Highway Engineering Design_Material Testing

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    Dr. Wasala Bandara

    1

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    Road Making Materials

     Aggregate

    Fine Course

    Bitumen

    2

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    In road construction are

    Crushed rock (from quarry)

    Stream gravel

    Concrete construction debris

    Hard materials like broken pieces of tiles from tile industry

    Slag (Slag is a waste product in metal extraction)

    3

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    Rock drill machines can be either hand held jack hammers or rig mounted

    Jack hammers are light weight. They are

    generally employed in drilling holes up to 38 mm

    diameter and are powered by compressed air 

    Jack hammers

    Handles

    Hammer Head

    Chuck

    Drill Rod

    Drill Bit

    The main action of rock drills is to provide impact, thrust and rotation to a

    drill rod attached to the drill

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    Drilling rig

    Can drill longer holes (100 m) with bigger diameter

    (50mm, above 100 mm)

    Rig mounted rock drills

    The rig mounted rock

    drills can be driven by

    compressed air or by

    hydraulic power.

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    The rock cuttings are removed by flushing

    Flushing is done by forcing water and/or

    compressed air down the whole through

    the drill rods and the drill bit

    The cuttings are brought out of the hole

    along the annular space between the drill

    rod and the wall

    Flushing medium also cools the bit during

    drilling

    Use of water in the flushing suppresses

    the rock dust created in the process of

    drilling

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    The drilling machines can also be classified by theirdrilling actions into two main groups.

    Drilling Machines

    Percussiondrilling

    machines

    Rotary drillingmachines

    Thrust, Impact

    and Rotation

    Only thrust and

    rotation

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    There are many types of drill bit used in rock drillingThe selection mainly depends on the drilling machine used, thediameter of the drilled holes and the required production rates

    Chisel bit

    Position of chisel bit

    and the zone of rock

    crushed at the first

    impact

    1st Zone of

    crushed rock

    Position of chisel bit

    and the zone of

    broken rock at the

    second impact

    2nd

     Zone of

    crushed rock

    Position of chisel bit

    and the zone of

    broken rock at the

    third impact

    3

    rd

     Zone ofcrushed rock

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    4-point cross-type bit Diamond bit

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    Button bit

    • Button bit diameters range from 100 mm to 225 mm

    • Drill heads with many roller cutters are used for very large diameter drilling above

    225 mm up to about 1500 mm

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    Drilling Rates

    • Dependent on:

    •Rock Hardness

    •Drill Type and Energy

    •Type of Drill Bit

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    Mixture of chemical compounds which rapidly decompose,instantly releasing large quantity of energy in form of  

    heated gas at a high pressure

     An explosive should essentially contain a combustible

    substance and an oxygen supplier 

     A good example is a mixture of carbon, sulphur and

    sodium nitrate in black powder • Sodium nitrate provides oxygen

    • Carbon and sulphur burn in oxygen and produce large

    quantities of gases at high temperature and pressure

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    List of ingredients in commercially available explosivesIngredients Chemical formula Function

    Ethylene glycol dinitrate C2H4(NO3)2 Explosive base: lowers freezing point

    Nitrocellulose (guncotton) C6H7(NO3)3O2 Explosive base; gelatinizing agent

    Nitro-glycerine Nitrostarch C3H5(NO3)3

    Explosive base

    Explosive base;   “non headache”

    explosives

    Trrinitroluene(TNT) C7H5N3O6 Explosive base

    Metallic Powder   Al

    Fuel-sensitizer; used in high density

    slurriesBlack Powder  NaNO3+C+S Explosive base; deflagratesPentaerythritoltetranitrate

    (PETN)C5H8N4O12

    Explosive base; caps, detonating

    cord

    Ammonium nitrate NH4NO3 Explosive base; oxygen carrier 

    Liquid oxygen O2 Oxygen carrier 

    Sodium nitrate NaNO3Oxygen carrier; reduces freezing

    point

    Potassium nitrate KNO3 Oxygen carrier 

    Ground coal C Combustible, or fuelCharcoal C Combustible, or fuel

    Paraffin CnH2n+ 2 Combustible, or fuel

    Sulphur  S Combustible, or fuel

    Fuel oil (CH3)2(CH2)n Combustible, or fuel

    Wood pulp (C6H10O5)n Combustible; absorbent

    Lampblack C Combustible

    Kieselguhr  SIO2 Absorbent; prevents caking

    Chalk CaCO3 Antacid

    Calcium carbonate CaCO3 Antacid

    Sodium chloride NaCl Flame depressant (permissibleexplosive)

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    Rock blasting is carried out using explosives from two or more of the types

    a) High power explosives

    b) Detonators  – plain or electrical

    c) Blasting agents

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    Velocity of Detonation (VOD)- How long it takes to get the chemical reaction

    completed and energy released

    Type of explosivesHigh explosivesHigh VOD, detonated with shock wave propagation associated with gas

    expansion

    For example: dynamite, water gels, emulsion

    Low explosivesLow VOD, deflagrated with gas expansion onlyFor example: such as black powder 

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    • Detonators are used for the initiation of an explosivecharge

    • They are made of high heat sensitive explosives and

    can be set off by fire (flame)

    •The explosion caused by them is capable of initiatingthe explosion of High explosives

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    The blasting agents are cheap and safe to handle

    FUSE WIRE

    SHOT

    EXPTODER

    STEMMING

    BLASTING

    AGENT

    (ANFO)

    PRIMER

    (Gelignite or

    Dynamite)

     DETONATOR

    The safest blasting agent ANFO is a mixture of 

    ammonium nitrate and

    fuel oil

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     ANFO blasting agents

    3NH4NO3 + CH2 →CO2 + 7H2O + 3N2+ heat

    m.w. 3 (80.1gm) +(14gm) = 254.3gm

    NH4NO3 = 94.5%

    CH2 = 5.5%

    ammonium fuel oil

    nitrate

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    hb = length of bottom charge

    (qbk kg/m)

    hp = length of

    column charge

    (qpk kg/m)

    ho = length ofstemming

    u = under drilling

    1

    3

    VV V V V

    K = Bench

    Height

    Free Face

    V

      E

      E

      E  E

      B  =   B e

     n c  h   W  i d  t  h

    K Vertical height of bench in (m) ho Length of stemming (m)

    B Bench width (m) hb Length of bottom charge (m)

    V Practical burden (m) hp Length of column charge (m)

    E Practical hole spacing (m) qbk Charge concentration of bottom charge (m)

    u Depth of under drilling (m) qpk Charge concentration of column charge (m)H Length of entire hole (m)

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    C - ground factor 

    d - blast hole diameter   = × (m)

    = 0.3 × (m)

    1) Maximum burden ()

    2) Under-drilling ()

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    3) Length of entire hole (H)

    = + (m)   = ( + ) × 1.05 (m)

    For vertical hole For inclined hole

    K

       H   =

       (   K   +

      u   )

    u

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    4) Faulty drilling factor (F)

    = 0.05 + 0.03 × (m)

    5 cm setting error 

    Hole with 5 cm setting error 

    Hole with 5 cm setting error

    + 3% deviation (worst

    possible)

    F = FAULTY DRILLING FACTOR

    F=.05+.03H

    Vmax

    Vmax

    Intended hole

    V

    Hole should

    start here

    V = Vmax - F

    H

    F

    5) Practical burden (V)

    =   (m)

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    6) Practical hole spacing (E)

    = 1.25 × (m)

    7) Length of stemming (ℎ)

    ℎ  = (m)

    8) Length of bottom charge (ℎ)

    ℎ  = 1.3 × (m)

    9) Length of column charge (ℎ)

    ℎ  = (ℎ + ℎ) (m)

    Inert material

    (rock dust, sand,

    clay, saw dust)

    Explosive

    Explosive

    Stemmingh0

    hp

    hb

    H

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    10) Density of bottom charge (): is in meters

     =  .4

    4  × × (kg/m) P- Density of explosive (kg/m3)

    11) Density of column charge ()

     = 0.5 × (kg/m)

    12) Total bottom charge per hole ()

     =   × ℎ (kg)

    13) Total column charge per hole ()

     =   × ℎ (kg)

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    14) Total charge per hole ()

     =  + (kg)

    15) Specific charge q

    Specific charge = 

    × × (kg/m3)

    16) Specific charge 

    Specific charge  = 

    × × ×(−)(kg/m3)

    Where KxVxE is the volume of rock broken per hole

    Generally for bench blasting q is around 400 g/m 3 

    Where KxVxEx(nbh-1) is the total volume of rock broken per blast. Also note that B=E X (nbh-1)

    hb = length of bottom charge

    (qbk kg/m)

    hp = length of

    column charge

    (qpk kg/m)

    ho = length of

    stemming

    u = under drilling

    1

    3

    V V V V V

    K = Bench

    Height

    Free Face

    V

      E

      E

      E  E

      B  =   B e

     n c  h   W  i d  t  h

    The specific charge for the whole blast with nbh holes per row given by:

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    Crushing is necessary to reduce further the size of particles

    created by blasting

    The blasting products vary in size from large boulders to fine

    fragments

    Large boulders are subject to secondary blasting and therock less than 1200mm can be reduced in size by crushing

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    Crushers

    Hammer

    mills

    Jaw

    crushers

    Gyratory

    crushers

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     A Hammer mill consists of heavy steel hammers hung bysteel chains or steel plate

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    The crushing action takes place

    between two jaws with manganesesteel liners

    One jaw is fixed while the other is

    movable.

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    Jaw crushers are used, where crusher gape is

    more important than the capacity

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    Gyratory crushers on the other hand have low tendency toproduce flaky and elongated products. The crushing

    surfaces are curved.

    It consists of a conical, suspended crushing head

    Gyratory crushers are used, where high capacity

    is required

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    Jaw crusher Gyratory crushers

    Crushes on half cycle Crushes on full cycle

    Installation cost is high Installation cost is low

    Capital & Maintenance cost isless

    Capital & Maintenance cost ismore

    Perform better on clayey,

    plastic material

    Particularly suitable for hard,

    abrasive material

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    40Bins

    Feed

     R o t a t  i n g  D r u

     m

    Perforations

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    The quality of an aggregate is affected by the production

    process in that:

    (a)Decomposed or inferior rock can find its way into the crushers, which can

    be eliminated by screening. If a considerable amount of clay is present

    washing of the aggregates may be necessary. Contamination affects both

    strength and adhesive qualities of aggregates.

    (b)Higher reduction of the crushing plant can result in flaky or elongated

    particles. The reduction ratio is the ratio of the size of feed to the size of 

    product. Experience shows that reduction ratio should be less than 4%.

    (c) Excess of undersize materials can be caused by overloading the screens.

    Flaky and elongated aggregates can contain more fines (undersize) than

    the cubical aggregates.

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    Fine Aggregate

    aggregate particles mainly between the 4.75 mm size and the 75um sieveCoarse Aggregate

    aggregate particles mainly larger than 4.75 mm

    Pit Run

    aggregate from a sand or gravel pit with no processing

    Crushed Gravel

    pit gravel (or sand) that has been put through a crusher either to break therounded gravel particles into smaller sizes or to produce rougher surfaces

    Crushed Rock

    aggregate from the crushing of bedrock. All particles are angular and not

    rounded as in gravel

    Screenings

    chips, dust, powder that are produced from crushingConcrete Sand

    sand that has been washed to remove dust and fines

    Fines

    silt, clay, or dust particles smaller than 75um usually the undesirable

    impurities in aggregates

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    The aggregates used in pavement construction should have

    the following qualities:a) Hard (strength) enough to withstand the load of traffic and rolling equipment

    b) Resistant to abrasion and weathering

    c) Non slipping (skid resistance)

    d)  Angular (friction between particles)

    e) Well graded (packing)

     Aggregate Testing

    Descriptive test Non-destructive test Durability test

     A visual examination of an aggregate

    and then describing the shape of and

    the surface texture of the particles

    • Rounded

    • Irregular 

    •  Angular 

    • Elongated

    • Gradation testso sieve analysis

    • Shape testso Flakiness index

    o Elongation index

    •  Abrasion testso The aggregate abrasion test

    o The accelerated polishing test

    • Toughness testso  Aggregate crushing test

    o Ten percent fines test

    o  Aggregate impact testo Specific gravity test

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    FlatElongated Angular Round

     A visual examination of an aggregate and then describing the shape of and the surface texture of the particles

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     A process in which an aggregate is

    separated into its various sizes by

    passing it through screens of various size

    openings for the purpose of determining

    the distribution of the quantities

    separated

    BS 812-103.1:1985

    Sieve tests (BS 812-103.1:1985)

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    Importance of sieving Grain size distribution for highway bases and asphalt mixes that will

    provide a dense strong mixture

    Ensure that the voids between the larger particles are filled with

    medium particles. The remaining voids are filled with still smallerparticles until the smallest voids are filled with a small amount of fines.

    Ensure maximum density and strength using a maximum density curve

    The gradation controls the amount of binder used and

    tight compaction of the aggregate

    BS 812-103.1:1985

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    Apparatus

    sample divider-  Appropriate to the

    maximum particle size to be handled

    ventilated oven - Thermostatically

    controlled to maintain a temperature of105 ± 5 °C.

    A balance - Suitable capacity

    accurate to 0.1 % of the mass of

    the test portion

    A mechanical sieve shaker 

    Test sieves

    Trays & Containers

    BS 812-103.1:1985

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    Test sieves

    BS 812-103.1:1985

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    Procedure

    Part 1 - Washed sieve analysis Dry aggregate and determine mass

    Wash and decant water through 0.075 mm sieve until water is clear 

    Dry aggregate to a constant mass

    BS 812-103.1:1985

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    Procedure

    Part 2 - Mechanical sieve analysis Place dry aggregate in standard stack of sieves

    Place sieve stack in mechanical shaker 

    Determine mass of aggregate retained on each sieve

    BS 812-103.1:1985

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    Computation

    Sieve Mass Cumulative

    (mm) Retained Mass Retained % Retained % Passing

    (g)

    9.5

    4.75

    2.36

    1.18

    0.60

    0.30

    0.150.075

    Pan

    0.0

    6.5

    127.4

    103.4

    72.8

    64.2

    60.083.0

    22.4

    BS 812-103.1:1985

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    Computation

    % Passing = Cum. Wt Retained

    Original Dry Wt.* 100% Retained =

    Cum. Wt Retained

    Original Dry Wt.* 100 [ 1 - ]

    Sieve Mass Cumulative

    (mm) Retained Mass Retained % Retained % Passing

    9.5

    4.75

    2.36

    1.18

    0.60

    0.300.15

    0.075

    Pan

    0.0

    6.5

    127.4

    103.4

    72.8

    64.260.0

    83.0

    22.4

    0.0

    6.5

    133.9

    237.3

    310.1

    374.3

    434.3

    517.3

    539.7

    0.0

    1.2

    24.8

    44.0

    57.5

    69.480.5

    95.8

    100.0

    100.0

    98.9

    75.2

    56.0

    42.6

    30.619.5

    4.2

    0.0

    BS 812-103.1:1985

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    Computation

    Chart for recording sieve analysis results

    BS 812-103.1:1985

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    Computation

    BS 812-103.1:1985

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    Computation

    BS 812-103.1:1985

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    Computation

    The coefficient of uniformity ,Cu is a crude shape parameter 

    The coefficient of curvature, Cc is a shape parameter 

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    Flakiness Index (BS 812-105.1:1989)

    Flaky is the term applied to aggregate or chippings that are flat and thin

    with respect to their length or width

     Aggregate particles are classified as flaky when they have a thickness(smallest dimension) of less than 0.6 of their mean sieve size

    The test is n ot app l icable to mater ial passing a 6.30mm BS test sieve or 

    retained on a 63.0mm BS test s ieve 

    Thickness gauge =3

    5

    Average sieve size

    BS 812-105.1:1989

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    Apparatus

    A sample divider -Size appropriate to the

    maximum particle size

    to be handled

    ventilated oven - Thermostatically

    controlled to maintain a temperatureof 105 ± 5 °C.

    A balance -

    Suitable capacity

    accurate to 0.1 %

    of the mass of the

    test portionA mechanical sieve shaker 

    Test sieves

    Trays & Containers

    A metal thickness gauge - The gauge

    shall be made from1.5mm thickness

    sheet steel

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    BS 812-105.1:1989

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    Procedure Carry out a sieve analysisDiscard all aggregates retained on the 63.0mm test sieve and all aggregate passing the

    6.30mm test sieve

    Weigh each of the individual size-fractions retained on the sieves,

    other than the 63.0mm BS test sieve, and store them in separate

    trays

    From the sums of the masses of the fractions in the trays (M1),

    calculate the individual percentage retained on each of the various

    sieves. Discard any fraction whose mass is 5% or less of mass M1. Record the

    mass remaining (M2 )

    Gauge each fraction by Using the gauge, select the thickness gauge

    appropriate to the size-fraction under test and gauge each particle of 

    that size-fraction separately by hand

    Combine and weigh all the particles passing each of the gauges (M 3)

    BS 812-105.1:1989

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    Computation

    Flakiness index =M3M2

    M2- Total weight of the sample taken (greater than 5 % of the total mass)

    M3- Total weight of passing through various thickness gauge

    BS 812-105.1:1989

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    ComputationSize of aggregate Weight of material Flaking Index

    (%)

    (individual

    size)

    BS test sieve nominal aperture sizeTotal

    Retainedthickness

    gauge

    Passingthickness

    gauge100% passing 100% retained

    63.0 50.0

    50.0 37.5

    37.5 28.0

    28.0 20.0

    20.0 14.0 732.2 613.9 118.3

    14.0 10.0 1166.5 1095.2 71.3

    10.0 6.3 542.0 463.7 78.3

    Total 2440.7 2172.8 267.9

    Flakiness index =Total weight of material passing through various thickness gauge

    Total weight of the sample taken (greater than 5 % of the total mass)

    Flakiness index =267.9

    2440.7X 100%

    Flakiness index = 11%

    BS 812-105.1:1989

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    Elongation Index (BS 812-105.2:1990)

     Aggregate particles are classified as elongated when they have a length

    (greatest dimension) of more than 1.8 of their mean sieve size

    The test is not applicable to material passing a 6.30 mm test sieve or retained ona 50.0 mm test sieve

    Thickness gauge =9

    5Average sieve size

    BS 812-105.2:1990

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    Apparatus

    A sample divider -Size appropriate to the

    maximum particle size

    to be handled

    ventilated oven - Thermostatically

    controlled to maintain a temperatureof 105 ± 5 °C.

    A balance -

    Suitable capacity

    accurate to 0.1 %

    of the mass of the

    test portionA mechanical sieve shaker 

    Test sieves

    Trays & Containers

    Metal length gauge

    BS 812-105.2:1990

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    Preparation of test portion

    Reduce the sample by the procedures described in clause 6 of BS812-

    102:1989 to produce a test

     Allowance for the later rejection of particles retained on a 50.0mm test

    sieve and passing a 6.30mm test sieve

    Dry the test portion by heating at a temperature of 105 ± 5°C to achieve a

    dry mass which is constant to within0.1%. Allow to cool and weigh

    Minimum mass of test portion

    BS 812-105.2:1990

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    Procedure

    Carry out a sieve analysisDiscard all aggregates retained on the 50.0mm test sieve and all aggregate passing the

    6.30mm test sieve

    Weigh each of the individual size-fractions retained on the sieves,other than the 50.0mm test sieve, and store them in separate trays

    From the sums of the masses of the fractions in the trays (M1),

    calculate the individual percentage retained on each of the various

    sieves. Discard any fraction whose mass is 5% or less of mass M1. Record themass remaining (M2 )

    BS 812-105.2:1990

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    Procedure

    Gauge each fraction as follows. Select the length gauge appropriate

    to the size fraction under test and gauge each particle separately by

    hand

    Elongated particles are those whose greatest dimension prevents

    them from passing through the gauge, and these are placed to one

    side

    Combine and weigh all the particles remaining each of the gauges

    (M 3)

    BS 812-105.2:1990

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    Computation

    Elongation index =M3M2

    M2- Total weight of the sample taken (greater than 5 % of the total mass)

    M3- Total weight of martial retained on various length gauges

    BS 812-105.2:1990

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    Computation

    Size of aggregate Weight of materialFlaking Index

    (%) (individual

    size)

    BS test sieve nominal aperture sizeTotal

    Retained length

    gauge100% passing 100% retained

    50.0 37.5

    37.5 28.0

    28.0 20.0

    20.0 14.0 732.2 613.9

    14.0 10.0 1166.5 1095.2

    10.0 6.3 542.0 463.7

    Total 2440.7 2172.8

    Elongation index = Total weight of martial retained on various length gauges

    Total weight of the sample taken (greater than 5 % of the total mass)

    Elongation index =2172.8

    2440.7X 100%

    Elongation index = 89%

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    Calculate the flakiness index and the elongation index of the aggregatesample shown in Table 1.

    Sieve size (mm)Weight retained

    (g)

    Weight passing

    through

    Flakinessgauge (g)

    Weight not retainedelongation gauge (g)100% passing

    100%Retained

    63.0 50.0 516550.0 37.5 4356 683 4256

    37.5 28 3526 558 3301

    28 20 2215 447 2058

    20 14 1154 640 1029

    14 10 570 128 481

    10 6.3 350 63 326

    AASHTO: T 85 (1996)

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    This procedure covers the determination of specific gravity andabsorption of coarse aggregate in accordance with AASHTO: T 85  

    (1996) 

    Absorption   – the increase in the mass of aggregate due to water being

    absorbed into the pores of the material, but not including water adhering to the

    outside surface of the particles, expressed as a percentage of the dry mass

    Specific Gravity – the ratio of the mass, in air, of a volume of a material to the

    mass of the same volume of gas-free distilled water at a stated temperature

    Specific gravity is critical information for the Hot Mix Asphalt Design

    Engineer. The value is used in calculating air voids, voids in mineral

    aggregate (VMA), and voids filled by asphalt (VFA)

    AASHTO: T 85 (1996)

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    Moisture Conditions of Aggregates:

    1. Oven dry- fully absorbent

    2. Air dry- dry at the particle surface but containing some

    interior moisture

    3. Saturated surface dry (SSD)   – neither absorbing water nor

    contributing water to the concrete mixture

    4. Wet or moist- containing an excess of moisture on thesurface

    AASHTO: T 85 (1996)

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    AASHTO: T 85 (1996)

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    Apparatus

    ventilated oven - Thermostatically

    controlled to maintain a temperature

    of 105 ± 5 °C.

    Balance

    Sample container 

    Suspension apparatus

    with Water tank

    Sieves

    AASHTO: T 85 (1996)

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    Procedure

    Thoroughly mix the sample of aggregate and reduce it to the approximatequantity needed using the applicable procedures in T 248

    Reject all material passing a 4.75-mm (No. 4) sieve by dry sieving and

    thoroughly washing to remove dust or other coatings from the surface

    Preparation of test portion

    Dry the test sample to constant mass at a temperature of 110 ±5°C and cool

    in air at room temperature for 1 to 3 hours. 2

    Sink the aggregate in water at room temperature for a period of 15 to 19

    hours

    Remove the test sample from the water and roll it in a large absorbent cloth

    until all visible films of water are removed (Wipe the larger particles individually)

    AASHTO: T 85 (1996)

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    Procedure

    Determine the saturated surface dry (SSD) weigh of the sample (Designate

    this mass as “B”)

    Place the SSD test sample in the sample container and weigh it in water  

    maintained at 23.0 ±1.7°C (Shake the container to release entrapped air 

    before recording the weight) (Designate this submerged weight as “C”)

    Remove the sample from the basket. Ensure all material has been removed

    and place in a container of known mass

    Dry the test sample to constant mass at a temperature of 110 ±5°C about

    24hrs (Designate this mass as “A”)

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    Bulk Dry Specific Gravity =A

    (B-C)

     A - Oven dry weight B = Saturated surface dry (SSD) weight C = Weight in water 

    Computation

    Bulk Dry Specific Gravity

    The ratio of the weight in air of a unit volume of aggregate at a stated

    temperature to the weight in air of an equal volume of gas-free distilled water at

    a stated temperature

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    Bulk SSD Specific Gravity =B

    (B-C)

    B = Saturated surface dry (SSD) weight C = Weight in water 

    Computation

    Bulk SSD Specific Gravity

    The ratio of the weight in air of a unit volume of aggregate, INCLUDING the

    weight of water within the voids filled to the extent achieved by submerging in

    water for approximately 15 hours, to the weight in air of an equal volume of gas-

    free distilled water at a stated temperature

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    Apparent Specific Gravity =A

    (A-C)

     A - Oven dry weight C = Weight in water 

    Computation

    Apparent Specific Gravity

    The ratio of the weight in air of a unit volume of aggregate at a stated

    temperature to the weight in air of an equal volume of gas-free distilled water at

    a stated temperature

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    Computation

    Absorption

    The increase in weight of aggregate due to water in the pores of the material, but

    not including water adhering to the outside surface of the particles

    Absorption = (B- A)

    A

     A - Oven dry weight B = Saturated surface dry (SSD) weight

    X 100 %

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    Bitumen is a black, oily, viscous material that isa naturally-occurring organic byproduct of decomposed organic materials.

    It is sticky, thick, Tar like form of petroleum

    derived from polycyclic aeromatic hydrocarbon

    83

    General uses of Bitumen:

    • Constructions of roads, runways and platforms

    • Water proofing to prevent water seepage

    • Canal lining to prevent erosion• Dump-proof courses for masonry

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    Petroleum based bitumen (refinery bitumen) is largely

    used in road construction in Sri Lanka

    In the petroleum refinery

    process in which the

    residuum contains largely

    the refinery bitumen

    Bitumen

    Bitumen

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    Asphalts Tars Pitches

    Natural

    deposits

    Petroleum

    asphalts

    Slow

    curing

    Medium

    curing

    Rapid

    curing

    Emulsifiers Stabilizer   Rubber 

    Rock

    asphalt

    Native

    asphalt

    Asphalt

    cement

    Cut back

    bitumen

    Bitumen

    Emulsion

    Asphalts Tars Pitches

    Natural

    deposits

    Petroleum

    asphalts

    Slow

    curing

    Medium

    curing

    Rapid

    curing

    Emulsifiers Stabilizer   Rubber 

    Rock

    asphalt

    Native

    asphalt

    Asphalt

    cement

    Cut back

    bitumen

    Bitumen

    Emulsion

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    The most common bituminous materials are, as follows:

    Asphalts (available as natural deposits or areproduced from petroleum processing)

    Tars (obtained through the destructive distillation ofmaterials such as wood, coal, and shale, i.e., byheating wood or coal or shale in absence of air)

    Pitches (obtained through further processing of tars)

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     Asphalt cement (also called paving asphalt) are theprimary asphalt products produced by the distillation of crude oil.

     At ambient temperatures asphalt cement is a black, sticky,semisolid and a highly viscous material

    It is strong and durable cement with excellent adhesive andwaterproofing characteristics. It is also highly resistant tothe action of most acids, alkalis and salts

    The largest use of asphalt cement is in the production of asphalt concrete, which is primarily used in the

    construction of flexible pavements throughout the world The asphalt cement can readily be liquefied by applying

    heat for mixing with mineral aggregates to produce asphaltconcrete

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    Several standard grades of asphalt cement, based onconsistency, are available commercially

    Two methods, viscosity and penetration are used toclassify asphalt cements into different grades, as follows:

    The viscosity grades based on original asphalt cements(AC), as specified in ASTM D3381 are: AC – 5; AC – 10; AC –20; AC – 30; and AC – 40 (The numerical values indicateviscosity at 140 ºF in hundreds of poise)

    The penetration grades, as specified in  ASTM D946  are:200-300; 120-150; 85-100; 60-70; and 40-50 (higher thepenetration, the softer the asphalt cement, therefore, 40-50 isthe hardest grade and 200-300 is the softest grade

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    Liquid asphalts or cutback asphalts are asphaltcements mixed with a solvent to reduce their  viscosity to make them easier to use at ordinarytemperatures

    They are commonly heated and then sprayed onaggregates

    Upon evaporation of the solvent, they cure or hardenand cement the aggregate particles together 

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    Types and grades, as given below, are based on the type of solvent, which governs viscosity and the rates of evaporationand curing

    Rapid-Curing (RC) - Produced by adding a light diluent of high volatility (generally gasoline or naphtha) to asphalt cement.These are used primarily for tack coat and surface treatments

    Medium-Curing (MC) - Produced by adding a mediumdiluent of intermediate volatility (generally kerosene) to asphaltcement. These are generally used for   prime coat, stockpilepatching mixtures, and road-mixing operations

    Slow-Curing (SC) - Produced by adding oils of low volatility(generally diesel or other gas oils) to asphalt cement. They arealso called road oils. They are generally used for prime coat,stockpile-patching mixtures, and as dust palliatives

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    Cutback asphalts are commercially available in differentgrades, as shown in the following Fig.:

    A viscosity of 30 is more fluid than a viscosity of 3000

    Prime coat is a coating applied directly to a prepared base before additional layers of support or coating are supplied. Prime coat asphalt preparation is a vital element, as itdirectly affects the shear strength of the final asphalt product.

    Tack coat is applied after the prime coat, to form an adhesive bond between the tackcoat and the next layer of coating

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    Emulsified asphalts are increasingly being used in lieu of cutback asphalts for the following reasons:

    Environmental regulations: Emulsions are relativelypollution free

    Loss of high-energy products: When cutback asphaltscure, the diluents which are high energy, high price

    products are wasted into atmosphere Safety: Emulsions are safe to use

    Lower application temperature: Emulsions can beapplied at relatively low temperatures saving the fuel

    costs. Emulsions can also be applied effectively to adamp pavement, whereas dry conditions are required for cutback asphalts

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    Emulsified asphalt (also simply called emulsion) is a mixture of asphalt cement, water, and emulsifying agent

    Because the asphalt cement will not dissolve in water,asphalt cement and water exist in separate phases asshown in the following figure:

    To mix the asphalt cement with water, an emulsifying

    agent (usually a type of soap) is added

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    1. Colloid mill Method

    2. High speed mixing method

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    Process of manufacture of emulsified asphalt consists passing

    the hot asphalt cement and water containing the emulsifyingagent under pressure through a colloid mill method

    • The colloid mill breaks up

    the asphalt cement and

    disperses it, in the form of  

    very fine droplets, in thewater carrier 

    • The emulsified asphalt when

    used, the emulsion sets as

    the water evaporates

    • The emulsion usually

    contains 55-75% asphalt

    cement and up to 3%

    emulsifying agent, with

    balance being water 

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    High speed mixing is a batch process in which hot

    bitumen, hot water, emulsifier, and stabilizer are added

    into a vessel and agitated using a high speed agitator 

    Bitumen

    +

    Water +

    Emulsifier 

    +

    Stabiliser 

    High speed

    rotation

     Agitator 

    Vessel

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    Two most commonly used types of emulsified asphalts are

    specified in ASTM D977 and ASTM D2397:

     Anionic – electro-negatively charged asphalt droplets

    Cationic  – electro-positively charged asphalt droplets

    Anionic emulsions adhere better to aggregate particleswith positive surface charges (e.g., limestone)

    Cationic emulsions adhere better to aggregate particleswith negative surface charges (e.g., sandstone, quartz,siliceous gravel). Cationic emulsions also work better withwet aggregates and in colder weather 

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    Structure of Cationic Bitumen Emulsion

     Asphalt particles have positive charge

     Adhere better with negative particles (e.g., sandstone, quartz, siliceous

    gravel)

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    The anionic emulsified asphalts include Rapid Setting (RS),

    Medium Setting (MS)

    Slow Setting (SS)

    as specified in ASTM D977 

    The cationic emulsified asphalts include

    Rapid Setting (CRS)

    Medium Setting (CMS)

    Slow Setting (CSS)

    as specified in ASTM D2397 

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    Selection and uses of emulsified asphalts are given in ASTMD3628. Generally, they are used as follows:

    Type of emulsified

    asphaltsUses

    Rapid-setting Surface treatments and penetrationmacadam's

    Medium-setting Open-graded cold asphalt-aggregate

    mixtures

    Slow-setting Track coat, fog seal, dense-graded coldasphalt-aggregate mixtures, and slurry

    seals

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    The amount of emulsifiers used in bitumen emulsions isbetween 0.5 to 1.0 %, which is just sufficient to preventcoagulation of globules

    However, in some applications it is necessary to providebetter protection against coagulation

    In such a case it is necessary to add a stabilizer, which canbe done during the manufacture of the emulsion or at alater stage

    Commonly used stabilizers are casein and the potassium

    soaps of tall oil (a liquid resin) or Vinsol resin

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    Emulsions are classified into three groups according to theresistance to coagulation as follows

    Labile emulsifiers  – contain a minimum of emulsifierand moderately stable

    Semi stable emulsions  – are more highly stabilized

    Fully stable emulsions  – contain very highproportion of stabilizer 

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    104

     A recent development in bitumen technology is the addition ofrubber to the bitumen mixtures to improve the performance of

    resulting bitumen mixture

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    Favourable effects of the presence of rubber in bituminousmaterials are:

    1.  A mixture of rubber  – bitumen provides aggregate binding facility

    2. Rubber bitumen reduces sensitivity to temperature changes of thebitumen.

    3. Rubber increases softening point, viscosity, elasticity and cohesion

    4. Loss of lighter fractions in bitumen though weathering is retarded

    5. Bitumen mixtures containing rubber are more resilient and thereforecan absorb vibrations and traffic shock

    6.  Addition of vulcanized rubber in bitumen mixture can reduce reflectioncracking.

    7.  Adding 5.5 to 7.0 % rubber by weight of bitumen can reduce surfaceki i ld t t