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    CE320 Highway MaterialsCE320 Highway Materials

    Testing ExperimentsTesting Experiments

    ByDr. Tom. V. Mathew

    IIT Bombay

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    Overview

    Pavement materials

    Soil (sub-grade, embankment)

    Aggregates (coarse, fine)

    Binders (Bitumen, cement)

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    Soil

    Soil is all unindurated mineral material lying above rock strataincluding air, water, and organic matter

    It is non-homogeneous and porous

    Properties greatly influenced by moisture, density andcompaction

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    Soil

    Soil is a very essential highway material

    1. Soil sub grade is part of the pavement

    structure; the design and behaviour of

    pavement depends to a great extent on the sub

    grade properties

    2. Soil is one of the principal materials of

    construction in stabilized soil base and sub

    base and also in embankment construction

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    Properties of soil

    Shape of soil particles (bulky, flaky)

    Particle size classification (clay, silt, sand, gravel)

    Gradation of soil

    Porosity and void ratio

    Soil density (dry and wet density)

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    Properties of soil

    Moisture-density relationship (Proctor density, OMC)

    Chemical properties (Organic matter, minerals, pH)

    Soil-water (Capillary water, water table)

    Physical properties (Permeability, compressibility, shear

    resistance)

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    Properties of soil

    Atterberg limits (Index properties)

    Liquid limit : Moisture content at which state changes from

    viscous liquid to plastic solid

    Plastic limit : Moisture content at which state changes from

    plastic solid to semi solid state

    Plasticity index : Range during which it acts as plasticPI = LL PL

    Liquidity index : (NMC PL) / PI

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    Desirable Properties of soil

    Stability: Adequate stability to resist permanent

    deformation under loads

    Incompressibility: Minimum variation in volume

    ensures minimum differential expansion and

    strength values

    Permanency of Strength: Should retain desired

    subgrade support i.e. resistance to weathering

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    Minimum changes in volume and stabilityunder adverse conditions of weatherand ground water

    Good drainage: Essential to avoidexcessive moisture retention and toreduce the potential

    frost action

    Ease of compaction: Ensures higher drydensity and strength under particulartype and amount of compaction

    Desirable Properties of soil

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    Bitumen is a petroleum product obtained by thedistillation of petroleum crude

    Bitumen is a hydrocarbon material of either natural or

    pyrogenous origin, found in gaseous, liquid, semisolid or

    solid form

    Highway construction: hydrocarbon material which are

    cementitious in character

    Bitumen

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    Bitumen

    1. Natural product (lake asphalt, rock asphalt)

    2. Fractional distillation of petroleum

    a. Asphalt cement (Penetration grade)

    b. Oxidised asphalt (softening point grade)

    c. Liquid asphalt

    3. Tar: destructive distillation of coal

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    Cutback: the viscosity of bitumen reduced byvolatile diluents: slow, medium, rapid curing

    Emulsion: bitumen is suspended in finely divided

    condition in an aqueous medium and stabilized

    with an emulsifier : slow, medium, rapid setting

    Liquid Bitumen

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    1. Normal Bitumen

    Production

    The portion of bituminous material present inpetroleum may widely differ depending on the source

    Almost all the crude petroleum's contain considerableamounts of water along with crude oil

    Hence the petroleum should be dehydrated before the

    distillation

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    Petroleum Bitumen Flow Chart

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    Types of Distillation Processes

    Fractional distillation:

    2. In the fractional distillation the various volatile

    constituents are separated at successively higher

    temperatures without substantial chemical change

    4. The fractions obtained yield gasoline, naphtha,

    kerosene and lubricating oil

    3. The residue would be petroleum bitumen

    4. In destructive distillation material undergoes chemical

    changes under the application of extreme heat and

    pressure

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    Steam distillation:

    2. Steam distillation is employed to produce steam

    refined petroleum bitumen without causing

    chemical change

    4. When the residue is distilled to a definite

    consistency without further treatment it is called

    as Straight-run Bitumen

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    It should be fluid enough at the time of mixing to

    coat the aggregate evenly by a thin film

    It should have low temperature susceptibility

    It should show uniform viscositycharacteristics

    Bitumen should have good amount of volatiles in

    it, and it should not lose them excessively when

    subjected to higher temperature

    Desirable Properties of Bitumen

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    The bitumen should be ductile and not brittle

    The bitumen should be capable of being heated to thetemperature at which it can be easily mixed without anyfire hazards

    The bitumen should have good affinity to the aggregateand should not be stripped off in the continued presenceoff water

    Desirable Properties of Bitumen

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    Aggregate

    Aggregate is the major component of all

    materials used in road construction

    It is used in granular bases and sub base,

    bituminous courses and in cement concrete

    pavements

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    Desirable properties of Aggregate

    Strength:The aggregate should be sufficiently strong towithstand the stresses due to traffic wheel load

    Hardness: Aggregate should have hard enough to resist

    the wear due to abrasive action of traffic

    Toughness: Aggregate should have resistance to impact

    or toughness

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    Continue.

    Durability: The aggregate used in pavementshould resistance to disintegration due to theaction of weather

    Shape of aggregate: Should not be Flakyand elongated

    Adhesion with Bitumen: Should have goodaffinity to bitumen

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    Quality Control Tests: Soil

    1. Gradation

    2. Atterberg Limits and indices (LL, PL,PI, SL)

    3. Laboratory Compaction (MDD and OMC)

    4. Field density test

    5. CBR Test (Demo)

    6. Plate bearing test

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    Quality control tests: Aggregate

    1. Sieve analysis

    2. Aggregate crushing test

    3. Aggregate impact test

    4. Abrasion Test (L.A. abrasion test)

    5. Shape test (FI, EI, Angul. No.)

    6. Soundness Test

    7. Specific gravity and Water absorption test

    8. Stripping value test

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    1. Penetration

    2. Ductility

    3. Softening point

    4. Specific gravity

    5. Loss on heating

    6. Flash & Fire point

    7. Viscosity (Demo)8. Solubility

    Quality control tests: Bitumen

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    California bearing ratio (CBR)

    A simple test that compares the bearingcapacity of a material with that of a well-graded

    crushed stone

    A high quality crushed stone material should

    have a CBR of about 100%

    CBR is basically a measure of strength

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    CBR

    The California Bearing Ratio (CBR) test was developed by theCalifornia Division of Highways in 1929 as a method ofclassifying the suitability of a soil for use as a subgrade or basecourse materials in highway construction

    During World War II, the U.S. Corps of Engineers adopted thetest for use in airfield construction

    The test is empirical and results cannot be related accuratelywith any fundamental property of the material.

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    CBR

    CBR value is the measure of resistance ofmaterial to the penetration of standard plunger

    under controlled density and moisture

    condition.

    The CBR test can be made in the laboratory on

    undisturbed or remoulded soil samples.

    The CBR value of sub grade is normally

    evaluated on a soaked sample compacted at

    optimum moisture content to maximum dry

    density.

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    Basic Test

    This consists of causing a plunger of 50 mmdiameter to penetrate a soil sample at the rate of1.25 mm/min.

    The force (load) required to cause the penetration is

    plotted against measured penetration.

    The loads at 2.5 mm and 5 mm penetration arerecorded.

    This load corresponding to 2.5 mm or 5 mmpenetration is expressed as a percentage ofstandard load sustained by the crushed aggregatesat the same penetration to obtain CBR value.

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    Definition of CBR

    California bearing ratio is defined as theratio (expressed as percentage) between

    the load sustained by the soil sample at a

    specified penetration of a standard

    plunger (50 mm diameter) and the load

    sustained by the standard crushed stones

    at the same penetration.

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    Standard Load values on Crushed Stones for

    Different Penetration Values

    183360012.5

    162318010.0

    13426307.5

    10520555.0

    7013702.5

    Unit Standard

    Load, kg/cm2Standard

    Load, kg

    Penetration,

    mm

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    Apparatus

    Loading frame

    Cylindrical mould, Collar, Base Plate and

    spacer Disc

    Compaction hammer

    Expansion Measuring Apparatus - Perforated

    plate with adjustable stem, tripod and dial

    gauge reading to 0.01 mm

    Annular Surcharge Weights

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    Loading Machine

    With a capacity of at least5000 kg and equipped

    with a movable head or

    base that travels at an

    uniform rate of 1.25

    mm/min.

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    Cylindrical Mould

    Cylindrical mould withinside diameter 150 mm

    and height 175 mm,

    provided with a

    detachable extension

    collar 50 mm height and

    a detachable perforated

    base plate 10 mm thick.

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    Compaction Rammer

    Weight 2.6 kg with adrop of 310 mm

    (or) Weight 4.89 kg a

    drop 450 mm.

    Adj t bl t f t d l t t i d

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    Adjustable stem, perforated plate, tripod

    and dial gauge

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    Annular Weights

    One annular metal weightand several slotted

    weights weighing 2.5 kg

    each, 147 mm in

    diameter, with a central

    hole 53 mm in diameter.

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    P ti f T t S i

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    Preparation of Test Specimen

    Prepare the remoulded specimen at Proctorsmaximum dry density or any other density at

    which C.B.R is required. Maintain the

    specimen at optimum moisture content or thefield moisture as required. The material used

    should pass 20 mm I.S. sieve. Prepare the

    specimen either by dynamic compaction or bystatic compaction.

    D i C ti

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    Dynamic Compaction

    Take about 4.5 to 5.5 kg ofsoil and mix thoroughly with

    the required water.

    Just before making the

    compacted mould of soil, takerepresentative sample for

    determining water content.

    Fix the extension collar and

    the base plate to the mould.Insert the spacer disc over

    the base. Place the filter

    paper on the top of the

    spacer disc.

    Dynamic Compaction

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    Dynamic Compaction

    Compact the soil in themould using either lightcompaction or heavycompaction. For light

    compaction, compact thesoil in 3 equal layers,each layer being given 55blows by the 2.6 kg

    rammer. For heavycompaction compact thesoil in 5 layers, by giving56 blows to each layer by

    the 4.89 kg rammer.

    Dynamic Compaction

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    Dynamic Compaction

    Remove the collar and trim the specimensmooth and flush with the mould.

    Remove the base plate and the displacer disc,

    weigh the mould with compacted soil, anddetermine the wet unit weight.

    Place a filter paper on the base plate, invert

    the specimen (5 cm gap is on the top) andattach the base plate so that the soil is in

    contact with the filter paper on the base.

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    Static Compaction

    Calculate the weight of the wet soil at the required watercontent to give the desired density when occupying the

    standard specimen volume in the mould from the

    expression.

    W= (1+w)*V*d

    Where,

    W= Weight of the wet soil, gm

    w= desired water content

    V= volume of the specimen in the mould, cc

    = 2209 cc

    d= required dry density in gm/cc

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    Static Compaction

    Place correct weight (W) of the soil in the mould.Place a filter paper and the spacer disc on the top of

    soil.

    Keep the mould assembly in static loading frame andcompact by pressing the spacer disc till the level of disc

    reaches the top of the mould.

    Keep the load for some time and then release the load.

    Remove the spacer disc.

    The test may be conducted for both soaked as well as

    unsoaked conditions.

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    Penetration Test

    Place the mould assembly with the surcharge weights on thepenetration test machine.

    Seat the penetration piston at the center of the specimen withthe smallest possible load, but in no case in excess of 4 kg sothat full contact of the piston on the sample is established.

    Set the stress and strain dial gauge to read zero. Apply the loadon the piston so that the penetration rate is about 1.25 mm/min.

    Record the load readings at penetrations of 0.5, 1.0, 1.5, 2.0,2.5, 3.0, 4.0, 5.0, 7.5, 10 and 12.5 mm. Note the maximum load

    and corresponding penetration if it occurs for a penetration lessthan 12.5 mm.

    Detach the mould from the loading equipment. Take about 20 to50 g of soil from the top 3 cm layer and determine the moisturecontent.

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    Data from a Typical CBR Test for

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    75

    72

    69

    58

    50

    38

    Proving

    Ring

    Readin

    g

    (div)

    49.95

    33.30

    18.50

    11.10

    3.70

    0

    Load

    on

    Plunger

    12.5

    10

    7.5

    5

    4

    3

    Penetratio

    n

    (mm)

    138.75

    133.20

    127.65

    107.30

    92.50

    70.30

    Load

    on

    Plunger

    272.5

    182

    101.5

    61

    20.5

    00

    Proving

    Ring

    Reading

    (div)

    Penetratio

    n

    (mm)

    Data from a Typical CBR Test for

    Sample No.1

    Load Vs Penetration Curve for

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    0

    20

    40

    60

    80

    100

    120

    140

    160

    0 2.5 5 7.5 10 12.5

    Penetration

    Load

    Load Vs Penetration Curve for

    Sample No.1

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    Initial Concavity

    The load penetration curve may show

    initial concavity due to the following

    reasons:The top layer of the sample might have become

    too soft due to soaking in water

    The surface of the plunger or the surface of thesample might not be horizontal

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    Correction

    Draw a tangent to the load-penetration curve

    where it changes concavity to convexity

    The point of intersection of this tangent line

    with the x-axis is taken as the new origin

    Shift the origin to this point (new origin) and

    correct all the penetration values

    Corrected Penetration Values for

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    Corrected Penetration Values for

    Sample No.1

    0

    20

    40

    60

    80

    100

    120

    140

    160

    0 2.5 5 7.5 10 12.5

    Penetration, mm

    Load,

    kg

    2.5 5

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    Computation of CBR for Sample No.1

    Compute CBR at 2.5 mm penetrationCBR of Specimen at 2.5 mm penetration =

    (80/1370)*100 = 5.84 %

    Compute CBR at 5 mm penetration

    CBR of Specimen at 5 mm penetration =

    (117/2055)*100 = 5.69 %

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    Variation in CBR Values

    At least three samples should be tested oneach type of soil at the same density and

    moisture content to take care of the variation in

    the valuesThis will enable a reliable average value to be

    obtained in most cases

    Where variation with in CBR values is morethan the permissible maximum variation the

    design CBR value should be the average of six

    samples and not three

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    Permissible Variation in CBR Value

    531 and above

    311-30

    25-10

    15

    Maximum variation

    in CBR value

    CBR (per cent)

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    Design CBR

    The average CBR values corresponding to 2.5 mm and5 mm penetration values should be worked out

    If the average CBR at 2.5 mm penetration is more than

    that at 5 mm penetration, then the design CBR is theaverage CBR at 2.5 mm penetration

    If the CBR at 5mm penetration is more than that at 2.5

    mm penetration, then the test should be repeated. Even

    after the repetition, if CBR at 5mm is more than CBR at2.5 mm, CBR at 5 mm could be adopted as the design

    CBR.

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    5.56

    5.71

    Mean

    5.71 %Design CBR

    5.565.445.695.0 mm

    5.765.545.842.5 mm

    321

    CBR (%)

    Penetration

    Computation of Design CBR

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    1. Sieve Analysis

    Significance of Test

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    Significance of Test

    Each type of aggregate test

    requires a specifiedaggregate size

    (E.g. 10-12.5 mm for crushingtest)

    Each bituminous mix typehas a recommendedaggregate gradation

    (% passing 26.5 mm in 55-90

    for GSB1) So aggregate is passed

    through a set of sieves to getmaterial of various sizes

    Sieves and Sieve shaker

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    Sieves and Sieve-shaker

    Procedure

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    Procedure

    Bring the sample to an air dry condition either by drying at

    room temperature or in oven at a temperature of 100oC to110oC.Take the weight of the sample.

    Clean all the sieves and sieve the sample successively onthe appropriate sieves starting with the largest.

    Shake each sieve separately over a clean tray.

    On completion of sieving note down the weight ofmaterial retained on each sieve.

    Report the results as cumulative percentage by weight ofsample passing each of the sieves.

    Observation Sheet

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    Observation Sheet

    IS:2386 Part I; IS: 383

    I.S. Sieve

    designation

    Weight of

    sample

    retained (gm)

    weight retained

    Percent of

    (%)

    Cumulativepercent of weight

    retained (%)

    Percentage

    passing

    (%)

    63 mm

    40 mm20 mm

    12.5 mm

    10 mm

    4.75 mm

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    2. Aggregate Crushing Test

    Significance

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    Significance

    Aggregate crushing value provides a relative

    measure of resistance to crushing under a graduallyapplied compressive load

    Aggregates subjected to high stresses during rolling

    and severe abrasion under traffic

    Also in India very severe stresses come on

    pavements due to rigid tyre rims of heavily loaded

    animal drawn vehicles

    Test Set-up

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    Test Set-up

    Procedure

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    Procedure

    Surface dry aggregates passing 12.5 mm and

    retained on 10 mm selected

    3.25 kg aggregate required for one test sample

    Cylindrical measure filled with aggregates in 3 layers,tamping each layer 25 times

    After leveling the aggregates at the top surface thetest sample is weighed

    The cylinder is now placed on the base plate

    Contd.

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    The cylinder with the test sample and plunger inposition is placed on compression machine

    Load is applied at a rate of 4 tonnes per minute upto40 tonnes

    The crushed aggregate is taken out, sieved through2.36 mm IS sieve and weighed to get materialpassing

    Aggregate crushing value = W2*100/W1

    W2= Weight of crushed material

    W1=Total weight of sample

    Load Application

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    Load Application

    Sample being loaded

    in the compression

    machine at 4 T per

    minute for 10 minutes

    (upto 40 T)

    Observation Sheet

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    Observation Sheet

    Note: Value recorded up to first decimal place

    Aggregate Crushing

    Value= W1/W2*100

    Wt. of AggregateSamplePassing 2.36 mmSieveAfter the Test= W2(gms)

    Wt. of Aggregate SampleFilling in The Cylinder=W1(gms)

    321AverageTest No.Observations

    Specifications

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    Specifications

    45% Max for

    Other Surfaces

    30% Max for

    Surface Course

    As per IRC:15

    1970

    And

    IS: 2386:Part IV

    Aggregate Crushing Value for

    Cement Concrete PavementsSpecified By

    Discussion

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    Discussion

    Indirect measure of crushing strength

    Low value indicate strong aggregates

    Surface course need more strength than base course

    Should not exceed 30% for cement concrete surface ,

    and 45% for others

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    3. Aggregate Impact Test

    Significance

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    Significance

    This test assesses the suitability of aggregate as

    regards the toughness for use in pavementconstruction

    Road aggregates subjected to pounding action due

    to traffic loads- so possibility of breaking

    Should be tough enough- so proper aggregates to

    be used

    Suitability to be checked by laboratory tests

    Test Set-up

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    Test Set up

    Procedure

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    1. Aggregate passing through 12.5 mm IS sieve and retained on

    10 mm sieve is filled in the cylindrical measure in 3 layers bytamping each layer by 25 blows. Determine the net weight of

    aggregate in the measure(W1)

    2. Sample is transferred from the measure to the cup of

    aggregate impact testing machine and compacted by tamping

    25 times

    3. The hammer is raised to height of 38 cm above the upper

    surface of the aggregates in the cup and is allowed to fall

    freely on the specimen

    Test In progress

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    Test In progress

    Contd.

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    After subjecting the test specimen to 15blows, the crushed aggregate is sievedthrough IS 2.36 mm sieve

    Weigh the fraction passing through IS 2.36mm sieve(w2)

    Aggregate impact value = w2/w1*100

    w2 = Weight of fines passing 2.36 mm

    w1 = Weight of sample

    Mean of the two values reported

    Observation Sheet

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    Observation Sheet

    Note: Value Recorded to the Nearest Whole Number

    Aggregate Impact Value=

    W2/W1*100

    Wt. of Aggregate

    Sample

    Passing 2.36 mm Sieve

    After the Test= W2

    (gms)

    Wt. of Aggregate Sample

    Filling in The Cylinder=

    W1(gms)

    321 Avg

    Test No.

    Observations

    Specifications

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    Specifications

    30Bituminous Wearing Surfaces

    IS: 2386: Part IV and IRC:15 1970; MORTH: 2001

    30WBM Surface course

    35

    Bituminous Macadam, Base

    course

    45Cement Concrete Base course

    50WBM Sub-base course

    Aggregate Impact

    Value, Max, %

    Type of Pavement

    Material/Layer

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    4. Los Angeles Abrasion Test

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    Test Set-up

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    p

    Procedure

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    1. Aggregates dried in oven at 105 -110 C. to constantweight conforming to any one of the gradings

    E.g. 1250 gm of 40-25 mm, 1250 gm of 25-20 mm,

    1250 gm of 20-12.5 mm, 1250 gm of 12.5-10 mm,

    with 12 steel balls

    2. Aggregate weighing 5 kg or 10 kg is placed in cylinder

    of the machine(W1gms)

    3. Machine is rotated at 30-33 rpm for 500 revolutions

    12. Machine is stopped and complete material is taken

    out including dust

    Grading Requirement

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    5000

    2512-----500

    05000---G

    50002512-----NA5000500

    0--F

    50002512-------500

    0250

    02500E

    5000256500

    0---------D

    5000258-250

    02500-------C

    50002511---250

    0

    250

    0-----B

    50002512---

    125

    0

    125

    0

    125

    01250---A

    Wt.of

    Charge,g

    No.of

    S

    heres

    4.7

    5-

    6.3-4.7

    5

    10-6.3

    12.5-1

    0

    20-12.5

    25-2

    0

    40-2

    5

    50-4

    0

    63-5

    0

    80-6

    3

    Abrasive

    ChargeWt. in gms of each Sample in the Size Range, mm

    Gradin

    g

    After 500 1000 revolutions

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    6.Sieved through 1.7 mm sieve

    7. Weight passing is determined by washing the

    portion retained, oven drying and weighing (W2

    gms)

    8. Aggregate abrasion value is determined

    A.A.V. = W2/W1*100

    W2 = Weight of fines passing 1.7 mm

    W1 = Weight of the sample

    Specifications

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    p

    60WBM Sub-base course

    IS: 2386: Part IV; IRC:15 1970; IS: 383

    30

    Bituminous/Cement concrete

    Wearing course

    35

    Bituminous Carpet, SD, Cement

    Concrete surface course

    40

    WBM Surface course, BM binder

    course

    50WBM Base course with bit.

    Surfacing, BM Base course

    L. A. Abrasion

    Value, Max, %Type of Pavement Layer

    Discussion

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    Select a grading close to the project for testing

    Simulate both abrasion and impact due to wheel loads

    It determines the hardness of the stone

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    7. Shape Tests

    Determination of:

    a.Flakiness Index

    b.Elongation Index

    c.Angularity Number

    Significance

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    g

    Shape of crushed aggregates determined by the percentage of

    flaky and elongated particles

    Shape of gravel determined by its angularity number

    Flaky and elongated aggregate particles tend to break under

    heavy traffic loads

    Rounded aggregates preferred in cement concrete pavements

    as more workability at less water cement ratio

    Angular shape preferred for granular courses/flexible pavement

    layers due to better interlocking and hence more stability

    Test Set-up

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    Length Gauge for Elongation Inde

    Thickness Gauge for Flakiness Index

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    Flakiness Index Test in Progress

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    Flakiness Index Test in Progress

    Flakiness

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    4.The amount of flaky material is weighed to an accuracy of

    0.1 percent of the test sample

    5. If W1,W2,W3,. are the total weights of each size ofaggregates taken and w1,w2,w3,.. are the weights ofmaterial passing the different thickness gauges then:

    Flakiness Index

    = (w1+w2+w3+.)*100

    (W1+W2+W3+.)

    = 100*w percent

    W

    Where,

    W = Total wt of material taken in gms

    w = Total wt of material passing in gms

    Observation sheet (Flakiness Index)

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    Passing

    through

    I.S. Seive,

    (mm)

    Retained

    on I.S.

    Seive,

    (mm)

    63 50 W1= 23.9 w1=50 40 W2= 27 w2=

    40 31.5 W3= 19.5 w3=

    31.5 25 W4= 16.95 w4=

    25 20 W5= 13.5 w5=

    20 16 W6= 10.8 w6=

    16 12.5 W7= 8.55 w7=

    12.5 10 W8= 6.75 w8=

    10 6.3 W9= 4.89 w9=

    Total W= w=

    Size of aggregateWt. Of the

    fraction

    consisting of at

    least 200

    pieces (gm)

    Thickness

    gauge size,

    (0.6 times the

    mean sieve)

    (mm)

    Weight of

    aggregate in each

    fraction passing

    thickness gauge

    (gms)

    Elongation Index

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    Elongation Index

    Elongation Index: The percentage by weight ofparticles whose greatest dimension is greater than one andfour fifth times (1.8 times) their mean dimension. Applicable

    to sizes >=6.3 mm

    1. The sample is sieved through sieve sizes, 50, 40, 25,

    20, 16, 12.5, 10 and 6.3

    2. Minimum 200 pieces of each fraction to be tested are

    taken and weighed (W1 gm)

    3. Separate the elongated

    material by using the standard length gauge

    Elongation Index Test in Progress

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    Elongation Index

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    4. The amount of elongated material is weighed to an accuracy of

    0.1 percent of the test sample

    5. If W1,W2,W3,. are the total weights of each size of

    aggregates taken and w1,w2,w3,.. are the weights of material

    retained on the different length gauge slots then:

    Elongation Index

    = (w1+w2+w3+.)*100

    (W1+W2+W3+.)

    = 100*w percent

    W

    Where,

    W = Total wt of material taken in gms

    w = Total wt of material retained in gms

    Observation sheet (Elongation Index)

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    Passing

    through

    I.S.

    Seive,

    (mm)

    Retainedon I.S.

    Seive,

    (mm)

    50 40 W1= 81 w1=40 25 W2= 58 w2=

    25 20 W3= 40.5 w3=

    20 16 W4= 32.4 w4=

    16 12.5 W5= 25.5 w5=

    12.5 10 W6= 20.2 w6=10 6.3 W7= 14.7 w7=

    Total W= w=

    Size of aggregate

    Wt. Of the

    fractionconsisting of

    at least 200

    pieces (gm)

    Length

    gauge size,(1.8 times

    the mean

    sieve) (mm)

    Weight of

    aggregate in

    each fraction

    retained on

    length gauge

    (gms)

    Specifications

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    15(do)Bit. Macadam, WBM base

    & surfacing

    course

    IS: 2386, Part I; IRC: 14-48 ; MORTH: 2001

    35Cement Concrete

    25(do)Asphaltic concrete

    Penetration macadam

    Bit. Surface dressing

    30(Combined FI and EI)Bituminous carpet

    Limit of Flakiness Index

    (%)

    Type of pavement

    construction

    Angularity number

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    The angularity number measures the percent

    voids in excess of 33 percent which is obtained inthe case of the most rounded gravel particles.Ranges from 0-11 (rounded gravel-crushedangular)

    1. The cylinder is calibrated by determining theweight of water at 27oC required to fill it

    2. Aggregate is sieved through 20, 16, 12.5, 10,

    6.3 and 4.75 mm IS sieves3. About 10 kg of the predominant size should

    be available

    Test in Progress

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    Contd.

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    4. The sample of single-size aggregate is dried in an oven at

    100o

    to 110o

    C for 24 hours and then cooled

    5. The scoop is filled with aggregate which is allowed to slide

    gently into the cylinder from the lowest possible height

    6. The aggregate is filled in three layers, tamping each layer

    evenly 100 times with a tamping rod

    7. After the third layer is tamped, the aggregates are struck off

    level with the help of tamping rod and surface finished

    8. The aggregate with cylinder is now weighed to the nearest 5 g.

    The mean weight of aggregate is found

    Calculations and Observation Sheet

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    Angularity number = 67-100*WC*G

    where, W = mean weight of aggregates in the cylinder,g

    C = Weight of water required to fill the cylinder,g

    G = Specific gravity of aggregate

    Angularity Number = 67 - 100*W/C*G =

    Mean weight of aggregate filling the cylinder, Wt =

    Weight of aggregate filling the

    cylinder to the nearest fivegrams, g

    321Mean

    Trial numberParticulars

    Specific gravity of the aggregate = G =Weight of water filling the cylinder = C g =

    Discussion

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    Elongated, flaky and angular materials decreases the workabilityof the mix, and not preferred in cement concrete

    Angular aggregates are preferred in flexible pavement at WBM /WMM

    Angularity number ranges from zero for perfectly roundedaggregate (rounded pebbles) to about 11 percent for freshlycrushed aggregates

    But for DBM & BC mix design may be modified to incorporatehigh angularity number

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    Penetration test for Bitumen

    Significance

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    The penetration test determine thehardness or softness of bitumen

    The bitumen grade is specified in terms of

    the penetration value

    30/40 and 80/100 grade bitumen arecommonly used

    In hot climates a lower penetration gradebitumen is preferred and vise versa

    Significance

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    Consistency of bitumen varies with temperature, constituents,

    refining process, etc.

    Viscosity is an absolute property, but could not be determined

    easily

    Viscosity of cutback bitumen by indirect method (orifice

    viscometer)

    Too soft for penetration, too hard for orifice then perform floattest

    Significance

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    Basic principle of penetration test:

    measurement of penetration in units of 1/10th of a mmof a standard needle of 100 gm in a bitumen sample

    kept at 25C for 5 seconds

    Higher penetration implies softer grade

    Purpose is classification

    Figure

    Penetrometere Water Bath

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    Penetrometere Water Bath

    Weight

    Dial

    Needle

    Mould

    Temperature Controller

    Procedure

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    Heat the bitumen to softening point +900 C

    Pour the bitumen into the container at least 10 mm above the

    expected penetration

    Place all the sample containers to cool in atmospheric temperature

    for 1 hour

    Place the sample containers in temperature controlled water bath at

    a temperature of 250 C 1o C for a period of 1 hour

    Fill the transfer dish with water from the water bath to cover the

    container completely

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    Continue. . . .

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    Take off the sample container from the water bath,

    place in transfer dish and place under the middle ofpenetrometer

    Adjust the needle to make a contact with surface of

    the sample See the dial reading and release the needle exactly

    for 5 seconds

    Note the final reading

    Difference between the initial and final readings is

    taken as the penetration value in 1/10th of mm

    (i) P i t t

    Observation Sheet

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    Average Value =

    Final

    Initial

    Mean

    value

    Test

    3

    Test

    2

    Test

    1

    Mean

    value

    Test

    3

    Test

    2

    Test

    1

    Sample No 2Sample No 1Penetro-

    meter dial

    readings

    (v) Actual test temperature =

    (iv) Period of cooling in water bath, minutes =

    (iii) Room temperature =

    (ii) Period of cooling in atmosphere, minutes =

    (i) Pouring temperature =

    IS Specifications

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    7%Above 225

    5%80-225

    4%0-80

    RepeatabilityPenetration

    Grade

    175-22580-10060-7040-5030-4020-30PenetrationValue

    A200 &

    S200

    A90 &

    S90

    A65 &

    S65

    A45 &

    S45

    A35 &

    S35A25

    Bitumen

    Grade

    Discussion

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    Test is highly influenced by the pouring temperature, size of

    needle, weight of needle, test temperature, duration of release of

    needle

    IRC suggests 30/40, 60/70, 80/100 for BM

    High penetration grade is desirable in colder regions

    Penetration below 20 will result in cracking

    For lower penetration, bonding is difficult, but once achieved will

    remain for a long time

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    Ductility Test

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    Ductility Machine

    Significance

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    The ductility of bitumen improves the physical

    interlocking of the aggregate bitumen mixes

    Under traffic loads the pavement layer is subjected to

    repeated deformation. The binder material of loductility would crack and thus provide pervious

    pavement surface

    The test is believed to measure the adhesive property ofbitumen and its ability to stretch

    Significance

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    Ductility and penetration go together, in general, but exception

    can happen

    Ductility is the distance in cm to which a standard briquette of

    bitumen can be stretched before the thread breaks

    Ductile materials is one which elongates when held in tension

    Procedure

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    The bitumen sample is melted to temperature of 75oC to

    100oC above the approx. softening point until it is fluid

    It is strained through IS sieve 30, poured in mould

    assembly and placed on a brass plate, after a solution of

    glycerine or dextrine is applied over all surfaces of the

    mould exposed to bitumen

    Thirty to forty minutes after the sample is poured into

    the moulds, the plate assembly along with the sample is

    placed in water bath maintained at 27oC for 30 minutes

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    Briquette Moulds

    Continue. . . .

    The sample and mould assembly are removed

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    The sample and mould assembly are removed

    from water bath and excess bitumen material is

    cut off by leveling the surface using hot knife

    After trimming the specimen, the mould assembly

    containing sample is replaced in water bath

    maintained at 27oC for 85 to 95 minutes

    The slides of the mould are then removed and the

    clips are carefully hooked on the machine withoutcausing any initial strain

    The pointer is set to read zero

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    Ductilometer In Operation

    Continue. . . .

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    The machine is started and the two clips are thus

    pulled apart horizontally

    While the test is in operation, it is checked whether

    the sample is immersed in water up to a depth of at

    least 10mm

    The distance at which the bitumen thread breaks is

    recorded (in cm) and reported as ductility value

    Breaking of Thread

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    Observation sheet(i) Grade of bitumen =

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    (i) Grade of bitumen

    (ii) Pouring temperature C =

    (iii) Test temperature =(iv) Period of cooling (minutes) in Air =

    In water bath before trimming =

    In water bath after trimming =

    Reproducibility

    %

    Repeatability %

    Ductility (cm)

    cbaMean Value

    Briquette NumberTest Property

    IS Specification

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    Note: S denotes sources other than Assam

    petroleum

    75S 45,S 65 & S 90

    50S 35

    Minimum

    Ductility (cm)

    Source of Paving Bitumen

    & Penetration Grade

    10%Reproducibility

    5%

    Repeatability

    Discussion

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    Ductility of bitumen is affected by the pouring temperature,

    briquette size, placement of briquette, test temperature, rate of

    pulling

    Ductility value ranges from 5-100. Low value implies cracking.

    Some minimum ductility is needed for flexural strength

    The lack of ductility does not necessarily indicate poor quality.

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    Softening Point

    Significance

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    Bitumen does not melt, but change gradually from solid

    to liquid

    Softening point is the temperature at which the bitumen

    attains particular degree of softening under specified

    test conditions

    Ring and ball apparatus is used for the test

    Ring & Ball Test Set-up

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    Glass Beaker

    Brass Rings

    (In =15.9 Mm & Out =17.5mmSteel Balls = 9.5 mm (2.5g)

    Metallic Support

    Thermometer

    Mechanical Stirrer

    Temp Controlled

    Heating Plate

    Procedure Heat the bitumen to a temperature between 125oC to

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    150oC

    Heat the rings at the same temperature on a hot plate

    & place on glass plate coated with glycerin

    Fill up the rings with bitumen

    Cool for 30 minutes in air and level the surface with

    a hot knife

    Set the rings in the assembly and place in the bath

    containing distilled water at 5oC and maintain that

    temperature for 15 minutes

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    Observation table

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    (i) Grade of bitumen =

    (ii) Approximate softening point =(iii) Liquid used in water bath(water/Glycerin) =

    (iv) Period of air cooling (minutes) =

    (v) Period of cooling in water bath(minutes) =

    IS Specifications

    ReproducibilityR t bilit ( C)S ft i P i t

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    42>80oC

    2130oC- 80oC42

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    Test is affected by quality of liquid, weight of ball, rate of heating

    etc

    It gives an idea of the temperature at which the bituminous

    material attains a certain viscosity

    Bitumen with higher softening point is used in warmer places

    Softening point is very critical for thick films like joint and crack

    fillers, to ensure they will not flow

    Other tests

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    Viscosity of bitumenCommon demo

    Brook field viscometer

    Marshall mix design

    Theory + lab

    Traffic studies: