GALT 473-31 of... · 2015. 2. 12. · GALT 473-31 Mobility of Dislocations in Aluminum at 74°K and...
Transcript of GALT 473-31 of... · 2015. 2. 12. · GALT 473-31 Mobility of Dislocations in Aluminum at 74°K and...
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GALT 473-31
Mobility of Dislocations in Aluminum at 74°K and 83°K*
J. A. Gorman, D. S. Wood, and T. Vreeland, Jr.
W. M. Keck Laboratories, California Institute of Technology, Pasadena, California
In a previous article1
the authors reported determinations of the velocity
of dislocations in high purity single crystals of aluminum as a function of applied
stress in the temperature range 123°K to 343°K. These results were obtained using
a stress pulse technique in which dislocation positions were observed before and
after the stress pulse using the Berg-Barrett x-ray technique. This note reports
an extension of the dislocation velocity measurements in aluminum to lower
temperatures, 74°K and 83°K, and discusses their significance.
Dislocation velocities at 74°K and 83°K were obtained by the method
1 described previously except that the aluminum single crystal test specimens
were bonded to the torsion stress pulse machine using mixtures of isopentane and
methylcyclohexane which form glasses at temperatures slightly below the test
temperatures. The dislocation velocity data obtained at 74°K and 83°K are
* This work was supported by the U. S. Atomic Energy Commission
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shown as functions of the applied resolved shear stress in Figure 1. The
dashed lines in Figure 1 are straight lines from the origin to a point obtained
by averaging all the stress-velocity data for the given temperature.
The dislocation drag coefficient, which is the ratio of the drag force
acting on a unit length of dislocation to the dislocation velocity, was obtained
from the stress-velocity data as described previously1
The values obtained
-4 2 0 -4 2 were 1.33 x 10 dyne-sec/em at 74 K and 1.31 x 10 dyne-sec/em at 83°K.
These values, together with the values reported previously for higher temperatures,
are plotted as circles in Figure 2. Figure 2 also shows dislocation drag
2 coefficients for aluminum obtained by Mason and Rosenberg from ultrasonic
attenuation measurements (indicated by+) and from the phonon viscosity3 ' 4 and
electron viscosity5
'6
theories (indicated by dashed lines). The experimental
drag coefficients from Mason and Rosenberg and the theoretical values from the
phonon and electron viscosity theories are plotted to a different scale than
the present results to facilitate comparison of their temperature dependencies.
For temperatures greater than 150°K, Figure 2 shows that the magnitude of
the dislocation drag coefficient obtained by the present authors is considerably
less than that obtained by Mason and Rosenberg by ultrasonic measurements and
by the phonon viscosity theory, but that the temperature dependencies agree
rather well. In the authors' previous paper1
possible reasons for the dif-
ferences in the magnitude of the dislocation drag coefficient were discussed and
will not be repeated here. It was concluded that the agreement in the temperature
dependence tended to support the phonon viscosity theory.
The temperature dependence of the dislocation drag coefficient obtained
by the present authors in the range 74 °K to 150 °K does not exhibit the increase
with decreasing temperature which is shown by Mason and Rosenberg's experimental
and theoretically predicted results.
The present results thus indicate in contrast to Mason and Rosenberg that
in aluminu.'Tl the dislocation drag due to electron viscosity is ne g ligible compared
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to the phonon drag for temperatures greater than 74°K. Further direct velocity
measurements at temperatures below 74°K are needed to establish the importance
of electron viscosity in aluminum.
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REFERENCES
1. J. A. Gorman, D. S. Wood, and T. Vreeland, Jr., submitted for publication
to J. Appl. Phys., 1968.
2. w. P. Mason and A. Rosenberg, Phys. Rev. 151, 434 ( 1966).
3. w. P. Mason, J . Acoust. Soc. Am. 32, 458 ( 1960).
4. w. P. Mason, J. Appl. Phys. 35, 2779 ( 1964).
5. w. P. Mason, Ph~sical Acoustics and the ProEerties of Solids (D. Van
Nostrand Co., Inc . , Princeton, 1958) p. 323.
6. W. P. Mason, Appl. Phys. Letters~. 111 (1965).
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u (J) (/)
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4000r-
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0
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oo /~ //
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(.) 2000fo
Oo o /o c
oo o/~J}, /o/o~c:J:Qo _j
w > o ,.,Co / o
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/ -6 0 / 00 74°K 83°K
/ / 0 v I I I I I I V I I I I J I
0 2 4 6 8 10 12 0 2 4 6 8 10 12 14
RESOLVED SHEAR STRESS, 106 dynes/cm2
Fig. 1 Dislocation velocity vs resolved shear stress.
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CJ) I-z w
5 30 ~ w I- o THIS EXPERIMENT, LEFT 0::: z :::::> w ORDINATE CJ) -... ~ (.0
I- ,_: <{
z + ULTRASONIC MEASUREMENTS, 25 z w (.0
w 0:::: 4 RIGHT ORDINATE w ~ 0 (J)
- w z-u (L u u <{¢
X lL w lL z zr0 lL + 20 lL 0 o¢ w CJ) w CJ) CJ) ... 0 - 0
I 3 <{ <{ l{)l u I- u 0::: ~ CD
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<{ 0
15 <{ :::::> 0 w 0:::: 0::: 0::: 0 0::: 0 ~ CJ)
lL 2 0 w (f)
ZC\J ... + PHONON z 0::: - >-0 E VISCOSITY 0 lL 0::: I r:~ THEORY 10 - 0 (L
I- C\J ... W <! (.) <{ EI -CD u Q) \ u ~I- 0::: 0 (/) 0 w _J I
\~ELECTRON VISCOSITY _J uO (f) Q) 5 (f) a>Z CD
c: THEORY '[><{ z ~ -
0 -o 0 Q) w ,..._ c: (f)
v ~ 0 '0 0 ---- 0 -o 0:::
0 100 200 300 400 v I
TEMPERATURE, °K 0
Fig . 2 Disloca ti on dr a g coe ffi c i e nt vs t emperature .