How to Prepare Gases
Transcript of How to Prepare Gases
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How to Prepare Gases
Chemistry Lab Instructions
You can use common chemistry lab chemicals and equipment to prepare several gases. A conical
flask, thistle funnel, delivery tube, pneumatic trough, and beehive are useful items to have on hand.Please make sure you are familiar with the use and functioning of the laboratory equipment you use,are aware of the characteristics of the substances (toxicity, flammability, explosivity, etc.), and takeproper safety precautions. Use a ventilation hood (fume cupboard) and keep flammable gases awayfrom heat or flame. I've tried to be as accurate as possible in my instructions, but you use them atyour own risk. For convenience, I've listed the gases in alphabetical order.
Gas Reagents Method Collection Reaction
Ammonia
NH3
Ammonium
chloride
Calcium
hydroxide
Gently heat a mixture of
ammonium chloride andcalcium hydroxide in water.
Upward
displacementof air in a
hood.
Ca(OH)2 +
2NH4Cl
2NH3 + CaCl2+ 2H2O
Carbon
DioxideCO2
Calcium
carbonate(marble chips)
5 M
Hydrochloric
acid
Add 5 M hydrochloric acid to 5
- 10 g marble chips.Upward
displacementof air in a
hood.
2HCl +CaCO3 CO2
+ CaCl2 +H2O
Chlorine
Cl2
Potassium
permanganate
Conc.Hydrochloric
acid
Add concentrated hydrochloric
acid dropwise onto a small
amount of potassiumpermanganate crystals (in
flask).
Upward
displacement
of air in ahood.
6HCl +
2KMnO4 +2H+ 3Cl2 +
2MnO2 +
4H2O + 2K+
Hydrogen
H2Zinc
(granulated)5 M
Hydrochloric
acid
Add 5 M hydrochloric acid to 5
- 10 g granulated zinc pieces.Collect over
water.
2HCl + Zn
H2 + ZnCl2
Hydrogen
ChlorideHCl
Sodium chloride
Conc. Sulfuricacid
Slowly add concentrated
sulfuric acid to solid sodiumchloride.
Displacement
of air in ahood.
2NaCl +H2SO4
Na2SO4 +2HCl
Methane
CH4
Sodium acetate
(anhydrous)Soda lime
Mix 1 part sodium acetate with
3 parts soda lime. Heat in adry pyrex test tube or flask.
Collect over
water.
CH3COONa +
NaOH
CH4+ Na2CO3
Nitrogen
N2Ammonia
Calciumhypochlorite
(bleachingpowder)
Shake 20 g calcium
hypochlorite into 100 mLwater for several minutes,
then filter. Add 10 mL conc.ammonia and heat mixture.
Use extreme caution!
Displacement
of air.2NH3 +
3CaOCl2 N2
+ 3H2O +
3CaCl2
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Chloramine and explosive
nitrogen trichloride may beproduced.
Nitrogen
N2Air
Lighted
Phosphorus (orheated Fe or
Cu)
Invert a bell jar over lighted
phosphorus. Oxygen and
phosphorus combine to formphosphorus pentoxide, which
is absorbed by the water over
which the bell jar stands (maybe violent reaction), producing
phosphoric acid and leaving
the nitrogen behind.
Removal of
oxygen.
5 O2 + 4 P
P4O10
NitrogenDioxide
NO2
Copper(turnings)
10 M Nitric acid
Add concentrated nitric acid to5 - 10 g copper.
Upwarddisplacement
of air in ahood.
Cu + 4HNO3 2NO2 +
Cu(NO3)2 +
2H2O
Nitrogen
MonoxideNO
Copper
(turnings)5 M Nitric acid
Add 5 M nitric acid to 5 - 10 g
copper.Collect over
water.3Cu + 8HNO
3
2NO +
3Cu(NO3)2 +
4H2O
NitrousOxide
N2O
Sodium nitrateAmmonium
sulfate
Mix 10 g powdered sodiumnitrate and 9 g ammonium
sulfate. Heat well.
Displacementof air.
NH4NO3
N2O + 2H2O
Oxygen
O2
6% Hydrogen
peroxideManganese
dioxide
(catalyst)
Add hydrogen peroxide to
about 5 g of MnO2.
Collect over
water.
2H2O2
2H2O + O2
Oxygen
O2Potassium
permanganateHeat solid KMnO4. Collect over
water.
2KMnO4
K2MnO4 +MnO2 + O2
Sulfur
DioxideSO2
Sodium sulfite
(or sodiumbisulfite)
2 MHydrochloric
acid
Add dilute hydrochloric acid to
5 - 10 g sodium sulfite (orbisulfite).
Upward
displacementof air in a
hood.
Na2SO3 +2HCl SO2
+ H2O +2NaCl
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It's easy to generatehydrogengas at home or in a lab using common household materials. Here'show to make hydrogen safely.
Make Hydrogen Gas - Method 1
One of the easiest ways to obtain hydrogen is to get it from water, H2O. This method employselectrolysis, which breaks water into hydrogen and oxygen gas.
water 9-volt battery 2 paperclips
1. Unbend the paperclips and connect one to each terminal of the battery.2. Place the other ends, not touching, into a container of water. That's it!3. You'll get bubbles off both wires. The one with more bubbles is giving off pure hydrogen. The
other bubbles are impure oxygen. You can test which gas is hydrogen by lighting a match orlighter over the container. The hydrogen bubbles will burn; the oxygen bubbles will not burn.
4. Collect the hydrogen gas by inverting a water-filled tube or jar over the wire producing thehydrogen gas. The reason you want water in the container is so you can collect hydrogen withoutobtaining air. Air contains 20% oxygen, which you want to keep out of the container in order tokeep it from becoming dangerously flammable. For the same reason, don't collect the gas comingoff both wires into the same container, since the mixture could burn explosively upon ignition. Ifyou wish, you can collect the oxygen in the same way as the hydrogen, but be aware this gas is
not very pure.5. Cap or seal the container before inverting it, to avoid exposure to air. Disconnect the battery.
Make Hydrogen Gas - Method 2
There are two simple improvements you can make to improve the efficiency of hydrogen gasproduction. You can use graphite (carbon) in the form of pencil "lead" as electrodes and you can add a
pinch of salt to the water to act as an electrolyte. The graphite makes good electrodes because it iselectrically neutral and won't dissolve during the electrolysis reaction. The salt is helpful because itdissociates into ions which increase the current flow.
2 pencils salt cardboard water battery (could go as low as 1.5 V with the electrolyte) 2 paperclips or (better yet) 2 pieces of electrical wire
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7/31/2019 How to Prepare Gases
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1. Prepare the pencils by removing the erase and metal caps and sharpening both ends of thepencil.
2. You're going to use the cardboard to support the pencils in the water. Lay the cardboard overyour container of water. Insert the pencils through the cardboard so that the lead is submerged
in the liquid, but not touching the bottom or side of the container.3. Set the cardboard with pencils aside for a moment and add a pinch of salt to the water. You could
use table salt, Epsom salts, etc.
4. Replace the cardboard/pencil. Attach a wire to each pencil and connect it to the terminals of thebattery.
5. Collect the gas as before, in a container that has been filled with water.Make Hydrogen Gas - Method 3
You can get hydrogen gas by reacting hydrochloric acid with zinc.
hydrochloric acid (muriatic acid) zinc granulesHydrogen gas bubbles will be released as soon as the acid and zinc are mixed. Be very careful to avoid
contact with the acid. Also, heat will be given off by this reaction.
You can prepare sodium silicate or water glass from gel beads (silica) and drain cleaner (sodiumhydroxide). Sodium silicate can be used to make chemical gardens, like those that result from MagicRocks (which you canmake yourself).
Sodium Silicate Materials
All you need to make a sodium silicate solution are water, silica, and sodium hydroxide. Silica comesin those little packets labelled 'do not eat' with electronics, shoes, etc. Sodium hydroxide is readilyavailable in its pure form or can be found as drain cleaner.
6 g silica gel beads (crushed) 4-8 g sodium hydroxide (4 g for water glass, used in the magic rock project, or 8 g for the
stoichiometric ratio for sodium silicate)
10 ml waterPrepare Sodium Silicate
1. Wear proper safety gear, which includes gloves.2. Heat 4-8 grams of sodium hydroxide in 10 ml of water.3. Once the sodium hydroxide is dissolved, slowly add the 6 grams of crushed silica gel beads. Heat
the solution between additions. If the crushed beads won't dissolve, add a little more water to thesolution.
http://chemistry.about.com/od/growingcrystals/a/aa060704a.htmhttp://chemistry.about.com/od/growingcrystals/a/aa060704a.htmhttp://chemistry.about.com/od/growingcrystals/a/aa060704a.htmhttp://chemistry.about.com/od/growingcrystals/a/aa060704a.htm -
7/31/2019 How to Prepare Gases
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Sand that you find on a beach consists of several minerals and organic matter. If you could separateout the impurities, you would have pure sand, which is silica or silicon dioxide. Here is how to preparepure sand yourself in the lab. It is an easy project that only requires a few chemicals.
Ingredients for Sand
sodium silicate (make sodium silicate yourself) sodium bisulfate waterMake Pure Sand
1. Mix together 5 ml sodium silicate solution and 5 ml water.2. In a separate container, use a glass stirrer to mix 3.5 grams sodium bisulfate into 10 mL of
water. Keep stirring until the sodium bisulfate dissolves.3. Mix the two solutions together. The resulting gel that forms at the bottom of the liquid is
orthosilicic acid.4. Place the orthosilicic acid into a heat-safe glass or porcelain dish and heat it over a burner flame
for about 5 minutes. The orthosilicic acid dries to form silicon dioxide, SiO2, which is your puresand. Sand is non-toxic, but it presents an inhalation hazard since the small particles couldbecome trapped in your lungs if inhaled. Therefore, enjoy your sand, but don't play with it likeyou might with natural sand.
These are easy instructions for making sodium carbonate, also known as washing soda or soda ash,from baking soda or sodium bicarbonate.
Make Sodium Carbonate
Sodium bicarbonateis CHNaO3 whilesodium carbonateis Na2CO3. Simply heat baking soda or sodium
bicarbonate in a 200F oven for about an hour. Carbon dioxide and water will be given off. Dry sodium
carbonate will remain.
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