , .. ~)'I
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Formula Estimation: HFCS Sugar Profile:
Sucrose None
Glucose Significant
Fructose 6.6%
lactose None
Maltose Some \ I ! \i ,
1 tiS' .aU cP 1 ,s,. :~)il\ cJ "'n · :.fo.d t..ti
".J! '1 j."fo.
.Ii...t=olo jfi.,l:,.
"",' jjiSl.,j
".J! '1 j.fGI ~uMl jjill.
41
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j 'I ,
I
I §
~ .i 'ii
11
I i"
~,
-,
I;
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42
Formula Estimation: HFCS
Ingredient Formula Fructose Cont.
(%) (0/0) (%)
Water 40.8 0 0.0 Tomato paste 30 0.7 0.2 Vinegar 4.5 0 0.0 HFCS 22 30 6.6 Comsymp 0 0 Salt 2.7 0 0
Totals 100 6.8
·~lM .JU:. J CJ-- ~ ~, ,s, :.4 'els AD ~ lia.
I'~I~ JJSJl4. 4.!s,.,m ~lU.,...an
(%) (%) (%)
, , ' .;i- to,A "t.. " y "V r. rlat..J.ll ~
••• .;i- £,0 ~
'1,'1 YO. n ~L..J:. j'p JI ?
j.JSS.I.;ilI
.;i- .;i- J,P.,J,..
.;i- .;i- V,V eL-',i. \ .. ~'11
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43
Formula Estimation; Carbohydrate
Label: 4 gm carbohydrate in 17 gm
4 gm/17gm X 100 = 23% Carbohydrate
~,v c}~'~Y..fi~t:~
d~y'.fi %YT' - , •• X ~'v/~t
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Formula Estimation: Carbohldrate
Ingredient Formula Carbo. Cont. (%) (%) (%)
Water 39 0 0.0
Tomato paste 30 21 6.3
Vinegar 4.5 0 0.0 HFCS 22 71 15.6
Comsymp 1.5 80 1
Salt 2.7 0 0 Totals 100 23
~')\t •. tJu~ :.4!tS~ ~.Ii:lll. t'lf..~1 ~ .::.IJJ;a,.,H.JS ~JIlI ",lli.II ~
(%) (%) (%)
••• .;i- 1"'1 .. l.
'\,1" '"
r. r-bWalI U-"i"'-"
••• .;i- t,o Jo. -~
1 , n VI n .,J~ jfiJ! ?
jfolJill , A. , ,0 Jfik. .;i- .;i- ", V cl.. '1''- I •• ,)4'11
44
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Formula Estimation: Iteration
Ingredient Formula Carbo. Cont. (%) (%) (%)
Water 43 0 0.0
Tomato paste 25 21 52 Vinegar 4.5 0 0.0
HFCS 22 71 15.6 Comsymp 2.7 80 22 Salt 2.7 0 0
Totals 100 23
'~l :.lH< JlD tJ,lia-,......1I4.,...J .:J.J¥tv 4,ysJill c;llU.,.,uI
( .. ) (9ft) ('10)
',' .;i- U' .1..
O,V V\ vo ,.w.101 u..-
',' .;i- t,o Ji. \0,' V\ VV .,. c J.P.} ..
.»&1.iJ Y,Y A. Y,V jfik .;i- .;i- V,v eLo ,.,. \ , , ~"il
I
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i , i , ,
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, ,
J
46
What Should be Right by Now
-Color - Consistency (Bostwick) -Sweetness -Brix - Total acid (and pH) -Salt
" ,ii' h l' !., ,"1 tS.J wi '"";.' iJ ,,In L..
U.,lll-
( ·l:..:lll L:i:i.1) ·6.:l!1 -(.)'IJ. J . (.)'IJ •
oJ')l::Jl-
J..,h..JI jfoJi(~.,.-ll 4.>l..,) JSlI ~WI -
c;LJI -
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What is Next?
-Spice -Onion powder -Natural flavoring
~'J~-
47
\
I ! '\
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i
I f
48
Spice
.Clove? Cassia? -Experiment with different levels
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49
Onion Powder
• Experiment with different levels
• You know the level is low
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'i
i
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50
Natural Flavoring
• You know it contains garlic • Also other flavors • Level is very low
r; ~ cJ jj::.:J '+1i r1.s Ult -~~yi..\l1 u4Sll1 ~.J
u.<:al.iiJ'l1 ~ ~jl.-ll -
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51
Natural Flavoring
• Sophisticated instrumentation or
• Consult flavor company
i';'.JJ I!.IWI rI.l.i:i...1 -
)
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:}
52
Will you get it Right the First Time?
No, but you will be 900/0 there the first time and if your refinements are consistent with the chemistry, you will get closer every time
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Processing
PaIJIe FfniIIh: water
O.7mm O.B4nm 1.14mm 1.5mrn
Men ImoIubIe IIOIId$; Men~lIfIer honiOjjilll/zilllo
53
FreJh totlJlto8$
YJe1r120S I/ifPIr
\ f 1
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\ \l I \l
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54
Yield (Tomatoes)
Tomatoes contribute most to thickness
If ketchup is too thick, reduce tomato Maintain Brix with sweeteners
This increases yield & reduces cost
rloW:J1 u.- Jli ,I~.l.l.#- ,+-I.,i ~I ~ I~J ~ r..j.fi...J1 J):-ll jf..y ~ .Jail.:..-,
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55
Processing (cont)
--'VIIIIUUm How much?
(baU) 61;·4;'1 W".f"I..J .i."J <>- 7. 7
• ,..--<>-r)IuJII.qar ""
fo
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j i , . ,
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56
Processing (cont.l
Why 43DC? This i8 an BWlIl'Ig& not center temp No need for futthar cooling Smoother labeling operation
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FED-REGS, §169.14O Mayonnaise.
(a) Description. Mayonnaise is the emulsified semisolid food prepared from vegetable oil(s), ... . .. acidifying ingredients... . .. egg yolk... • . .ingredients specified ...... maya/so be used ... '" The name of the food is "Mayonnaise" ... .. . Each of the ingredients... . .. shall be dec/ared on the label ...
• _... • .1:__ "'. :S.-J';..::. ~ ~ ...... ~ ~ ...... .,.,0."'. ~ ......
L -I)'" , '.< _. ":'1 l' D· -' d • ••• .......... ' I" ~ 'I'*' •••••• ! J!'4 ~'
• '" '" " •• _.I _,,- , 'tl _ . ..1 ••• • •• ~.Jl ~ ••• ••• JI'~' ~ fl&lal1 r--••• Ut 1..1D ~ ~ c)4 J' 0;" JS
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58
Summary, Must Contain:
1. Vegetable oil (min. 65%) 2.Acidifying agent(s)
a.Vinegars b. Lemon or lime juices
3.Egg yolks a. Yolks/whole eggs
(%, 0 ~l ~) ~~ WD . , WOJ4,1 (J,oIJC') J,o\.c. ."
~.i
#.1 .Jli.....a • r J,o\S ~/ #.1 .Jli.....a .1
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59
Summary, May Contain:
• Egg whites • Salt • Nutritive
Sweeteners • Spices (Except 2) • Natural flavoring
• Water • MSG • Sequesterants
(EDT A) • Citric or malic
acids • Crystal inhibitors • Nitrogen or CO2
.l. _ ~~_
~'11 r.Jlol.,....J..:l..Il."l,. - eL. -c:y..'il ..,111 uP.) 'Jt.I.:a. JI,. - ~ ,·",6· -{~ vA- w"'lw up'p 1.»1.4).:;,!J4I -(~)~~ _ (I.loo
( ...... ) c1lil vA-.J ~ ,· •• s;. -
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;
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60
Summary, May Not Contain:
Anything not specifically permitted For example:
Saffron or turmeric Anything yellow Starch/gum Artificial flavor/color
'4.Jo'lI.J' 0; 1\ ~.J ~ '+! c. -"""""'" ..»f:- o.lL. c.jl :l.t..i
rS..f. .,1 wI,).c. j "I";"'" o.ll... 'it
~/1.1l..i ~u~/~
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'11
Standards Seem Restrictive
They are intended to be restrictive but they may be used creatively:
Lemon or lime concentrate Spices Flavorings
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How to design a Mayonnaise Product
"Imitation is the sincerest form of flattery"
... as usual
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Product Emulation: Tools Available
• Label • Product characteristics
• Chemistry • Experimentation
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Label: Ingredient declaration
• Oil, soy • Salt • Eggs (whole) • Vinegar
• Lemon juice • Mustard flour
• Water • EDTA • Egg yolk
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Label: Nutritional Facts
• Serving size 14 9
• Totaltat 11 9 • Sat Fat 1.5 9
• Cholesterol 5 mg
• Sodium 75 mg
• Total cam 0 9 • FiberOg
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• SugarsOg • Protein 0 9 • Vitamin A 0% • Vitamin C 0% • Calcium 0% • Iron OOA.
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First Calculated Formula:
Soy oil Eggs, whole Vinegar (5%) Water Egg yolk Lemon juice Salt Mustard Flour EDTA
Total
77% 9.0 6.0 1.2 3.0 2.0 1.4 0.5 0.02 100%
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USDA Nutrient Data Base
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Formula Estimation: Acid
Ingredient Formula Acid Contribution (%) (%) (%)
Oil 77 0 0 Eggs, whole 9.0 0 0 Vinegar (5%) 6.0 5 0.3 Water 1.2 0 0 Egg yolk 3.0 0 0 Salt 1.4 0 0
Totals 97.5 0.3
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Formula Estimation: Water
Ingredient Fonnula Water Contribution
(%) (%) (%)
Oil n 0 0 Eggs, whole 9.0 75.8 6.8 Vinegar (5%) 6.0 95 5.7 Water 1.2 100 1.2 Egg yolk 3.0 48.8 1.5
Salt 1.4 0 0
Totals 97.5 15.0
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Shelf Stability
Mayonnaise is not heat processed
It is stabilized by: Acid combined with Low water content
In this case, acidlwater x 100 = 2.0
Hazards for the consumer?
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