Genevac Accessories and Spares - SP Scientific...Rocket Sample Holders 04-8931 Issue 1-14 October...

Genevac

Accessories and Spares

For Rocket™ Synergy Evaporators

Original instructions in English Part number 04-8931 Issue 1-14 October 2015

Contents

Introduction ......................................................................................................................... 2 Maintenance of sample holders .................................................................................................. 2 Limitations of use ....................................................................................................................... 3 Colour variation of surface finish................................................................................................. 3

Rotors ................................................................................................................................... 4 Flask rotor .................................................................................................................................. 4 Bowl rotor ................................................................................................................................... 4 Rotor Spares .............................................................................................................................. 5 Rotor accessories ....................................................................................................................... 7

Sample Holders for Flask Rotors ....................................................................................... 8 SampleGenie4 ............................................................................................................................ 8 SampleGenie4 spares ................................................................................................................. 9 GC Vial System2 ....................................................................................................................... 12 GC Vial System2 spares ........................................................................................................... 13 Standard Flask ......................................................................................................................... 15 Standard flask spares ............................................................................................................... 15 ASE Tube Puck ........................................................................................................................ 16 ASE Tube Puck spares ............................................................................................................. 16 Flip-Flop ................................................................................................................................... 17 Flip-Flop Spares ....................................................................................................................... 18

Accessories ....................................................................................................................... 20 Sampleholder accessories........................................................................................................ 20 Infinity Trolley ........................................................................................................................... 21

General Spares .................................................................................................................. 22 Main lid seal ............................................................................................................................. 22 Sample viewing window ........................................................................................................... 22 Waste solvent container ........................................................................................................... 22 Lid joint coupling (for feed system) ........................................................................................... 22 Feed hoses .............................................................................................................................. 23 Fittings for coolant, drain and exhaust hoses ............................................................................ 23

Quick Reference ................................................................................................................ 24 Part numbers ............................................................................................................................ 24 Amendment control .................................................................................................................. 25

Rocket Sample Holders

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Introduction

Genevac produce a range of sample holders and accessories that can be used to enhance the performance and increase the flexibility of Rocket™ Synergy and Rocket 4D Synergy high speed evaporation systems. Sample holders are manufactured using high quality materials such as boroscilicate glass and high grade alluminium. Where applicable, seals can be specified in low leachable viton or in highly resistant perfluoroelastomer.

Maintenance of sample holders

The Rocket evaporator controls pressure levels in inner and outer vacuum chambers independently and sample holders form part of the seal between these chambers; it is therefore vitaly important that a perfect seal is formed around each of the sample holders. To achieve this, the sample holders must be maintained in good condition and must be used correctly. Sample holders must be clean and free from imperfections around the area of the sealing surfaces; chips, scratches or labels applied to the flasks may cause leaks which can slow down the evaporation process. Refer to the Genevac Rocket™ Sample Holders User Manual for advice on day to day maintenance and use of the Rocket sample holders.


04-8931 Issue 1-14 October 2015 3

Limitations of use

This brochure contains informantion on a range of accessories and sample holders that are intended for use with Rocket Synergy and Rocket 4D Syenrgy evaporators. Some of the accessories and sample holders are also compatible with earlier (“pre-Synergy”) Rocket evaporators, although limitations may apply. Where limitations do apply, they shall be indicated as shown in the following example:

For use with Rocket 4D Synergy feed systems only In this example, the accessory must not be used with any system other than that which is specified.

Colour variation of surface finish

For some components the colouring of surface finish may vary slightly from batch to batch; for instance, one batch of vial adapters may appear darker than another. Where this occurs it does not affect the performance or integrity of the component.


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Rotors

Flask rotor

Part number

Flask rotor 70-1734/S

Details Six position flask rotor assembly for Rocket Synergy or Rocket 4D Synergy includes inner lid and six blanking plugs.

Bowl rotor - batch

Part number

Bowl rotor - batch 70-1820/S

Details

Five litre bowl rotor for Rocket 4D Synergy or Rocket Synergy, includes batch (non-feed) inner lid, batch baffles, lifting handles and USB data-key with Rocket Synergy batch methods.

Bowl rotor - feed

Part number

Bowl rotor - feed 70-1752/S

Details

Five litre bowl rotor for Rocket 4D Rocket 4D Synergy, includes feed inner lid, feed baffle, lifting handles and USB data-key with Rocket Synergy feed methods.


04-8931 Issue 1-14 October 2015 5

Rotor Spares

Part number

Inner lid 70-1548/S Non-feed

Details Inner lid for flask or non-feed bowl rotor.

Part number

Inner lid 70-1547/S Feed

Details Inner lid for bowl rotor For use with Rocket 4D Synergy feed systems only.

Part number

Batch baffle 70-1549/S

Details Batch baffle for bowl rotor. Set of two.

Part number

Feed baffle 04-7652/S

Details Single feed baffle for bowl rotor.


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Part number

Inner lid seal 04-7448/S

Details Seal for inner lid, fits flask rotor and bowl rotor.

Part number

Flask seals 70-1180

Details Flask seals used on Rocket Synergy flask rotor and pre-Synergy Rocket. Set of six.

Part number

O-ring 04-5676

Details O-ring (viton) for rotor hub.

Seal

Cap

Part number

Seal 70-1556/S

Details Seal kit (consisting of plug and O-ring) for bowl rotor pouring spout.

Part number

Cap 70-1557/S

Details Cap for bowl rotor pouring spout.


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Rotor accessories

Part number

Lid stand 70-1186

Details Stand for inner lid. Suitable for use with all variants.

Part number

Lifting handles 70-1552/S

Details Lifting handles for Rocket Synergy bowl rotor. Set of two.

Part number

Blanking plug 70-2004/S

Details Blanking plug for flask rotor. Set of two.

Part number

Pouring stand 70-1798

Details Pouring stand. Suitable for use with bowl rotors that have a pouring spout.

Part number

Synergy methods 04-8844

Details

USB data key (flash-drive) containing method files for Rocket Synergy flask rotor and Rocket Synergy bowl rotor feed and batch methods.


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Sample Holders for Flask Rotors

SampleGenie4

Part number

SampleGenie4 70-1740

Details

SampleGenie4 flask assembly. For use in Rocket Synergy evaporators and Rocket 4D Synergy evaporators with optional flask rotor. Evaporators with serial numbers lower than RK0399 (pre-Synergy) require low speed upgrade. Set of six. Note: Excludes vial adapter, vial adapter pad and vial seal. When ordering: please select vial adapter from table below. Information on vial seals can be found in the following section: Sample Holder Spares.

Vial adapter

Details

Vial adapter for SampleGenie4. Note: Includes vial adapter pad. Set of six.

Max vial diameter ( mm) Vial length (mm) Seal required Part number

DG 15.3 36.5 to 41.5 One part 70-1766

DD 15.3 41.5 to 46.5 One part 70-1763

DJ 17.3 46.5 to 51.5 Two part 70-1769

DC 17.3 56.5 to 61.5 One part 70-1762

DH 20.8 39.5 to 44.5 Two part 70-1767

DF 23.3 42.5 to 47.5 Two part 70-1765

DI 23.2 54.5 to 59.5 Two part 70-1768

DE 23.3 66.5 to 71.5 Two part 70-1764

DB 28.0 56.5 to 61.5 Two part 70-1761

DA 28.0 66.5 to 71.5 Two part 70-1760


04-8931 Issue 1-14 October 2015 9

SampleGenie4 spares

Part number

SG4 Flask 70-1741

Details Flask assembly only, for SampleGenie4. Set of six.

Part number

Collar pad 70-1743

Details Collar pad for SampleGenie4. Set of six.

Part number

Collar 70-1742

Details Collar for SampleGenie4. Set of six.

Part number

Holder 70-1744

Details Holder for SampleGenie4 vial adapter. Set of six


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Part number

Insert 70-1757

Details

Insert for SampleGenie4 two-part vial seal. For use with viton vial seal: 70-1758 or perfluoroelastomer vial seal: 70-1759. Set of six.

Part number

Vial seal 70-1758 Viton

Details

Viton seal for SampleGenie4 two-part vial seal. Requires insert: 70-1757. Set of six.

Note: Green mark in periphery indicates perfluoro.

Part number

Vial seal 70-1759 Perfluoroelastomer

Details

Perfluoroelastomer seal for SampleGenie4 two-part vial seal. Requires insert: 70-1757. Set of six.

Part number

Vial seal 70-1196 White viton

Details One-part, low leachable white viton, vial seal for use with SampleGenie4 Set of six.

Note: Notch in periphery indicates perflouro.

Part number

Vial seal 70-1197 Perfluoro

Details

One-part, highly resistant perfluoroelastomer, vial seal for use with SampleGenie4 Set of six.


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Part number

Vial adapter pad 70-1745 Diameter 16 mm

Details Vial adapter pad for SampleGenie4. Set of six.

Part number



Part number



Part number




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GC Vial System2

Part number

GC Vial System2 70-1423 Viton seals

Details GC Vial System2 flask assembly with low leachable white viton vial seals. Set of six.

Part number

GC Vial System2 70-1424 Perfluoro seals

Details

GC Vial System2 flask assembly with highly resistant perfluoroelastomer vial seals. Set of six.


04-8931 Issue 1-14 October 2015 13

GC Vial System2 spares

Part number

GC2 Flask 70-1425

Details Flask only, for GC Vial System2. Set of six.

Part number


Details Low leachable white viton vial seal for GC Vial system2. Set of six.

Note: Notch in periphery indicates perfluoro.

Part number


Details Highly resistant perfluoroelastomer vial seal for GC Vial System2. Set of six.


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Part number

Vial adapter 70-1800

Details

Two-piece vial adapter with O-ring, for CG Vial System2 (backward compatible with all CG Vial System2 flask aseemblies, replaces one-piece vial adapter: 70-1428) Set of six.

Part number

O-ring 70-1801

Details O-ring for CG Vial System2 vial adapter: 70-1800. Set of six.

Part number

Collar pad 70-1317

Details Collar pad for GC Vial System2. Set of six.

Part number

GC2 collar 70-1320

Details Collar for GC Vial System2. Set of six.

Part number

Cap 70-1176

Details Cap for GC Vial System2. Set of six.


04-8931 Issue 1-14 October 2015 15

Standard Flask

Part number

Standard flask assy 70-1321

Details Standard Flask with collar pad and collar. Set of six.

Standard flask spares

Part number

Standard flask 70-1170

Details Standard evaporation flask only. Set of six.

Part number

Collar pad 70-1317

Details

Collar pad for standard flask. For evaporators with serial numbers below RK0133, flask adapters must be removed from the rotor. Set of six.

Part number

Collar 70-1319

Details

Collar for standard flask. For evaporators with serial numbers below RK0133, flask adapters must be removed from the rotor. Set of six.


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ASE Tube Puck

Part number

Puck 70-1282

Details ASE* tube puck assembly. Set of six.

ASE Tube Puck spares

Part number

Puck seal 70-1287

Details Seal (viton O-ring) for ASE tube puck. Set of 18.


04-8931 Issue 1-14 October 2015 17

Flip-Flop

Part number

Flip-Flop 70-1295 Viton seals

Details

Flip-Flop assembly with low leachable white viton seals. For use with ASE tube puck. Set of 18.

Part number

Flip-Flop 70-1296 Perfluoro seals

Details

Flip-Flop assembly with highly resistant perfluoroelastomer seals. For use with ASE tube puck. Set of 18.

*ASE is a registered trademark of Dionex Corporation.


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Flip-Flop Spares

Part number

Flip-Flop tube 70-1297

Details Double ended tube for Flip-Flop. Pack of 100 (plus 10 spare).

Part number

Tube seal 70-1304 White viton

Details Low leachable white viton tube seal for Flip-Flop (tube to funnel). Pack of 20.

Part number

Tube seal 70-1306 Perfluoro

Details Highly resistant perfluoroelastomer tube seal for Flip-Flop (tube to funnel). Pack of 20.

Part number

Funnel 70-1298

Details Funnel for Flip-Flop. Pack of 18.

Part number

O-ring 70-1299

Details O-ring for Flip-Flop (funnel to vial cover). Pack of 20.


04-8931 Issue 1-14 October 2015 19

Part number


Details Low leachable white viton vial seal for Flip-Flop. Pack of 20.

Note: Notch in periphery indicates perfluoro.

Part number


Details Highly resistant perfluoroelastomer vial seal for Flip-Flop. Pack of 20.

Part number

Ejector peg 70-1301

Details Vial ejector peg for Flip-Flop. Set of 18.

Part number

O-ring 70-1302

Details O-ring for Flip-Flop vial ejector peg. Pack of 20.

Part number

Vial cover 70-1300

Details Vial cover for Flip-Flop. Set of 18.


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Accessories

Sampleholder accessories

Part number

Flask carrier 70-1187

Details

Coated steel flask carrier for safe transportation or storage of six standard flasks, CG vial system flasks or SampleGenie flasks.

Part number

Flask stand 70-1797

Details Single flask stand for use as a balance nest with: standard flask, GC Vial system flask or SampleGenie flask.

Part number

Splash cap 70-1265

Details

Viton splash cap for use with: standard flask, GC vial system flask or SampleGenie flask. Set of six.

Part number

Seal tool 04-8321

Details

Tool for safe removal of vial seal from SampleGenie flask or GC vial system flask, without risk of damage to flask or seals.


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Infinity Trolley

Part number

Trolley 70-1650

Details

Infinity Trolley for Rocket and Rocket Synergy. Accommodates one Rocket high speed evaporator, Julao FL601 re-circulating chiller and five litre waste solvent container.

Part number

Trolley 70-1630

Details

Infinity Trolley for Rocket 4D and Rocket 4D Synergy. Accommodates one Rocket 4D and Julabo FL1701 recirculating chiller.

Part number

Shelf 70-1635

Details

Shelf kit for Infinity Trolley. Accommodates one Edwards nXDS6i vacuum pump or may be used as sample preparation area.


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General Spares

Main lid seal

Part number

Main lid seal 04-5818/S

Details Seal for main (outer) lid for Rocket Synergy, Rocket 4D Synergy and pre-Synergy Rockets.

Sample viewing window

Part number

Window 70-1182

Details Sample viewing window and gasket assembly for systems with strobe.

Waste solvent container

Part number

Waste container 70-1247/S 5 litre

Details

Waste solvent container kit comprising polypropylene waste solvent container, two port cap, drain hose (five metres) and fittings.

Lid joint coupling (for feed system)

Part number

O-ring 04-7943

Details O-ring (green perfluoroelastomer) for lid joint coupling (of feed system).


04-8931 Issue 1-14 October 2015 23

Feed hoses

Part number

Feed hose 70-1553/S

Details Replacement feed hose. 50 metre length.

Fittings for coolant, drain and exhaust hoses

Part number

Hose fittings 70-1651/S

Details

Hose fittings kit comprising two type 1A fittings and two type 2N fittings for coolant, drain and exhaust hose connections.


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Quick Reference

Part numbers

04-1247/S ..................... 22 04-5676 .......................... 6 04-5818/S ..................... 22 04-7448/S ....................... 6 04-7652/S ....................... 5 04-7943 ........................ 22 04-8321 ........................ 20 04-8844 .......................... 7 04-8850/S ....................... 7 70-1170 ........................ 15 70-1176 ........................ 14 70-1177 ........................ 13 70-1178 ........................ 13 70-1180 .......................... 6 70-1182 ........................ 22 70-1186 .......................... 7 70-1187 ........................ 20 70-1196 ........................ 10 70-1197 ........................ 10 70-1265 ........................ 20 70-1282 ........................ 16 70-1287 ........................ 16 70-1295 ........................ 17 70-1296 ........................ 17 70-1297 ........................ 18 70-1298 ........................ 18 70-1299 ........................ 18

70-1300 ........................ 19 70-1301 ........................ 19 70-1302 ........................ 19 70-1303 ........................ 19 70-1304 ........................ 18 70-1305 ........................ 19 70-1306 ........................ 18 70-1317 .................. 14, 15 70-1319 ........................ 15 70-1320 ........................ 14 70-1321 ........................ 15 70-1423 ........................ 12 70-1424 ........................ 12 70-1425 ........................ 13 70-1547/S ...................... 5 70-1548/S ...................... 5 70-1549/S ...................... 5 70-1552/S ...................... 7 70-1553/S .................... 23 70-1556/S ...................... 6 70-1557/S ...................... 6 70-1630 ........................ 21 70-1635 ........................ 21 70-1650 ........................ 21 70-1651/S .................... 23 70-1734/S ...................... 4 70-1740 .......................... 8

70-1741 .......................... 9 70-1742 .......................... 9 70-1743 .......................... 9 70-1744 .......................... 9 70-1745 ........................ 11 70-1746 ........................ 11 70-1747 ........................ 11 70-1748 ........................ 11 70-1752/S ....................... 4 70-1757 ........................ 10 70-1758 ........................ 10 70-1759 ........................ 10 70-1760 .......................... 8 70-1761 .......................... 8 70-1762 .......................... 8 70-1763 .......................... 8 70-1764 .......................... 8 70-1765 .......................... 8 70-1766 .......................... 8 70-1767 .......................... 8 70-1768 .......................... 8 70-1769 .......................... 8 70-1797 ........................ 20 70-1798 .......................... 7 70-1800 ........................ 14 70-1801 ........................ 14 70-1820/S ....................... 4


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Amendment control

Issue Reason for Change Date Issued

1-1 First release 19-Dec-14

1-2 70-1759 images updated. Serial number limit for pre-Synergy systems added.

08-Jan-15

1-3 SG4 vial seal part number correction and duplications removed. Flip-Flop vial seal part number changed for pack of 20. Perflouro identification notes added.

09-Jan-15

1-4 70-1196, 70-1197, 70-1177, 70-1178 reintroduced. “Also used in” comments removed. Rotor hub O-ring removed.

29-Jan-15

1-5 Waste connection kit part number corrected. 17-Feb-15

1-6 04-5676, 04-7943, 70-1557/S included. 26-Mar-15

1-7 Pouring stand for bowl rotor – part number updated to reflect design change. Flask stand (balance nest) part number updated.

30-Apr-15

1-8 SG4 vials adapter DJ introduced. 14-May-15

1-9 70-1820/S introduced. Batch baffles added to 70-1820/S, feed baffles added to 70-1752/S.

22-May-15

1-10 GC Vial System2 vial addapter: 70-1800 replaces 70-1428, 70-1801 replaces 70-1429.

30-Jul-15

1-11 Address: SpScientific replaces SP industries. 10-Aug-15

1-12 Cap separated from GC Collar2; added as separate item. 27-Aug-15

1-13 V3 Blanking Plug added. 30-Sept-15

1-14 Minor correction. 07-Oct-15

Genevac Ltd The Sovereign Centre Farthing Road Ipswich IP1 5AP United Kingdom

Service: +44 (0) 1473 243000

Sales: +44 (0) 1473 240000 Fax: +44 (0) 1473 461176

Email: [email protected] [email protected] [email protected]

Web site: http://www.genevac.com

Genevac Inc SP Scientific 3538 Main Street Stone Ridge NY12484 United States of America

Sales & Service: (1) 845 267 2211 Fax: Fax (1) 845 267 2212

Email: [email protected]

Genevac Ltd operates a continuous development programme aimed at further improving products, all specifications are therefore subject to change. Coolheat® VacRamp™, Dri-Pure®, SampleGuard™, SampleGenie™ and associated logos are trade-marks of Genevac Ltd, unauthorised use is prohibited. Your Genevac Sales Representative will be happy to advise on the availability of special order items in addition to the sample holders listed in this Accessories Brochure All rights reserved, © Genevac Ltd 2015.

mailto:[email protected]

http://www.genevac.com/

mailto:[email protected]

Genevac Accessories and Spares - SP Scientific...Rocket Sample Holders 04-8931 Issue 1-14 October...

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