FINAL REPORT CYLINDER DECOMMISSIONING · FINAL REPORT CYLINDER DECOMMISSIONING MALTA ROCKET FUEL...

FINAL REPORT

CYLINDER DECOMMISSIONING

MALTA ROCKET FUEL AREA SITEMALTA, NEW YORK

October 1995

Prepared by:

ERM-NORTHEAST, INC.501 New Kamer RoadSuite 7Albany, New York 12205

ERM306222

^^ __ a

ERM-Northeast's Commitment to QualityM

Our Quality Policy ,

We will fully understand and document our clients' **requirements for each assignment. j

We will conform to those requirements at all times and ^satisfy the requirements in the most efficient and cost- .1effective manner.

Our quality policy and procedures include an absolute *••»commitment to provide superior service andresponsiveness to our clients. "1

Our Quality Goals1

To serve you. ™

To serve you well. I

To continually improve that service. _1

Our Quality Improvement Process

ITrain each employee.

Establish and implement requirements based on a •preventative approach. |

IMaintain a standing Quality Improvement Team to ensurecontinuous improvement.

Empower Corrective Action Teams to analyze, correct •and eliminate problems. I

Continually strive to improve our client relationships. •

Iohn A. DeFilippi, President Howard Wiseman, Vice President

Chief Executive Officer Chief Operating Officer •

'Jtt^LS* f/l/x^/UL^' yLJxO-C ,LtL*~J____ •Craib A. Werle, Principal Brian 3. /tzc^j Principal m

306223 rikj

FINAL REPORT

CYLINDER DECOMMISSIONING

MALTA ROCKET FUEL AREA SITEMALTA, NEW YORK

October 1995

Prepared by:

ERM-NORTHEAST, INC.501 New Karner RoadSuite 7Albany, New York 12205

306224

TABLE OF CONTENTS

LO INTRODUCTION l-l

1.1 BACKGROUND 1-1

1.2 SITE DESCRIPTION 1-2

1.3 CYLINDER DESCRIPTION 1-3

1.3.1 UNLABELED (BORON TRIFL UORIDE) CYLINDER 1-3

1.3.2 PENTABORANE CYLINDER 1-4

2.0 VENDOR SELECTION 2-1

3.0 METHODOLOGY 3-1

3.1 DECOMMISSIONING 3-1

3.2 WASTE DISPOSAL 3-3

4.0 REFERENCES 4-1

LIST OF FIGURES

Figure 1 Site Location MapFigure 2 Test Station Map

LIST OF TABLES

Table 1 Test Pit Soil Analytical Results - Inorganic AnalytesTable 2 Test Pit Soil Analytical Results - Organic CompoundsTable 3 Summary of Waste Profile Analytical Results

LIST OF APPENDICES

Appendix A PHOTOGRAPHS OF CYLINDERSAppendix B ERC FINAL REPORT ON DECOMMISSIONING OF COMPRESSED GAS

CYLINDERSAppendix C WASTE PROFILE ANAL YTICAL RESULTS

306225

1.0 INTRODUCTION

A Remedial Investigation (RI) to characterize and define environmental conditions

at the Malta Rocket Fuel Area (MRFA) Site was conducted from 1991 to 1995 by

ERM-Northeast, Inc. (ERM). The RI was conducted pursuant to protocols setforth in the Revised RI Work Plan (WP) and Project Operations Plan (POP), bothprepared by Geraghty and Miller, Inc. (1991a and b, respectively), and as amendedwith United States Environmental Protection Agency (USEPA) approval duringthe RI (ERM-Northeast, Inc., 1995a). The RI consisted of numerous intrusive

tasks including soil borings and test pitting. During test pitting activities, twocompressed gas cylinders were unearthed These cylinders were intact; one wasunlabeled and the other was labeled as containing pentaborane. This reportdocuments the decommissioning process including the selection of the vendor,methodology, and disposal of wastes generated.

1.1 BACKGROUND

In July 1987, the MRFA Site was placed on the National Priorities List, and inSeptember 1989, the USEPA issued a Unilateral Administrative Order (UAO) toAdvanced Nuclear Fuels, Inc., Curtiss-Wright Corporation, General ElectricCompany (GE), Mechanical Technology, Inc. (MTI), New York State EnergyResearch and Development Authority (NYSERDA), Olin Corporation, Power

Technologies, Inc. (PTI), and Wright-Malta Corporation as potentially responsibleparties (PRPs). The UAO required that the PRPs conduct an RI and FeasibilityStudy (FS) at the MRFA Site. In March 1990, GE, NYSERDA, and theDepartment of Defense (DOD) (the Participating Parties) entered into aparticipation agreement to perform the RI and FS. The Final RI report was

submitted to the USEPA on 14 February 1995 (ERM-Northeast, Inc., 1995b) andapproved in 1995, while the Revised FS was submitted to the USEPA on 5October 1995 (Rust Environment and Infrastructure, 1995). FS approval is

pending.306226

ERM-NORTHEAST, INC. ,_, 380\206\CYLIND.DOC

The cylinder decommissioning described below was performed as a responseaction under the RI pursuant to paragraph 87 of the UAO and the protocols set

forth in the USEPA-approved Work Plan prepared by Earth ResourcesCorporation (1994a).

1.2 SITE DESCRIPTION

The MRFA Site, also known as the Saratoga Research and Development Center, islocated on Plains Road in the Towns of Malta and Stillwater, Saratoga County,New York. The site includes a parcel of land consisting of approximately 165developed acres, known as the Malta Test Station, and additional undevelopedwoodlands surrounding the Test Station. Figure 1 identifies the location and arealextent of the MRFA Site.

A Literature Search Report (LSR) (Geraghty and Miller, Inc., 1992), prepared aspart of the RI, summarizes the history of operations at the MRFA Site. The U.S.Government established the Malta Test Station in 1945, and since then it has beenused for a wide range of rocket and weapons testing programs as well as for spaceresearch. Thirty-three buildings and sixteen storage or disposal areas wereconstructed or established at the Test Station during its use as a research anddevelopment facility.

The Test Station is surrounded by a restrictive one-mile radius circular "easementarea" in which human habitation is prohibited. A fence surrounding the 165-acre

Test Station, a single access road, and strict security also restrict public access.The central portion of the Test Station (property of the Wright-Malta Corporation)is still being used as a weapons and propellant testing facility.

30622'

ERM-NORTHEA3T, INC. . n 380\206\CYLIND.DOC1-2

13 CYLINDER DESCRIPTION

Forty-eight distinct Areas of Concern (AOC) were investigated during the RI. Intwo of these AOCs, two single compressed gas cylinders were unearthed during

test pitting activities. These cylinders were intact; one was unlabeled (which was

later determined to contain boron trifluoride) and the other was labeled ascontaining pentaborane.

According to the LSR, pentaborane was stored at the MRFA Site in Buildings 8,9,20, 25, and 27, and drums containing residual pentaborane were reportedlyburied in Area D-5. The LSR also reports that pentaborane was manufactured inBuilding 20 and tested in rocket engines at the Building 25 test structure. On 21

June 1955, an explosion destroyed Building 20 while the pentaboranemanufacturing plant was being permanently shut down. The buildings/structures,storage areas, and disposal areas in which pentaborane was reportedly

manufactured, used, stored, and/or disposed, including Buildings 25G and 25Hand Area D-5, were investigated, and no evidence of pentaborane was found.

Boron trifluoride (BF3) was reportedly used only at Building 20 at the MRFA Site.

As with pentaborane, Building 20 was investigated, and no evidence of BFs wasfound.

1.3.1 UNLABELED (BORON TRIFLUORIDE) CYLINDER

The unlabeled compressed gas cylinder was unearthed in Area S-l during test

pitting activities on 21 October 1993. Area S-l is an open area surrounded bytrees with no buildings or paving, located in the south-central portion of the TestStation, south of Areas D-l and D-6 and at least 300 feet from the nearest TestStation building (Figure 2). According to the LSR, the area was reportedly usedfor all-purpose, above-ground storage of materials, such as scrap metal, domestic

garbage, lumber, roofing, pipes, spray cans, and drums. q n r* o 9 o

ERM-NORTHEAST. INC. | n 380\205\CYLIND.DOC

The RI field work (geophysical surveying and 12 test pits) indicated that Area S-lwas also used historically for the subsurface disposal of crushed drums and a

single, unlabeled compressed gas cylinder. The RI test pits also contained othermiscellaneous metal such as shavings, metal chunks, sheet metal, plate metal,

banding, wire, cans, pipe, and angle iron. The test pits also contained wood,concrete, plastic sheeting, and styrofoam. There is no current use of this area.

The cylinder was found at a depth of approximately two feet below grade in testpit P-57 (Figure 2). The cylinder was a typical high pressure compressed gascontainer measuring approximately 52 inches long and 8.5 inches in diameter. Ithad an intact valve that appeared to be in fair condition, though both the cylinder

and the valve were considerably rusted. Portions of the cylinder without rustappeared to have been painted light green or silver gray. The cylinder wascarefully removed by the test pitting backhoe and staged on the ground near thetest pit Photographs in Appendix A show the cylinder as it was staged.

No elevated photoionization detector (PID) readings were noted during theremoval of the cylinder. A soil sample was collected directly below the cylinderlocation (P-57/2-4) and analyzed for Target Compound List (TCL) organics and

Target Analyte List (TAL) inorganics plus boron. The analytical results of thissample are included on Tables 1 and 2. Upon reaching the completion depth of thetest pit (10 feet), the pit was backfilled with soil from the test pit, and the cylinder

was left in place on the ground surface near the test pit pending appropriatedecommissioning. Caution tape was placed around the cylinder and across the

opening of Area S-l to restrict unauthorized access to the cylinder.

7.3.2 PENTABORANE CYLINDER

The compressed gas cylinder, labeled as containing pentaborane, was unearthed in

Area D-4 during test pitting activities on 15 October 1993. Area D-4 is an open

ERM-NORTHEAST. INC. . . 380\20S\CYUND.DOC1-4 306220

grassy area with no buildings or paving, located in the eastern portion of the TestStation, approximately 100 feet east of Building 5 and immediately south of AreaD-2 (Figure 2). Large brush and/or woods surround the northeast and south sidesof the area in addition to a relatively steep bank, approximately five to fifteen feethigh. The area was reportedly used for surface storage of bulk metal.

The RI field work (geophysical surveying and 11 test pits) indicated that Area D-4was also used historically for the subsurface disposal of domestic trash includingpaper, wood, glass, spray cans, bottles, beverage cans, light bulbs, plasticcontainers, wire, and a single compressed gas cylinder. There is no current use ofthis area.

The cylinder was found at a depth of approximately three feet below grade in testpit P-35 (Figure 2). The cylinder was a large, low pressure container measuringapproximately 48 inches high and 30 inches in diameter. The cylinder and its intactvalve appeared to be in good condition. The cylinder was painted light green andlabeled as follows:

SHIPPED TO

TRANSPORTATION OFFICER

EDWARDS AFB CALIFORNIAAFB 2805M/F FTRFS

BATCH NO. 129PENTABORANE LOT NUMBER 2

SHIPPED BY

GALLERY CHEMICAL COMPANYMUSKOGEE OKLAHOMA

CONTRACT ?????? (800) 40844

306230

ERM-NORTHEAST. INC. . mf 380\206\CYUND.DOC1-5

The question marks indicate illegible numbers or letters. The cylinder wascarefully removed by the test pitting backhoe and staged on the ground near thetest pit Photographs in Appendix A show the cylinder as it was staged.

No elevated photoionization detector (PID) readings were noted during theremoval of the cylinder. A soil sample was collected in the area where the cylinderwas found (P-35/2-4) and analyzed for TCL/TAL plus boron. The analyticalresults of this sample are included on Tables 1 and 2. Upon reaching thecompletion depth of the test pit (10 feet), the pit was backfilled with soil from thetest pit, and the cylinder was left in place on the ground surface near the test pitpending appropriate decommissioning. Caution tape was placed around thecylinder and across the opening of Area D-4 to restrict unauthorized access to thecylinder.

306231

ERM-NORTHEAST, INC. - « 380\205\CYLIND.DOC1-6

2.0 VENDOR SELECTION

Early in 1994, ERM-EnviroClean Northeast, Inc. (ECNE) (the construction andremediation affiliate of ERM-Northeast, Inc.) began soliciting bids from vendors to

decommission the two cylinders in response to a request by the ParticipatingParties. Bids were solicited from a total of nine vendors. Bids were received fromfour of the vendors, while the other five declined to bid. The vendors that declinedto bid are listed below:

• Rollins ChemPack, Inc., Milford, Connecticut• SET Environmental, Inc., Wheeling, Illinois• Reactive Hazards Reduction, Inc., Newfoundland, New Jersey• Westinghouse Remediation Services, Clarkston, Georgia

Mr. Carmelo Vasi, Specialty Gas Consultant, Nutley, New Jersey

The four vendors that submitted bids are listed below:

• Emergency Technical Services Corporation, Schaumburg, Illinois• Advanced Environmental Technology, Inc., Latham, New York

• National Environmental Management Services, Inc., Virginia Beach,Virginia

• Earth Resources Corporation, Inc., Ocoee, Florida

Upon careful review of the four bidding vendors, including a thorough study oftheir previous projects completed, Earth Resources Corporation, Inc. (ERC) wasselected to perform the cylinder decommissioning at the MRFA Site. The decision

to retain ERC was based on referrals that ERC was able to perform cylinderdecommissioning work in a timely and safe manner, and because of their state-of-the-art secondary containment units and remote sampling, treatment, andsurveillance technologies.

306232

ERM-NORTHEAST, INC. n •* 3SO\206\CYUND.DOC

3.0 METHODOLOGY

Prior to any on-site work activities, ERC prepared a proprietary Work Plan dated

October 1994 that was approved by the USEPA. The Work Plan described thesite-specific tasks to be completed by ERC including health and safety protocols.In addition, a meeting was held at the site field office (Building 17) beforemobilizing to the work area (Area D-6, between Areas S-l and D-4). Thismeeting was attended by the entire ERC and ECNE field teams, representativesfrom the Participating Parties, Wright-Malta personnel, and representatives fromthe Malta Ridge Fire and Ambulance Services. During this meeting, the general

scope of work was discussed and details regarding the chemical hazards andemergency response procedures, in the event of a release, were presented.

3.1 DECOMMISSIONING

ERC began mobilizing equipment to the MRFA Site on 13 October 1994. ERCmobilized a Cylinder Recovery Vessel (CRV) trailer, Large Cylinder Transfer Unit

(LCTU) trailer, Mobile Laboratory, trained and certified personnel, and requiredsupport equipment. The CRV and LCTU are secondary containment units usedfor remotely sampling and treating the contents of cylinders using video

surveillance within an inert atmosphere (i.e., the secondary containment space isflooded with an inert gas such as nitrogen). The mobile laboratory was equippedwith an infrared (IR) spectrophotometer and a mass spectrometer (MS).

The setup and checkout of the CRV, LCTU, Mobile Lab, and supportingequipment continued through 21 October 1994. ECNE personnel were on site at

all times to monitor the activities of ERC personnel and to serve as liaison betweenthe Participating Parties, USEPA, local emergency response services, and thecompanies operating at the Test Station (i.e., Wright-Malta Corporation, MTI,

Advanced Liquid Polymer Silicones, Martin Marietta).

306233

ERM-NORTHEAOT, INC. « . 380\205\CYUND.DOC

On Friday, 21 October 1994, the pentaborane-labeled cylinder from Area D-4

(referred to as ERM-002 by ERC) was moved from its location in Area D-4 andplaced within the decommissioning exclusion zone (Area D-6); where it remained

for several days while the unlabeled, high pressure cylinder (referred to as ERM-

001 by ERC) was decommissioned. The pentaborane cylinder was moved byforklift after attaching it to a shipping pallet. On Monday, 24 October 1994, theunlabeled high-pressure cylinder was moved from Area S-l using a secondarycontainment unit (i.e., a solkatronic overpack) and placed directly into the CRVtrailer. Cylinder handling personnel wore Level A Personnel Protective Equipment(PPE), and air monitoring was accomplished by ERC throughout the relocationactivities, which both occurred without incident

On 24 October 1994, using remote techniques, the outside of the unlabeledcylinder was pierced and the vapor contents were sampled and analyzed by the on-

site laboratory. Analytical results indicated the cylinder contained BFs at oneatmosphere of pressure. The residual BFs gases were purged, using nitrogen, intoa water scrubber. All gases were then pumped through a Nixtox scrubbercontaining activated carbon and vented to the atmosphere. All treatment solutionsand spent carbon were containerized and staged in appropriate DOT-approved 55-gallon drums for subsequent sampling and disposal by ECNE as described inSection 3.2.

The pentaborane cylinder was prepared for processing on 25 and 26 October 1994.On 27 October 1994, the pentaborane cylinder was placed inside the LCTU trailer

using a forklift and manpower; again, all cylinder handling personnel wore Level A

PPE. Using remote techniques, the outside of the pentaborane cylinder was thenpierced and the vapor contents were sampled and analyzed by the on-sitelaboratory. Analytical results indicated the cylinder contained liquid pentaboraneat 5 pounds per square inch gauge (psig). The pentaborane was treated by

repeatedly purging the cylinder with nitrogen and then evacuating to the lowest

attainable pressure. All gases removed during evacuation were passed through a

ERM-NORTHEAST, INC. 380\206\CYLIND.DOC

306234

liquid scrubber containing caustic soda solution to hydrolyze the pentaborane.

These gases were then pumped through a Nixtox scrubber containing activated

carbon and then through a flare after-burner to burn off hydrogen generated by the

liquid scrubbing process. Flushing and evacuating continued for several days until

the vacuum level achieved in each cycle became constant. This indicated that all

liquid pentaborane had been evaporated and only residue remained. The residualpentaborane was treated as described above one last time on 1 November 1994.On 3 November 1994, the cylinder was drained and checked. All treatment

solutions and spent carbon were containerized and staged in appropriate DOT-

approved 55-gallon drums for subsequent sampling and disposal by ECNE as

described in Section 3.2.

After treatment, both cylinders were cut completely in half with a saw. On 4November 1994, ERG demobilized from the site. On 23 December 1994, ERC

submitted a Final Report which described the decommissioning activities

performed and included the on-site laboratory analytical results. This report is

attached in Appendix B.

3.2 WASTE DISPOSAL

Four waste streams were generated during the cylinder decommissioning activitiesincluding:

Decon Rinsate: Level A PPE was deconned upon exiting the "work

zone" during all the decommissioning operations. Liquids associated with

the decon process were collected, labeled, and staged in two 55-gallondrums.

• Spent BF3 Treatment Solutions: Liquids associated with the

decommissioning of the BFs cylinder were collected, labeled, and staged in

two 55-gallon drums.

306235

ERM-NORTHEAST, INC. " 380\205\CYLIND.DOC

• Spent Pentaborane Treatment Solutions: Liquids associated with thedecommissioning of the pentaborane cylinder were collected, labeled, andstaged in twenty three 55-gallon drums.

• Spent Carbon: Carbon was used in ERC's Nixtox scrubber during the

decommissioning of the BFs and pentaborane cylinders. Upon completionof the decommissioning, the spent carbon was transferred to three 55-gallon drums.

United Industrial Services (UIS) of Meriden, Connecticut was selected andapproved by the USEPA to transport and receive the wastes. Composite samplesof each of the four waste streams were collected by ECNE personnel on 7November 1994 and shipped to UIS for waste profile analyses. Two quarts ofeach waste stream were composited by placing equal amounts of liquid (or carbon)

from each drum into sample containers. Analytical results for the four wastestreams, which are summarized on Table 3 and attached as Appendix C, indicatedthat all wastes generated during the cylinder decommissioning activities were non-hazardous. Based on the non-hazardous characterization, the 30 drums of wastewere transported to the UIS facilities in Meriden, Connecticut on 27 December1994 for treatment and disposal.

As stated above, the two cylinders were cut completely in half by ERC afterneutralizing the contents. The four cylinder halves were considered to be non-

hazardous scrap metal and were transported by ECNE personnel to Schiabo-

Hudson Scrapyard at the Port of Albany in Albany, New York for recycling.

306236

ERM-NORTHEAST, INC. n M 380\206\CYUND.DOC3-4

4.0 REFERENCES

Earth Resources Corporation, 1994a, Work, Safety, Health and Emergency

Response Plan, Malta Rocket Fuel Area Site, October 1994.

Earth Resources Corporation, 19945, Final Report, Decommissioning ofCompressed Gas Cylinders, Malta Rocket Fuel Area Site, December 231994.

ERM-Northeast, Inc., 1995a, Correspondence Documenting Changes in Scope or

Field Protocol, Remedial Investigation Report Malta Rocket Fuel Area Site

Towns of Malta and Stillwater Saratoga County, New York, February1995.

ERM-Northeast, Inc., 1995b, Final Remedial Investigation Report, Malta RocketFuel Area Site, Towns of Malta and Stillwater, Saratoga County, NewYork, February 1995.

Geraghty and Miller, Inc., 1991a, Revised Remedial Investigation Work Plan forthe Malta Rocket Fuel Area Site, Towns of Malta and Stillwater Saratoga

County, New York, February, 1991.

Geraghty and Miller, Inc., 1991b, Project Operations Plan for the Malta RocketFuel Area Site, Towns of Malta and Stillwater, Saratoga County, NewYork, August 1991.

Geraghty and Miller, Inc., 1992, Literature Search Report for the Malta RocketFuel Area Site, Towns of Malta and Stillwater, Saratoga County, NewYork, May 1992.

Rust Environment and Infrastructure, Inc., 1995, Draft Feasibility Study, Malta

Rocket Fuel Area Site, Saratoga County, New York, May 1995.

ERM-NORTHEAST, INC. A-1 Q C\ C O Q **} 380\206\CYLIND.DOC

FIGURES

306238

S A R A T O G A L A K E

1 RoundLake

-\ '

SITE LOCATION MAP

306239MALTA ROCKET FUEL AREA SITE

;ERM Hortheast-•2 OOP

LEGEND:D~'/—

O - Rl AREA OF CONCERN

• - TEST PIT LOCATIONP-57

SCALE IN FEET

300 600

cvCDOCO

MRFA TEST STATION MAPMALTA ROCKET FUEL AREA SITE

MALTA, NYPREPARED FOR

MALTA ROCKET FUEL AREA SITE

ERM-NortheastERM

SCALE

DATE9/95

FIGURE

2

TABLES

06241

TABLE 1TEST PIT SOIL ANALYTICAL RESULTS

INORGANIC ANALYTESMALTA ROCKET FUEL AREA SITE

AnalytesAluminumAntimonyAnenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanideBoron

MRFAComparative

Criteria7830013.28.13001.013.5

50000013530999

90000500

50000027008.1540

5250002

135325000

1.89189

81005402400

AreaD-4P-35/2-4

3770< 8.2 UJ

1.4 B14.7 B0.19 B

<OJ1 U6830432.8 B7.578702.41820161

< 0.04 U6 B463 B

< 0.18 U< 1.0 U

40.8 B< 0.19 U

8.517.3

< 0.63 U< 15.5 U

AreaS-1P-57/2-4

5500< 7.8 UJ

1.614.4 B0.25 B

< 0.49 U326 B5.43.0 B7.889903.71350190

< 0.04 U6.9432 B

< 0.17 U< 0.99 U

24.2 B< 0.18 U

10.116.8 R

< 0.62 U< 14.8 U

Notes:1. All concentrations are in milligrams per kilogram (mg/kg = put* per million (ppm)).2. U = Analyte was not detected.3. J = Semi-quantitative value due to QA/QC data validation requirements.4. B = Value is above the Instrument Detection Limit (IDL) but below the Contract Required Detection Limit (CRDL).5. R = Analysis rejected.

P35J7IKXLS KW/95

306242

TABLE 2TEST PIT SOIL ANALYTICAL RESULTS

ORGANIC COMPOUNDSMALTA ROCKET FUEL AREA SITE

Volatile Organic TICs*| Cyclotetrasiloxane, Octamethyl

MRFAComparative

Criterianone

AreaD-4P-35/2-4

NF

AreaS-1P-57/2-4

7 NJ

Semi-Volatile Organic TIC**Unknown Aliphatic EsterUnknown Cycloalkene

5000050000

NF76 J

89 JNF

Pestldde/PCB Compounds*4,4'-DDT 2100 UJ 2.0 PJ

Notes:1. All concentrations are in micrograms per kilogram (ug/kg = parts per billion (ppb)>.2. * = Only compounds that were detected in one or more samples are listed No target VOCs or S VOCs were detected.3. U = Analyte was not detected.4. J = Semi-quantitative value due to QA/QC data validation requirements.5. P = >25% difference for detected concentrations between the two OC columns. The lower value is reported.6. N = Compound was identified with a Chemical Abstract Servivei (CAS) number.7. NF = Compound not found on TIC list

P35.57ORJCLS \CW9S

306243

TABLE 3SUMMARY OF WASTE PROFILE ANALYTICAL RESULTS

MALTA ROCKET FUEL AREA SITE

AnalytesArsenicBariumCadmiumChromiumCopperIronLeadMercuryNickelSilverSodiumZincPhenolsPCBsPHFlash Point

DeconWash Water

NDNDND

0.020.162.980.03NA

0.04NDNA0.55NDND7.56

>200°C

BF3

Wash Water0.010.010.010.100.0832.50.01NA

0.110.02NA1.35ND

ND*7.87

>200°C

PentaboraneWash Water

NDNDNDND

0.030.29NDNA0.160.01NA

0.03NDND8.44

>200°C

Charcoal

NDNDNDNDNANANDNDNANANDNANANA8.65

>200°C

Notes:1. All concentrations are in parts per million (ppm).2. ND = Analyte was not detected.3. NA = Not analyzed* PCBs were reported in the original analytical results for this sample. However, the

detection of PCBs was not considered reasonable since PCBs were not associatedwith any of the cylinder decommissioning processes. A re-analysis of this sampleconfirmed that PCBs were not detected.

WST_PRO.XLS 1(V1»9S 21 23

306244

Appendix APhotographs of Cylinders

306245

Pentaborane Cylinder, Test Pit P-35, Area D-4

306246

Unlabeled Cylinder, Test Pit P-57, Area S-1

306247

Appendix BERC Final Report on Decommissioning of

Compressed Gas Cylinders

306248

EARTH RESOURCES CORPORATION1227 Marshall Farms Road • Ocoee, Florida 34761

(407) 877-0877FAX (407) 877-3622

December 23, 1994

Mr. David W. MyersERM-EnviroClean-Northeast501 New Karner RoadSuite 7Albany, NY 12205

Subject: Final Report, Decommissioning of Compressed Gas Cylinders,Malta Rocket Fuel Site, Malta, New York

Dear Mr. Myers:

Earth Resources Corporation (ERC), under EnviroClean-Northeast, Inc.contract dated 7 October 1994 decommissioned two compressed gascylinders for EnviroClean-Northeast Project No. 132.04 at the MaltaRocket Fuel Site in Malta, New York. This report summarizes theoperation.

ERC's Director of Operations, Mr. Ed Van Schoick, was the on-siteproject director. He was assisted by Mr. Charles Mattern, ERCQuality Control Manager, and Mr. Tom Gysin, ERC's Site Manager.

Equipment and personnel began arriving at the job site on 13October. ERC mobilized the Cylinder Recovery Vessel (CRV) trailer,Large Cylinder Transfer Unit (LCTU) trailer, Mobile Laboratory,trained and certified personnel, and required support equipment.Site power was supplied by rental generators.

On 14 October, ERC's site management personnel met withrepresentatives from other project participants to review theproject schedule, site setup, and anticipated operations.

Cylinder designated ERM-001 was a high pressure container measuring52" in length and 8.5" in diameter. The cylinder had a 330 CGAvalve and the cylinder and valve had extensive exterior corrosion.The contents of the cylinder were unknown. ERC's approach was toplace the cylinder into the CRV, pierce the cylinder remotely,obtain a vapor sample for on-site laboratory analysis, and determinethe appropriate treatment methodology.

Cylinder designated ERM-002 was a low pressure container measuring48" high and 94" in circumference. The cylinder was labeled ascontaining pentaborane from Gallery Chemical Company. Liquidmaterial was known to be inside the cylinder. ERC's approach was

3062413

basically the same as towards cylinder ERM-001 except, due to thelarge size of the cylinder, the cylinder's contents were to beaccessed via an external tapping collar with the LCTU providingsecondary containment during the process.

The setup and checkout of the CRV, LCTU, Mobile Lab and supportingequipment continued through 21 October.

On 21 October, ERG relocated cylinder ERM-002 from an area whoseaccess would be restricted to ERC's processing area. The cylinderwas moved by forklift after it had been strapped to a shippingpallet. Cylinder handling personnel wore Level A PersonnelProtective Equipment (PPE) and air monitoring was accomplishedthroughout the relocation activity. After relocation, access to thearea of the cylinder was restricted by caution tape.

On Monday, 24 October, cylinder ERM-001 was placed inside theSolkatronic overpack for moving to the cylinder processing area. At11:45AM, the cylinder was removed from the overpack and placedinside the CRV. At 2:14PM the cylinder was drilled and sampled.Analysis determined the cylinder contained boron trifluoride at oneatmosphere. The residual boron trifluoride gases were purged usingnitrogen into a water scrubber.

Site activities October 25 through October 26 involved preparationsfor processing cylinder ERM-002 in the LCTU.

On 27 October, at 10:12AM, cylinder ERM-002 was drilled and a samplewas taken. Analysis determined the cylinder contained pentaboraneat 5 pounds psig. The liquid pentaborane was slowly hydrolyzed ina liquid scrubber. The cylinder was repetitively purged withnitrogen into a liquid scrubber. On 1 November, water was injectedinto the source cylinder to hydrolyze any remaining pentaborane.

On 3 November, cylinder ERM-002 was drained and checked forcontamination. Both cylinders were cut completely in half andchecked for contamination.

On 4 November, site restoration began. The carbon adsorbent fromthe nixtox was removed and placed into three drums for disposal byERM. The liquids from the pentaborane scrubber and cylinderrinseates were placed in drums for disposal by ERM also.

All major equipment items were checked for contaminates,decontaminated if necessary, and were removed from the project siteby the end of the day, 4 November.

306250

Cylinder analytical documentation and additional documentationpertaining to site operations is enclosed.

Sincerely Yours,

EARTH RESOURCES CORPORATION

Robert R. McBrideAssistant Director of Operations

Enclosures:

1. Cylinder Inspection Logs and Analysis Data2. Daily Safety Meeting Logs3. Quality Control Daily Reports4. Confined Space Entry Permits6. Air Analysis Data

306251

306252

Project Name:

Cylinder Serial »:

DOT Rating:

Other:

Form 2

CYLINDER INSPECTION LOG

Cylinder Type: H.P.

Inspector: jL.,

-2___

L.P.

Labels and/or Markings:

ERC *:

Dimensions : 52 "r ? '4

Owner Stamp:

3E1800 3A2015 3AA2400 JA221—————•—•

Test Date(s): __

Valve Type: 33£>

General Condition:

Comments:

Good Fair Poor

Valve Condition:

Comments:

Good Fair Poor

Pre-operation Weight:

Approved to Handle:

Handling Precautions:

Post-operation Weight:

Yes /_^-

/?

Approved for Valve Sampling:

Sample Method:

Yes

Large CRV Small CRV

No

No

Val

Comments:

Sample Date: C ? (J> Pressure:

Identified Contents:

Analytical Method:

Disposition:

j_ •

/hi f / u o •/• ,

Mass Spec FTIR

fa

Other

•Camtie •Scrub

Recontainerized:

Recontalnerlzed Cylinder #:

Acid Scrub ______ Oxidizing Carbon

Mole Sieve Flare

Yes No

306253'Use or disclosure of data contained on this sheet is subject to the

restrictions on the title page of this plan.'

Form 4ANALYTICAL SUMMARY FORM

OVERPACK it: __________ CYLINDER ff:

MASS SPECTRUM INTERPRETATION /

_________________£>i~ r^-' / r l f i t l r . f i r/(- • flJ,tlfrr-r>.^I/

Analyst Signature: ^jJ^^JL^ .. OK^>M.L~-.—______________ Date: to s-ctQA Confirmation Yes D No DComments: _____ __

FT1R INTERPRETATION

Analyst Signature: ______{JuL*sJL~, c. rn\^^AL^^L.__________ Date: to - ^QA Confirmation Yes D No DComments:

COLORIMETRIC OR OTHER INTERPRETATION

Analyst Signature: ________________________________________ Date:QA Confirmation Yes D No DComments:

INTERPRETED RESULTS: PW,^ TV', ftn« ^ < J t

QA or Document Officer Signature:

DATE: 306254'Use or disclosure of the data contained on this sheet is subject to the

restrictions on the title page of this plan. '

GGZ908

c.q

i ii in i is Hoxyn.) , j, _.-a.-,7 s-^'s^'M'^aiv-fl s w' ' '« .• • i r ' 4

fSQ Pin

fj •.' Z 2 I'J .2

1 !! J

Biii HHHli IttBISi

'*\ r-L-L"! i* i SSO^ 'j 0 w V r«

.'• ' r°i : A A f> "• n '

:•? dP it Bt tC ?

JjjlFiH

r^pyi ilv yJL:3,'.tVjtil

j c- b i t f

IND

":-] IA 1;' .3

nnfnr9

ilt.i «

Tt-1

>v

*• i~ *-1 . T r • *•* ->. ^r? *-? ri v *.•,.* • f r

.-.,-•>- 1 Iu v , ~>< .

"! '•••! * T '•'• '•• ."• J'.-. T ••:f^ , o« i .!, f '.

vi-v. t » _»

11? M o

Elapsed Iiwl8§ s »**!

HI

riIHAGNIFV• i jI V 1

(SPAN

45 58 55 SO 8524-Oct-34

PCiiRSOR |l! l .8-23 . 1

306256

CO

enroen

• " ' •"-' ';;</ 'i)/i Y !,' •• ! !' i < t1

:

' : i .'' .'"

.-'•,'•..'.. .'.'A',:/..;.'. .'.'..'•• •••' .•••.••'••• ' ' - ••-- .

,

j

., •,, -.

•::'-:l

. . \ ,< i,\ " '. •

I-''.*- T

'U.: '-'.,:• '

u' ^j • • ,

;' i .: . • .?.' U> i,

1 ' '• < 4.

i' \

i

,:

•i• •

•- is ;CP'!

:»•:•:';

'jl ' ^j^.'':;;;^^:;:i;

; i' ' '•••• -u . '.';:r-tji'i'i' f ' ' ., . ,. .. • /.d 5 > - - ' ,• jj : !•..,' 't I ' -. ...',.

r ,,. .—-.., -.

w: .'

H• 1

ii

''.'•: • :.::II-';.T:?••: '-i.v, ;•' '. • Muu;;.;

f'';' V.i."' i-.i''.:

.

•

i!

!

,,;H!J,

•^; :*'•..

.'''•i

_:

;::•{ :::=. :,iUJ

•' '"^ • " • *• J

b , jj ' , '* i !

'• *• •"••-•- -•• ' •

J. . '. .*"

\ :

5V ;

•) '

1

1! i'

1 . 1

i , i.( !

ll, / !

[,'.'•"•

a u T <= •:• ^ :

ICT,-: :

T *.« - T r:od^.-v"Ld=.^«5£,

- ft *. J«-* J(. J(. * i. »•

1 — vj "•i.' t ". '4 i"i T c = = w

.......V

---J

»"r •'i

II f.-.•"''"

•-;

9 -3 :f !

!,!

r.\F!!•!rl

. _>

.;; '

i: .

, , -:

:••>;

;;•-•- ^.•

r:r :

•

= ^

•,"• " -- — ••—

- --

•:

306259

.-'-.::. pi. ,:, .1 f: : . Io I

R e s o l u t i o n : -'>. CC cm-.I

M o d s : I."•*• X * )r •> 'L -*••*•*-*• •* * *:**••> * *!*- -Sr •*-»•*••> *•*••>[•#*•!

\_' LJ 5 . :71 S '. • ':'. 1 I'l .^. <

w 1 .. r''i_ i J — X i i ';' 71

?sa^ ;p l i i ; t 5 r - : KC1A p o ci i .^ i", "7 i :> :~i : C o 5 i r. 3

3062GO

Project Name:

Date: /Q -c?/-

DOT Rating:

Other:

Form 2CYLINDER INSPECTION LOG

Inspector:

Cylinder Serial »: 33~

Color:

3E1800 3A2015

Cylinder Type: H.P.

Labels and/or Markings:

L.P.

D.mensions: ;/ X

Owner Stamp:

3AA2400 3A2215

Test Date(s): ly - (j> (

Valve Type: ^/D -

C&

General Condition:

Comments:

Good

Valve Condition:

Comments:

Good

Pre-operation Weight:

Approved to Handle:

Handling Precautions:

Approved for Valve Sampling:

Sample Method:

Comments:

Sample Date: <0 ' ^ ? "

Identified Contents:_

Analytical Method:

Disposition:

L

Fair Poor

Fair Poor

Post-operation Weight:

Yes t^^"

Yes

Large CRV Small CRV

Pressure:

~ VMass Spec

HyJ,

FTIR

No

No

Val

Other

Caustic Scrub

Recontainerized:

Recontalnerlzed Cylinder

Acid Scrub .______ Oxidizing Carbon

Mole Sieve ______ Flare

Yes No

disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan.'

30B2G1

•t-1-4

.

jr,

—J

;.*fc

'.De-a

tr;«

r; *•; M"<:,' c*-

.CKS

la".'

'-. — 3

- - LO

L?!

cccv?CDoCO

£98908

inn [~{r-\ :W-.

en^r20ft-

KI 9111 ex i if • i i r-, , rrr. : »»rf i I •: 1 T T Ti l*% 1 it

ft1

- T?M

-9

«'• ^ -r I - * A „ > J f t" ^4 I

r v •' ' .-' L '.• C t ' 'J r

, . . , . — .,, . ,., ... ... ,- .. . .

I - —••"••• — - •1

:•;

it: •- . "i .. i. -,i- , . .- I • . f :• -.'

:.UJ|V V / •.••''..-*>• •-.•••,-.-

<

,:j-j.£!

!

!

i

;

.• , .' . Jj

::;':;-::!

i•; i •' •<

oo ; ;J

0 i: V)-

C7DfOCD

.., ..... . ., ... . ...., ............. , ,. r - ^ - - - •

f^".'-\,-Yi; i/!;;;;:^;::

) i ; '; L

"VI

.,:/::' . • j r:^n /-. i.i i . • • %!•

, , • n. - - ••, -, ,. -t

'

Cur'.'j; O'i:':; !•';••i t -i i i i

i'^il. i.;ij: •-:::].•••? }>-i. ;o:j i---~

i,i^:.!i-" ••:;

'!. ;

5.t";;i i'':;''' •

"

; r

;::

• •';-', .

• .

i?V(A, ,

:'i

,' '".. — ;--^-— ,-;^- "'".^r:", —— """";..";:~". ," ;';i' ?-li**' f ' ',

•'•V| ',

1 i n /"i " •"• • • - j . i). ifi" ~fj i i:

••••--,--———— -•-,._ ,. ., ,- '.....- \\' '-••• •

;,'.-' I ',

V 1 V.\\ 1 li {

•... i _ji

i iI :1

i

•]

iI:

?:, S-:f;li^'.'t; and Sr-, •..-.; i

•i n

ju'^eJio^pin^•i^-i; ;.>cr;;xjit

G9^90C

; ..<*.- -,• -•

• f i. t—-£, ; ^

v~ ui 5 i -

HI ' spou -r- u r ? •:3 : uo t ^.^:•: i p z-dy^ L_; '£• — t : - « .'""'• ~ - d ^ :"

T _ U t —, ••*, ,-v • J ,

9989

08

>. :••-

•"-|-

1 ....

M ., I' !5 i ! IV

C'. b 1--

\i .

.., ..

.....

... i

i f -i1

i..,,,

.„.„ ..

...W

.....<

V

,

-

i .i-

'v I •

c p:

1

-1- .:-. r •

!! \i

L:

L ••--

.- -:

• s

r--;

••.;:

:

I.._

-

-i

• •-

. .-

• y

.;

: kc

i "i

-ft:

,. .

!I

> -•

. -

. I

. -_: :; o L '.:. t i o PI

l_l -•—. _ _Tt Cj C c.\ . . '.i

S;:c-J

Cbs. T i n ; Ll t.! J t^ C

'' ""l ct i

i:- s a ri s p j. i -; ; e j-M p o d i z c-» t i o n

" -K- •* * ->f ->: -:i * t -fr V *• »• -A i=:

_

306267

Form 9

DAILY SAFETY MEETING

DATE: /G //?C"1/

TIME:

CYLINDER MANAGEMENT PROJECT FOR:

EMPLOYEES PRESENT:

l/d/J S.^-nt/^fc1. & &

A ^ f c /tV 752. _ CT A fife-tV 75-

3. _

4. _

5- _

6. _

7. _

8. _

9- _

10.

PLANNED ACIVITIES:

TOPICS DISCUSSED:

'Use or disclosure of the data contained on this sheet is subject to therestrictions on the title page of this plan.'

306268

Form 9


•//£/DATE: / 6 //.

TIME: ~ A.


EMPLOYEES PRESENT:

1. _

2. ______

3. _ £.

4. _

5.

S" •-rz^AK.'TI- /1*JJ*

6. ____0_

1. _____ I ,

8. ___

9. ___

10.

PLANNED ACTIVITIES: /

Sc-f-

TOPICS DISCUSSED:

O Ti P p fi Qor disclosure of the data contained on this sheet is subject to the \J\J\J£,\J\J

restrictions on the title page of this plan.'

Form 9


DATE:/ /

TIME: ;


EMPLOYEES PRESENT:

/£V l/tl* Sc/Itit/<1. ____

2.

3. ________£ L\J: ///A*- J.

4. L. 5-^,^-15. __g.6. ______(J.

7. ____ ~T

8. ____

9. ____

10.

PLANNED ACTIVITIES:

G £*j£/i

TOPICS DISCUSSED:

/fx/y 7^57^

'Use or disclosure of the data contained on this sheet is subject to the O U D <« * Urestrictions on the title page of this plan. '

Form 9


DATE:/ /

TIME:


EMPLOYEES PRESENT:

2. _____

3. ^-

4. ____L_

5. (l__

6. __ ()'

7. __

8. __

9. __

10.

g. ^'11^ Ut*)

PLANNED ACTIVITIES:

' G F .5& /-

/^s t///^t-/g^5 >/g:-77rg ofy

TOPICS DISCUSSED:

r

'Use or disclosure of the data contained on this sheet is subject to thesure or tne oata contained on tnis sneet is suojeci to tne O A C* O *"} 1restrictions on the title page of this plan.' O U D £ ( 1

Form 9


DATE: __

TIME:

/?. 1/4/b

CYLINDER MANAGEMENT PROJECT FOR

EMPLOYEES PRESENT:

1. _

2. _

3. ___

4. ________

5- ^-

6. _£_7- ^T

8. _____U .

9. ________

10. _______

PLANNED ACTIVITIES:

Sc-£-ttn

ft If

TOPICS DISCUSSED:

"Use oc disclosure of the data contained on this sheet is subject to the O U U ^ ' *•restrictions on the title page of this plan.'

Form 9


DATE:7 7^

TIME:


EMPLOYEES PRESENT:

1. __

2. __

3.

4. / • 5 'TiC^'l * T

5. C. A6. ___

7. ____

8. ___

9. ____

10.

PLANNED ACTIVITIES:

C- - fll

TOPICS DISCUSSED:


Form 9


DATE: J0_r**S-

TIME:

CYLINDER MANAGEMENT PROJECT FOR: //X/fX //}

EMPLOYEES PRESENT:

2.

3.

4.

5.

6.

~1- A.//!& A

8.

10.

PLANNED ACTIVITIES:

TOPICS DISCUSSED:

/- disclosure of the data contained on this sheet is subject to the U U »D ^ I 4restrictions on the title page of this plan."

Form 9


DATE:

TIME:


EMPLOYEES PRESENT:

i.2.

3.

4.

5.

6.

7.8.

9.

10.

PLANNED ACTIVITIES

-^

TOPICS DISCUSSED:

/ x

or disclosure of the data contained on this sheet is subject to the Q p. r» Q M frestrictions on the title page of this plan. ' O U U £> ' «'

Form 9


DATE: //) - 7

TIME:


EMPLOYEES PRESENT:

2.

3.

5.

6.

7.

8.

Q

10.

PLANNED ACTIVITIES:

TOPICS DISCUSSED:

st f- -

or disclosure of the data contained on (his sheet /s subject to therestrictions on the title page of this plan. '

*3 (\ C O *7 C

Form 9


DATE:

TIME:


EMPLOYEES PRESENT:

2. Z

o

4. (/-'

6.

7.

8.

10. /

PLANNED ACTIVITIES:

TOPICS DISCUSSED:

"C/se or disclosure of the data contained on this sheet is subject to therestrictions on the title page of this plan. '

306277

Form 9


DATE:

TIME:


EMPLOYEES PRESENT:

2.

3.

4.

5.

6.

8.

9.

10.

PLANNED ACTIVITIES:

TOPICS DISCUSSED:

"C/se or disclosure of the data contained on this sheet is subject to the «J U U *« • Orestrictions on the title page of this plan. '

Form 9


DATE: //- J>-

TIME:


EMPLOYEES PRESENT:

1 -7 S7 aI • //TJ^J Lryf/.

2.

3.

4.

5.

6.

8.

9.

10.

PLANNED ACTIVITIES:

TOPICS DISCUSSED:

or disclosure of the data contained on this sheet /s subject to the O U U ^ I Urestrictions on the title page of this plan. '

Form 9


DATE: //-3-?</

TIME: j


EMPLOYEES PRESENT:

1.

2.

3.

4.

5.

6.

7.

8.

10.

PLANNED ACTIVITIES:

Zs f----

TOPICS DISCUSSED:

306280'i/se or disclosure of the data contained on this sheet ;s subject to the


Form 9


DATE:

TIME:

CYLINDER MANAGEMENT PROJECT FOR:.X

EMPLOYEES PRESENT:

1.

2. fe

3.

4.

6.

7.

8.

Q

10.

PLANNED ACTIVITIES:

TOPICS DISCUSSED:

"L/se or disclosure of the data contained on this sheet is subject to the O 0 O *restrictions on the title page of this plan. '

Form 1

QUALITY CONTROL DAILY REPORT Page 1 of 2

PROJECT N«

WEATHER

/?<y<?y.3fo^/FA,*, TEMP. WIN.

DATE /o-J«-?*'TEMP. MAX.

/

1. Phase of operation in progress: ~7%'?'Z5f><Mft "<? £t//. {Z^.t/ £ tf/"? teg'tL

2. Results of operational check:

A. SAFETY EQUIPMENT CHECK:

If not, list deficiencies:

SUPPLIED AIR EQUIPMENT INCLUDES:

Compressor(10kavjxAir Lines (Okay)Air Bank (Okay)MasksctCkayV

5 Min Packs (Okay)

MONITORING EQUIPMENT:

Explosion/02 Meter <£OkayVHNudgkayiDetector Tubes

B. Cylinder Recovery Vessel'Hydraulic SystemPneumaticPumps (Vac &Pressure Temp. ReadoutsClQjcIFyj}

List Deficiencies

Other Deficiencies

'Use or disclosure of data contained on this sheet is subject to therestrictions on th» title page of this plan.' 306282

Form 1


C. HazGAS" (Okay)Pneumatic System (Okay)Pumps (Okay)Pressure Temp. Readouts (Okay)Valves (Okay)Video (Okay)Other Deficiencies

-,

NOTE: Deficiencies listed will be recorded in the maintenance log by date andreport number.

3. Verbal instructions - received from Client Representative on deficiencies or retesting required:

4. Remarks:

SIGNATURE OF PROJECT MANAGER

5. CERTIFICATION: I certify that the above report is complete and correct, and that all material andequipment used and work performed during this reporting period are in strict compliance with the plansand specifications except as may be noted above.

AUTHORIZED REPRESENTATIVE

'Use or disclosure of data contained on this sheet is subject to the O 0 D 2 8 Srestrictions on the title page of this plan. '

Form 1


PROJECT N«

WEATHER Cc& /^k TEMP. MIN.

DATE

ft*?

lo -(3S-9<s

TEMP. MAX.

1. Phase of operation in progress: v^V/// '/?t 'fc-rr



. If not, list deficiencies:


B.

CompressorAir Lines (Okay)Air Bank (Okay)MasksSCBA's <5 Min Packs (Okay)


Explosion/02 Meter {Gjcfy?HNugjgtgjJDetector Tubes t ?£J

Cylinder Recovery VesseRCRVfHydraulic SystendQ^T)Pneumatic Systemcfflla^VPumps (Vac & Comp)Pressure Temp. ReadoutsValves

List Deficiencies

Other Deficiencies

'Use or disclosure of deta contained on this sheet is subject to therestrictions on the title paga of this plan.' 306284

Form 1


C. HazGAS™ (Okay)Pneumatic System (Okay)Pumps (Okay)Pressure Temp. Readouts (Okay) ————————ff /'/AValves (Okay) ———————/ //Video (Okay) ————————————Other Deficiencies ————————————



4. Remarks:




'Use or disclosure of data contained on this sheet is subject to thelosure of data contained on this sheet is subject to the Q /"I £? O C) r-restrictions on the title page of this plan.' \J \J O C O J

Form 1


PROJECT N«

WEATHER

&<*></ 3~&n>lfa TEMP. MIN.

DATE

^'^

JO -d*. 5V

TEMP. MAX.

/

1. Phase of operation in progress: ^/2/// "fiflP 3)J?dCf5'S '?. ~7s~>?-'



Suits <{Cf£ayi. If not, list deficiencies:


Compressor (Okay)Air Lines (Okay)Air Bank (Okay)

SCBA'scGgay)5 Min Packs (Okay)


Explosion/02

Detector Tubes<^0^>

B. Cylinder Recovery VesselHydraulic SysterrK£0^|y)PneumaticPumps (Vac &Pressure Temp. Readouts

List Deficiencies

Other Deficiencies

'Use or disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan.' 306286

Form 1


C. HazGAS" (Okay) ——————————————Pneumatic System (Okay) ————————————-j—Pumps (Okay) ————————>.—) f *Pressure Temp. Readouts (Okay) ——————— / } . ' /^yValves (Okay) ——————L——! IVideo (Okay) —————————————Other Deficiencies —————————————



4. Remarks:




'Use or disclosure of data contained on this sheet is subject to the 306287restrictions on the title page of this plan.'

Form 1


PROJECT N«

WEATHER

WW^**y>Ja^ TEMP. WIN.

DATE /& -<p:7-ryTEMP. MAX.

1. Phase of operation in progress: 2-4// /jf^7£> /^tftie^ss ^- Tfr^-^



). If not, list deficiencies:


Compressor (2£ayfAir Lines (Okay)Air Bank (Okay)MasksSCBA's5 Min Packs (Okay)


Explosion/02 Meter KJEfJ}

Detector Tubes

B. Cylinder Recovery VesselHydraulicPneumatic SystemPumps (Vac & Comp) g&Pressure Temp. Readouts

VideoOther Deficiencies

List Deficiencies

'Use or disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan.' :06288

Form 1


C. HazGAS" (Okay)Pneumatic System (Okay)Pumps (Okay)Pressure Temp. Readouts (Okay)Valves (Okay)Video (Okay)Other Deficiencies

mNOTE: Deficiencies listed will be recorded in the maintenance log by date and

report number.


4. Remarks:




'Use or disclosure of data contained on this sheet is subject to the O U U C Q «Jrestrictions on the title page of this plan. '

Form 1


PROJECT N«

WEATHER

tfW^

TEMP. M1N.

DATE /t>-j.?-9<tTEMP. MAX.

1. Phase of operation in progress: £fo(?f'Z''> ^ 7&?i C-6r///7b££>



). 'f n°t. list deficiencies:

SUPPLIED AIR EQUIPMENT INCLUDES: List Deficiencies

Air Lines (Okay)Air Bank (Okay)

SCBA's5 Min Packs (Okay)


Explosion/02

HNu (Okay)Detector

B. Cylinder Recovery VesselHydraulicPneumaticPumps (Vac & Comp)Pressure Temp. Readouts

Other Deficiencies

'Use or disclosure of data contained on this sheet is subject to therestrictions on the title p»g» of this plan.' 306290

Form 1


C. HazGAS™ (Okay! ————————————————Pneumatic System (Okay) ———————————— . — J.

————————— - — —-Pumps (Okay) -A ..Pressure Temp. Readouts (Okay) ———————— ./

Valves (Okay)Video (Okay)Other Deficiencies



4. Remarks:




'Use or disclosure of data contained on this sheet is subject to the ^\ 0 D 2 vJ 1restrictions on the title page of this plan.'

Form 1


PROJECT N«

WEATHER

>cf</£>mTEMP. MIN.

DATE /& -3'- 94TEMP. MAX.

1 . Phase of operation in progress: OftZXleSS /Z- 7<?>' <Z.*/ /Js/£t<^



Suits (Q£ay£ If not. list deficiencies:

SUPPLIED AIR EQUIPMENT INCLUDES: List Deficiencies

CompressorAir Lines (Okay)Air Bank (Okay)Masks fQfcfy)SCBA's tS£a&5 Min Packs (Okay)


Exp!osion/02 MeterHNu-tSiDetector

B. Cylinder Recovery VesselHydraulic SystemPneumatic SystemPumps (Vac & Comp)Pressure Temp. Readouts (Olcasli

Other Deficiencies

'Use or disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan.' 30R292

Form 1


C. HazGAS" (Okay) —————————Pneumatic System (Okay) ————————Pumps (Okay) ———————-t-Pressure Temp. Readouts (Okay) ——————AValves (Okay) ——————/U7/ / IVideo (Okay) ————————Other Deficiencies ————————



4. Remarks:



' AUTHORIZED REPRESENTATIVE

'Ust or disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan. '

Form 1


PROJECT N«

WEATHER

MW3.TEMP. MIN.

DATE / / - / -^TEMP. MAX.

1. Phase of operation in progress: <7ffi<3CFS 5" ^2. /&?? (^?&'//s7/)f>£>



Suits If not, list deficiencies:


Compressor (tpjay?Air Lines (Okay)Air Bank (Okay)Masks tfSay?

B.

5 Min Packs (Okay)


Ej(plosion/02 MeterHNuct2B$>Detector Tubes

Cylinder Recovery Vessel <Hydraulic System fgfcaS?Pneumatic System <t0E§JPPumps (Vac & Comp) XOTcaJPPressure Temp. Readouts <fd£|jj

List Deficiencies

Other -""Deficiencies

'Ust or disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan.' 306294

Form 1


C. HazGAS™ (Okay) —————————————Pneumatic System (Okay) ———————————— ,

———————— - — —-—L

Pumps (Okay) ————————jPressure Temp. Readouts (Okay) ———————JLValves (Okay) ——————/ \.t IVideo (Okay) ———————————Other Deficiencies ———————————



4. Remarks:




'Use or disclosure of data contained on this sheet is subject to the O /"• P O Q f!restrictions on the title page of this plan.' O \J \J £. O \)

Form 1


PROJECT N«

WEATHER

Ifaort

1. Phase of operation in progress


TEMP. MIN.

DATE //•<P-9yTEMP. MAX.

ofta^r ^ -72™ *»****»*. s,./^~./ ' ' '


Suits . If not, list deficiencies:


B.

CompressorAir Lines (Okay)Air Bank (Okay)Masks {OffifiSCBA's {QlEy}5 Min Packs (Okay)


Explosion/Oj Meter (OJ35>HNu frPklrzkDetector Tubes Kjka$1

Cylinder Recovery Vessel ((Hydraulic System (0jtf^Pneumatic System {tfitay^lPumps (Vac & Comp) (Qg;Pressure Temp. Readouts tValves ({^kj PVideo (O^yfOther Deficiencies

List Deficiencies

'Use or disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan.' 106296

Form 1


C. HazGAS" (Okay) ———————Pneumatic System (Okay) ———————Pumps (Okay) ———————Pressure Temp. Readouts (Okay) ————————Valves (Okay) ———————/Video (Okay) ———————Other Deficiencies ———————



4. Remarks:



' AUTHORIZED REPRESENTATIVE

'Use or disclosure of data contained on this sheet is subject to the Q Cl C O Q **)restrictions on the title page of this plan.'

Form 1


PROJECT N«

WEATHER

/9W3TEMP. MIN.

DATE S/-3-9*TEMP. MAX.

1 . Phase of operation in progress: £>/}JCe'^3 ^z. 7&>? £?**//» £>fi.



Suits fcQSy). If not, list deficiencies:


Compressor <Qk2y>)Air Lines (Okay)Air Bank (Okay)

5 Min Packs (Okay)


Explosion/Oj Meter <QSE^

Detector

B. Cylinder Recovery VesselHydraulic System jQZayfrPneumaticPumps (Vac & Comp)Pressure Temp.

Video Ig^aJ3

Other Deficiencies

List Deficiencies

*L/s» or disclosure of data contained on this sheet is subject to therestrictions on the title page of this plan.' 306298

Form 1


C. HazGAS™ (Okay) —————————————Pneumatic System (Okay) ————————————?—Pumps (Okay) —————————J J APressure Temp. Readouts (Okay) ——————fl/ ///Valves (Okay) _____L——L_LVideo (Okay) _______________________Other Deficiencies ————————————————————————



4. Remarks:




'Use or disclosure of data contained on this sheet is subject to the O U O <w U !jrestrictions on the title page of this plan.'

/

This Page Was Intentionally Left Blank.

30S300

Form 7CONFINED SPACE ENTRY PERMIT Page 1 of 2

A permit is required for entering any tank or enclosed space for any purpose and may be grantedonly in accordance with review and approval by the Health and Safety Officer.

This permit can be used only during the date and time specified. Additional permits must be usedfor different dates and extended time periods - No Exceptions.

SITE:

LOCATION:

PURPOSE:

/O, (/.-

ENTRY DATE: /6' • &</-

TIME:

Person(s) to enter confined space:/? c h>f4 75 _____

Standby person(s):

Entry Conditions:1. All vessel inlet lines locked out?

2. All electrical switches locked out?

3. Vessel atmosphere tested for flammable concentration?

4. Vessel atmosphere tested for poisonous gases?

5. Surrounding area checked for flammable and/or poisonousgases?

6. Vessel tested for oxygen deficiency?

7. Standby person(s) assigned and properly instructed?

8. Persons properly instructed for safe entry into vessel?

9. Rescue harness provided?

10. Lifeline attached?

'Use or disclosure of the data contained on this sheet /s subject to therestrictions on the title page of this plan. '

Necessary

Yes/Not Necessary"

<Yes7Not Necessary

Necessary

Ye^TNot Necessar/J?

Necessary

Necessary

Necessary

Form 7CONFINED SPACE ENTRY PERMIT

11. Rescue equipment available?

12. PPE provided and worn?

ATMOSPHERIC ANALYSIS:

Lower Explosive Limit (LED Analysis:

Oxygen Content Analysis:

Additional Precautionary Remarks:

mg/m3 or ppm

mg/m3 or ppm

mg/m3 or ppm

Page 2 of 2

Necessary

Necessary

Time:

Time:

Time:

I certify that all necessary precautions have been taken to make this confined space entry job safe

for entering and carrying on the prescribed work.

Project Manager:

Site Supervisor:

Field Technician:

Field Technician:

Field Technician: _____

Approval for entry:

Health and Safety Off icer:

Date:

Q-Y-e's D No

Date:

Date:

Date:

Date:

Date:

Time:

'Use or disclosure of the data contained on this sheet is subject to therestrictions on the title page of this plan. '

r\ 0630:


A permit is required for entering any tank or enclosed space for any purpose and may be granteonly in accordance with review and approval by the Health and Safety Off icer.


LOCATION:

PURPOSE:

ENTRY DATE:

TIME: £ TO:

Person(s) to enter confined space:

Standby person(s):












"SSsYNot Necessary

Necessary

Necessary

306303





mg/m3 or ppm

mg/m3 or ppm

mg/m3 or ppm

Page 2 of 2

Necessary

Necessary

Time:

Lower Explosive Limit (LED Analysis: Time:



% Time:



Project Manager:

Site Supervisor:

Field Technician:

Field Technician:

Date:

Date:

Date:

Date:

/ i

Field Technician: Date:

Approval for entry: D No

Health and Safety Officer: d

Date: Time:

'Use or disclosure of the data contained on this sheet is subject to therestrictions on the title page of this plan. ' 306304

Form 7CONFINED SPACE ENTRY PERMIT Page J of 2

A permit is required for entering any tank or enclosed space for any purpose and may be grantedonly in accordance with review and approval by the Health and Safety Officer.


SITE:

LOCATION:

PURPOSE:

ENTRY DATE: fd -<3 & ' *2 </

TIME: 8 TO:Personis) to enter confined space:

Standby person(s):

xsEntry Conditions:

1. All vessel inlet lines locked out?










</Yjjl#Slot Necessary

Necessary

Necessary

Necessary

Y e

0630n'Use or disclosure of the data contained on this sheet /5 subject to the






mg/m3 or ppm

mg/m3 or ppm

mg/mj or ppm

Page 2 of 2

Yes/Not Necessary

Yes/Not Necessary

Time:

Lower Explosive Limit (LED Analysis: Time:



Time:



Project Manager: Date:

Site Supervisor:

Field Technician:

Field Technician:

Field Technician:

Approval for entry:

Health and Safety Officer:

Date:

Date:

0"Yes D No

-J?

Date: {0 2.^-9 </

Date: .

Time:


30630G


A permit is required for entering any tank or enclosed space for any purpose and may be gronly in accordance with review and approval by the Health and Safety Officer.


SITE:

LOCATION:

PURPOSE:

fik&s

ENTRY DATE:

TIME: TO:


Standby person(s):












Necessary

Necessary

Necessary

Necessary

Necessary

Necessary

306307






Oxygen Content


mg/m3 or ppm

mg/m3 or ppm

mg/m3 or ppm

%

Page 2 of 2

Necessar

Necessary

Time:

Time:

Time:



Project Manager: Date:

Site Supervisor:

Field Technician:

Field Technician:

Field Technician:

Approval for entry:


B-Tes D No

Date:

Date:

Date:

Date:

Time:

'Use or disclosure of the data contained on this sheet is subject to therestrictions on the title page of this plan. ' 306308


A permit is required for entering any tank or enclosed space for any purpose and may be granteeonly in accordance with review and approval by the Health and Safety Officer.

This permit can be used only during the date and time specif ied. Additional permits must be usedfor different dates and extended time periods • No Exceptions.

SITE:

LOCATION:

PURPOSE:/* Lf/'f/bfO

/

ENTRY DATE:

TIME: X TO:


Standby person(s):

AS











Necessary

t^ecesjar

Necessary

Necessary

Necessary

Necessary

j£ef)Not Necessary

Y e s (NoTNe cl3s?aZv>


306309








mg/m1 or ppm

mg/mj or ppm

mg/mj or ppm

Page 2 of 2

Yes/Not Necessar-

Yes/Not Necessary

Time:

Time:

% Time:



Project Manager:

Site Supervisor:

Field Technician:

Field Technician:

Field Technician:

Approval for entry:

Health and Safety Offi

Date: /I

£XYes D No

Date:

Date:

Date: J$ •£% •<?(/

Date:

Time:


306310


A permit is required for entering any tank or enclosed space for any purpose and may be granteonly in accordance with review and approval by the Health and Safety Officer.


SITE:LOCATION: ffi&TTI

PURPOSE: ,

ENTRY DATE:

TIME:

~3/-


Standby person(s):











01 Necessary

Necessary

Necessary

frtefejsajy1

Necessary

Necessary

Necessary

Yes/NorNgceTsaTy^

'Use or disclosure of Iht data contained on this sheet is subject to therestrictions on the title page of this plan. '

306311






Oxygen Content Analysis: //, 7


mg/m3 or ppm

mg/mj or ppm

mg/m1 or ppm

Page 2 of 2

)t Necessary

Jot Necessary

Time:

Time:

Time:



Project Manager:

Site Supervisor:

Field Technician:

Field Technician:

Date:

Date:

Date:

Date:

Field Technician:

Approval for entry:

Health and Safety Officer:

Date:

D No

Date:

Time:

'Use or disclosure of the data contained on this sheer is subject to therestrictions on the title page of this plan. '

306312



This permit can be used only during the date and time specified. Additional permits must be usedfor dif ferent dates and extended time periods - No Exceptions.

LOCATION:

PURPOSE:

ENTRY DATE: //- /-

TIME:


Standby person(s):











ot Necessary

Necessary

Necessary

'Use or disclosure of the data contained on this sheer is subject to therestrictions on the title page of this plan. '

306313





Lower Explosive Limit (LEL) Analysis:

Oxygen Content Analysis: ___/<-)•


mg/m1 or ppm

mg/m3 or ppm

mg/mj or ppm

Page 2 of 2

ot Necessa

Jot Necessai,

Time:

Time:

Time: /l



Project Manager: _

Site Supervisor: _

Field Technician: _

Field Technician: _

Field Technician: _

Approval for entry:

Health and Safety Officer;

Date: //-/-<?«/

D No

Date:

Date:

Date:

Date:

Date:

Time:


306314




SITE: /?7/rV7/f

LOCATION: /?/,'/ 7%

PURPOSE:7)>

ENTRY DATE: U_

TIME: TO:


Standby person(s):

- AS











Necessary

Y e

Necessary

Necessary

Yes ffiffiT" N

Necessary

cSSsTNot Necessary

Necessary

'Use or disclosure of the data contained on this sheet is subject ro therestrictions on the title page of this plan. '

30631:r;






mg/m3 or ppm

mg/m1 or ppm

mg/m3 or ppm

Page 2 of 2

Necessary

Necessary

Time:

Time:



% Time:



Project Manager:

Site Supervisor:

Date:

Date:

Field Technician: Date:

Field Technician:

Field Technician:

Approval for entry:


Q-Yes" D No

, (

Date: //-

Date:

Date:

Time:


30631H


A permit is required for entering any tank or enclosed space for any purpose and may be gnonly in accordance with review and approval by the Health and Safety Off icer.


SITE: (.

LOCATION:

PURPOSE:

ENTRY DATE:

TIME: J?. TO:


Standby person(s):







1'. Standby person(s) assigned and properly instructed?




Necessary

Necessary

Necessary

fifisssacs

Necessary

Necessary

Necessary

YestfJot

'Use Of disclosure of the data contained on this sheet is subject to therestrictions on the tills page of this plan. '

30R317








mg/m1 or ppm

mg/m3 or ppm

mg/m* or ppm

Page 2 of 2

Jot Necessa

'Yes<JNot Necessary

Time:

Time:

Time:



Project Manager:

Site Supervisor:

Field Technician:

Field Technician:

Field Technician:

Approval for entry:

Health and Safety

Date: //- 3 -9<f

D No

Date:

Date:

Date:

Date:

Date:

Time:

'Use o/ disclosure of the data contained on this sheet is subject to therestrictions on r/)e ;/'f/« page of this plan. '

306318

Form 11

AIR ANALYSIS DATA

Date: it> -.J V -

SUSPECTED COMPOUNDS EXPOSURE LIP.'.ITS ERC'S ACTION LEVELS

1)

2)

3)

TIME

LOCATION /L^. <- /

TEMPERATURE

WINDDIRECTION

0- / 4/SJ.

WEATHERCONDITION

OVA-128 orHNu C

EXPLOSI-OZMETER

READING(s)ppm 0

COMPOUND(s)

SURVEYOR'SINITIALS sf.J.

Field Calibration for OVA-128:

Calibration Gas Used: Potentiometer Setting: Instrument Reading:

o/- disclosure of ihe data ccntained on :.-,s sheet /i sub/ect lo therestrictions en the title page o! this plan. '

306319

Form 11

AIR ANALYSIS DATA

Date:

SUSPECTED COMPOUNDS EXPOSURE LIMITS ERG'S ACTION LEVELS

1)

21

3)

TIME

LOCATION

TEMPERATURE

1*5WIND

DIRECTIONmpt)

•3. j.WEATHER

CONDITION

OVA-128 orHNu

-£LEXPLOSI-Oj

METER

"77 ^^T^ 7* ~rr

READING(s)ppm

£ A.COMPOUND(s)

SJ/t

SURVEYOR'SINITIALS


Calibration Gas Used: Potentiometer Setting: Instrument Reading:

O

'Use of d.siiasute of the da;a contained on :his sheet is subject to therestrictions on the title page ol this plan. '

306320

Form 11

AIR ANALYSIS DATA

Date: If)

SUSPECTED COMPOUNDS EXPOSURE LIMITS ERC'S ACTION LEVELS

1)

2)

3)

TIME

LOCATION

TEMPERATURE

WINDDIRECTION

WEATHERCONDITION

OVA-128 orHNu

EXPLOSI-OjMETER

READING(s)ppm

COMPOUND(s)

SURVEYOR'SINITIALS

#'*2?

Mm-yj'ft>~:i/xpt+

<s.(fu*

?f.$.

r*. . £^ /0£t>


Calibration Gas Used: Potentiometer Setting:

?. M______

Instrument Reading:

'Use or disclosure of the data contained on this sheet is subject !o therestriction! on the title page of this plan. '

306321

Appendix CWaste Profile Analytical Results

306323

aUNITEDINDUSTRIAL.

VICES. INC-

No.

WASTE STREAM PROFILE SHEET

I _______p l>-f>^. , *-r- ~ I-.K1___________,——————————." Coo-act ^^.-^ urJ m~€--r phone r/fl- *rz- <KL<t.

Shipping ContaclBusiness ContactEPA I O NumOer

resi A?6 Cracev Ave.Meriden. CT

(2O3) 238-6n NJ,.-TI»O. CTD02l866a9

DESCRIPTIOhCoerrvcal f. Physical Slalas

TL.qu.—— ————S^m,OSoi.d

PROCESS DESCRIPTION ^^ _______ . ______________ ——————————— —rat.n waste stream Please include a list ol vrgm male,,ais and ihe-r Malcr.ai Safety Data Sheets

kjof-oro A-rl-

T-OC4-

CHEMICAL CONSTITUENTSPetroleum Phase Suspecteo Leveii Aclija' Levelspce-s A/D<2-aiooens ^ l\SolventsA'senic (AsiCadmium fCd) .Chromium fCr) \ /Lead (Pbl ' '

T

SHIPPING INFORMATIONU DOT Regulated Material O Non-Regulated

DOT Maimrd Class A/C>/J':

OOT Shipping N«m« C. 7" /?£Q iJLfi J f. f} VJS)( T 1-Rooortatjle Quantity 'J

UN/NA Number fJr> /J i;Amount of Waste Per Shioment 3*1Fr-Quency of Shipments

Please submit a one (1) quart representative sample of tr"»waste stream Also describe the sampling method below.

/~\ \ r^ (^^-OV\pe_J* "T A Q.y^£i\e Â-TciyvV "TUÔ

__ i / \0*3 â_Uo,vi Q<~i_<,v>v5 ^"^"ÔB *K>O. I O04-^

FACILITYReceived On.Sarnple ContamorCommonts:

Aqueous Phase SuSoecteC Levels Actual _^Copper (Cu) f' C/3Cad-n.urn ;Cd) ^^Chromium (Cr) ^//.Lead ;Pt>) Ao?"VArser"c (As) r\j f3.SrxJu.m ;Na)Barium (8a)Tin (Sn) -_7NiCHel (Ni) f-} / 4.

Silver (Ag) j°"5. O/Zinc (Zn) n Q"^

Phenols _ , ,. — \ AJ-i-

This Waste is:CJRCRA Listed -OCOA lumbarCJ State Peculated State Number C RO^^jNon- Regu'atedIJ\/i»gin KXff'9ria<

Notes & Spectat HgiPKjIirg Information

•— --.-m -. ..—», »_i » .__- .... -._ -„_-_« __._. .-»_„-, _^«_. i,,,,. ,_. ii -i, , _

•"" ' ———— ™*~ — ' —— ~ —— '-' ———— - ——— '"* —— "• ——— 'r /T<^\ i r * ^^^ **' J * »- • l-F i TII .1 n n_ » im i ii ii ^_ i i_.

. —— 1^_ — ".ir.-.., . __ , _S.anat_«e iSiuÔ?" Jr>T. [\ticM "*" T / ' ""

USE ONL^ '

Approved/Roj»d«cJ By J1^/*-^- Date:/ ' . ' y'-' '^

306324

oUN1TKOmpu.T!«>JNC<

MIMIOCN. CT Oa4M (JOO) J3S.17S3. » WASTE »TR6AM PROP".! SHEET

l * Phyaloal StajaaO Liputc) UfMultilavfraO pH O?'4 CJB-lO

. liquid QaHA/arad *'6Pha»a

TSS .ColO'

Pom!

No.prdiie

Bottom

A»h. SpGC.IIe Gravity

prates* ganpratl^o w»»ta atreaov Pl*a»e include a list o» virgin material! and their Material 5«f»ly Data Shaais

C coo used \ tfT

wHa

CHEMICAL CONSTITUENTS

8o!v«ntAAraanic (Aj)Cadmium (Cd)Chramium (Cr)Lead (Pi>)»t»a»aU»t /) Lj Q~ / <*^

AOUOCUB Phat*Cooper (Cu)

(Cf)

Arienie (Aa;Sodium [Na)Barlwm CBft)

Zinc (Zn)Pri»nol»

(GN)

Suocxctaa L»v«lc Actual LI

K^a

INFORMATION

DOT Haiara Clfta* _DOT Shipping N»m»R»portable QuantityUN/NA Numftar

Nen-Raguiat*dThi»Wact»iOPiCRA LlstadOat ate n«gulalac)

RCHA Numb«rState Numb«' _

Amount ol Wa»t« Par Sfney ol SMIpmonti

-asLin Malarial

Nptet A Spac-al Handling in.'orrnBlign ,

"leaia tubmil a on* (1) quart reore*»n(atlva cample o< ^wiiitia alroam Also floscrtbo |h« aamplInQ m»<hod balow.

''^ lOTAM^^rttfvolMIPWH

Signature ___Titla ______

-ri^»ivi». j^nm.>c»»

Omia

On:Sampla Container.

USE ONLY

By-

306325

Date Sar.ples Received : 11-18-94

Client Name: United Oil Recovery inc.Report Date: 11-21-94

CTL Lab No. 114-170-1P?0/Job No. 94-1393

RESULTS OF ANALYSIS

EPA 8080

Matrix TypaCTL Sample No.Field ID

Total FCB's-ppb____

W1446794-1393

ND<1

Matrix Types : W = Water/AqueousS = Soil/SolidO •= Oil/Hydrocarbons

CONNECTICUT TESTING LABORATORIES. INC.165 Gracey Avenue / Meriden, CT 06451-2268

(203)-634-3731Connecticut Certification No. PH-0547

306326

November 21, 1994

United Oil Recover)' Inc.136 Gracev Ave.Meriden, CT 06450Attn: Mr. David Carabetta

Please find attached laboratory report(s) for the samples submitted on :November 18, 1994

All pertinent information for this analysis is located on the report. Should it benecessary to contact us regarding billing and or the test results, please have thefollowing information readily available :

LAB No. I 114-170-1?PO/JOB No. ; 94-1393INVOICE NO. : 47924ORDER No. : 27853CUSTOMER No.: 319

Please feel free to contact us if you have any questions.

Very truly yours,

Stephen J. FrancoLaboratory DirectorPH-0547

Connecticuttesting

=-- - WATER • SOIL • AIR

STEPHEN J.FRANCOLaboratory Director

inc. PHONE • 203/634-3731165 CRACEY AVENUE • MERIDEN. CTB 0645'

306327

UNITEDINDUSTRIAL No.

lit GRACtV AVENUE ME«IOEN CTOMSO :2<XJ12DST7S3WASTE STREAM

Profile * f-MI T-l '-/•ooncn F IHPPT ^ Da'° Submmeo

•f GFNEHATOR ! BROKER OR SALESPERSONx- p^ \^ P^L.0Jf fo*^ Arwo. £. j.*rkWu»J T V4t» iNnrr-- ft*a ^. N „', ,-Q r \ cy -j — fO«r^V\co^~\

~T"r, ic <->4 rTi l4-« a r-»O S^tluMT-e/- Ariarnii * t> 1 txi.î Kourvi* r- " 4. «a fiS« rt-Wv* ^^"^tJ i K)<^~1 V.r-U 1 _ ————— Mâruw. KJ-V- — I tiT —————————

u>,i,r>a •* fi(Vor«l U£ UcA .N- ~ ' rCooiact 1^>£U»'A UJ . V^ÂJ-J: phone £-|9-4£Z-.Tv A rt " I ^!o *\ -V^--- "hr-ioe — AVLoys-M W e^ \?«rk. !22oS1 °

- , ,- . ~. k'-^cjL , T>.n.«^- phSjrVc ^|A-4r8-6L2x3 ' TRANSPORTER"" S^-'pp-g C-nntar. °. pnone Narne United Industrial Services, ITIC .

Busies". Cofliact phone

X~<ie.>c KJo. "IT CfeRCi-A -qo2,i^

Anriro..^ 136 Gracev Ave.Meriden, CT O6A51

^

4s?

Contar-i phone (2O3) 238-6;PPA i n M,,rT,n«r CTDO2181.6889

WAST^ pESCRIPTION ————————————————————————————————————————Cb.em.cal * Physical Slates

lU Semi-iiquid CjBNayerecJ SI? ** O'O''2U Solid (^ysmgle Phase £Up5-8 O>>2

TSS •>•• DeOrisCOlO' % Ath

Flasti Po.ni ~^ ^ r>C~> ° Soecific Gravity

PROCESS DESCRIPTIONOosc-ibe process generating wavto stream Please include a list ol virgin -nate"ais and ine.r Material Safely Data Sheets

~^<?c.o.o ooc^r^ C-ow^ oo^Vt~ a£ P oÂ>raVttôe ^- -*» e»A

A, • 4^ A v . . C A V \, \ 1au<-^c. TV\€. Q € CO <v^ iV\ >S5 > OrJ'rViQ, O"l O~ f, e jToOtit) (~«*jv €_ C.M \ i rJQ C.i- Q.r-<i *^-

J off V ^JOD *^ <-^f1'

CHEMICAL CONSTITUENTS '' ' ———————————————————— —————Petroleum Pnase Susoecteq lêveij Actual I fwgisPCB-s Nfi<l"aiogens l\J PvSolvents fVjlV

Agueous Phase Suspected Levels AcCoppor (Cu) ————

Cadi-i urn ;Cd)C^. i r~ \ ' ——————— " — ' ——————— —————hrom.uTi (Cr)

Arsenic (As) i Lead 'Pe»Cadmium (Cd)Chro.Tiiunn fCr) ,Lead (Pb) \(

Piaase List Specific Solvents s\IJ — ~) ^~/

SHIPPING INFORMATIONU DOT Regulated Material U Non-Reguialed

DOT Hazard Class fi/O}J£.DOT Shipp.no Name &T RvCiLit. f) 7£ 7) Ul.'XJFReportable Quantity /UN/MA Numoe' A/tf IJ £Amount ol Waste Per Shipment galPreauency of Shipments

Please submit a one (1) quart representative sample of thuwaste stream Also describe the sampling method below.

ti S~- °t6-*Xtiio O>~vj>-«»vJ . f Y\ r\r* <C L. \ QQ / \

oat ..

&

Arsen.c (As) ^ , J*Sodium ;Na)Barium (8a)Tin (Sn(Nickel (Ni) ~ (•Silver (Ag)Zmc (2n; ,»

t êN, -j -r^-nr-r^ —————————— —— tThis Waste is.ORCRA Listed RCHA Num&«rCJ State Regulated State Number (" P O <-iC^ Non- RegulatedCJv/irg.n Material

Notes « Special Handlir-o Information

\J~

y'.C*,^J A

^

'~ — *— — ..—.... ——— .^.^-^-^^. — -^.^..^_. —— ,^ — =^. _ ._ . ____ , __ . rl- , - - ^rrjrrrr5c i tii0' — \. ^ . __ T "Sionaiure CyÔV^X^ 1 VU-g-cp ^ J" C"" ~j"Title p5efl»'n,u«J1 fY-l<* -^-Vfl *^~ Date It 71

PACILCTY USE ONLY^Received On Received By ^

^v*^nv

Sample Container AoDravBd/Ro.eclec! By ,' / V Date /, /"Comments: A- • * ' ~ ———————————————— — ~*~

UNITEDIMDUSTR1AL.SERVICES, INC.

No.1MCRAC6V »VENU6 7S3 .._-_-,.WASTE STREAM PROFILE SHEET

Oate Submiited

MakingAddress *• v-«J*->pii - -"-r—'

()- Technical Contact KI"-'ST<0 Shipping Contact

Busines* ContactEPA i D Number

phonephone

Name United Industrial Services. Inc.Address 136 Gracey Ave.

Meriden. CT O6451.Contact —————————————————————.E P A i n Number CTDO21616889

phone (2O3) 238-^

DESCRIPTION^Crvprnical * Physical States/rtX_,Quid U Muttiiayered pH U 2-*^JSomi-iiqu'O rjBllayrored Si*'6U Solid (JJtemgle Phase (O)6-8

'2O-12

OdO'TSS

_*t* Bottom_*r. Oeons _r. Ath __

Flasi- Pom! Specific Gravity

PROCESS DESCRIPTION^ P^ U ., C Jj ^JC-JV-.|r-»ir l^'Jfc^'-^ __ _______ _ _ — --_ _ _ - - ——————— ———— ...^ —— • ——————————————————————

Ooscribe process generating waste stream Please .nclude a l.st ol virgin materials and tr-e.r Matcr.ai Safety Data Sheets

P 062-

CHEMICAL CONSTITUENTSPotroieum Phasa Suspected Levels ,-.•,,-,. Actual Levelspca-s ' "^V^) 7.T <yvnnaiooans WV\Solvents TArsenic (As)Cadmium (Cd)Chromium (Cr] 5 ;Lead (Pb) ^

SHIPPING INFORMATIONU DOT Regulated MatenaJ^ C^ Non-Regulated

DOT Haj-ard Class ^ ri W'lO .DOT Shipping Name O " — <2 i?" Ov v \ f\ *^-f> C^ <v Xfv"5V-f:>Reoortable Quar-rnv ~VUN/NA Numoer t ?i CN,(-- -QAmount o' Waste Per Shipment galF'rBcjuency o/ Shipments

pia,ase submit a one (1) quan representative sample of thewaste stream Also describe the sampling method below.

/""^ 1 I \ \ \Lo^^v-V^ A-rtvA T^'fcKfVi -nVre^_ ,,Q f\ /• f>ool Poo2\

S4., C<:ij<.t>r-> oLriA vi...- V Po^rj . fi£>2r7 /FACILfTY

Received OnSarnple ContainerComments:

f

Aqueous Phase Suspected Levels Actual -Coponr (Cu) f ) _''Cadm.un ;Cd) f C'lChromium (Cr) C' / CLeao1 ;Pb) C' OlArsenic (As) fV Sodium (N3) \Barium {BaJ 1Tin (Sn) ^/

Nickel (Mi) OUJSilver (Ag) T C2.Zinc (2n) i 55Phenols /^/fL^ —— r.J^ ^'^j-JT^yj ' ..'

This Waste is:OnCHA Listed RCHA Number • —U State Peculated Stato Number (_/?. f it-/^.fNon- RegulatedOVi'gm Malerral

Notes & Snecial HarxJIing information

.T^7*T r !»^*^?~*ri'r '"*'-^r"*^-*rrrT"*T'**r"j'*'.t- j '" "* '" *~-~ *~ — • ~"~ •— *~~ "• ' — " "•• •» -'~— "*>" - • • '* **' Ij -^ '** ' l*~*^"^ ** - •* ••-•ui i_ i r u w * —— _ u it _l — — r "-

T"T ~ J^ *^

Signature LVxtti/) tl) ^<J. ~jVC-Yt->_3 / /Title Rtt*>V_j« ! /V\« _A_-?-£/^ Date V//'? 7< -

USE ONLY ^_Rocsived 8y '/V / , / /ADprovBa/noioct»d By /^/ 1 / Date: / ' / ' _ ; /

" 3063Z9

FINAL REPORT CYLINDER DECOMMISSIONING · FINAL REPORT CYLINDER DECOMMISSIONING MALTA ROCKET FUEL...

Documents

Transcript of FINAL REPORT CYLINDER DECOMMISSIONING · FINAL REPORT CYLINDER DECOMMISSIONING MALTA ROCKET FUEL...